JP5913197B2 - Saturated air temperature control method and spray corrosion test apparatus in spray corrosion test - Google Patents

Saturated air temperature control method and spray corrosion test apparatus in spray corrosion test Download PDF

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JP5913197B2
JP5913197B2 JP2013111555A JP2013111555A JP5913197B2 JP 5913197 B2 JP5913197 B2 JP 5913197B2 JP 2013111555 A JP2013111555 A JP 2013111555A JP 2013111555 A JP2013111555 A JP 2013111555A JP 5913197 B2 JP5913197 B2 JP 5913197B2
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茂雄 須賀
茂雄 須賀
信治 菊川
信治 菊川
長谷川 和哉
和哉 長谷川
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Suga Test Instruments Co Ltd
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Description

本発明は噴霧腐食試験における飽和空気温度制御方法及び噴霧腐食試験装置に係り、特に噴霧腐食試験を行う試験槽内の噴霧器に導入される飽和空気の温度を正確に制御し、噴霧時に腐食性溶液の濃度変動を防止する飽和空気温度制御方法及び噴霧腐食試験装置に関するものである。   The present invention relates to a saturated air temperature control method and a spray corrosion test apparatus in a spray corrosion test, and more particularly, to accurately control the temperature of saturated air introduced into a sprayer in a test tank for performing a spray corrosion test, and a corrosive solution during spraying. The present invention relates to a saturated air temperature control method and a spray corrosion test apparatus that prevent fluctuations in the concentration of water.

従来から用いられている噴霧腐食試験装置は、試験槽内に空気ノズルと液ノズルからなる噴霧器を備えており、空気ノズルから噴出される圧縮空気のベンチュリ効果により液ノズル内の腐食性溶液を吸い上げ、微細な粒子として試験槽内の試料に均一に噴霧するように構成されている(非特許文献1参照)。   Conventional spray corrosion test equipment is equipped with a sprayer consisting of an air nozzle and a liquid nozzle in a test tank, and the corrosive solution in the liquid nozzle is sucked up by the venturi effect of the compressed air ejected from the air nozzle. The sample is configured to be sprayed uniformly as fine particles on the sample in the test tank (see Non-Patent Document 1).

以前より、試験槽内に腐食性溶液を噴霧する際に、乾燥した圧縮空気を使用して腐食性溶液を噴霧すると、所定の濃度に調整した腐食性溶液の濃度が変動してしまうという問題がある。そのため、乾燥した圧縮空気を空気飽和器内の水に通過させて飽和空気とすることにより、噴霧時の腐食性溶液の濃度変動を抑制している。   When spraying a corrosive solution in a test tank from the past, if the corrosive solution is sprayed using dry compressed air, the concentration of the corrosive solution adjusted to a predetermined concentration will fluctuate. is there. Therefore, the density fluctuation | variation of the corrosive solution at the time of spraying is suppressed by passing dry compressed air through the water in an air saturator, and making it saturated air.

ところで、圧縮された飽和空気が噴霧器から試験槽内に噴出すると断熱膨張により温度が低下する。したがって、試験槽内に飽和空気を噴出する際に、槽内温度と同温の飽和空気とするために、空気飽和器の水温を槽内温度と噴霧圧力との相関関係から求める温度に設定して、圧縮空気を加湿及び加熱していた。   By the way, when compressed saturated air is ejected from the sprayer into the test tank, the temperature is lowered by adiabatic expansion. Therefore, when injecting saturated air into the test tank, the water temperature of the air saturator is set to the temperature obtained from the correlation between the tank temperature and the spray pressure in order to obtain saturated air at the same temperature as the tank temperature. The compressed air was humidified and heated.

例えば、非特許文献2記載の中性塩水噴霧試験では、噴霧室(試験槽)内の温度を35±2℃に制御し、また、噴霧器に供給する圧縮空気は、噴霧室の温度よりも10度以上高い水を有する飽和塔(空気飽和器)の中を通過させて加湿及び加熱する必要があると規定している。飽和塔内の水温は使用する圧力や噴霧器のノズルタイプによって異なるが、非特許文献2では一例として、噴霧過圧(噴霧圧力)が98kPa(0.098MPa)のとき、飽和塔(空気飽和器)の水温を48℃に制御すると記載している。   For example, in the neutral salt spray test described in Non-Patent Document 2, the temperature in the spray chamber (test tank) is controlled to 35 ± 2 ° C., and the compressed air supplied to the sprayer is 10 times higher than the temperature in the spray chamber. It stipulates that it needs to be humidified and heated by passing it through a saturation tower (air saturator) having higher water than that. Although the water temperature in the saturation tower varies depending on the pressure used and the nozzle type of the sprayer, in Non-Patent Document 2, as an example, when the spray overpressure (spray pressure) is 98 kPa (0.098 MPa), the saturation tower (air saturator) The water temperature is controlled to 48 ° C.

以下、「圧縮された飽和空気が噴霧器から試験槽内に噴出する際に、槽内温度と同温の飽和空気となる、槽内温度と飽和空気の噴霧圧力との相関関係から求める空気飽和器内で制御する温度」を、圧縮された飽和空気の「誘導値」という。なお、槽内温度とは、噴霧腐食試験の規格で定められた試験槽内の温度を意味している。   Hereinafter, "When the compressed saturated air is ejected from the nebulizer into the test chamber, it becomes saturated air having the same temperature as the chamber temperature. The air saturator is obtained from the correlation between the chamber temperature and the spray pressure of the saturated air. "Temperature to be controlled" is called "Induction value" of compressed saturated air. In addition, the temperature in a tank means the temperature in the test tank defined by the standard of the spray corrosion test.

JIS Z2371:2000「塩水噴霧試験方法」JIS Z2371: 2000 “Salt spray test method” ISO 9227:2012「Corrosion tests in artificial atmospheres ― Saltspray tests」ISO 9227: 2012 "Corrosion tests in artificial atmospheres-Saltspray tests"

上記の通り、従来の噴霧腐食試験装置では、圧縮された飽和空気を用いて試験槽内に腐食性溶液を噴霧する際に、空気飽和器内の水温を「誘導値」に設定し、この空気飽和器を通過して加湿及び加熱された飽和空気を試験槽内の噴霧器に導入していた。
しかし、この噴霧器に導入される飽和空気の温度は、空気飽和器内の水温によって制御される間接的制御であり、直接制御されておらず、下記の課題を有していた。
As described above, in the conventional spray corrosion test apparatus, when the corrosive solution is sprayed into the test tank using the compressed saturated air, the water temperature in the air saturator is set to the “induction value”, and this air Saturated air that had been humidified and heated through the saturator was introduced into a sprayer in the test chamber.
However, the temperature of the saturated air introduced into the nebulizer is an indirect control controlled by the water temperature in the air saturator, is not directly controlled, and has the following problems.

空気飽和器の水位が低下すると飽和空気が空気飽和器内の上部で冷却されてしまい、空気飽和器内で「誘導値」に制御された水温よりも低い温度の飽和空気が試験槽内の噴霧器に導入されてしまう。したがって、この飽和空気が噴霧器の空気ノズルから噴出すると、断熱膨張によりさらに温度が低下して、槽内温度よりも低い温度の飽和空気となる。この槽内温度よりも低い温度の飽和空気は槽内雰囲気によりただちに加熱されるため、不飽和な空気となる。その結果、微細粒子となった腐食性溶液の水分が不飽和な空気によって蒸発し、腐食性溶液の濃度が上昇してしまう恐れがあった。   When the water level of the air saturator drops, the saturated air is cooled at the top of the air saturator, and saturated air with a temperature lower than the water temperature controlled to the “inductive value” in the air saturator Will be introduced. Therefore, when this saturated air is ejected from the air nozzle of the sprayer, the temperature is further lowered by adiabatic expansion, and becomes saturated air having a temperature lower than the temperature in the tank. Since the saturated air having a temperature lower than the temperature in the tank is immediately heated by the atmosphere in the tank, it becomes unsaturated air. As a result, the moisture of the corrosive solution that has become fine particles may be evaporated by the unsaturated air, and the concentration of the corrosive solution may increase.

また、試験槽内の噴霧器と空気飽和器とを繋ぐ導管を通過する際、飽和空気が冷却され、飽和空気中の水分が凝縮して水滴を生じることがある。この水滴が飽和空気に混入して噴霧器の空気ノズルから噴出すると、微細粒子となった腐食性溶液に水滴が結びついて、腐食性溶液の濃度が低下してしまう恐れがあった。   Moreover, when passing through the conduit | pipe which connects the sprayer and air saturator in a test tank, saturated air may be cooled and the water | moisture content in saturated air may condense and produce a water droplet. When these water droplets are mixed with saturated air and ejected from the air nozzle of the atomizer, the water droplets are combined with the corrosive solution that has become fine particles, which may reduce the concentration of the corrosive solution.

さらに、噴霧腐食試験においては、飽和空気の噴霧圧力を変動させることにより腐食性溶液の噴霧量を調節できることが知られている。しかし、従来の噴霧腐食試験装置では、上記非特許文献1に記載の条件(噴霧圧力0.098±0.01MPa、空気飽和器の水温47±2℃)に設定値を固定している。したがって、噴霧量を調節するために装置出荷時に設定された値とは異なる噴霧圧力で腐食性溶液の噴霧を行う場合には、槽内温度と噴霧圧力との相関関係から求める新たな「誘導値」となるように、飽和空気の温度の設定を技術者が手動で変更する必要があった。   Furthermore, in the spray corrosion test, it is known that the spray amount of the corrosive solution can be adjusted by changing the spray pressure of saturated air. However, in the conventional spray corrosion test apparatus, the set values are fixed to the conditions described in Non-Patent Document 1 (spray pressure 0.098 ± 0.01 MPa, air saturator water temperature 47 ± 2 ° C.). Therefore, when the corrosive solution is sprayed at a spray pressure different from the value set at the time of shipment to adjust the spray amount, a new “induction value” obtained from the correlation between the tank temperature and the spray pressure is used. The engineer had to manually change the temperature setting of the saturated air so that

本発明は、上記課題を解決するためになされたものであり、試験槽内の噴霧器に導入する飽和空気の温度を直接制御し、噴霧器に一定温度の飽和空気を導入して噴霧時の腐食性溶液の濃度の変動を防止し得る飽和空気温度制御方法及び噴霧腐食試験装置を実現することを目的とする。   The present invention has been made in order to solve the above-mentioned problems, and directly controls the temperature of saturated air introduced into the sprayer in the test tank, and introduces saturated air at a constant temperature into the sprayer to cause corrosivity during spraying. It is an object of the present invention to realize a saturated air temperature control method and a spray corrosion test apparatus that can prevent fluctuations in solution concentration.

また、飽和空気を「誘導値」に調温し、噴霧圧力を変動させて噴霧量を調節する場合においても、試験槽内に所定の温度の飽和空気を導入し得る飽和空気温度制御方法及び噴霧腐食試験装置を実現することを目的とする。   In addition, even when adjusting the spray amount by adjusting the temperature of the saturated air to the “induction value” and changing the spray pressure, the saturated air temperature control method and the spray that can introduce saturated air at a predetermined temperature into the test tank The purpose is to realize a corrosion tester.

本発明は、上記目的を達成するために、噴霧腐食試験における飽和空気温度制御方法において、圧縮空気を空気飽和器に通して飽和空気とし、この飽和空気を噴霧器に導入する流路であり、前記空気飽和器の上部と前記空気飽和器と前記噴霧器とを繋げる導管のいずれかの部位に第1温度センサを設け、前記噴霧器に導入する飽和空気の温度を測定し、測定した温度情報に基づいて制御部が前記空気飽和器内の第1ヒータを作動させ、飽和空気の温度を制御することを特徴とする。   In order to achieve the above object, the present invention provides a flow path for introducing compressed air into saturated air by passing the compressed air through the air saturator in the saturated air temperature control method in the spray corrosion test, A first temperature sensor is provided in any part of a conduit connecting the upper part of the air saturator and the air saturator and the sprayer, the temperature of the saturated air introduced into the sprayer is measured, and based on the measured temperature information The control unit operates the first heater in the air saturator to control the temperature of the saturated air.

本発明の噴霧腐食試験における飽和空気温度制御方法は、上記に加えて、前記第1温度センサを前記空気飽和器の上部または前記導管内の前記空気飽和器との接続部近傍のいずれかの部位に設ける一方、前記導管の前記噴霧器との接続部近傍に位置する第2温度センサ及び前記導管の全体を覆う第2ヒータを設け、前記第1温度センサ及び前記第2温度センサとで測定された飽和空気の温度情報を前記制御部に送り、その温度情報に基づいて前記噴霧器に送られる飽和空気が前記試験槽内で槽内温度と同温の飽和空気となるように前記第2ヒータを作動させて飽和空気を加熱することを特徴とする。In addition to the above, the method for controlling the saturated air temperature in the spray corrosion test of the present invention may be arranged such that the first temperature sensor is located at any position above the air saturator or in the vicinity of the connection with the air saturator in the conduit On the other hand, a second temperature sensor located in the vicinity of the connection portion of the conduit with the sprayer and a second heater covering the entire conduit are provided, and measured by the first temperature sensor and the second temperature sensor. The temperature information of the saturated air is sent to the control unit, and the second heater is operated so that the saturated air sent to the sprayer becomes the saturated air having the same temperature as the temperature inside the test tank based on the temperature information. And saturated air is heated.

本発明の噴霧腐食試験における飽和空気温度制御方法は、上記に加えて、圧縮空気の圧力を任意に設定可能とし、前記制御部が、前記噴霧器に導入される飽和空気が、前記試験槽内で噴出する際に槽内温度と同温の飽和空気となるように、槽内温度と前記空気飽和器で測定された実際の圧力との相関関係から求める温度に飽和空気の温度を設定することを特徴とする。   In addition to the above, the saturated air temperature control method in the spray corrosion test of the present invention can arbitrarily set the pressure of the compressed air, and the control unit allows the saturated air introduced into the sprayer to be in the test tank. The temperature of the saturated air is set to the temperature obtained from the correlation between the temperature in the tank and the actual pressure measured by the air saturator so that saturated air having the same temperature as the temperature in the tank is obtained when jetting. Features.

本発明の噴霧腐食試験における噴霧腐食試験装置は、圧縮空気を生成するコンプレッサと、圧縮空気の圧力を制御する圧力調節手段と、圧縮空気を飽和空気にするための空気飽和器と、圧縮空気を前記空気飽和器内の水に通して飽和空気とする加湿手段と、前記空気飽和器内の水を加熱する第1ヒータと、飽和空気を前記空気飽和器から試験槽内の噴霧器に送る導管と、飽和空気の温度を測定するために飽和空気を前記噴霧器に導入する流路である前記空気飽和器の上部から前記導管のいずれかの部位に位置する第1温度センサと、前記第1温度センサで測定された温度情報を基に前記第1ヒータを制御する制御部とを備えることを特徴とする。   The spray corrosion test apparatus in the spray corrosion test of the present invention comprises a compressor that generates compressed air, a pressure adjusting means that controls the pressure of the compressed air, an air saturator that makes the compressed air saturated, and a compressed air. Humidification means for passing saturated water through the water in the air saturator, a first heater for heating the water in the air saturator, and a conduit for sending the saturated air from the air saturator to the sprayer in the test chamber A first temperature sensor located in any part of the conduit from the top of the air saturator, which is a flow path for introducing saturated air into the nebulizer to measure the temperature of the saturated air; and the first temperature sensor And a control unit for controlling the first heater based on the temperature information measured in (1).

本発明の噴霧腐食試験における噴霧腐食試験装置は、上記に加えて、前記第1温度センサを前記空気飽和器の上部または前記導管内の前記空気飽和器との接続部近傍のいずれかの部位に設け、前記導管の前記噴霧器との接続部近傍に位置し、前記噴霧器に導入する直前の飽和空気の温度を測定し、その温度情報を前記制御部に出力する第2温度センサと、前記導管の全体を覆うように設けられ、前記制御部によって制御される第2ヒータとを有することを特徴とする。In addition to the above, the spray corrosion test apparatus in the spray corrosion test according to the present invention may be configured such that the first temperature sensor is placed at any location near the connection with the air saturator in the upper part of the air saturator or in the conduit. provided, located in the connecting portion vicinity of the sprayer of the conduit, wherein the temperature of the saturated air just before introducing the nebulizer was determined, and a second temperature sensor to output the temperature information to the control unit, of said conduit The second heater is provided so as to cover the whole, and is controlled by the control unit.

本発明の噴霧腐食試験における噴霧腐食試験装置は、上記に加えて、前記圧力調節手段は前記空気飽和器に通す圧縮空気の圧力を任意に設定可能とし、前記制御部は、前記空気飽和器内の飽和空気の圧力を測定する圧力センサの情報を基に前記試験槽内の噴霧器に導入する飽和空気が前記試験槽内で噴出する際に槽内温度と同温の飽和空気となるように飽和空気の温度を設定することを特徴とする。   In addition to the above, the spray corrosion test apparatus in the spray corrosion test according to the present invention enables the pressure adjusting means to arbitrarily set the pressure of the compressed air passed through the air saturator, and the control unit is provided in the air saturator. Based on the information of the pressure sensor that measures the pressure of saturated air, the saturated air to be introduced into the sprayer in the test tank is saturated so that it becomes saturated air at the same temperature as the temperature inside the test tank. It is characterized by setting the temperature of air.

本発明の噴霧腐食試験における飽和空気温度制御方法及び噴霧腐食試験装置は、上記の通りであるので、試験槽内の噴霧器に導入する圧縮された飽和空気の温度を直接制御することができる。また、導管の位置で加熱することで、飽和空気の温度を噴霧器に導入するまで空気飽和器で設定した温度に維持することができる。したがって、圧縮された飽和空気を噴霧器へ温度の変動無く導入することができ、噴霧時の腐食性溶液の濃度の変動を防止することができる。   Since the saturated air temperature control method and the spray corrosion test apparatus in the spray corrosion test of the present invention are as described above, the temperature of the compressed saturated air introduced into the sprayer in the test tank can be directly controlled. Further, by heating at the position of the conduit, the temperature of the saturated air can be maintained at the temperature set by the air saturator until it is introduced into the sprayer. Therefore, the compressed saturated air can be introduced into the sprayer without fluctuation in temperature, and fluctuations in the concentration of the corrosive solution during spraying can be prevented.

さらに、実際の噴霧圧力に基づいて飽和空気の温度を制御することができるため、噴霧圧力を一般的な制御値と異なる値に設定した場合においても、試験槽内に噴出する際に槽内温度と同温の飽和空気とすることができ、腐食性溶液の濃度の変動を防止することができる。   Furthermore, since the temperature of the saturated air can be controlled based on the actual spray pressure, even when the spray pressure is set to a value different from the general control value, Saturated air having the same temperature as that of the aqueous solution can be prevented, and fluctuations in the concentration of the corrosive solution can be prevented.

本発明の噴霧腐食試験装置の構成図である(実施例1)。It is a block diagram of the spray corrosion test apparatus of this invention (Example 1). 本発明の噴霧腐食試験装置の構成図である(実施例2)。It is a block diagram of the spray corrosion test apparatus of this invention (Example 2). 本発明の噴霧腐食試験装置のブロック図である(実施例3)。(Example 3) which is a block diagram of the spray corrosion test apparatus of this invention.

以下、図面に基づいて本発明の実施例を詳細に説明するが、本発明はこれらに限定されるものではない。   Hereinafter, examples of the present invention will be described in detail with reference to the drawings, but the present invention is not limited thereto.

図1は本発明の実施例1における噴霧腐食試験装置を示すものである。   FIG. 1 shows a spray corrosion test apparatus in Example 1 of the present invention.

噴霧腐食試験装置1は、圧縮空気を生成するコンプレッサ2と、圧縮空気の圧力を制御する圧力調節手段3と、圧縮空気を飽和空気にするための空気飽和器4と、圧縮空気を空気飽和器4内の水に通して飽和空気とする加湿手段5と、空気飽和器4内の水を加熱する第1ヒータ6と、飽和空気を空気飽和器4から試験槽8内の噴霧器9に送る導管12と、飽和空気の温度を測定するために飽和空気を噴霧器9に導入する流路13である空気飽和器4の上部から導管12のいずれかの部位に位置する第1温度センサ14と、第1温度センサ14で測定された温度情報を基に第1ヒータ6を制御する制御部100を備えている。   The spray corrosion test apparatus 1 includes a compressor 2 for generating compressed air, a pressure adjusting means 3 for controlling the pressure of the compressed air, an air saturator 4 for making the compressed air into saturated air, and an air saturator for compressing air. Humidification means 5 for passing saturated water through the water in 4, a first heater 6 for heating the water in the air saturator 4, and a conduit for sending the saturated air from the air saturator 4 to the sprayer 9 in the test tank 8. 12, a first temperature sensor 14 located in any part of the conduit 12 from the top of the air saturator 4, which is a flow path 13 for introducing saturated air into the nebulizer 9 in order to measure the temperature of the saturated air, A control unit 100 that controls the first heater 6 based on the temperature information measured by the one temperature sensor 14 is provided.

この噴霧腐食試験装置1は、空気飽和器4と試験槽8内の噴霧器9の空気ノズル10とを導管12によって連絡する一方、噴霧器9の液ノズル11には溶液タンク17内の腐食性溶液を供給する供給管18を接続している。空気飽和器4と導管12を接続する位置は、空気飽和器4の底部から上昇した飽和空気を速やかに噴霧器9に導入するため空気飽和器4の天井面が好ましいが、空気飽和器4内の水が導管12内に流入しない位置であれば、空気飽和器4の上部側面でもよい。また、導管12は、空気飽和器4から発生した飽和空気が導管12内を通過する間に冷却されることを防止するため、断熱加工を施すことが好ましい。
また、噴霧腐食試験装置1の前面には、タッチパネル20を有する操作パネル19が設けられている。タッチパネル20は、噴霧腐食試験装置1の運転状態に係る各種情報や操作用の画面を表示する表示画面を有し、この表示画面に対する接触操作を検出する機能を備えている。
In this spray corrosion test apparatus 1, an air saturator 4 and an air nozzle 10 of a sprayer 9 in a test tank 8 are connected by a conduit 12, while a corrosive solution in a solution tank 17 is supplied to a liquid nozzle 11 of the sprayer 9. A supply pipe 18 to be supplied is connected. The position where the air saturator 4 and the conduit 12 are connected is preferably the ceiling surface of the air saturator 4 in order to quickly introduce the saturated air rising from the bottom of the air saturator 4 into the sprayer 9. The upper side surface of the air saturator 4 may be used as long as water does not flow into the conduit 12. The conduit 12 is preferably heat-insulated to prevent the saturated air generated from the air saturator 4 from being cooled while passing through the conduit 12.
An operation panel 19 having a touch panel 20 is provided on the front surface of the spray corrosion test apparatus 1. The touch panel 20 has a display screen for displaying various information related to the operation state of the spray corrosion test apparatus 1 and a screen for operation, and has a function of detecting a contact operation on the display screen.

圧力調節手段3は、コンプレッサ2と加湿手段5を連絡する配管の途中に設置されており、空気飽和器4へ供給する圧縮空気の圧力の値を制御する。一般的には圧力の制御調整が行える圧力調節弁が用いられる。本実施例においては上記の位置に設置されているが、コンプレッサ2を構成する部品の一部として設置されてもよい。また、圧力調節手段3は、図示しない圧力調節部を有している。圧力調節部は、圧力操作パネルにより圧力の値を設定し、また、マイクロコンピュータなどの演算装置によって圧力調節手段3を作動させる信号を生成することで、設定した値に自動で圧力を制御する。なお、圧力調節部には他の種類の調節機構を用いてもよい。   The pressure adjusting means 3 is installed in the middle of the piping connecting the compressor 2 and the humidifying means 5 and controls the pressure value of the compressed air supplied to the air saturator 4. Generally, a pressure control valve capable of controlling and adjusting the pressure is used. Although it is installed at the above position in the present embodiment, it may be installed as a part of the components constituting the compressor 2. The pressure adjusting means 3 has a pressure adjusting unit (not shown). The pressure adjusting unit sets the pressure value by the pressure operation panel, and generates a signal for operating the pressure adjusting means 3 by an arithmetic device such as a microcomputer, thereby automatically controlling the pressure to the set value. Note that other types of adjusting mechanisms may be used for the pressure adjusting unit.

加湿手段5は、空気飽和器4内底部に内設されており、空気飽和器4外に設置されたコンプレッサ2と連絡している。この加湿手段5には、内部に気体を通すことができる円形または馬蹄形の金属管であり、気体を発泡させるための細孔を備えた発泡管が一般的に用いられる。   The humidifying means 5 is installed in the bottom of the air saturator 4 and communicates with the compressor 2 installed outside the air saturator 4. The humidifying means 5 is generally a circular or horseshoe-shaped metal tube that allows gas to pass therethrough, and a foamed tube having pores for foaming the gas is generally used.

第1温度センサ14は、飽和空気の流路13の上流側である空気飽和器4の上部に設けられている。第1温度センサ14は、例えば熱電対や白金抵抗測温体であるが、他の構成のセンサが用いられてもよい。ここで、第1温度センサ14を空気飽和器4の上部に設けた理由は、空気飽和器4内の水位が低下している際に、加湿手段5により発生した飽和空気が空気飽和器4の上部に達するまでに冷却されることを考慮し、導管12に入る直前の飽和空気温度を直接測定するのに適しているためである。本実施例においては、上記理由により空気飽和器4の上部に第1温度センサ14を設けることが好ましいが、飽和空気の流路13内であれば、例えば、導管12内の空気飽和器4との接続部近傍に第1温度センサ14を設けてもよい。また、この第1温度センサ14は、制御部100へ温度情報を出力する。   The first temperature sensor 14 is provided above the air saturator 4 on the upstream side of the flow path 13 for saturated air. The first temperature sensor 14 is, for example, a thermocouple or a platinum resistance temperature sensor, but a sensor having another configuration may be used. Here, the reason why the first temperature sensor 14 is provided in the upper part of the air saturator 4 is that the saturated air generated by the humidifying means 5 is reduced in the air saturator 4 when the water level in the air saturator 4 is lowered. This is because it is suitable for directly measuring the saturated air temperature just before entering the conduit 12 in consideration of cooling before reaching the upper part. In the present embodiment, it is preferable to provide the first temperature sensor 14 on the upper portion of the air saturator 4 for the above reason. However, if it is in the flow path 13 of the saturated air, for example, the air saturator 4 in the conduit 12 and The first temperature sensor 14 may be provided in the vicinity of the connecting portion. Further, the first temperature sensor 14 outputs temperature information to the control unit 100.

制御部100はコンピュータを利用したものであり、メモリに予め記憶させた所定プログラムと、予め設定される噴霧腐食試験の噴霧時間、試験槽または腐食性溶液の設定温度などの各種データにしたがってCPUや周辺機器が動作することにより噴霧腐食試験を実行する。これらのデータは、例えば、タッチパネル20の操作により入力されるものとしてもよい。この制御部100の中には、空気飽和器4内の飽和空気の「誘導値」を設定する温度設定部101や、「誘導値」と第1温度センサ14で検出した飽和空気の温度情報とを取り入れ、第1温度センサ14で検出される温度情報が「誘導値」となるように第1ヒータ6に出力信号を与えて制御する温度制御部102が設けられている。   The control unit 100 uses a computer, and according to various data such as a predetermined program stored in a memory in advance and a spray time of a spray corrosion test set in advance, a set temperature of a test tank or a corrosive solution, a CPU, A spray corrosion test is performed by operating peripheral devices. These data may be input by operating the touch panel 20, for example. The control unit 100 includes a temperature setting unit 101 for setting an “inductive value” of saturated air in the air saturator 4, an “inductive value” and temperature information of the saturated air detected by the first temperature sensor 14. Is provided, and a temperature control unit 102 is provided that controls the first heater 6 by giving an output signal so that the temperature information detected by the first temperature sensor 14 becomes an “induction value”.

圧力センサ16は、空気飽和器4の上部に内設されており、空気飽和器4内の飽和空気の圧力を測定する。この圧力センサ16は、ダイヤフラムが変形して発生する電気抵抗の変化を電気信号に変換するゆがみゲージ型や、ダイヤフラムの変形を静電容量として検出する静電容量型であるが、他の種類のセンサが用いられてもよい。圧力センサ16の測定値は、圧力センサ16と接続している圧力表示部(図示しない)に表示され、試験者は飽和空気の圧力を確認することができる。   The pressure sensor 16 is provided in the upper part of the air saturator 4 and measures the pressure of the saturated air in the air saturator 4. The pressure sensor 16 is a distortion gauge type that converts a change in electric resistance generated by the deformation of the diaphragm into an electric signal, or a capacitance type that detects the deformation of the diaphragm as a capacitance. A sensor may be used. The measured value of the pressure sensor 16 is displayed on a pressure display unit (not shown) connected to the pressure sensor 16, and the tester can check the pressure of saturated air.

図1の噴霧腐食試験装置1による、飽和空気温度制御方法について説明する。   A saturated air temperature control method by the spray corrosion test apparatus 1 of FIG. 1 will be described.

コンプレッサ2から送られる圧縮空気は、空気飽和器4の底部近傍にある加湿手段5に導入され、空気飽和器4内の水に通して飽和状態の圧縮空気、つまり、「飽和空気」となる。本実施例において、コンプレッサ2から空気飽和器4に供給される空気の圧力は、圧力調節手段3により一般的な噴霧腐食試験の規格に定められた0.098MPaに設定、制御される。その後、圧縮された飽和空気は空気飽和器4の上部から導管12内を介して噴霧器9に導入され、空気ノズル10から噴出する。このとき、液ノズル11内の腐食性溶液が空気ノズル10から噴出する飽和空気のベンチュリ効果によって吸い上げられ、腐食性溶液は微細な粒子として試験槽8内に載置された試料Sへ噴霧される。   The compressed air sent from the compressor 2 is introduced into the humidifying means 5 near the bottom of the air saturator 4 and passes through the water in the air saturator 4 to become saturated compressed air, that is, “saturated air”. In the present embodiment, the pressure of the air supplied from the compressor 2 to the air saturator 4 is set and controlled by the pressure adjusting means 3 at 0.098 MPa defined in the standard of a general spray corrosion test. Thereafter, the compressed saturated air is introduced from the upper part of the air saturator 4 into the sprayer 9 through the inside of the conduit 12 and is ejected from the air nozzle 10. At this time, the corrosive solution in the liquid nozzle 11 is sucked up by the venturi effect of the saturated air ejected from the air nozzle 10, and the corrosive solution is sprayed as fine particles on the sample S placed in the test tank 8. .

このとき、第1温度センサ14は飽和空気の流路13の上流側である空気飽和器4内の上部で、圧縮された飽和空気の温度を直接測定している。この第1温度センサ14が測定した温度情報は制御部100に入力される。制御部100の温度制御部102は、温度設定部101で予め設定した飽和空気の「誘導値」と第1温度センサ14より入力された温度情報に基づいて、空気飽和器4内の第1ヒータ6へ出力信号を与えて制御する。第1ヒータ6は、第1温度センサ14で測定される飽和空気の温度が、試験槽8内で噴霧する際に槽内温度と同温の飽和空気として噴霧されるための「誘導値」(噴霧圧力0.098MPaの場合、47℃)になるように空気飽和器4内の水を加熱する。   At this time, the first temperature sensor 14 directly measures the temperature of the compressed saturated air at the upper part in the air saturator 4 on the upstream side of the saturated air flow path 13. The temperature information measured by the first temperature sensor 14 is input to the control unit 100. The temperature control unit 102 of the control unit 100 includes a first heater in the air saturator 4 based on the “induction value” of saturated air set in advance by the temperature setting unit 101 and the temperature information input from the first temperature sensor 14. An output signal is given to 6 and controlled. The first heater 6 is an “inductive value” for spraying the saturated air temperature measured by the first temperature sensor 14 as saturated air having the same temperature as the temperature in the tank when spraying in the test tank 8. The water in the air saturator 4 is heated to 47 ° C. when the spraying pressure is 0.098 MPa.

上記の通り、図1に示す本実施例の噴霧腐食試験装置1及び飽和空気温度制御方法においては、試験槽8内の噴霧器9に圧縮された飽和空気が導入される際に、空気飽和器4の水温ではなく、飽和空気が通過する流路13に備えた第1温度センサ14の温度情報によって、制御部100が空気飽和器4内の第1ヒータ6を制御して圧縮された飽和空気の温度を直接制御するため、設定した温度が変動することなく噴霧器9に圧縮された飽和空気を導入することができ、噴霧時の腐食性溶液の濃度の変動を防止することができる。   As described above, in the spray corrosion test apparatus 1 and the saturated air temperature control method of this embodiment shown in FIG. 1, when the saturated air compressed is introduced into the sprayer 9 in the test tank 8, the air saturator 4. The controller 100 controls the first heater 6 in the air saturator 4 based on the temperature information of the first temperature sensor 14 provided in the flow path 13 through which the saturated air passes, instead of the water temperature of the saturated air. Since the temperature is directly controlled, saturated air compressed into the sprayer 9 can be introduced without the set temperature changing, and fluctuations in the concentration of the corrosive solution during spraying can be prevented.

図2は、本発明の実施例2における噴霧腐食試験装置の構造を示すものである。
以下の実施例2においては、上記実施例1と同一機能を果たす箇所には、同一符号を付して説明する。
FIG. 2 shows the structure of a spray corrosion test apparatus in Example 2 of the present invention.
In the following second embodiment, portions having the same functions as those of the first embodiment will be described with the same reference numerals.

噴霧腐食試験装置1’は、上記実施例1の噴霧腐食試験装置1の構造に加えて、第1温度センサ14を流路13の上流側に設け、流路13の下流側に位置する噴霧器9に導入する直前の飽和空気の温度を測定しその温度情報を制御部100に出力する第2温度センサ15と、導管12の全体を覆うように設けられ、制御部100によって制御される第2ヒータ7を備えている。In addition to the structure of the spray corrosion test apparatus 1 of the first embodiment, the spray corrosion test apparatus 1 ′ is provided with the first temperature sensor 14 on the upstream side of the flow path 13 and the sprayer 9 located on the downstream side of the flow path 13. A second temperature sensor 15 that measures the temperature of saturated air immediately before being introduced into the sensor and outputs the temperature information to the control unit 100, and a second heater that is provided so as to cover the entire conduit 12 and is controlled by the control unit 100 7 is provided.

第2ヒータ7は、空気飽和器4と噴霧器9とを繋げる導管12を覆うように設けられている。本実施例の第2ヒータ7は導管12全体を覆うように設けているが、例えば導管12が冷却されにくい環境にある場合には、導管12の一部分のみを覆う形で設けてもよい。また、この第2ヒータ7は、制御部100によって加熱を制御されている。   The second heater 7 is provided so as to cover the conduit 12 that connects the air saturator 4 and the sprayer 9. Although the second heater 7 of the present embodiment is provided so as to cover the entire conduit 12, for example, when the conduit 12 is in an environment where it is difficult to cool, it may be provided so as to cover only a part of the conduit 12. Further, the heating of the second heater 7 is controlled by the control unit 100.

第1温度センサ14は、上記実施例1と同様に飽和空気の流路13の上流側である空気飽和器4の上部に設けられている。第1温度センサ14の位置は、上記実施例1と同様の理由で、空気飽和器4の上部に設けられることが好ましいが、飽和空気の流路13内の上流側であれば、例えば、導管12内の空気飽和器4との接続部近傍に第1温度センサ14を設けてもよい。   The first temperature sensor 14 is provided in the upper part of the air saturator 4 on the upstream side of the saturated air flow path 13 as in the first embodiment. The position of the first temperature sensor 14 is preferably provided in the upper part of the air saturator 4 for the same reason as in the first embodiment. The first temperature sensor 14 may be provided in the vicinity of the connection portion with the air saturator 4 in the inside 12.

一方、第2温度センサ15は、飽和空気の流路13の下流側である導管12の噴霧器9との接続部近傍に設けられている。第2温度センサ15は、第1温度センサ14と同様に熱電対や白金抵抗測温体が用いられるが、他の構成のセンサを用いてもよい。本実施例の第2温度センサ15は、導管12の外周面に接して設けられているが、導管12内の飽和空気の温度をより精度よく測定するために、導管12の内部に設けてもよい。この第2温度センサ15は、制御部100へ温度情報を出力する。また、制御部100内には、温度偏差制御部103が設けられている。   On the other hand, the second temperature sensor 15 is provided in the vicinity of the connection portion with the sprayer 9 of the conduit 12 on the downstream side of the saturated air flow path 13. As the second temperature sensor 15, a thermocouple or a platinum resistance thermometer is used similarly to the first temperature sensor 14, but a sensor having another configuration may be used. The second temperature sensor 15 of this embodiment is provided in contact with the outer peripheral surface of the conduit 12, but may be provided inside the conduit 12 in order to measure the temperature of the saturated air in the conduit 12 with higher accuracy. Good. The second temperature sensor 15 outputs temperature information to the control unit 100. A temperature deviation control unit 103 is provided in the control unit 100.

図2の噴霧腐食試験装置1’による、飽和空気温度制御方法について説明する。   A saturated air temperature control method using the spray corrosion test apparatus 1 ′ in FIG. 2 will be described.

本実施例の飽和空気温度の制御方法の特徴は、上記実施例1の制御方法に加えて、以下の通りである。
空気飽和器4内の水を通過して加湿及び加熱された飽和空気の流路13の上流側における温度を、空気飽和器4の上部に設けられた第1温度センサ14により測定する。
また、空気飽和器4から導管12内を通過して噴霧器9に導入される直前の飽和空気の温度を、導管12の噴霧器9との接続部近傍に設けられた第2温度センサ15により測定する。
The feature of the control method of the saturation air temperature of the present embodiment is as follows in addition to the control method of the first embodiment.
The temperature on the upstream side of the flow path 13 of the saturated air that has passed through the water in the air saturator 4 and has been humidified and heated is measured by a first temperature sensor 14 provided in the upper part of the air saturator 4.
Further, the temperature of the saturated air immediately before being introduced into the sprayer 9 from the air saturator 4 through the conduit 12 is measured by a second temperature sensor 15 provided in the vicinity of the connection portion of the conduit 12 with the sprayer 9. .

第1温度センサ14が測定する流路13上流部における飽和空気の温度情報は、制御部100に入力される。また、第2温度センサ15が測定する流路13下流部における飽和空気の温度情報も、同様に制御部100に入力される。   The temperature information of the saturated air in the upstream portion of the flow path 13 measured by the first temperature sensor 14 is input to the control unit 100. Similarly, temperature information of saturated air in the downstream portion of the flow path 13 measured by the second temperature sensor 15 is also input to the control unit 100.

制御部100内の温度偏差制御部103は、第1温度センサ14及び第2温度センサ15で測定された温度情報を基に、空気飽和器4内における飽和空気の温度(本実施例の場合「誘導値」)と噴霧器9に導入される直前の飽和空気の温度を比較し、噴霧器9に導入される直前の飽和空気の温度が「誘導値」となるように、導管12を覆うように設けられた第2ヒータ7に出力信号を与えて制御する。   The temperature deviation control unit 103 in the control unit 100 is based on the temperature information measured by the first temperature sensor 14 and the second temperature sensor 15, and the temperature of the saturated air in the air saturator 4 (in the case of this embodiment, “ The induction value ") is compared with the temperature of saturated air immediately before being introduced into the sprayer 9, and the temperature of the saturated air immediately before being introduced into the sprayer 9 is" inductive value "so as to cover the conduit 12. The second heater 7 is controlled by giving an output signal.

第2ヒータ7は、制御部100の制御によって、導管12の内部を通過する飽和空気の温度が「誘導値」となるまで加熱する。第2ヒータ7の温度制御は、制御が容易なON/OFF動作が通常用いられるが、比例動作やPID動作によって制御してもよい。   The second heater 7 is heated by the control of the control unit 100 until the temperature of the saturated air passing through the inside of the conduit 12 reaches an “induction value”. The temperature control of the second heater 7 is normally performed by an ON / OFF operation that is easy to control, but may be controlled by a proportional operation or a PID operation.

上記の通り、図2に示す本実施例の噴霧腐食試験装置1’及び飽和空気温度制御方法においては、流路13の上流側と下流側にそれぞれ設けられた第1温度センサ14と第2温度センサ15によって飽和空気の温度を測定し、その温度情報を基に導管12の第2ヒータ7を制御することで、噴霧器9に導入される飽和空気の温度を一定に保つことができるため、噴霧時の腐食性溶液の濃度の変動を防止することができる。   As described above, in the spray corrosion test apparatus 1 ′ and the saturated air temperature control method of the present embodiment shown in FIG. 2, the first temperature sensor 14 and the second temperature provided respectively on the upstream side and the downstream side of the flow path 13. Since the temperature of the saturated air is measured by the sensor 15 and the second heater 7 of the conduit 12 is controlled based on the temperature information, the temperature of the saturated air introduced into the sprayer 9 can be kept constant. The fluctuation of the concentration of the corrosive solution at the time can be prevented.

図3は、本発明における噴霧腐食試験装置のブロック図を示すものである。
以下の実施例3においては、上記実施例2と同一機能を果たす箇所には、同一符号を付して説明する。
FIG. 3 shows a block diagram of a spray corrosion test apparatus according to the present invention.
In the following third embodiment, parts having the same functions as those of the second embodiment will be described with the same reference numerals.

本実施例の噴霧腐食試験装置は、図2に示す上記実施例2の噴霧腐食試験装置1’の構造に加えて、圧力調節手段3が空気飽和器4に通す圧縮空気の圧力を任意に設定可能とし、制御部100は、空気飽和器4内の飽和空気の圧力を測定する圧力センサ16の情報を基に試験槽8内の噴霧器9に導入する飽和空気が試験槽8内で噴霧する際に槽内温度と同温の飽和空気となるように飽和空気の温度を設定することを特徴とする。   In addition to the structure of the spray corrosion test apparatus 1 ′ of the second embodiment shown in FIG. 2, the spray corrosion test apparatus of the present embodiment arbitrarily sets the pressure of the compressed air that the pressure adjusting means 3 passes through the air saturator 4. The control unit 100 enables the saturated air to be introduced into the sprayer 9 in the test tank 8 based on the information of the pressure sensor 16 that measures the pressure of the saturated air in the air saturator 4 to spray in the test tank 8. The temperature of the saturated air is set so that the saturated air has the same temperature as the temperature inside the tank.

制御部100内の温度設定部101は、試験槽8内の噴霧器9に導入される圧縮された飽和空気が試験槽8内で噴出する際に、槽内温度と同温の飽和空気になるように、予め設定した槽内温度と圧力センサ16で測定された実際の圧力情報から新たな「誘導値」を設定する。温度制御部102は新たな「誘導値」を基に飽和空気の温度を制御する。   When the compressed saturated air introduced into the sprayer 9 in the test tank 8 is jetted in the test tank 8, the temperature setting unit 101 in the control unit 100 becomes saturated air having the same temperature as the temperature in the tank. In addition, a new “induction value” is set from the tank temperature set in advance and the actual pressure information measured by the pressure sensor 16. The temperature control unit 102 controls the temperature of the saturated air based on the new “induction value”.

図3に示す制御部100を備えた噴霧腐食試験装置による、飽和空気温度制御方法について説明する。   The saturated air temperature control method by the spray corrosion test apparatus provided with the control part 100 shown in FIG. 3 is demonstrated.

本実施例の飽和空気温度の制御方法の特徴は、上記実施例2の飽和空気温度制御方法に加えて以下の点にある。
すなわち、圧縮空気の圧力を任意に設定可能とし、また、制御部100は、噴霧器9に導入される飽和空気が、試験槽8内で噴出する際に槽内温度と同温の飽和空気となるように、槽内温度と空気飽和器4で測定された実際の圧力との相関関係から求める温度となるように制御している。
In addition to the saturation air temperature control method of the second embodiment, the feature of the saturation air temperature control method of the present embodiment is as follows.
That is, the pressure of the compressed air can be arbitrarily set, and the control unit 100 becomes saturated air having the same temperature as the temperature in the tank when the saturated air introduced into the sprayer 9 is ejected in the test tank 8. Thus, it controls so that it may become the temperature calculated | required from the correlation of the tank internal temperature and the actual pressure measured with the air saturator 4. FIG.

コンプレッサ2から空気飽和器4内の加湿手段5に送られる圧縮空気の圧力を、圧力調節手段3の図示しない圧力調節部によって設定する。ここで設定する圧縮空気の圧力値は、試料Sへ落下する微細粒子となった腐食性溶液の噴霧量に基づいて、非特許文献2に記載の噴霧圧力の制御範囲0.07〜0.17MPaから試験者が任意に設定する。一般的に、噴霧圧力を低圧に設定すると低噴霧量となり、高圧に設定すると高噴霧量となる。   The pressure of the compressed air sent from the compressor 2 to the humidifying means 5 in the air saturator 4 is set by a pressure adjusting unit (not shown) of the pressure adjusting means 3. The pressure value of the compressed air set here is based on the spray amount of the corrosive solution that has become fine particles falling on the sample S, and the control range of the spray pressure described in Non-Patent Document 2 is 0.07 to 0.17 MPa. To be set arbitrarily by the examiner. Generally, when the spray pressure is set to a low pressure, a low spray amount is obtained, and when the spray pressure is set to a high pressure, a high spray amount is obtained.

コンプレッサ2から空気飽和器4内に送られた飽和空気の圧力の値を、空気飽和器4内の上部に内設されている圧力センサ16が測定し、その圧力情報は制御部100に入力される。制御部100内の温度設定部101は、噴霧器9に導入する飽和空気が試験槽8内で噴出する際に、槽内温度と同温の飽和空気になるように、予め設定した槽内温度と圧力センサ16より入力された実際の圧力情報を基に新たな「誘導値」を設定する。その後、温度制御部102は新たな「誘導値」と第1温度センサ14より入力された温度情報に基づいて第1ヒータ6を制御する。   The pressure sensor 16 installed in the upper part of the air saturator 4 measures the pressure value of the saturated air sent from the compressor 2 into the air saturator 4, and the pressure information is input to the control unit 100. The The temperature setting unit 101 in the control unit 100 has a tank internal temperature set in advance so that saturated air to be introduced into the sprayer 9 is jetted in the test tank 8 to become saturated air having the same temperature as the tank internal temperature. A new “induction value” is set based on the actual pressure information input from the pressure sensor 16. Thereafter, the temperature control unit 102 controls the first heater 6 based on the new “induction value” and the temperature information input from the first temperature sensor 14.

ここで、温度設定部101による、圧力を変動させた際の飽和空気の「誘導値」の設定方法について説明する。   Here, a method of setting the “induction value” of saturated air when the pressure is changed by the temperature setting unit 101 will be described.

大気圧をP、圧力センサ16が測定する空気飽和器4内の飽和空気の圧力の値をP、試験槽8の槽内温度と同温の水の飽和蒸気圧をPsat1とすると、以下の式(1)によって飽和空気の「誘導値」となる水温の飽和蒸気圧Psat2が求められる。

Figure 0005913197
ここで、大気圧Pは標準気圧0.101325MPaとする。 If the atmospheric pressure is P A , the pressure value of saturated air in the air saturator 4 measured by the pressure sensor 16 is P B , and the saturated vapor pressure of water having the same temperature as the temperature in the test tank 8 is P sat1 , The saturated vapor pressure P sat2 of the water temperature that becomes the “induction value” of saturated air is obtained by the following equation (1).
Figure 0005913197
Here, the atmospheric pressure P A is the standard pressure 0.101325MPa.

本実施例では、微細粒子となった腐食性溶液の噴霧量を増やすため、圧力調節手段3で制御する圧縮空気の圧力の値及び圧力センサで測定される飽和空気の圧力の値Pを0.135MPaとした。 In this embodiment, in order to increase the spray amount of the corrosive solution that has become fine particles, the pressure value of compressed air controlled by the pressure adjusting means 3 and the pressure value P B of saturated air measured by the pressure sensor are set to 0. 135 MPa.

温度設定部101には、以下の表(1)に示すような水の温度と飽和蒸気圧との関係がデータとして記録されている。前記JIS Z2371規定の塩水噴霧試験の槽内温度は35℃であるため、本実施例の式(1)における槽内温度と同温の水の飽和蒸気圧Psat1は、温度設定部101に記録されているデータより42.2mmHgとなる。

Figure 0005913197
In the temperature setting unit 101, the relationship between the water temperature and the saturated vapor pressure as shown in the following table (1) is recorded as data. Since the temperature in the tank of the salt spray test specified in JIS Z2371 is 35 ° C., the saturated vapor pressure P sat1 of water having the same temperature as the temperature in the tank in the equation (1) of this example is recorded in the temperature setting unit 101. It is 42.2 mmHg from the measured data.
Figure 0005913197

空気飽和器4内における飽和空気の圧力値Pと槽内温度と同温の水の飽和蒸気圧Psat1から前記式(1)を用いて算出すると、飽和空気の「誘導値」となる水温の飽和蒸気圧Psat2は97.175mmHgとなる。 When calculated by using the formula from the saturated vapor pressure P sat1 pressure value P B and the chamber temperature and the same temperature of the water in the saturated air in the air saturator 4 (1), the water temperature as the "induction value" of saturated air The saturated vapor pressure P sat2 is 97.175 mmHg.

温度設定部101は、式(1)により算出された飽和蒸気圧値に最も近い飽和蒸気圧である水温を、空気飽和器で設定する飽和空気の「誘導値」として、水の温度と飽和蒸気圧の関係データ(表1)より選択する。本実施例において、算出された飽和蒸気圧値Psat2は97.175mmHgであるため、飽和空気の「誘導値」は前記飽和蒸気圧値に最も近い飽和蒸気圧である51℃となる。 The temperature setting unit 101 uses the water temperature, which is the saturated vapor pressure closest to the saturated vapor pressure value calculated by the equation (1), as the “induction value” of saturated air set by the air saturator, and the temperature of water and saturated steam. Select from pressure relationship data (Table 1). In this embodiment, the calculated saturated vapor pressure value P sat2 is 97.175 mmHg, so the “induction value” of saturated air is 51 ° C., which is the saturated vapor pressure closest to the saturated vapor pressure value.

上記の通り、図3に示す制御部100を備えた噴霧腐食試験装置1及び飽和空気温度制御方法においては、空気飽和器4に送る空気の圧力を任意に設定可能とし、空気飽和器4内に内設された圧力センサ16で測定した圧力値に基づいて飽和空気の温度を設定することにより、圧力を変化させた場合においても、試験槽8内に噴出する際に槽内温度と同温の飽和空気とすることができるため、試験槽8内での腐食性溶液の噴霧量を調節可能とし、かつ濃度の変動を防止することができる。   As described above, in the spray corrosion test apparatus 1 and the saturated air temperature control method including the control unit 100 shown in FIG. 3, the pressure of the air sent to the air saturator 4 can be arbitrarily set, and the air saturator 4 Even when the pressure is changed by setting the temperature of the saturated air based on the pressure value measured by the pressure sensor 16 provided therein, when the pressure is changed, the temperature is the same as the temperature in the tank. Since saturated air can be used, the spray amount of the corrosive solution in the test tank 8 can be adjusted, and fluctuations in concentration can be prevented.

なお、本実施例においては、第2ヒータ7と、流路13の上流と下流にそれぞれ位置する第1温度センサ14及び第2温度センサ15を備えた構成の例を示したが、本発明はこれに限定されるものではない。例えば、図1の第1温度センサ14を1つのみ設けた噴霧腐食試験装置1においても、圧縮空気の圧力を任意に設定可能とし、飽和空気の温度を実際の噴霧圧力との相関関係から求めた「誘導値」に制御することができる。   In the present embodiment, an example of a configuration provided with the second heater 7 and the first temperature sensor 14 and the second temperature sensor 15 respectively positioned upstream and downstream of the flow path 13 is shown. It is not limited to this. For example, even in the spray corrosion test apparatus 1 provided with only one first temperature sensor 14 of FIG. 1, the pressure of the compressed air can be arbitrarily set, and the temperature of the saturated air is obtained from the correlation with the actual spray pressure. It can be controlled to “induction value”.

また、本実施例において、飽和空気の圧力は圧力調節手段3の図示しない圧力調節部によって温度とは独立に制御しているが、例えば、制御部100内に圧力設定部(図示しない)を設け、制御部100に各種データを入力するタッチパネル20により圧力の設定値を入力し、圧力調節手段3へ出力信号を与えて制御してもよい。   In the present embodiment, the pressure of the saturated air is controlled independently of the temperature by a pressure adjusting unit (not shown) of the pressure adjusting means 3. For example, a pressure setting unit (not shown) is provided in the control unit 100. Alternatively, a pressure set value may be input by the touch panel 20 for inputting various data to the control unit 100, and an output signal may be given to the pressure adjusting means 3 for control.

1、1’ 噴霧腐食試験装置
2 コンプレッサ
3 圧力調節手段
4 空気飽和器
5 加湿手段
6 第1ヒータ
7 第2ヒータ
8 試験槽
9 噴霧器
10 空気ノズル
11 液ノズル
12 導管
13 流路
14 第1温度センサ
15 第2温度センサ
16 圧力センサ
17 溶液タンク
18 供給管
19 操作パネル
20 タッチパネル
100 制御部
101 温度設定部
102 温度制御部
103 温度偏差制御部

S 試料
DESCRIPTION OF SYMBOLS 1, 1 'Spray corrosion test apparatus 2 Compressor 3 Pressure adjustment means 4 Air saturator 5 Humidification means 6 1st heater 7 2nd heater 8 Test tank 9 Sprayer 10 Air nozzle 11 Liquid nozzle 12 Pipe 13 Flow path 14 1st temperature sensor DESCRIPTION OF SYMBOLS 15 2nd temperature sensor 16 Pressure sensor 17 Solution tank 18 Supply pipe 19 Operation panel 20 Touch panel 100 Control part 101 Temperature setting part 102 Temperature control part 103 Temperature deviation control part

S sample

Claims (6)

噴霧腐食試験における飽和空気温度制御方法において、圧縮空気を空気飽和器に通して飽和空気とし、この飽和空気を噴霧器に導入する流路であり、前記空気飽和器の上部と前記空気飽和器と前記噴霧器とを繋げる導管のいずれかの部位に第1温度センサを設け、前記噴霧器に導入する飽和空気の温度を測定し、測定した温度情報に基づいて制御部が前記空気飽和器内の第1ヒータを作動させ、飽和空気の温度を制御することを特徴とする噴霧腐食試験における飽和空気温度制御方法。  In the saturated air temperature control method in the spray corrosion test, compressed air is passed through an air saturator to form saturated air, and the saturated air is introduced into the sprayer. The upper part of the air saturator, the air saturator, and the A first temperature sensor is provided in any part of the conduit connecting the sprayer, the temperature of the saturated air introduced into the sprayer is measured, and the control unit controls the first heater in the air saturationr based on the measured temperature information And controlling the saturated air temperature in the spray corrosion test. 前記第1温度センサを前記空気飽和器の上部または前記導管内の前記空気飽和器との接続部近傍のいずれかの部位に設ける一方、前記導管の前記噴霧器との接続部近傍に位置する第2温度センサ及び前記導管の全体を覆う第2ヒータを設け、前記第1温度センサ及び前記第2温度センサとで測定された飽和空気の温度情報を前記制御部に送り、その温度情報に基づいて前記噴霧器に送られる飽和空気が前記試験槽内で槽内温度と同温の飽和空気となるように前記第2ヒータを作動させて飽和空気を加熱することを特徴とする請求項1記載の噴霧腐食試験における飽和空気温度制御方法。The first temperature sensor is provided at any location near the connection with the air saturator in the conduit or at the top of the air saturator, while the second temperature sensor is located near the connection with the sprayer in the conduit . A temperature sensor and a second heater that covers the entire conduit are provided, temperature information of saturated air measured by the first temperature sensor and the second temperature sensor is sent to the control unit, and the temperature information is based on the temperature information. 2. The spray corrosion according to claim 1, wherein the second heater is operated to heat the saturated air so that the saturated air sent to the sprayer becomes saturated air having the same temperature as the inside temperature in the test tank. Saturated air temperature control method in the test. 圧縮空気の圧力を任意に設定可能とし、前記制御部が、前記噴霧器に導入される飽和空気が、前記試験槽内で噴出する際に槽内温度と同温の飽和空気となるように、槽内温度と前記空気飽和器で測定された実際の圧力との相関関係から求める温度に飽和空気の温度を設定することを特徴とする請求項1または2記載の噴霧腐食試験における飽和空気温度制御方法。  The pressure of the compressed air can be arbitrarily set, and the control unit allows the saturated air introduced into the sprayer to become saturated air having the same temperature as the temperature in the tank when jetted in the test tank. 3. The saturated air temperature control method in the spray corrosion test according to claim 1, wherein the temperature of the saturated air is set to a temperature obtained from a correlation between an internal temperature and an actual pressure measured by the air saturator. . 圧縮空気を生成するコンプレッサと、圧縮空気の圧力を制御する圧力調節手段と、圧縮空気を飽和空気にするための空気飽和器と、圧縮空気を前記空気飽和器内の水に通して飽和空気とする加湿手段と、前記空気飽和器内の水を加熱する第1ヒータと、飽和空気を前記空気飽和器から試験槽内の噴霧器に送る導管と、飽和空気の温度を測定するために飽和空気を前記噴霧器に導入する流路である前記空気飽和器の上部から前記導管のいずれかの部位に位置する第1温度センサと、前記第1温度センサで測定された温度情報を基に前記第1ヒータを制御する制御部とを備えることを特徴とする噴霧腐食試験装置。  A compressor for generating compressed air; pressure adjusting means for controlling the pressure of the compressed air; an air saturator for making compressed air into saturated air; and saturated air by passing compressed air through water in the air saturator; Humidifying means, a first heater for heating water in the air saturator, a conduit for sending saturated air from the air saturator to a sprayer in a test tank, and saturated air for measuring the temperature of the saturated air. A first temperature sensor located in any part of the conduit from above the air saturator, which is a flow path to be introduced into the sprayer, and the first heater based on temperature information measured by the first temperature sensor A spray corrosion test apparatus comprising: a control unit that controls 前記第1温度センサを前記空気飽和器の上部または前記導管内の前記空気飽和器との接続部近傍のいずれかの部位に設け、前記導管の前記噴霧器との接続部近傍に位置し、前記噴霧器に導入する直前の飽和空気の温度を測定し、その温度情報を前記制御部に出力する第2温度センサと、前記導管の全体を覆うように設けられ、前記制御部によって制御される第2ヒータとを有することを特徴とする請求項4記載の噴霧腐食試験装置。The first temperature sensor is provided in any part of the conduit in the vicinity of the connection with the air saturator in the upper part of the air saturator, and located in the vicinity of the connection of the conduit with the sprayer. A second temperature sensor that measures the temperature of the saturated air immediately before being introduced to the controller and outputs the temperature information to the controller, and a second heater that is provided so as to cover the entire conduit and is controlled by the controller The spray corrosion test apparatus according to claim 4, wherein 前記圧力調節手段は前記空気飽和器に通す圧縮空気の圧力を任意に設定可能とし、前記制御部は、前記空気飽和器内の飽和空気の圧力を測定する圧力センサの情報を基に前記試験槽内の噴霧器に導入する飽和空気が前記試験槽内で噴出する際に槽内温度と同温の飽和空気となるように飽和空気の温度を設定することを特徴とする請求項4または5記載の噴霧腐食試験装置。  The pressure adjusting means can arbitrarily set the pressure of the compressed air that passes through the air saturator, and the control unit is based on information from a pressure sensor that measures the pressure of the saturated air in the air saturator. 6. The temperature of the saturated air is set so that the saturated air introduced into the inside sprayer becomes saturated air having the same temperature as the temperature inside the tank when the saturated air is ejected in the test tank. Spray corrosion test equipment.
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