JP5857434B2

JP5857434B2 - 非水系電解液及びそれを用いた非水系電解液電池

非水系電解液及びそれを用いた非水系電解液電池 Download PDF

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Publication number: JP5857434B2
Authority: JP; Japan
Prior art keywords: carbonate; aqueous electrolyte; group; less; mass
Prior art date: 2011-04-21
Legal status : Active

Application number

JP2011095370A

Other languages

English (en)

Japanese (ja)

Other versions

JP2012227060A (ja

JP2012227060A5 (https=

Inventor

浩二深水

脩平澤

Current Assignee

Mitsubishi Chemical Corp

Original Assignee

Mitsubishi Chemical Corp

Priority date

2011-04-21

Filing date

2011-04-21

Publication date

2016-02-10

2011-04-21 Priority to JP2011095370A priority Critical patent/JP5857434B2/ja

2011-04-21 Application filed by Mitsubishi Chemical Corp filed Critical Mitsubishi Chemical Corp

2011-05-12 Priority to KR1020137006082A priority patent/KR20130108286A/ko

2011-05-12 Priority to PCT/JP2011/060926 priority patent/WO2012035821A1/ja

2011-05-12 Priority to EP11824833.5A priority patent/EP2618418A4/en

2011-05-12 Priority to CN2011800438576A priority patent/CN103109410A/zh

2012-11-15 Publication of JP2012227060A publication Critical patent/JP2012227060A/ja

2013-03-15 Priority to US13/842,473 priority patent/US9553333B2/en

2014-04-24 Publication of JP2012227060A5 publication Critical patent/JP2012227060A5/ja

2016-02-10 Application granted granted Critical

2016-02-10 Publication of JP5857434B2 publication Critical patent/JP5857434B2/ja

Status Active legal-status Critical Current

2031-04-21 Anticipated expiration legal-status Critical

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239000011255 nonaqueous electrolyte Substances 0.000 title claims description 144
150000001875 compounds Chemical class 0.000 claims description 83
150000005676 cyclic carbonates Chemical class 0.000 claims description 68
239000003125 aqueous solvent Substances 0.000 claims description 35
125000004432 carbon atom Chemical group C* 0.000 claims description 34
229910052731 fluorine Inorganic materials 0.000 claims description 28
125000001153 fluoro group Chemical group F* 0.000 claims description 22
125000001261 isocyanato group Chemical group *N=C=O 0.000 claims description 22
229910052799 carbon Inorganic materials 0.000 claims description 19
229910003002 lithium salt Inorganic materials 0.000 claims description 18
HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 17
229910001416 lithium ion Inorganic materials 0.000 claims description 17
159000000002 lithium salts Chemical class 0.000 claims description 17
125000000524 functional group Chemical group 0.000 claims description 15
229910052760 oxygen Inorganic materials 0.000 claims description 15
229910052717 sulfur Inorganic materials 0.000 claims description 15
229910052757 nitrogen Inorganic materials 0.000 claims description 14
239000003792 electrolyte Substances 0.000 claims description 13
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 13
125000000962 organic group Chemical group 0.000 claims description 11
125000005843 halogen group Chemical group 0.000 claims description 9
125000004429 atom Chemical group 0.000 claims description 8
125000004433 nitrogen atom Chemical group N* 0.000 claims description 8
229910052698 phosphorus Inorganic materials 0.000 claims description 7
125000004430 oxygen atom Chemical group O* 0.000 claims description 6
125000004437 phosphorous atom Chemical group 0.000 claims description 6
125000004434 sulfur atom Chemical group 0.000 claims description 6
125000001183 hydrocarbyl group Chemical group 0.000 claims 3
-1 cyclic carboxylic acid esters Chemical class 0.000 description 90
229940021013 electrolyte solution Drugs 0.000 description 70
229910052744 lithium Inorganic materials 0.000 description 55
239000007774 positive electrode material Substances 0.000 description 54
229910052751 metal Inorganic materials 0.000 description 51
239000002184 metal Substances 0.000 description 44
238000003860 storage Methods 0.000 description 44
239000003575 carbonaceous material Substances 0.000 description 43
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 42
230000000694 effects Effects 0.000 description 40
KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 description 39
239000010410 layer Substances 0.000 description 39
239000007773 negative electrode material Substances 0.000 description 37
150000005678 chain carbonates Chemical class 0.000 description 29
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 27
125000001424 substituent group Chemical group 0.000 description 27
239000002245 particle Substances 0.000 description 25
IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 24
239000007789 gas Substances 0.000 description 24
239000000463 material Substances 0.000 description 24
238000000034 method Methods 0.000 description 24
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 23
239000011230 binding agent Substances 0.000 description 21
JBTWLSYIZRCDFO-UHFFFAOYSA-N ethyl methyl carbonate Chemical compound CCOC(=O)OC JBTWLSYIZRCDFO-UHFFFAOYSA-N 0.000 description 21
239000002904 solvent Substances 0.000 description 21
230000007423 decrease Effects 0.000 description 20
RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 description 20
238000004519 manufacturing process Methods 0.000 description 19
OIFBSDVPJOWBCH-UHFFFAOYSA-N Diethyl carbonate Chemical compound CCOC(=O)OCC OIFBSDVPJOWBCH-UHFFFAOYSA-N 0.000 description 18
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PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 14
239000000956 alloy Substances 0.000 description 14
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239000008151 electrolyte solution Substances 0.000 description 14
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239000010936 titanium Substances 0.000 description 14
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 13
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238000013329 compounding Methods 0.000 description 12
239000011737 fluorine Substances 0.000 description 12
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239000010409 thin film Substances 0.000 description 11
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IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
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239000012752 auxiliary agent Substances 0.000 description 10
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UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
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229920003048 styrene butadiene rubber Polymers 0.000 description 9
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CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 8
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101150058243 Lipf gene Proteins 0.000 description 8
239000002033 PVDF binder Substances 0.000 description 8
238000001069 Raman spectroscopy Methods 0.000 description 8
239000011149 active material Substances 0.000 description 8
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 8
125000000217 alkyl group Chemical group 0.000 description 8
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 8
239000011203 carbon fibre reinforced carbon Substances 0.000 description 8
238000000576 coating method Methods 0.000 description 8
230000000052 comparative effect Effects 0.000 description 8
238000012423 maintenance Methods 0.000 description 8
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 8
239000003960 organic solvent Substances 0.000 description 8
229920002981 polyvinylidene fluoride Polymers 0.000 description 8
239000011164 primary particle Substances 0.000 description 8
YTZKOQUCBOVLHL-UHFFFAOYSA-N tert-butylbenzene Chemical compound CC(C)(C)C1=CC=CC=C1 YTZKOQUCBOVLHL-UHFFFAOYSA-N 0.000 description 8
150000003624 transition metals Chemical class 0.000 description 8
VAYTZRYEBVHVLE-UHFFFAOYSA-N 1,3-dioxol-2-one Chemical compound O=C1OC=CO1 VAYTZRYEBVHVLE-UHFFFAOYSA-N 0.000 description 7
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 7
SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 7
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 7
125000003118 aryl group Chemical group 0.000 description 7
235000011132 calcium sulphate Nutrition 0.000 description 7
239000011248 coating agent Substances 0.000 description 7
229920001971 elastomer Polymers 0.000 description 7
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 7
230000002349 favourable effect Effects 0.000 description 7
239000011888 foil Substances 0.000 description 7
239000001257 hydrogen Substances 0.000 description 7
229910052739 hydrogen Inorganic materials 0.000 description 7
230000009257 reactivity Effects 0.000 description 7
238000007086 side reaction Methods 0.000 description 7
YJTKZCDBKVTVBY-UHFFFAOYSA-N 1,3-Diphenylbenzene Chemical group C1=CC=CC=C1C1=CC=CC(C=2C=CC=CC=2)=C1 YJTKZCDBKVTVBY-UHFFFAOYSA-N 0.000 description 6
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 6
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 6
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 6
150000001491 aromatic compounds Chemical class 0.000 description 6
150000001733 carboxylic acid esters Chemical class 0.000 description 6
229910052804 chromium Inorganic materials 0.000 description 6
239000011651 chromium Substances 0.000 description 6
TXCDCPKCNAJMEE-UHFFFAOYSA-N dibenzofuran Chemical compound C1=CC=C2C3=CC=CC=C3OC2=C1 TXCDCPKCNAJMEE-UHFFFAOYSA-N 0.000 description 6
DGTVXEHQMSJRPE-UHFFFAOYSA-M difluorophosphinate Chemical compound [O-]P(F)(F)=O DGTVXEHQMSJRPE-UHFFFAOYSA-M 0.000 description 6
ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 6
USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 6
238000011049 filling Methods 0.000 description 6
239000003112 inhibitor Substances 0.000 description 6
229910052742 iron Inorganic materials 0.000 description 6
239000011572 manganese Substances 0.000 description 6
239000002905 metal composite material Substances 0.000 description 6
239000007769 metal material Substances 0.000 description 6
229940074371 monofluorophosphate Drugs 0.000 description 6
239000000843 powder Substances 0.000 description 6
239000005060 rubber Substances 0.000 description 6
229910052710 silicon Inorganic materials 0.000 description 6
229910052718 tin Inorganic materials 0.000 description 6
IKYNWXNXXHWHLL-UHFFFAOYSA-N 1,3-diisocyanatopropane Chemical compound O=C=NCCCN=C=O IKYNWXNXXHWHLL-UHFFFAOYSA-N 0.000 description 5
239000005977 Ethylene Substances 0.000 description 5
229910013870 LiPF 6 Inorganic materials 0.000 description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
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ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 5
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
238000002441 X-ray diffraction Methods 0.000 description 5
125000001931 aliphatic group Chemical group 0.000 description 5
125000002947 alkylene group Chemical group 0.000 description 5
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150000001721 carbon Chemical group 0.000 description 5
150000004649 carbonic acid derivatives Chemical class 0.000 description 5
238000001035 drying Methods 0.000 description 5
125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 5
238000011156 evaluation Methods 0.000 description 5
239000011521 glass Substances 0.000 description 5
229910052736 halogen Inorganic materials 0.000 description 5
150000002367 halogens Chemical class 0.000 description 5
230000020169 heat generation Effects 0.000 description 5
239000005001 laminate film Substances 0.000 description 5
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229910001386 lithium phosphate Inorganic materials 0.000 description 5
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150000002739 metals Chemical class 0.000 description 5
229920001343 polytetrafluoroethylene Polymers 0.000 description 5
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239000011148 porous material Substances 0.000 description 5
238000012360 testing method Methods 0.000 description 5
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 5
TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 description 5
239000008096 xylene Substances 0.000 description 5
QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 4
125000004206 2,2,2-trifluoroethyl group Chemical group [H]C([H])(*)C(F)(F)F 0.000 description 4
QHTJSSMHBLGUHV-UHFFFAOYSA-N 2-methylbutan-2-ylbenzene Chemical compound CCC(C)(C)C1=CC=CC=C1 QHTJSSMHBLGUHV-UHFFFAOYSA-N 0.000 description 4
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 4
229910013063 LiBF 4 Inorganic materials 0.000 description 4
229910012851 LiCoO 2 Inorganic materials 0.000 description 4
BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 description 4
239000004698 Polyethylene Substances 0.000 description 4
XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 4
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
238000001237 Raman spectrum Methods 0.000 description 4
KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 4
239000001569 carbon dioxide Substances 0.000 description 4
229910002092 carbon dioxide Inorganic materials 0.000 description 4
239000011889 copper foil Substances 0.000 description 4
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
HHNHBFLGXIUXCM-GFCCVEGCSA-N cyclohexylbenzene Chemical compound [CH]1CCCC[C@@H]1C1=CC=CC=C1 HHNHBFLGXIUXCM-GFCCVEGCSA-N 0.000 description 4
230000006866 deterioration Effects 0.000 description 4
238000010494 dissociation reaction Methods 0.000 description 4
230000005593 dissociations Effects 0.000 description 4
FKRCODPIKNYEAC-UHFFFAOYSA-N ethyl propionate Chemical compound CCOC(=O)CC FKRCODPIKNYEAC-UHFFFAOYSA-N 0.000 description 4
125000004216 fluoromethyl group Chemical group [H]C([H])(F)* 0.000 description 4
GAEKPEKOJKCEMS-UHFFFAOYSA-N gamma-valerolactone Chemical compound CC1CCC(=O)O1 GAEKPEKOJKCEMS-UHFFFAOYSA-N 0.000 description 4
229910002804 graphite Inorganic materials 0.000 description 4
239000010439 graphite Substances 0.000 description 4
150000002500 ions Chemical class 0.000 description 4
SWAIALBIBWIKKQ-UHFFFAOYSA-N lithium titanium Chemical compound [Li].[Ti] SWAIALBIBWIKKQ-UHFFFAOYSA-N 0.000 description 4
230000014759 maintenance of location Effects 0.000 description 4
150000001247 metal acetylides Chemical class 0.000 description 4
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
229910052758 niobium Inorganic materials 0.000 description 4
150000004767 nitrides Chemical class 0.000 description 4
238000006864 oxidative decomposition reaction Methods 0.000 description 4
229920000573 polyethylene Polymers 0.000 description 4
229910052700 potassium Inorganic materials 0.000 description 4
239000011163 secondary particle Substances 0.000 description 4
239000010703 silicon Substances 0.000 description 4
229910052708 sodium Inorganic materials 0.000 description 4
239000011734 sodium Substances 0.000 description 4
229920006132 styrene block copolymer Polymers 0.000 description 4
HHVIBTZHLRERCL-UHFFFAOYSA-N sulfonyldimethane Chemical compound CS(C)(=O)=O HHVIBTZHLRERCL-UHFFFAOYSA-N 0.000 description 4
150000003467 sulfuric acid derivatives Chemical class 0.000 description 4
DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 4
229910052720 vanadium Inorganic materials 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
238000003466 welding Methods 0.000 description 4
229910052725 zinc Inorganic materials 0.000 description 4
JCSRVIQQOQNBKC-UHFFFAOYSA-N 1,1,2,2-tetrafluoro-3-(2,2,3,3-tetrafluoropropoxy)propane Chemical compound FC(F)C(F)(F)COCC(F)(F)C(F)F JCSRVIQQOQNBKC-UHFFFAOYSA-N 0.000 description 3
XSCLFFBWRKTMTE-UHFFFAOYSA-N 1,3-bis(isocyanatomethyl)cyclohexane Chemical compound O=C=NCC1CCCC(CN=C=O)C1 XSCLFFBWRKTMTE-UHFFFAOYSA-N 0.000 description 3
239000005057 Hexamethylene diisocyanate Substances 0.000 description 3
FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 3
229920000459 Nitrile rubber Polymers 0.000 description 3
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 3
AUBNQVSSTJZVMY-UHFFFAOYSA-M P(=O)([O-])(O)O.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.[Li+] Chemical compound P(=O)([O-])(O)O.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.C(C(=O)O)(=O)F.[Li+] AUBNQVSSTJZVMY-UHFFFAOYSA-M 0.000 description 3
239000005062 Polybutadiene Substances 0.000 description 3
239000004743 Polypropylene Substances 0.000 description 3
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
230000002159 abnormal effect Effects 0.000 description 3
239000006230 acetylene black Substances 0.000 description 3
DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 3
229910000410 antimony oxide Inorganic materials 0.000 description 3
239000007864 aqueous solution Substances 0.000 description 3
239000004760 aramid Substances 0.000 description 3
XKRFYHLGVUSROY-UHFFFAOYSA-N argon Substances [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 3
229910052786 argon Inorganic materials 0.000 description 3
229920003235 aromatic polyamide Polymers 0.000 description 3
229910021383 artificial graphite Inorganic materials 0.000 description 3
230000001588 bifunctional effect Effects 0.000 description 3
239000004305 biphenyl Substances 0.000 description 3
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229910000416 bismuth oxide Inorganic materials 0.000 description 3
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230000001590 oxidative effect Effects 0.000 description 1
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QIIPQYDSKRYMFG-UHFFFAOYSA-N phenyl hydrogen carbonate Chemical class OC(=O)OC1=CC=CC=C1 QIIPQYDSKRYMFG-UHFFFAOYSA-N 0.000 description 1
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JAELLLITIZHOGQ-UHFFFAOYSA-N tert-butyl propanoate Chemical compound CCC(=O)OC(C)(C)C JAELLLITIZHOGQ-UHFFFAOYSA-N 0.000 description 1
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
FCFMKFHUNDYKEG-UHFFFAOYSA-N thietane 1,1-dioxide Chemical class O=S1(=O)CCC1 FCFMKFHUNDYKEG-UHFFFAOYSA-N 0.000 description 1
125000000101 thioether group Chemical group 0.000 description 1
229910052721 tungsten Inorganic materials 0.000 description 1
238000001132 ultrasonic dispersion Methods 0.000 description 1
238000007740 vapor deposition Methods 0.000 description 1
239000011800 void material Substances 0.000 description 1
239000013585 weight reducing agent Substances 0.000 description 1
238000004804 winding Methods 0.000 description 1
239000002759 woven fabric Substances 0.000 description 1
PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 1