JP5177703B2 - Foreign matter concentration measurement device in continuous annealing furnace - Google Patents

Foreign matter concentration measurement device in continuous annealing furnace Download PDF

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JP5177703B2
JP5177703B2 JP2010054047A JP2010054047A JP5177703B2 JP 5177703 B2 JP5177703 B2 JP 5177703B2 JP 2010054047 A JP2010054047 A JP 2010054047A JP 2010054047 A JP2010054047 A JP 2010054047A JP 5177703 B2 JP5177703 B2 JP 5177703B2
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三喜夫 川村
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Nippon Steel Corp
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Description

本発明は連続焼鈍炉内の異物濃度測定装置に関するものである。   The present invention relates to a foreign matter concentration measuring apparatus in a continuous annealing furnace.

鋼帯の連続焼鈍炉においては、炉内の異物がロールと鋼板の間に噛みこまれて押し疵となり、鋼帯表面に製品欠陥を生じることがある。特に冷却ガスを直接鋼帯に噴射して鋼帯の冷却を行ういわゆるジェットクーラー式の冷却装置を備えた連続焼鈍炉では、炉内の構造物に堆積した異物が冷却ガスにより巻き上がり、疵を誘発し易い傾向があった。特に粒径が50μm以上の異物が押し疵の原因となっている。   In a continuous annealing furnace for steel strip, foreign matter in the furnace may be caught between the roll and the steel sheet to become a pushing rod, resulting in product defects on the steel strip surface. In particular, in a continuous annealing furnace equipped with a so-called jet cooler type cooling device that cools a steel strip by injecting a cooling gas directly onto the steel strip, foreign matter accumulated in the structure in the furnace is rolled up by the cooling gas, There was a tendency to trigger. In particular, foreign matters having a particle size of 50 μm or more cause the push.

ジェットクーラーにおける、前記製品欠陥の問題に対し、本願出願人は、鋼帯とジェットクーラーのノズルヘッダーとの間にメッシュフェンスを設ける構成によって冷却用ガスに混入していたゴミ・錆等の微粉を、メッシュフェンスで除去し、さらに、メッシュフェンスに冷却水を散水する散水ノズルを設ける構成によってメッシュフェンスに付着したゴミ、錆等の微粉を洗い落す技術を開示している(特許文献1)。   In response to the above-mentioned product defect problem in a jet cooler, the applicant of the present application removes fine powder such as dust and rust mixed in the cooling gas by a configuration in which a mesh fence is provided between the steel strip and the nozzle header of the jet cooler. In addition, a technique is disclosed in which fine particles such as dust and rust adhered to the mesh fence are washed away by a configuration in which the mesh fence is provided with a water spray nozzle for spraying cooling water on the mesh fence (Patent Document 1).

自動車用外板など、特に美麗な鋼板を製造する連続焼鈍炉においては、これらの押し疵の発生原因を特定したり、解決策を検討することによって、押し疵の発生を効果的に回避することが求められており、そのために炉内の異物濃度(粒子径と数)を連続して高精度に測定する技術への需要がある。   In continuous annealing furnaces that produce particularly beautiful steel sheets, such as automotive outer panels, to effectively prevent the occurrence of pushers by identifying the causes of these pushers and examining solutions Therefore, there is a demand for a technique for continuously measuring the concentration of foreign matters (particle diameter and number) in the furnace with high accuracy.

従来、炉内の異物濃度を測定する方法としては、炉内ガスを吸引して円筒ろ紙や円形ろ紙で濾過して異物を採取し、顕微鏡などで観察して定量化する方法が一般に知られている。しかし、この方法は、連続的なデータが得られず、炉内の状況を詳細に把握することが困難であるという問題や、多大な労力と時間が必要であるという問題があった。   Conventionally, as a method for measuring the concentration of foreign matter in the furnace, a method is generally known in which the gas in the furnace is sucked and filtered through a cylindrical filter paper or a circular filter paper to collect foreign matter, and observed and quantified with a microscope or the like. Yes. However, this method has a problem that continuous data cannot be obtained, and it is difficult to grasp the details in the furnace in detail, and that a lot of labor and time are required.

なお、粉塵濃度を連続測定する装置として従来から市販されているパーティクルカウンターでは、測定ガス温度の上限は40℃程度であって、当該上限温度を超える試料を流した場合、高温ガスによってセンサーが破損される。連続焼鈍炉内雰囲気ガス温度は200〜300℃程度になるため、従来市販のパーティクルカウンターによる異物濃度測定は不可能であるという問題があった。また、高温ガスを熱交交換器で冷却する方法も考えられるが伝熱面との接触時間を確保するためにはガスの流速を小さくする必要があるが、その場合、異物が伝熱面に堆積して計測部まで導入することが困難となる。更には流速を低下させずに熱交換器で冷却する場合は伝熱面を相当長くする必要があり、熱交換器が膨大な
規模になるため、現実的には困難である。
In addition, in the particle counter that has been commercially available as a device for continuously measuring the dust concentration, the upper limit of the measurement gas temperature is about 40 ° C. When a sample exceeding the upper limit temperature is flowed, the sensor is damaged by the high-temperature gas. Is done. Since the atmospheric gas temperature in the continuous annealing furnace is about 200 to 300 ° C., there is a problem that it is impossible to measure the concentration of foreign matter using a commercially available particle counter. Although a method of cooling high-temperature gas with a heat exchanger is also conceivable, it is necessary to reduce the gas flow rate in order to ensure contact time with the heat transfer surface. It is difficult to deposit and introduce it to the measuring unit. Furthermore, in the case of cooling with a heat exchanger without reducing the flow velocity, it is necessary to make the heat transfer surface considerably long and the heat exchanger becomes enormous in scale, which is difficult in practice.

特開平7−3337号公報Japanese Patent Laid-Open No. 7-3337

本発明の目的は前記問題を解決し、鋼帯の冷却装置としてジェットクーラーを採用した連続焼鈍炉において、高温の連続焼鈍炉内雰囲気ガス中の異物濃度を、従来市販のパーティクルカウンターを用いて、連続して高精度に測定可能な連続焼鈍炉内の異物濃度測定装置を提供することである。   The object of the present invention is to solve the above problems, and in a continuous annealing furnace adopting a jet cooler as a steel strip cooling device, the foreign matter concentration in the high-temperature continuous annealing furnace atmosphere gas, using a conventional commercially available particle counter, An object of the present invention is to provide a foreign matter concentration measuring device in a continuous annealing furnace capable of continuously measuring with high accuracy.

上記課題を解決するためになされた本発明の連続焼鈍炉内の異物濃度測定装置は、上部に連続焼鈍炉内雰囲気ガスの一部を導入する高温ガス導入口と、異物除去処理後の清浄ガスを排出する清浄ガス排出口を、各々有し、下部に異物を排出する異物排出口を有するサイクロンと、該異物排出口に連結した異物排出管と、該異物排出管を流れる気体に対し、レーザ発振器からのレーザを照射して、該気体中に含まれる異物から反射される散乱光を検知して、その異物数をカウントするパーティクルカウンターからなり、該パーティクルカウンターの前段に、異物排出管内に冷却ガスを吹き込む冷却ガス供給手段を設けたことを特徴とするものである。   The foreign matter concentration measuring device in the continuous annealing furnace of the present invention made to solve the above problems is a high-temperature gas inlet for introducing a part of the atmospheric gas in the continuous annealing furnace to the upper part, and a clean gas after the foreign matter removing treatment A cyclone having a clean gas discharge port for discharging foreign matter at the bottom, a foreign matter discharge port connected to the foreign matter discharge port, and a gas flowing through the foreign matter discharge tube. It consists of a particle counter that irradiates a laser from an oscillator, detects scattered light reflected from the foreign matter contained in the gas, and counts the number of foreign matters, and cools the foreign matter discharge pipe in front of the particle counter. A cooling gas supply means for blowing gas is provided.

請求項2記載の発明は、請求項1記載の連続焼鈍炉内の異物濃度測定装置において、冷却ガス供給手段は、パーティクルカウンターの前段で異物排出管内の気体温度を測定する温度測定手段と、該温度測定手段の温度測定結果に基づいて冷却ガス供給量を決定する冷却ガス供給量決定手段を備えることを特徴とするものである。   The invention according to claim 2 is the foreign matter concentration measuring apparatus in the continuous annealing furnace according to claim 1, wherein the cooling gas supply means is a temperature measuring means for measuring the gas temperature in the foreign matter discharge pipe at the front stage of the particle counter, Cooling gas supply amount determining means for determining the cooling gas supply amount based on the temperature measurement result of the temperature measuring means is provided.

請求項3記載の発明は、請求項2記載の連続焼鈍炉内の異物濃度測定装置を用いて、連続焼鈍炉内の異物濃度測定を行う方法であって、パーティクルカウンターの前段での異物排出管内の気体温度がパーティクルカウンターの使用上限温度以下となるように冷却ガスの供給量を決定することを特徴とするものである。   The invention according to claim 3 is a method for measuring the concentration of foreign matter in the continuous annealing furnace using the foreign matter concentration measuring device in the continuous annealing furnace according to claim 2, wherein the foreign matter concentration in the foreign matter discharge pipe is in front of the particle counter. The supply amount of the cooling gas is determined so that the gas temperature is equal to or lower than the use upper limit temperature of the particle counter.

本発明に係る連続焼鈍炉内の異物濃度測定装置によれば、上部に連続焼鈍炉内雰囲気ガスの一部を導入する高温ガス導入口と、異物除去処理後の清浄ガスを排出する清浄ガスの排出口を、各々有し、下部に異物を排出する異物排出口を有するサイクロンによる処理を経て、異物濃度が濃縮されたガスに、冷却ガスを吹き込んで冷却する構成により、高温ガスによるセンサー破損等の問題を生じることなく、市販のパーティクルカウンターで異物濃度を連続測定することができる。異物濃度を濃縮したガスを試料として、パーティクルカウンターで濃度測定を行うことにより、炉内の異物濃度を連続して高精度に把握することができる。   According to the foreign matter concentration measuring apparatus in the continuous annealing furnace according to the present invention, the high temperature gas inlet for introducing a part of the atmospheric gas in the continuous annealing furnace to the upper part and the clean gas for discharging the clean gas after the foreign matter removal treatment The sensor is damaged by high-temperature gas, etc., by having a cooling gas blown into a gas that has a discharge port, each having a foreign matter discharge port at the lower part, and a process that uses a cyclone that has a foreign matter discharge port to concentrate the concentration of the foreign matter. Thus, the foreign matter concentration can be continuously measured with a commercially available particle counter. By measuring the concentration with a particle counter using a gas with a concentrated foreign matter concentration as a sample, the foreign matter concentration in the furnace can be grasped continuously and with high accuracy.

本発明に係る連続焼鈍炉内の異物濃度測定装置の全体説明図である。It is a whole explanatory view of the foreign substance concentration measuring device in the continuous annealing furnace concerning the present invention. 実施例により、本発明の効果を示す図である。It is a figure which shows the effect of this invention by an Example.

以下に本発明の好ましい実施形態を示す。   Preferred embodiments of the present invention are shown below.

本発明に係る連続焼鈍炉内の異物濃度測定装置は、図1に示すように、サイクロン1と、サイクロン1で分離された異物を排出するためにサイクロン1の下部に設けられた異物排出口4の直下に垂直方向に連結した異物排出管6と、異物排出管6内部に冷却ガスを吹き込む冷却ガス供給手段7と、冷却されたガス中の粒子数を測定するパーティクルカウンター9とから構成されている。パーティクルカウンター9は、従来公知の構成を有するものであって、気体に対し、レーザ発振器からのレーザを、ガルバノミラーを介して照射した際、気体中に含まれる異物(微粒子)から反射される散乱光をレンズ、スリット(を介してフォトマルで検知して、信号処理回路で処理し、その数をカウントし、計数表示器等に表示するものである。   As shown in FIG. 1, the apparatus for measuring the concentration of foreign matter in a continuous annealing furnace according to the present invention includes a cyclone 1 and a foreign matter discharge port 4 provided at the lower part of the cyclone 1 for discharging foreign matter separated by the cyclone 1. A foreign matter discharge pipe 6 connected in the vertical direction directly below the cooling gas supply means 7, a cooling gas supply means 7 for blowing cooling gas into the foreign substance discharge pipe 6, and a particle counter 9 for measuring the number of particles in the cooled gas. Yes. The particle counter 9 has a conventionally known configuration, and when the gas is irradiated with a laser from a laser oscillator via a galvano mirror, the particle counter 9 is reflected from foreign matter (fine particles) contained in the gas. Light is detected by a photomultiplier through a lens and a slit, processed by a signal processing circuit, counted, and displayed on a counting display or the like.

サイクロン1の全体形状は、除去したい異物の直径と密度、および流体の物性と風量をパラメータとする従来公知の一般式により決定することができる。   The overall shape of the cyclone 1 can be determined by a conventionally known general formula using parameters such as the diameter and density of a foreign substance to be removed and the physical properties and air volume of a fluid.

サイクロン1は、上部に連続焼鈍炉内雰囲気ガスの一部を導入する高温ガス導入口2と、異物除去処理後の清浄ガスを排出する清浄ガス排出口3を、各々有し、下部に異物を排出する異物排出口4を有する。またサイクロン下部にバイブレータ5を設置して、サイクロン下部の傾斜部分への異物堆積を防止することが好ましい。   The cyclone 1 has a high-temperature gas introduction port 2 for introducing a part of the atmospheric gas in the continuous annealing furnace at the upper portion and a clean gas discharge port 3 for discharging the clean gas after the foreign matter removal treatment, and has a foreign matter at the lower portion. It has a foreign matter discharge port 4 for discharging. Moreover, it is preferable to install a vibrator 5 at the lower part of the cyclone to prevent foreign matter from accumulating on the inclined part at the lower part of the cyclone.

連続焼鈍炉内雰囲気ガスは、清浄ガス排出口3の後段に設置した連続焼鈍炉内雰囲気ガス吸引手段10によって、サイクロン1内へと吸引される。連続焼鈍炉内雰囲気ガス吸引手段10としては、耐熱性の吸引ポンプやイジェクタ等、任意の吸引手段を採用することができるが、コスト面からイジェクタを採用することが特に好ましい。   The atmosphere gas in the continuous annealing furnace is sucked into the cyclone 1 by the atmosphere gas suction means 10 in the continuous annealing furnace installed at the subsequent stage of the clean gas discharge port 3. As the atmospheric gas suction means 10 in the continuous annealing furnace, any suction means such as a heat-resistant suction pump or ejector can be adopted, but it is particularly preferable to adopt an ejector from the viewpoint of cost.

連続焼鈍炉内雰囲気ガスは、約200〜300℃の高温ガスである。サイクロン1で異物濃度を濃縮して異物排出管6へ排出されるガスの温度は、約150〜250℃である。   The atmospheric gas in the continuous annealing furnace is a high temperature gas of about 200 to 300 ° C. The temperature of the gas concentrated in the cyclone 1 and discharged to the foreign matter discharge pipe 6 is about 150 to 250 ° C.

異物排出管6は、異物排出管6内部に冷却ガスを、従来市販のパーティクルカウンターの使用上限温度(約40℃)以下にまで、冷却する冷却ガス供給手段7を備えている。パーティクルカウンターの使用上限温度は、パーティクルカウンターのセンサーの耐熱温度により規定されている。   The foreign matter discharge pipe 6 is provided with a cooling gas supply means 7 for cooling the cooling gas inside the foreign matter discharge pipe 6 to below the upper limit temperature (about 40 ° C.) of a commercially available particle counter. The upper limit temperature of the particle counter is defined by the heat resistant temperature of the particle counter sensor.

冷却ガス供給手段7は、パーティクルカウンター9の前段で異物排出管6内の気体温度を測定する温度測定手段8と、該温度測定手段8の温度測定結果に基づいて冷却ガス供給量を決定する冷却ガス供給量決定手段11を備えている。   The cooling gas supply means 7 is a temperature measurement means 8 that measures the gas temperature in the foreign matter discharge pipe 6 in the previous stage of the particle counter 9, and a cooling that determines a cooling gas supply amount based on the temperature measurement result of the temperature measurement means 8. Gas supply amount determination means 11 is provided.

冷却ガス供給量決定手段11では、該温度測定手段8の温度測定結果に基づいて、パーティクルカウンター9の前段での異物排出管6内の気体温度がパーティクルカウンター9の使用上限温度(約40℃)以下となるように、冷却ガスの供給量を決定して、冷却ガス供給量調節弁12の開閉制御が行われる。   In the cooling gas supply amount determination means 11, the gas temperature in the foreign matter discharge pipe 6 at the front stage of the particle counter 9 is based on the temperature measurement result of the temperature measurement means 8 and the upper limit temperature (about 40 ° C.) of the particle counter 9 is used. The supply amount of the cooling gas is determined and the opening / closing control of the cooling gas supply amount adjustment valve 12 is performed so as to be as follows.

上記構成の本発明では、サイクロン1で分離された高温の濃縮異物混入ガスが、冷却ガスと混合してからパーティクルカウンター9に導入されるため、市販のパーティクルカウンターで異物濃度を連続測定し、炉内の異物濃度を高精度に把握することができる。   In the present invention having the above-described configuration, the high-temperature concentrated foreign substance mixed gas separated by the cyclone 1 is introduced into the particle counter 9 after being mixed with the cooling gas. It is possible to grasp the concentration of foreign matter in the inside with high accuracy.

図1に示す連続焼鈍炉内の異物濃度測定装置を用いて本発明の効果を検討した結果を以下に示す。   The result of having examined the effect of this invention using the foreign material density | concentration measuring apparatus in the continuous annealing furnace shown in FIG. 1 is shown below.

連続焼鈍炉内から炉内雰囲気ガス(200〜300℃)をサイクロン1(φ100mm*L300mm)に導入した。   Furnace atmosphere gas (200 to 300 ° C.) was introduced into the cyclone 1 (φ100 mm * L300 mm) from the continuous annealing furnace.

導入されたガスは、サイクロン1内で旋回を繰り返した後、清浄ガス排出口3から排気されていく。ガスが旋回する際、粒子径の大きな異物(10μm以上)はサイクロン1の下部に沈降してくる。ここで、沈降する際、異物はバイブレータ5で加振されるため、サイクロン1内壁に付着堆積することなく沈降していく。   The introduced gas is repeatedly exhausted in the cyclone 1 and then exhausted from the clean gas discharge port 3. When the gas swirls, foreign matter having a large particle diameter (10 μm or more) settles in the lower part of the cyclone 1. Here, since the foreign matter is vibrated by the vibrator 5 when it settles, it settles without adhering to the inner wall of the cyclone 1.

沈降してきた異物を、異物排出管6内に排出し、冷却ガスと混合してパーティクルカウンターの使用上限温度(40℃程度)以下とした後、パーティクルカウンター9に導入して異物の直径と数を計測した。   The settled foreign matter is discharged into the foreign matter discharge pipe 6 and mixed with the cooling gas so as to be lower than the upper limit temperature (about 40 ° C.) of the particle counter, and then introduced into the particle counter 9 to determine the diameter and number of the foreign matter. Measured.

図2には、上記実施例により異物濃度測定を行った結果を示している。図2に示すように、本発明によれば、高温ガス中の異物濃度を連続計測することが可能となり、
炉内疵発生との因果関係調査を迅速に行うことができる。
FIG. 2 shows the result of measuring the concentration of foreign matter according to the above example. As shown in FIG. 2, according to the present invention, it is possible to continuously measure the concentration of foreign matter in a high-temperature gas,
It is possible to quickly investigate the causal relationship with the occurrence of soot in the furnace.

1 サイクロン
2 高温ガス導入口
3 清浄ガス排出口
4 異物排出口
5 バイブレータ
6 異物排出管
7 冷却ガス供給手段
8 温度測定手段
9 パーティクルカウンター
10 連続焼鈍炉内雰囲気ガス吸引手段
11 冷却ガス供給量決定手段
12 冷却ガス供給量調節弁
DESCRIPTION OF SYMBOLS 1 Cyclone 2 High temperature gas introduction port 3 Clean gas discharge port 4 Foreign material discharge port 5 Vibrator 6 Foreign material discharge pipe 7 Cooling gas supply means 8 Temperature measurement means 9 Particle counter 10 Continuous annealing furnace atmosphere gas suction means 11 Cooling gas supply amount determination means 12 Cooling gas supply control valve

Claims (3)

上部に連続焼鈍炉内雰囲気ガスの一部を導入する高温ガス導入口と、異物除去処理後の清浄ガスを排出する清浄ガス排出口を、各々有し、下部に異物を排出する異物排出口を有するサイクロンと、該異物排出口に連結した異物排出管と、該異物排出管を流れる気体に対し、レーザ発振器からのレーザを照射して、該気体中に含まれる異物から反射される散乱光を検知して、その異物数をカウントするパーティクルカウンターからなり、該パーティクルカウンターの前段に、異物排出管内に冷却ガスを吹き込む冷却ガス供給手段を設けたことを特徴とする連続焼鈍炉内の異物濃度測定装置。   The upper part has a high-temperature gas inlet that introduces part of the atmospheric gas in the continuous annealing furnace and a clean gas outlet that discharges the clean gas after the foreign substance removal treatment, and a foreign substance outlet that discharges foreign substances at the lower part. A cyclone having a foreign substance discharge pipe connected to the foreign substance discharge port, and a gas flowing through the foreign substance discharge pipe is irradiated with a laser from a laser oscillator to reflect scattered light reflected from the foreign substance contained in the gas. Contaminant concentration measurement in a continuous annealing furnace characterized by comprising a particle counter that detects and counts the number of foreign substances, and provided with a cooling gas supply means for blowing cooling gas into the foreign substance discharge pipe in front of the particle counter apparatus. 冷却ガス供給手段は、パーティクルカウンターの前段で異物排出管内の気体温度を測定する温度測定手段と、該温度測定手段の温度測定結果に基づいて冷却ガス供給量を決定する冷却ガス供給量決定手段を備えることを特徴とする請求項1記載の連続焼鈍炉内の異物濃度測定装置。   The cooling gas supply means includes a temperature measurement means for measuring the gas temperature in the foreign matter discharge pipe at the front stage of the particle counter, and a cooling gas supply amount determination means for determining the cooling gas supply amount based on the temperature measurement result of the temperature measurement means. The apparatus for measuring a foreign matter concentration in a continuous annealing furnace according to claim 1, comprising: 請求項2記載の連続焼鈍炉内の異物濃度測定装置を用いて、連続焼鈍炉内の異物濃度測定を行う方法であって、パーティクルカウンターの前段での異物排出管内の気体温度がパーティクルカウンターの使用上限温度以下となるように冷却ガスの供給量を決定することを特徴とする連続焼鈍炉内の異物濃度測定方法。
A method for measuring the concentration of foreign matter in a continuous annealing furnace using the foreign matter concentration measuring device in a continuous annealing furnace according to claim 2, wherein the gas temperature in the foreign matter discharge pipe at the front stage of the particle counter is the use of the particle counter. A foreign matter concentration measurement method in a continuous annealing furnace, wherein a supply amount of a cooling gas is determined so as to be equal to or lower than an upper limit temperature.
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