JP5149171B2 - 機能強化製剤 - Google Patents
機能強化製剤 Download PDFInfo
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- JP5149171B2 JP5149171B2 JP2008518716A JP2008518716A JP5149171B2 JP 5149171 B2 JP5149171 B2 JP 5149171B2 JP 2008518716 A JP2008518716 A JP 2008518716A JP 2008518716 A JP2008518716 A JP 2008518716A JP 5149171 B2 JP5149171 B2 JP 5149171B2
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
Description
−植物繁殖材料に対する前記粒子の接着をどのように改善するか;
−処理した種子の流動性、特に懸濁組成物中での流動性をどのように改善するか;
−種子上に塗布する農薬が、処理した種子のバッチ又はロット間で均一になるのをどのように確実にするか、
という課題に直面している。
1)アルキルラジカル中に8〜24個の炭素原子を有する、ポリアルコキシル化、好ましくはポリエトキシル化、飽和及び不飽和脂肪族アルコールであって、相当の脂肪酸又は石油化学製品に由来し、且つ1〜100、好ましくは2〜50個のエチレンオキシド単位(EO)を有し、遊離ヒドロキシル基がアルコキシル化可能であるもの、例えば、GENAPOL X、GENAPOL OA、GENAPOL OX、GENAPOL UD、GENAPOL LA及びGENAPOL Oシリーズ(CLARIANT)、CROVOL Mシリーズ(CRODA)又はLUTENSOLシリーズ(BASF)、あるいはこれらからエーテル化によって得られるもの、例えばGENAPOL X060メチルエーテル、
2)ポリアルコキシル化、好ましくはポリエトキシル化された、アリールアルキルフェノール、例えば2,4,6−トリス(1−フェニルエチル)フェノール(トリスチリルフェノール)であって、平均エトキシル化度が10〜80、好ましくは16〜40のもの、例えばSOPROPHOR BSU(RHODIA)、EMULSOGEN TSシリーズ(CLARIANT)又はHOE S 3474(CLARIANT)、
3)ポリアルコキシル化、好ましくはポリエトキシル化されたアルキルフェノールであって、1又は複数のアルキルラジカル、例えばノニルフェノール又はトリ−sec−ブチルフェノールを有し、且つ2〜40、好ましくは4〜15のエトキシル化度を有するもの、例えばARKOPAL Nシリーズ又はSAPOGENAT Tシリーズ(CLARIANT)、
4)ポリアルコキシル化、好ましくはポリエトキシル化された、ヒドロキシ脂肪酸又はグリセリドであって、ヒドロキシ脂肪酸、例えばリシニン又はひまし油を含み、エトキシル化度が10〜80、好ましくは25〜40のもの、例えばEMULSOGEN ELシリーズ(CLARIANT)又はAGNIQUE CSOシリーズ(COGNIS)、並びに
5)ポリアルコキシル化、好ましくはポリエトキシル化された、ソルビタンエステル、例えばATPLUS 309F(UNIQEMA)又はALKAMULSシリーズ(RHODIA)、
である。
6)少なくとも第一のポリアルキレンオキシドブロック領域及び第二のポリアルキレンオキシドブロック領域を有し、前記第一領域のポリアルキレンオキシドが前記第二領域のポリアルキレンオキシドと異なるポリC2−4アルキレンオキシドブロックコポリマーのモノC2−6アルキルエーテル、である。好ましくは、C2−6アルキルエーテル部分は、前記アルキレンオキシオキシドブロックコポリマーのC3アルキルエーテル、より好ましくはC4アルキルエーテルである。また、好ましくは、アルキレンオキシドブロックコポリマー部分は、好ましくはエチレンオキシド/プロピレンオキシドブロックコポリマーである。好ましくは、エチレンオキシド部分は、約10〜約90モル%から約25〜約75モル%のブロックコポリマーを示す。特に好ましい材料は、WitcoからNS−500LQの商品名のもと市販されている。ブロックコポリマーは、ジ−及びトリ−ブロックコポリマー、例えばアルキレンオキシド由来のもの、例えばエチレンオキシド及びプロピレンオキシド由来のものであって、平均分子量が200〜10000未満、好ましくは1000〜4000g/モル、例えばGENAPOL PFシリーズ(CLARIANT)、PLURONICシリーズ(BASF)、SYNPERONIC PEシリーズ(UNIQEMA)、又はTOXIMULシリーズ(STEPAN)であってもよい。本発明の組成物に使用するのに好ましいエチレンオキシド/プロピレンオキシドブロックコポリマー群は、ブチルベースのポリ(オキシプロピレン)ポリ(オキシエチレン)ブロックコポリマーであって、平均分子量が2,400〜3,500のもの(例えば、TOXIMUL 8320、Stepan Chemical Co.)である。
表1の実施例C1〜C3及びEx.1〜4は、同一農薬組成物に関するものであり、表面活性化合物(b)ブチルPO/EOとC9−C18PO/EO混合物が、他の慣習上の製剤用助剤(以下の表1には示していない)と同様に既に農薬製剤中に存在している。これに対し、表示した表面活性化合物、適切な場合には水で希釈したものを添加して混合し、種子処理組成物(又は製品又はスラリー)を調製した。
実施例C5〜C9並びにEx.7〜12(表29)は、活性成分を細かくすり潰し、そして製剤用助剤と密に混合することで(化合物(a)及び/又は(b)を含む)調製され、その結果種子処理用の懸濁濃縮物が生じる。
コムギ種子は例C1〜C8及びEx.1〜12の種子処理組成物で、Hege種子処理器具で処理し、そして農薬、固体、界面活性剤及び化合物(a)と(b)の塗布量は、表の塗布量についての情報の項に提示する。
流動性
種子が処理後に流動する能力は、タイマーで接続され、空気で閉じることができるゲートを備えた漏斗に種子を通過させるで未処理種子と比較した。当該ゲートは2秒間開き、そしてゲートを通過した種子の重量をはかりで計量する。結果は、種子処理直後〜処理後10分間に実施された複数の流動性評価の平均値である。実施例の流動性について表中に示した結果は、未処理種子の流動性のパーセンテージである。重量が重くなるほど、種子の流動性が向上するため、パーセンテージが高いほど、優れた流動性を示す(表1及び2を参照のこと)。
種子から放出される「ダスト」の量は、隆起部を有するドラムであって、回転すると処理済の種子のハンドリング及び運搬を促進するドラム内に処理済みの種子を据えることによって測定する。正確な空気流制御システムにより、空気で運ばれる粒子を粗ろ過機からフィルター上に運ぶ一定の気流がもたらされる。ダストの量は、フィルターを計量することで測定される。「ダストオフ」の測定値のデータを、種子100kg当たりのダストのグラムとして表2に示す。量が少ないほど、ダストオフが向上する(表1及び2を参照のこと)。
何百個の種子のバッチを種子処理から選び、そして、溶媒混合物を用いて超音波バスにおいて2秒間、色素を各種子から個別に抽出する。抽出された色素の量を分光計で定量し、そして種子上に接着した活性成分の量を、種子処理組成物の詳細をベースに算出し、そして農薬の塗布量に従い種子を分類する。農薬の濃度範囲(例えば予想される農薬の塗布量の80〜140%)内で種子の数が多いほど、その種子処理組成物の農薬分布特性が向上する(表3を参照のこと)。
Claims (20)
- 種子ロットについて種子処理する方法であって、当該ロットを、(a)1又は複数のアルコキシラート及び(b)1又は複数のブロックポリオキシアルキレンポリマーと、1又は複数の農薬を含んで成る種子処理組成物とを含んで成る混合物で処理すること、を含んで成り、但し、前記ロットに対する、前記混合物に由来する(a)+(b)の総塗布量は、少なくとも10g/100kg種子であり;前記農薬の組成物由来のジフェノコナゾールの塗布量が3.6g/100kgである場合又は前記農薬の組成物由来のフルジオキソニルの塗布量が3.75g若しくは5g/100kg種子である場合、オレイルポリグリコールエーテルの塗布量が16〜20g/100kg種子であること、を除く、方法。
- ジフェノコナゾールの塗布量が3.6g/100kgである場合又はフルジオキソニルが3.75g若しくは5g/100kg種子である場合、前記混合物由来のオレイルポリグリコールエーテルの塗布量が18〜24g/100kg種子であること、を除く、請求項1に記載の方法。
- 前記ロットの流動性、均一性及び/又はダストオフ特性が向上する、請求項1又は2に記載の方法。
- 前記ロットに対する1又は複数の農薬の塗布量が、1〜100g/100kg種子の範囲内である、請求項1〜3のいずれか1項に記載の方法。
- (a)+(b)の総塗布量が10〜100g/100kg種子の範囲内である、請求項1〜4のいずれか1項に記載の方法。
- 種子ロットについて種子処理する方法であって、水性懸濁液の形態にあり、且つ(I)(α)活性成分として、1又は複数の農薬、及び(β)30℃超の融点を有する1又は複数の物質、並びに(II)(a)1又は複数のアルコキシラート及び(b)1又は複数のブロックポリオキシアルキレンポリマーを含んで成る製剤助剤を含んで成る農薬製剤(A)を含んで成る種子処理組成物で前記ロットが処理され;ここで、(α)+(β)の総量が多くても20質量%であり、且つ(a)+(b)の総量が少なくとも4質量%であり、各量が製剤の質量ベースであり、但し、(a)+(b)対(α)+(β)の質量比が0.5〜2.0の範囲内にあり、そして製剤(A)由来の(a)+(b)の総塗布量が少なくとも10g/100kg種子である、方法。
- 前記ロットの流動性、均一性及び/又はダストオフ特性が向上する、請求項1又は2に記載の方法。
- 農薬が、1又は複数のベナラキシル、ベナラキシル−M、フベルジアゾール、チアベンダゾール、アゾキシストロビン、フルオキサストロビン、ビテルタノール、シプロコナゾール、ジフェノコナゾール、ジニコナゾール、フルキンコナゾール、フルトリアフォル、メタラキシル、メタラキシル−M、プロチオコナゾール、テブコナゾール、トリアジメノール、トリチコナゾール、フルジオキソニル、トリアゾキシド、シプロジニル、カルボキシン、シルチオファム、イプコナゾール、トリフロキシストロビン、イマザリル、グアザチン、3−ジフルオロメチル−1−メチル−1Hピラゾール−4−カルボン酸(2−ビシクロプロピル−2−イル−フェニル)−アミド、チアメトキサム、イミダクロプリド、アバメクチン、スピノサッド、ビスアミド、チアクロプリド、ラムダシハロトリン、クロチアニジン、テフルトリン、ベータ−シフルトリン、シペルメトリン、アルファ−シペルメトリン、ベータ−シペルメトリン、シータ−シペルメトリン、ゼータ−シペルメトリン、及びフィプロニルから選択される、請求項1〜7のいずれか1項に記載の方法。
- (α)及び(β)の総量が3〜15質量%の範囲内である、請求項6〜8のいずれか1項に記載の方法。
- (a)及び(b)の総量が、5〜25質量%の範囲内である、請求項6〜9のいずれか1項に記載の方法。
- (a)が脂肪族アルコールアルコキシラート、オキソアルコールアルコキシラート、芳香族アルコールアルコキシラート、オイルアルコキシラート、脂肪族アルコールアルコキシラート及び脂肪酸アルコキシラートから選択される、請求項1〜10のいずれか1項に記載の方法。
- (b)がエチレンオキシド及びプロピレンオキシドブロックコポリマーである、請求項1〜11のいずれか1項に記載の方法。
- 30℃超の融点を有する物質が色素である、請求項6〜12のいずれか1項に記載の方法。
- 製剤(A)が、追加の助剤(c)として他の表面活性化合物を更に含んで成り、そして(a)及び(b)対(c)の重量比は1.5超の範囲内であり;但し、種子に対する(a)、(b)及び(c)の総塗布量は15〜120g/100kg種子の範囲内である、請求項6〜13のいずれか1項に記載の方法。
- 種子処理組成物が、他の農薬製剤(B)及び/又は製剤用助剤(C)を更に含んで成る、請求項6〜14のいずれか1項に記載の方法。
- 請求項6〜14のいずれか1項で規定されている農薬製剤(A)、及び任意に液体担体、を含んで成る種子処理組成物。
- (i)他の農薬製剤(B)及び/又は(ii)製剤用助剤(C)を更に含んで成る、請求項16に記載の種子処理組成物。
- 請求項6〜14のいずれか1項において農薬製剤(A)として規定されている、懸濁液の形態の水性農薬製剤。
- 種子及び遅れて生育する植物器官を、害虫の攻撃から保護する方法であって、当該種子を、農薬として有効量の請求項16で規定されている種子処理組成物で処理するか、あるいは請求項1〜5のいずれか1項で規定されている方法により保護する方法。
- 多くても100g/100kg種子の1又は複数の農薬及び請求項1〜12のいずれか1項で規定されている少なくとも10g/100kg種子の(a)と(b)を含んで成る虫害抵抗性種子ロットであって;前記農薬の組成物物由来のジフェノコナゾールの塗布量が3.6g/100kgである場合又は前記農薬の組成物物由来のフルジオキソニルが3.75g若しくは5g/100kg種子である場合、(a)及び(b)の塗布量が18〜24g/100kg種子であること、を除く、種子ロット。
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2006
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- 2006-06-28 CN CN2006800281969A patent/CN101232805B/zh active Active
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- 2006-06-28 CA CA2611848A patent/CA2611848C/en active Active
- 2006-06-28 WO PCT/EP2006/006259 patent/WO2007003319A2/en active Application Filing
- 2006-06-28 ES ES06776094.2T patent/ES2537555T3/es active Active
- 2006-06-28 AR ARP060102783A patent/AR053940A1/es active IP Right Grant
- 2006-06-28 US US11/994,215 patent/US20090124499A1/en not_active Abandoned
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- 2006-06-28 EP EP06776094.2A patent/EP1906730B1/en active Active
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Also Published As
Publication number | Publication date |
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CA2611848A1 (en) | 2007-01-11 |
ZA200710912B (en) | 2008-10-29 |
ES2537555T3 (es) | 2015-06-09 |
EP1906730B1 (en) | 2015-03-04 |
US20090124499A1 (en) | 2009-05-14 |
AU2006265356A1 (en) | 2007-01-11 |
CN101232805B (zh) | 2012-11-14 |
WO2007003319A2 (en) | 2007-01-11 |
EA200800105A1 (ru) | 2008-10-30 |
EP1906730A2 (en) | 2008-04-09 |
CN101232805A (zh) | 2008-07-30 |
BRPI0613157B1 (pt) | 2015-12-29 |
AR053940A1 (es) | 2007-05-23 |
JP2008544966A (ja) | 2008-12-11 |
CA2611848C (en) | 2014-03-25 |
UA96128C2 (ru) | 2011-10-10 |
BRPI0613157A2 (pt) | 2010-12-21 |
EA021460B1 (ru) | 2015-06-30 |
WO2007003319A3 (en) | 2007-02-22 |
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