JP4380408B2 - Electronic component sealing method - Google Patents

Electronic component sealing method Download PDF

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Publication number
JP4380408B2
JP4380408B2 JP2004134413A JP2004134413A JP4380408B2 JP 4380408 B2 JP4380408 B2 JP 4380408B2 JP 2004134413 A JP2004134413 A JP 2004134413A JP 2004134413 A JP2004134413 A JP 2004134413A JP 4380408 B2 JP4380408 B2 JP 4380408B2
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Prior art keywords
container
sealing
electronic component
sealing member
lid part
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JP2005317794A (en
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喜弘 角田
勇二 保田
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Kyocera Crystal Device Corp
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Kyocera Crystal Device Corp
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L2224/00Indexing scheme for arrangements for connecting or disconnecting semiconductor or solid-state bodies and methods related thereto as covered by H01L24/00
    • H01L2224/01Means for bonding being attached to, or being formed on, the surface to be connected, e.g. chip-to-package, die-attach, "first-level" interconnects; Manufacturing methods related thereto
    • H01L2224/10Bump connectors; Manufacturing methods related thereto
    • H01L2224/15Structure, shape, material or disposition of the bump connectors after the connecting process
    • H01L2224/16Structure, shape, material or disposition of the bump connectors after the connecting process of an individual bump connector
    • H01L2224/161Disposition
    • H01L2224/16151Disposition the bump connector connecting between a semiconductor or solid-state body and an item not being a semiconductor or solid-state body, e.g. chip-to-substrate, chip-to-passive
    • H01L2224/16221Disposition the bump connector connecting between a semiconductor or solid-state body and an item not being a semiconductor or solid-state body, e.g. chip-to-substrate, chip-to-passive the body and the item being stacked
    • H01L2224/16225Disposition the bump connector connecting between a semiconductor or solid-state body and an item not being a semiconductor or solid-state body, e.g. chip-to-substrate, chip-to-passive the body and the item being stacked the item being non-metallic, e.g. insulating substrate with or without metallisation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L2924/00Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
    • H01L2924/15Details of package parts other than the semiconductor or other solid state devices to be connected
    • H01L2924/161Cap
    • H01L2924/1615Shape
    • H01L2924/16195Flat cap [not enclosing an internal cavity]

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  • Oscillators With Electromechanical Resonators (AREA)

Description

本発明は、電子部品、圧電素子や弾性表面波素子の小型化に対応する気密封止に適した封止と封止方法に関する。   The present invention relates to a sealing and a sealing method suitable for hermetic sealing corresponding to miniaturization of electronic components, piezoelectric elements, and surface acoustic wave elements.

従来から広く利用されている封止方法にはクラッド材料を用いた封止容器や、シーム封止による封止容器が用いられている。封止の一例としては、圧電発振器や圧電振動子を構成する密閉容器の場合を例にとると、高い気密環境と信頼性を考慮するとシーム溶接封止が広く使用されている。   Conventionally widely used sealing methods include a sealing container using a clad material and a sealing container using seam sealing. As an example of sealing, in the case of a sealed container constituting a piezoelectric oscillator or a piezoelectric vibrator, seam welded sealing is widely used in consideration of a high airtight environment and reliability.

このシーム溶接封止とは、封止部付近にシールリングと称する部材を例えばセラミック材料からなる容器の封止部にロウ付けで付けて、金属製のフタのニッケルメッキを施しロウ材とし、容器の封止部とフタとを接合するために封止部分にローラによる電流と圧力をかけてシールリングから発する熱により前記ロウ材(メッキ)を溶解して容器とフタとを接合し気密容器を構成する封止工法が主流として使われている。
特開2002−203921号公報 特開平11−312748号公報
This seam welded seal is a member called a seal ring in the vicinity of the sealing portion, for example, brazed to the sealing portion of a container made of a ceramic material, and nickel plating of a metal lid is performed to form a brazing material. In order to join the sealing part and lid of the container, a current and pressure by a roller are applied to the sealing part to melt the brazing material (plating) by heat generated from the seal ring, and the container and the lid are joined to form an airtight container. Constructing sealing method is used as mainstream.
JP 2002-203921 A JP 11-31748 A

上述する従来シーム溶接封止では、ロウ材の溶融温度が高いため金属製のフタと容器とに封止時に発生する温度により熱ストレスが加わり、場合によってはセラミック材質の容器を破損していまうおそれがある。   In the conventional seam welded sealing described above, since the melting temperature of the brazing material is high, heat stress is applied to the metal lid and the container due to the temperature generated during sealing, and the ceramic container may be damaged in some cases. There is.

また、封止時にはメッキであるロウ材が高温で溶融した状態となっており、高温になっているメッキ材料が容器の内側すなわち、圧電部品を収納する容器内側にメッキ材料が飛散する可能性も考えられる。   In addition, the brazing material that is plating is melted at a high temperature at the time of sealing, and there is a possibility that the plating material at a high temperature may be scattered inside the container, that is, inside the container that stores the piezoelectric components. Conceivable.

加えて、シーム溶接封止の場合には、従来の背景技術にも記載があるように、シーム溶接封止にはシームリングを配置することは必要不可欠な部材であることから、封止部分にはこのシームリングを配置するだけの容器の壁幅(厚み)が必要となってくる。その一方で容器自体(例えば圧電振動子や圧電発振器)を小型化、軽量化を望まれる現状から、シームリングを配置する容器の壁幅を薄くする必要性も発生する。   In addition, in the case of a seam welded seal, as described in the background art of the related art, it is an indispensable member to arrange a seam ring in the seam welded seal. Therefore, the wall width (thickness) of the container is required to arrange the seam ring. On the other hand, since the container itself (for example, a piezoelectric vibrator or a piezoelectric oscillator) is desired to be reduced in size and weight, it is also necessary to reduce the wall width of the container in which the seam ring is arranged.

以上のように従来の封止方法を用いた気密容器では、封止時の温度環境、封止環境の問題と小型化、軽量に対する問題があることから、より良い封止条件を選択する必要があるといった課題がある。   As described above, in the airtight container using the conventional sealing method, there are problems with the temperature environment at the time of sealing, the problem of the sealing environment and the reduction in size and weight, so it is necessary to select better sealing conditions. There is a problem that there is.

課題を解決するため、容器部とフタ部を接合することで密閉容器構造を成す電子部品容器の封止方法において、前記フタ部の形成は凹型の内側に剥離材を施し、その中に封止部材を注入し容器の封止面が封止部材と当たるようにした状態で硬化させ、封止部材が硬化した後に型から取り出すことでフタ部と容器が接合し密閉容器を構成することを特徴とする電子部品容器の封止方法である。 In order to solve the problem, in the method of sealing an electronic component container that forms a sealed container structure by joining the container part and the lid part, the lid part is formed by applying a release material to the inside of the concave mold and sealing it inside Injecting the member and curing in a state where the sealing surface of the container contacts the sealing member, and taking out from the mold after the sealing member is cured, the lid part and the container are joined to form a sealed container It is the sealing method of the electronic component container.

本発明によりフタ部を数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材から成る材質にすることで、封止作業の手間を大幅に削減することができる。またフタ部材の構成が数ナノメートル粒子であることから容器との接合部の歪み成分も低減できることから、密閉容器内に収納する各種素子に及ぼす歪み成分も低減することができる。また、フタ部が導電性で構成できることから、容器内に収納する素子に対する高周波ノイズを遮断する効果も兼ね備えることができる。   According to the present invention, when the lid portion is made of a material composed of metal fine particles of several nanometers and a dispersion material that can be combined with the metal fine particles, the labor of the sealing operation can be greatly reduced. Moreover, since the structure of the lid member is a few nanometer particles, the strain component at the joint with the container can be reduced, so that the strain component exerted on various elements housed in the sealed container can also be reduced. In addition, since the lid portion can be made of a conductive material, it can also have an effect of blocking high frequency noise with respect to an element stored in the container.

そこで本発明は、容器部とフタ部を接合することで密閉容器構造を成す電子部品容器において、該フタ部は数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材から成ることを特徴とする電子部品容器である。   Therefore, the present invention relates to an electronic component container that forms a sealed container structure by joining a container part and a lid part, wherein the lid part is made of metal fine particles of several nanometer particles and a dispersion material that can be combined with the metal fine particles. This is an electronic component container.

このとき、金属微粒子は平均粒径が1〜100nmの、金、銀、銅、白金、パラジウム、ロジウム、オスミウム、ルテニウム、イリジウム、鉄、錫、亜鉛、コバルト、ニッケル、クロム、チタン、タンタル、タングステン、インジウム、ケイ素の中の少なくとも1種類、あるいは2種類以上の金属合金の微粒子を用いるもので、分散材にはアミン、アルコール、チオールであることを特徴とするものである。   At this time, the metal fine particles have an average particle diameter of 1 to 100 nm, gold, silver, copper, platinum, palladium, rhodium, osmium, ruthenium, iridium, iron, tin, zinc, cobalt, nickel, chromium, titanium, tantalum, tungsten. In addition, at least one kind of indium and silicon, or two or more kinds of metal alloy fine particles are used, and the dispersing material is amine, alcohol, or thiol.

また、容器部とフタ部を接合することで密閉容器構造を成す電子部品容器の封止方法において、前記フタ部の形成は凹型の内側に剥離材を施し、その中に封止部材を注入し容器の封止面が封止部材と当たるようにした状態で硬化させ、封止部材が硬化した後に型から取り出すことでフタ部と容器が接合し密閉容器を構成することで、フタ部を数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材とで兼用した密閉容器を構成するものである。   Further, in the method of sealing an electronic component container having a sealed container structure by joining the container part and the lid part, the lid part is formed by applying a release material to the inside of the concave mold, and injecting a sealing member therein. Curing in a state where the sealing surface of the container is in contact with the sealing member, and taking out from the mold after the sealing member is cured, the lid part and the container are joined to form a sealed container. The airtight container is composed of both nanometer-sized metal fine particles and a dispersing material that can be combined with the metal fine particles.

要するに本発明では、従来のシーム溶接封止の課題である封止時の温度環境、封止環境の問題と小型化、軽量に対する問題から、より良い封止条件を選択する条件として、数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材から成る封止部材を用いるもので、圧電振動子、圧電発振器(駆動用電子部品を含む)、弾性表面波素子をはじめ各種電子部品を収納するものである。   In short, in the present invention, several nanometers as a condition for selecting a better sealing condition from the temperature environment at the time of sealing, which is a problem of the conventional seam welding sealing, the problem of the sealing environment and the miniaturization, the problem with respect to light weight It uses a metal particle fine particle and a sealing member made of a dispersion material that can be combined with the metal fine particle, and houses various electronic components such as piezoelectric vibrators, piezoelectric oscillators (including electronic components for driving), and surface acoustic wave devices. To do.

以下、添付図面に従ってこの発明の実施例を説明する。なお、各図において同一の符号は同様の対象を示すものとする。図1は本発明の電子部品容器4の構造を示す部分断面図である。フタ部2は封止部材3である数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材から成る材質で容器部1はセラミック材料で構成されており、フタ部2と容器部1で密閉容器構造を構成するものである。   Embodiments of the present invention will be described below with reference to the accompanying drawings. In each figure, the same numerals indicate the same objects. FIG. 1 is a partial cross-sectional view showing the structure of an electronic component container 4 of the present invention. The lid part 2 is made of a material composed of metal particles of several nanometers as a sealing member 3 and a dispersion material that can be combined with the metal fine particles, and the container part 1 is made of a ceramic material. The lid part 2 and the container part 1 This constitutes a sealed container structure.

このとき、金属微粒子は平均粒径が1〜100nmの、金、銀、銅、白金、パラジウム、ロジウム、オスミウム、ルテニウム、イリジウム、鉄、錫、亜鉛、コバルト、ニッケル、クロム、チタン、タンタル、タングステン、インジウム、ケイ素の中の少なくとも1種類、あるいは2種類以上の金属合金の微粒子を用いるもので、分散材にはアミン、アルコール、チオールを用いることを特徴とするものである。   At this time, the metal fine particles have an average particle diameter of 1 to 100 nm, gold, silver, copper, platinum, palladium, rhodium, osmium, ruthenium, iridium, iron, tin, zinc, cobalt, nickel, chromium, titanium, tantalum, tungsten. , Indium, and silicon, at least one type or two or more types of metal alloy fine particles are used, and amine, alcohol, and thiol are used as the dispersion material.

図2には封止形態の断面図を示すものであるが、容器内に収納する部品については、圧電振動子、水晶素板、弾性表面波素子、電子部品(コンデンサ、抵抗、コイル、集積回路)が挙げられる。なお、図2(a)は凹部容器であり、図2(b)は水晶素板と集積回路を分離した容器形態を示すものである。   FIG. 2 shows a cross-sectional view of the sealing form, but the components housed in the container include a piezoelectric vibrator, a quartz base plate, a surface acoustic wave element, an electronic component (capacitor, resistor, coil, integrated circuit). ). 2A shows a concave container, and FIG. 2B shows a container form in which the crystal base plate and the integrated circuit are separated.

一方、図3に示すフロー図は本発明で用いる封止部材3(数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材)でフタ部2と容器部1を密閉容器構造にするための製造工程の一例を示すものである。   On the other hand, the flow chart shown in FIG. 3 shows that the lid part 2 and the container part 1 are made into a sealed container structure with the sealing member 3 (metal fine particles of several nanometer particles and a dispersing material that can be combined with the metal fine particles) used in the present invention. An example of the manufacturing process for this is shown.

具体的には、容器部1とフタ部2を接合することで密閉容器構造を成す電子部品容器4の封止方法において、前記フタ部2の形成は凹型の内側に剥離材を施し、その中に封止部材3を注入し容器の封止面が封止部材3と当たるようにした状態で硬化させ、封止部材3が硬化した後に型から取り出すことでフタ部2と容器が接合し密閉容器を構成するものである。   Specifically, in the sealing method of the electronic component container 4 which forms a sealed container structure by joining the container part 1 and the lid part 2, the lid part 2 is formed by applying a release material to the inside of the concave mold, The sealing member 3 is injected into the container and cured in a state where the sealing surface of the container is in contact with the sealing member 3. After the sealing member 3 is cured, the lid part 2 and the container are joined and sealed. It constitutes a container.

要するに封止方法に関しては、数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材を予定の寸法でシート状にし、このシート状になった状態をそのままフタ部2として利用するものである。実際の封止部材3によるシート状の製作方法としては、図3に示すように型の内側に剥離材を施し、その中に封止部材3を注入(図3(a))し、容器の封止面が封止部材3と当たるようにした状態で硬化させ(図3(b)、封止部材3が硬化した後に型から出せば封止部材3がフタ部2を兼用した状態で密閉容器を構成((図3(c))することができる。このとき、容器の封止面との当接具合を安定にするために、封止部材3を注入した時点で封止部材3を仮硬化させる場合もある。   In short, regarding the sealing method, a metal fine particle of several nanometers and a dispersion material that can be bonded to the metal fine particle are formed into a sheet shape with a predetermined size, and this sheet-like state is used as the lid portion 2 as it is. is there. As a sheet-like manufacturing method using the actual sealing member 3, a release material is applied to the inside of the mold as shown in FIG. 3, and the sealing member 3 is injected into the mold (FIG. 3 (a)). It hardens | cures in the state which made the sealing surface contact | abut the sealing member 3 (FIG.3 (b)), and if it removes from a type | mold after the sealing member 3 hardens | cures, it will seal in the state which the sealing member 3 used as the cover part 2 The container can be configured ((FIG. 3C). At this time, in order to stabilize the contact state with the sealing surface of the container, the sealing member 3 is formed at the time when the sealing member 3 is injected. It may be temporarily cured.

以上のように数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材を封止部材3として用いることと、フタ部2に代用することにより、従来の課題として挙げられる各種課題を解決することができる。なお、上述内容で容器部1の材質としてセラミックを一例に挙げているが、樹脂で形成する容器部1であっても同様の効果を奏するものであり、数ナノメートル粒子の金属微粒子と前記金属微粒子と結合可能な分散材をフタ部2に形成する手法に拘るものでは無い。   As described above, by using a metal nanoparticle of several nanometers and a dispersing material capable of binding to the metal microparticle as the sealing member 3 and substituting for the lid part 2, various problems listed as conventional problems are solved. can do. In addition, although ceramic is mentioned as an example as a material of the container part 1 by the above-mentioned content, even if it is the container part 1 formed with resin, there exists the same effect, The metal microparticle of several nanometer particle | grains, and the said metal It is not related to a method of forming a dispersion material that can be combined with fine particles in the lid portion 2.

本発明で用いる封止部材はフタ部と容器部の接合だけでなく、フタ部に用いる材質自体がフタ部を代用するところにあることから、同材質を所望とする形状に加工することで、より用途の広い形状、構造を得ることにも応用、展開することができる。   The sealing member used in the present invention is not only for joining the lid part and the container part, but because the material itself used for the lid part is in place of the lid part, by processing the same material into a desired shape, It can also be applied and developed to obtain more versatile shapes and structures.

本発明の1実施例を示す電子部品容器の断面図である。It is sectional drawing of the electronic component container which shows one Example of this invention. 本発明の封止形態を示す断面図である。It is sectional drawing which shows the sealing form of this invention. 本発明の封止方法を示すフロー図である。It is a flowchart which shows the sealing method of this invention.

符号の説明Explanation of symbols

1 容器部
2 フタ部
3 封止部材
4 電子部品容器
DESCRIPTION OF SYMBOLS 1 Container part 2 Lid part 3 Sealing member 4 Electronic component container

Claims (1)

容器部とフタ部を接合することで密閉容器構造を成す電子部品容器の封止方法において、前記フタ部の形成は凹型の内側に剥離材を施し、その中に封止部材を注入し容器の封止面が封止部材と当たるようにした状態で硬化させ、封止部材が硬化した後に型から取り出すことでフタ部と容器が接合し密閉容器を構成することを特徴とする電子部品容器の封止方法。In the method of sealing an electronic component container that forms a sealed container structure by joining the container part and the lid part, the lid part is formed by applying a release material to the inside of the concave mold, injecting a sealing member into the container, An electronic component container characterized by being cured in a state where the sealing surface is in contact with the sealing member, and taking out from the mold after the sealing member is cured, thereby joining the lid part and the container to form a sealed container. Sealing method.
JP2004134413A 2004-04-28 2004-04-28 Electronic component sealing method Expired - Fee Related JP4380408B2 (en)

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