JP3265626B2 - Termite control agent - Google Patents
Termite control agentInfo
- Publication number
- JP3265626B2 JP3265626B2 JP18804492A JP18804492A JP3265626B2 JP 3265626 B2 JP3265626 B2 JP 3265626B2 JP 18804492 A JP18804492 A JP 18804492A JP 18804492 A JP18804492 A JP 18804492A JP 3265626 B2 JP3265626 B2 JP 3265626B2
- Authority
- JP
- Japan
- Prior art keywords
- acid ester
- parts
- dihalovinyl
- cyano group
- dicarboximide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Description
【０００１】[0001]
【産業上の利用分野】本発明は、シロアリ防除剤および
シロアリ防除方法に関するものである。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a termite controlling agent and a method for controlling termites.
【０００２】[0002]
【従来の技術および発明が解決しようとする課題】従来
より種々のシロアリ防除剤が知られているが、一般にピ
レスロイド系化合物をシロアリ防除剤として用いる場
合、木材処理用としてはともかく、土壌処理用として用
いた場合の効力の持続性において、必ずしも充分とはい
えないものであった。2. Description of the Related Art Various termite control agents have been known. However, when a pyrethroid compound is used as a termite control agent, it is generally used not only for treating wood but also for treating soil. It was not always sufficient in terms of sustained efficacy when used.
【０００３】[0003]
【課題を解決するための手段】本発明者らは、効力の持
続性に優れたシロアリ防除剤、特に土壌処理用として用
いた場合においても有効なシロアリ防除剤を見出すべく
検討した結果、α−位にシアノ基を有していてもよい３
−フェノキシベンジルアルコールの３−（２，２−ジハ
ロビニル）−２，２−ジメチルシクロプロパンカルボン
酸エステルおよびＮ−（２−エチルヘキシル）−ビシク
ロ［２．２．１］ヘプタ−５−エン−２，３−ジカルボ
キシイミド〔以下、化合物Ａと記す。〕を有効成分とし
て含有する組成物〔以下、本発明組成物と記す。〕が、
上記の課題を解決する優れたシロアリ防除剤であること
を見出し本発明を完成した。DISCLOSURE OF THE INVENTION The present inventors have studied to find a termite controlling agent excellent in sustainability of an effect, particularly an effective termite controlling agent even when used for soil treatment. Which may have a cyano group at the 3-position
3- (2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester of -phenoxybenzyl alcohol and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-2, 3-dicarboximide [hereinafter referred to as compound A. ] As an active ingredient [hereinafter referred to as the composition of the present invention. 〕But,
The present invention was found to be an excellent termite controlling agent which solves the above-mentioned problems, and completed the present invention.
【０００４】本発明において用いられるα−位にシアノ
基を有していてもよい３−フェノキシベンジルアルコー
ルの３−（２，２−ジハロビニル）−２，２−ジメチル
シクロプロパンカルボン酸エステルとしては、例えば以
下の化合物が挙げられる。 ３−フェノキシベンジル ３−（２，２−ジクロロビニ
ル）−２，２−ジメチルシクロプロパンカルボキシラー
ト〔ペルメトリン〕 α−シアノ−３−フェノキシベンジル ３−（２，２−
ジクロロビニル）−２，２−ジメチルシクロプロパンカ
ルボキシラート〔シペルメトリン〕 （Ｓ）−α−シアノ−３−フェノキシベンジル ｄ−シ
ス−３−（２，２−ジブロモビニル）−２，２−ジメチ
ルシクロプロパンカルボキシラート〔デルタメスリン〕The 3- (2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester of 3-phenoxybenzyl alcohol which may have a cyano group at the α-position used in the present invention includes: For example, the following compounds may be mentioned. 3-phenoxybenzyl 3- (2,2-dichlorovinyl) -2,2-dimethylcyclopropanecarboxylate [permethrin] α-cyano-3-phenoxybenzyl 3- (2,2-
Dichlorovinyl) -2,2-dimethylcyclopropanecarboxylate [cypermethrin] (S) -α-cyano-3-phenoxybenzyl d-cis-3- (2,2-dibromovinyl) -2,2-dimethylcyclo Propane carboxylate (deltamethrin)
【０００５】本発明組成物において、α−位にシアノ基
を有していてもよい３−フェノキシベンジルアルコール
の３−（２，２−ジハロビニル）−２，２−ジメチルシ
クロプロパンカルボン酸エステルと化合物Ａとの量比
は、重量比で通常１：１〜１：２０、好ましくは１：２
〜１：８の範囲内である。本発明組成物は、上記のシク
ロプロパンカルボン酸エステルと化合物Ａの他に適当な
製剤用担体を含有することができ、組成物中の上記のシ
クロプロパンカルボン酸エステルの割合は通常０．０１
〜５０重量部、好ましくは０．１〜２０重量部であり、
化合物Ａの割合は通常０．０５〜５０重量部、好ましく
は０．５〜３０重量部である。本発明組成物は、通常の
殺虫剤を製剤化するのと同様に製剤化される。例えば上
記のシクロプロパンカルボン酸エステルと化合物Ａとを
芳香族炭化水素、脂肪族炭化水素、脂環式炭化水素、ア
ルコール類、グリコールエステル類、ケトン類、エステ
ル類等の有機溶媒に溶解し、必要により固体担体に吸着
させ、乳化剤、分散剤、湿潤剤等の補助剤を添加するな
どして、乳剤、油剤、水和剤、粉剤、粒剤、懸濁剤、泡
剤、噴霧剤、マイクロカプセル化製剤等に製剤化され
る。これらの製剤中には、他の殺シロアリ活性成分、安
定化剤、防腐剤等を含有させることもできる。In the composition of the present invention, 3- (2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester of 3-phenoxybenzyl alcohol, which may have a cyano group at the α-position, and a compound The amount ratio with A is usually 1: 1 to 1:20, preferably 1: 2 by weight.
１ ： 1: 8. The composition of the present invention can contain a suitable pharmaceutical carrier in addition to the cyclopropane carboxylate and the compound A, and the ratio of the cyclopropane carboxylate in the composition is usually 0.01%.
To 50 parts by weight, preferably 0.1 to 20 parts by weight,
The ratio of compound A is usually 0.05 to 50 parts by weight, preferably 0.5 to 30 parts by weight. The composition of the present invention is formulated in the same manner as an ordinary insecticide is formulated. For example, the above-mentioned cyclopropanecarboxylic acid ester and compound A are dissolved in an organic solvent such as an aromatic hydrocarbon, an aliphatic hydrocarbon, an alicyclic hydrocarbon, an alcohol, a glycol ester, a ketone, or an ester to obtain And emulsifiers, dispersants, wetting agents and other auxiliaries, for example, emulsions, oils, wettable powders, powders, granules, suspensions, foams, sprays, microcapsules It is formulated into a formulated preparation. These formulations may also contain other termiticidal active ingredients, stabilizers, preservatives and the like.
【０００６】本発明組成物は、土壌処理用として用いた
場合においても有効であるという特徴を有するものであ
る。土壌処理というのは土壌表面に薬剤の層を作る方法
である。より具体的には、例えば液剤を木造建築物の人
の侵入可能な床下土壌等に処理する場合には、動力噴霧
器を用いて散布し、特に蟻道が形成され易い建築物基礎
部を重点的に処理するのが良い。また、風呂場、玄関等
の人の侵入不可能な床下土壌等に処理する場合には、ド
リルで穿孔し、そこから土壌に薬剤を注入する方法が採
られる。本発明組成物をシロアリ防除に用いる際の処理
量は、用いられる上記のシクロプロパンカルボン酸エス
テルの種類、本発明組成物の処理方法、製剤形態、その
他種々の条件により異なるが、一般に、土壌処理の場
合、上記のシクロプロパンカルボン酸エステルと化合物
Ａとの合計量で１〜100 ｇ／ｍ2 、好ましくは５〜50ｇ
／ｍ2 であり、木材処理の場合、該合計量が 0.1〜10ｇ
／ｍ2 、好ましくは１〜５ｇ／ｍ2 である。[0006] The composition of the present invention is characterized in that it is effective even when used for soil treatment. Soil treatment is a method of forming a drug layer on the soil surface. More specifically, for example, when a liquid agent is to be applied to underfloor soil or the like of a wooden building that can be intruded by humans, it is sprayed using a power sprayer, and the emphasis is particularly placed on a building base where an ant passage is easily formed. It is better to process. Further, in the case of treating underfloor soil or the like where a person cannot enter such as a bathroom or entrance, a method of piercing with a drill and injecting a drug into the soil from there is adopted. The treatment amount when the composition of the present invention is used for termite control varies depending on the type of the cyclopropane carboxylate used, the treatment method of the composition of the present invention, the form of preparation, and other various conditions. In the case of the above, the total amount of the above-mentioned cyclopropanecarboxylic acid ester and compound A is 1 to 100 g / m 2 , preferably 5 to 50 g.
/ M 2 , and in the case of wood treatment, the total amount is 0.1 to 10 g.
/ M 2 , preferably 1 to 5 g / m 2 .
【０００７】[0007]
【実施例】以下、製剤例および試験例を挙げて本発明を
より詳細に説明するが、本発明はこれらの例のみに限定
されるものではない。尚、以下の例において部は重量部
を表す。 製剤例１ ペルメトリン １部、化合物Ａ ４部にソルポールＳＭ
−２００（東邦化学株式会社製界面活性剤） １０部お
よびキシレン ８５部を加え、よく混合して乳剤を得
る。 製剤例２ ペルメトリン １部、化合物Ａ ８部にソルポールＳＭ
−２００ １０部およびキシレン ８１部を加え、よく
混合して乳剤を得る。 製剤例３ ペルメトリン ０．２５部、化合物Ａ ０．５部、キシ
レン ２部および白灯油９７．２５部を混合して油剤を
得る。 製剤例４ ペルメトリン ０．２５部、化合物Ａ ０．５部、カオ
リンクレー ８９部およびタルク１０．２５部をよく粉
砕混合して粉剤を得る。 製剤例５ シペルメトリン １部、化合物Ａ ４部にソルポールＳ
Ｍ−２００ １０部およびキシレン ８５部を加え、よ
く混合して乳剤を得る。 製剤例６ デルタメスリン １部、化合物Ａ ４部にソルポール３
００５ １０部およびキシレン ８５部を加え、よく混
合して乳剤を得る。The present invention will be described in more detail with reference to formulation examples and test examples, but the present invention is not limited to these examples. In the following examples, parts represent parts by weight. Formulation Example 1 Permethrin (1 part), Compound A (4 parts) and Solpol SM
Add 10 parts of -200 (a surfactant manufactured by Toho Chemical Co., Ltd.) and 85 parts of xylene and mix well to obtain an emulsion. Formulation Example 2 1 part of permethrin and 8 parts of compound A were added to Solpol SM
-200 10 parts and xylene 81 parts are added and mixed well to obtain an emulsion. Formulation Example 3 An oil is obtained by mixing 0.25 part of permethrin, 0.5 part of compound A, 2 parts of xylene and 97.25 parts of white kerosene. Formulation Example 4 0.25 part of permethrin, 0.5 part of compound A, 89 parts of kaolin clay and 10.25 parts of talc are thoroughly pulverized and mixed to obtain a powder. Formulation Example 5 1 part of cypermethrin and 4 parts of compound A were combined with Solpol S
10 parts of M-200 and 85 parts of xylene are added and mixed well to obtain an emulsion. Formulation Example 6 Solpart 3 in 1 part of deltamethrin and 4 parts of compound A
Add 10 parts of 005 and 85 parts of xylene and mix well to obtain an emulsion.
【０００８】試験例 製剤例１または２で得られた乳剤を蒸留水で所定濃度に
希釈した。予め加熱滅菌された砂壌土１００ｇに、上記
の希釈薬剤５mlを加え、よく混合して試験用土壌とし、
４０℃、暗条件にて保存した。所定期間（２カ月または
３カ月）保存後の試験用土壌約１５ｇをプラスチックシ
ャーレ（直径９cm、高さ２cm）に入れ、湿らせた後、イ
エシロアリ（Coptotermes formosanus）職蟻２０頭を放
し、３日間室温に保った後シロアリの状態を観察した。
また、比較対照のため、ペルメトリン単独の場合および
化合物Ａ単独の場合についても同様の試験を行った。結
果を表１に示す。Test Example The emulsion obtained in Preparation Example 1 or 2 was diluted to a predetermined concentration with distilled water. To 100 g of sand loam previously sterilized by heat, 5 ml of the above-mentioned diluent was added and mixed well to obtain test soil.
Stored at 40 ° C. under dark conditions. Approximately 15 g of the test soil after storage for a predetermined period (2 months or 3 months) was placed in a plastic petri dish (9 cm in diameter, 2 cm in height), moistened, and 20 termites ( Coptoterme s formosanus ) were released. After keeping at room temperature for a day, the state of the termites was observed.
For comparison, the same test was performed for permethrin alone and compound A alone. Table 1 shows the results.
【０００９】[0009]
【表１】 [Table 1]
【００１０】[0010]
【発明の効果】本発明組成物は、効力の持続性に優れた
シロアリ防除剤であり、特に土壌処理用として用いた場
合においても極めて有効なものである。Industrial Applicability The composition of the present invention is a termite controlling agent excellent in sustainability of the effect, and is extremely effective especially when used for soil treatment.
───────────────────────────────────────────────────── フロントページの続き (56)参考文献 特開 平１−313407（ＪＰ，Ａ) 特開 平１−294603（ＪＰ，Ａ) 特開 昭63−315670（ＪＰ，Ａ) 特開 平２−73001（ＪＰ，Ａ) 特開 平６−9320（ＪＰ，Ａ) 特公 昭48−10206（ＪＰ，Ｂ１) (58)調査した分野(Int.Cl.7，ＤＢ名) A01N 53/08 ＣＡ（ＳＴＮ) ＲＥＧＩＳＴＲＹ（ＳＴＮ)────────────────────────────────────────────────── ─── Continuation of the front page (56) References JP-A-1-313407 (JP, A) JP-A-1-294603 (JP, A) JP-A-63-315670 (JP, A) JP-A-2- 73001 (JP, A) JP-A-6-9320 (JP, A) JP-B-48-10206 (JP, B1) (58) Fields investigated (Int. Cl. 7 , DB name) A01N 53/08 CA ( STN) REGISTRY (STN)
Claims (6)
ていてもよい３−フェノキシベンジルアルコールの３−
（２，２−ジハロビニル）−２，２−ジメチルシクロプ
ロパンカルボン酸エステルおよびＮ−（２−エチルヘキ
シル）−ビシクロ［２．２．１］ヘプタ−５−エン−
２，３−ジカルボキシイミドを含有することを特徴とす
るシロアリ防除剤(1) As an active ingredient, 3-phenoxybenzyl alcohol, which may have a cyano group at the α-position,
(2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-
A termite control agent containing 2,3-dicarboximide
ていてもよい３−フェノキシベンジルアルコールの３−
（２，２−ジハロビニル）−２，２−ジメチルシクロプ
ロパンカルボン酸エステルおよびＮ−（２−エチルヘキ
シル）−ビシクロ［２．２．１］ヘプタ−５−エン−
２，３−ジカルボキシイミドを含有することを特徴とす
る土壌処理用シロアリ防除剤2. An active ingredient comprising 3-phenoxybenzyl alcohol which may have a cyano group at the α-position.
(2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-
A termite control agent for soil treatment, comprising 2,3-dicarboximide
ていてもよい３−フェノキシベンジルアルコールの３−
（２，２−ジハロビニル）−２，２−ジメチルシクロプ
ロパンカルボン酸エステルおよびＮ−（２−エチルヘキ
シル）−ビシクロ［２．２．１］ヘプタ−５−エン−
２，３−ジカルボキシイミドを含有する組成物を用いる
ことを特徴とするシロアリ防除方法3. An active ingredient comprising 3-phenoxybenzyl alcohol which may have a cyano group at the α-position.
(2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-
A method for controlling termites, comprising using a composition containing 2,3-dicarboximide.
ていてもよい３−フェノキシベンジルアルコールの３−
（２，２−ジハロビニル）−２，２−ジメチルシクロプ
ロパンカルボン酸エステルおよびＮ−（２−エチルヘキ
シル）−ビシクロ［２．２．１］ヘプタ−５−エン−
２，３−ジカルボキシイミドを含有する組成物を土壌に
処理することを特徴とするシロアリ防除方法4. An active ingredient comprising 3-phenoxybenzyl alcohol which may have a cyano group at the α-position.
(2,2-dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-
A method for controlling termites, comprising applying a composition containing 2,3-dicarboximide to soil.
フェノキシベンジルアルコールの３−（２，２−ジハロ
ビニル）−２，２−ジメチルシクロプロパンカルボン酸
エステルとＮ−（２−エチルヘキシル）−ビシクロ
［２．２．１］ヘプタ−５−エン−２，３−ジカルボキ
シイミドとが、重量比で１：２〜１：８の範囲内である
請求項１または２記載のシロアリ防除剤5. A 3- (3-) group which may have a cyano group at the α-position.
3- (2,2-Dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester of phenoxybenzyl alcohol and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-2,3 The termite control agent according to claim 1 or 2, wherein the weight ratio of -dicarboximide is 1: 2 to 1: 8.
フェノキシベンジルアルコールの３−（２，２−ジハロ
ビニル）−２，２−ジメチルシクロプロパンカルボン酸
エステルとＮ−（２−エチルヘキシル）−ビシクロ
［２．２．１］ヘプタ−５−エン−２，３−ジカルボキ
シイミドとが、重量比で１：２〜１：８の範囲内である
請求項３または４記載のシロアリ防除方法6. A 3- (3-) group which may have a cyano group at the α-position.
3- (2,2-Dihalovinyl) -2,2-dimethylcyclopropanecarboxylic acid ester of phenoxybenzyl alcohol and N- (2-ethylhexyl) -bicyclo [2.2.1] hept-5-ene-2,3 5. The method for controlling termites according to claim 3, wherein the weight ratio with -dicarboximide is in the range of 1: 2 to 1: 8. 6.
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18804492A JP3265626B2 (en) | 1992-07-15 | 1992-07-15 | Termite control agent |
| AU36830/93A AU652314B2 (en) | 1992-07-15 | 1993-04-08 | A termite-controlling agent and a controlling method thereof |
| TW082102607A TW224041B (en) | 1992-07-15 | 1993-04-08 | |
| US08/056,882 US6207707B1 (en) | 1992-07-15 | 1993-05-05 | Method for controlling termites |
| MX9303955A MX9303955A (en) | 1992-07-15 | 1993-06-30 | COMPOSITION AND METHOD FOR TERMITE CONTROL. |
| BR9302814A BR9302814A (en) | 1992-07-15 | 1993-07-09 | COMPOSITION AND PROCESS FOR COUPIM CONTROL |
| IL106309A IL106309A (en) | 1992-07-15 | 1993-07-12 | Termite-controlling composition and method |
| CN93108462A CN1047501C (en) | 1992-07-15 | 1993-07-14 | A termite-controlling agent and a controlling method thereof |
| US08/479,977 US6723331B1 (en) | 1992-07-15 | 1995-06-07 | Termite-controlling agent and a controlling method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18804492A JP3265626B2 (en) | 1992-07-15 | 1992-07-15 | Termite control agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0632705A JPH0632705A (en) | 1994-02-08 |
| JP3265626B2 true JP3265626B2 (en) | 2002-03-11 |
Family
ID=16216705
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18804492A Expired - Fee Related JP3265626B2 (en) | 1992-07-15 | 1992-07-15 | Termite control agent |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP3265626B2 (en) |
-
1992
- 1992-07-15 JP JP18804492A patent/JP3265626B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0632705A (en) | 1994-02-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4668666A (en) | Long-acting pyrethrum/pyrethroid based pesticides with silicone stabilizers | |
| KR100404646B1 (en) | Emulsifiable composition for insect control | |
| AU2005231132A1 (en) | Liquid termiticide compositions of pyrethroids and a neonicitinoids | |
| JPH08225414A (en) | Emulsifying composition for controlling termites and method for using the same | |
| JPH10130103A (en) | Agrochemical composition | |
| JP3272105B2 (en) | Aerosol insecticide and insecticide method | |
| JPH069320A (en) | New composition containing pyrethrinoid for extermination for noxious living organism | |
| EP0090178B1 (en) | Pesticidal formulations | |
| JP3882236B2 (en) | Agrochemical composition | |
| JP3265626B2 (en) | Termite control agent | |
| US6207707B1 (en) | Method for controlling termites | |
| JP3266954B2 (en) | Termite control agent | |
| JP3838661B2 (en) | Emulsifying composition for insect control | |
| JP3166326B2 (en) | Termite control agent | |
| US6723331B1 (en) | Termite-controlling agent and a controlling method thereof | |
| JPH07196419A (en) | Termite controlling agent | |
| JPH07196421A (en) | Termite controlling agent | |
| JP4182239B2 (en) | Insecticidal composition and insecticidal aerosol | |
| JPH07196420A (en) | Termite controlling agent | |
| JPH07196406A (en) | Termite controlling agent | |
| JPH08259403A (en) | Aerosol insecticide for coating use and insecticidal method using the same | |
| JPH07196422A (en) | Termite controlling agent | |
| JPH08761B2 (en) | Pest control agent | |
| JPH01299203A (en) | Termite-controlling agent for soil-treatment | |
| JPS61291502A (en) | Method for controlling noxious life |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| S531 | Written request for registration of change of domicile |
Free format text: JAPANESE INTERMEDIATE CODE: R313531 |
|
| S533 | Written request for registration of change of name |
Free format text: JAPANESE INTERMEDIATE CODE: R313533 |
|
| R350 | Written notification of registration of transfer |
Free format text: JAPANESE INTERMEDIATE CODE: R350 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090111 Year of fee payment: 7 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090111 Year of fee payment: 7 |
|
| RD05 | Notification of revocation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: R3D05 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090111 Year of fee payment: 7 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100111 Year of fee payment: 8 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20110111 Year of fee payment: 9 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20110111 Year of fee payment: 9 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20120111 Year of fee payment: 10 |
|
| LAPS | Cancellation because of no payment of annual fees |