JP2925521B2 - Electric furnace for gold smelting - Google Patents

Electric furnace for gold smelting

Info

Publication number
JP2925521B2
JP2925521B2 JP9240216A JP24021697A JP2925521B2 JP 2925521 B2 JP2925521 B2 JP 2925521B2 JP 9240216 A JP9240216 A JP 9240216A JP 24021697 A JP24021697 A JP 24021697A JP 2925521 B2 JP2925521 B2 JP 2925521B2
Authority
JP
Japan
Prior art keywords
gold
electric furnace
crucible
inner cylinder
refractory
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP9240216A
Other languages
Japanese (ja)
Other versions
JPH10185438A (en
Inventor
基 一 金
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of JPH10185438A publication Critical patent/JPH10185438A/en
Application granted granted Critical
Publication of JP2925521B2 publication Critical patent/JP2925521B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/06Crucible or pot furnaces heated electrically, e.g. induction crucible furnaces with or without any other source of heat
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00Obtaining noble metals
    • C22B11/02Obtaining noble metals by dry processes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • F27B14/10Crucibles
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • F27B2014/0843Lining or casing

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Vertical, Hearth, Or Arc Furnaces (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)
  • Processing Of Solid Wastes (AREA)

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は貴金属細工時に発生
する金残屑等に含有されている金成分を抽出する作業に
おいて、貴金属細工時に発生する金細残屑中の不純物を
高温にて焼却させて良質の金を回収するために有用に使
用でき、又は金の合金、或いは鋳物の製造時にも有用に
使用できる金製錬(精錬)用電気炉に関するものであ
る。
BACKGROUND OF THE INVENTION The present invention relates to a process for extracting a gold component contained in gold debris and the like generated at the time of precious metal processing, by incinerating impurities in the gold debris at the time of precious metal processing at a high temperature. TECHNICAL FIELD The present invention relates to an electric furnace for gold smelting (refining) that can be usefully used to recover high-quality gold, or can be usefully used in the production of gold alloys or castings.

【0002】[0002]

【従来の技術】従来、貴金属細工時に発生する金細残屑
等から金を回収するには化学薬品である濃い硝酸に濃い
塩酸を混合した王水を利用して金屑を溶解させ、これに
より金を抽出しているが、前記王水が強酸であるため、
その溶解作業に当たっては格別な注意を払わなければな
らず、又、王水が強酸であるから、これを使用して貴金
属細工残屑より金を抽出するまでに発生する有毒ガス、
液体等により環境を汚染させる等の多くの問題点があっ
た。
2. Description of the Related Art Conventionally, in order to recover gold from fine gold debris and the like generated during precious metal work, gold dust is dissolved using aqua regia in which concentrated nitric acid, which is a chemical, is mixed with concentrated hydrochloric acid. Although gold is extracted, since the aqua regia is a strong acid,
Special care must be taken in the dissolving work, and since aqua regia is a strong acid, toxic gases generated before using it to extract gold from precious metalwork debris,
There are many problems such as polluting the environment with liquids and the like.

【0003】又、金の合金、鋳物の製造時にも合金や鋳
物を製造するための適当な小型製錬機が無いため、容器
に合金又は鋳物にする金材料を入れて、酸素溶接機等に
より材料を加熱させ、合金、又は鋳物の製造作業を施工
しているため、酸素溶接機の噴出火炎等により金の含量
が減少し、その減量を埋め合わせるためには定量以上の
金を入れて合金作業を行う等、経済的な損失があった
し、又、開放された空間にて合金、又は鋳物の製造作業
を実施していたため、公害が多く発生する等の問題点が
あった。
[0003] Also, when manufacturing gold alloys and castings, there is no suitable small smelting machine for manufacturing alloys and castings. Therefore, a gold material to be alloyed or cast is put in a container, and an oxygen welding machine or the like is used. Since the material is heated and the alloy or casting is being manufactured, the content of gold decreases due to the flame of the oxygen welder, etc., and to compensate for the reduction, put more than a certain amount of gold in the alloy work. In addition, there was a problem that there was an economical loss, and that the production of alloys or castings was carried out in an open space, so that a lot of pollution occurred.

【0004】[0004]

【発明が解決しようとする課題】本発明は前記のような
従来の問題点を解決するものであり、化学薬品、即ち、
強酸を使用せずに貴金属細工細残屑より金を抽出するた
めにこの金残屑を高温に加熱して不純物を焼却させて良
質の金を抽出することができ、金の合金、鋳物の製造時
には金含量を容易に維持することができ、又、作業時に
は公害発生無しに金を製錬できるようにした小型電気炉
を提供しようとするものである。
SUMMARY OF THE INVENTION The present invention has been made to solve the above-mentioned conventional problems, and has been developed in consideration of chemicals, namely,
To extract gold from precious metalwork fines without the use of strong acids, this gold waste can be heated to a high temperature to incinerate impurities to extract good quality gold, and to produce gold alloys and castings An object of the present invention is to provide a small electric furnace which can easily maintain the gold content at times and can smelt gold without generating pollution during operation.

【0005】[0005]

【課題を解決するための手段】前記課題を解決するため
に本発明の金製錬用電気炉は、コントロールボックス1
上に回動支持台2、2′を設け、回動支持台2、2′間
に回動棒3を軸着して、これに電気炉4を回動できるよ
うに設置し、電気炉4は外筒体5と内筒体6、覆蓋体7
を以って構成し、内筒体6の内側上部には坩堝設置口8
が設けられ、且つ一側が切欠された耐火セメント、又は
セラミック材等から成る耐火煉瓦9を内設し、下部には
収納溝10が形成された耐火セメント、又はセラミック
材等から成る耐火煉瓦11を内設し、耐火煉瓦9、11
間には加熱棒12、12′を貫通挿入させ、耐火煉瓦
9、11間の加熱棒12、12′と内筒体6との間をセ
ラミックボート13にて断熱させるようにし、加熱棒1
2、12′を電気的に結線することを特徴とするもので
ある。
To solve the above-mentioned problems, an electric furnace for smelting gold according to the present invention comprises a control box (1).
The rotating supports 2 and 2 'are provided on the upper side, and the rotating rod 3 is pivotally mounted between the rotating supports 2 and 2'. Is an outer cylinder 5, an inner cylinder 6, and a cover 7
The crucible installation port 8 is provided at the upper inside of the inner cylindrical body 6.
A refractory brick 9 made of a refractory cement or a ceramic material or the like with a cutout on one side is provided therein, and a refractory brick 11 made of a refractory cement or a ceramic material or the like in which a storage groove 10 is formed at a lower portion. Built inside, refractory bricks 9, 11
Heating rods 12, 12 ′ are inserted between the heating rods 12, 12 ′ to insulate the heating rods 12, 12 ′ between the refractory bricks 9, 11 and the inner cylinder 6 with a ceramic boat 13.
2, 12 'are electrically connected.

【0006】[0006]

【発明の実施の形態】以下、本発明の要旨を添付図面に
より詳細に説明すれば次の通りである。図1ないし図3
に示すようにコントロールボックス1上に回動支持台
2、2′を設け、回動支持台2、2′間に回動棒3を軸
着し、これに電気炉4が回動できるように構成する。電
気炉4は外筒体5と内筒体6、及び覆蓋体7を以って構
成する。
DESCRIPTION OF THE PREFERRED EMBODIMENTS The gist of the present invention will be described below in detail with reference to the accompanying drawings. 1 to 3
As shown in the figure, a rotation support 2, 2 'is provided on the control box 1, and a rotation rod 3 is pivotally mounted between the rotation support 2, 2' so that the electric furnace 4 can rotate. Constitute. The electric furnace 4 includes an outer cylinder 5, an inner cylinder 6, and a cover 7.

【0007】内筒体6の内側上部には坩堝(るつぼ)設
置口8が設けられ、且つ坩堝設置口8に連通して一側が
切欠された耐火セメント、又はセラミック材の耐火煉瓦
9を設ける。内筒体6の内側下部には非常収納溝10が
形成された耐火セメント、又はセラミック材の耐火煉瓦
11を設けて、耐火煉瓦9、11間には加熱棒(商品
名:テコランダム、TECORUNDUM)12、1
2′を貫通挿入させる。耐火煉瓦9、11間の加熱棒1
2、12′と内筒体6との間はセラミックボート13に
て断熱されるようにし、前記加熱棒12、12′は電気
的に結線をする。なお、図中の符号7は覆蓋体、14は
坩堝設置口8および切欠に設置された坩堝、15はコン
トロールボックス1上に設置された支持台、16は支持
台15に支持された回収容器である。
A crucible (crucible) installation port 8 is provided in the upper inside of the inner cylinder 6, and a refractory brick 9 made of a refractory cement or a ceramic material cut off on one side is provided in communication with the crucible installation port 8. A refractory brick 11 made of a refractory cement or a ceramic material in which an emergency storage groove 10 is formed is provided at a lower portion inside the inner cylinder 6, and a heating rod (trade name: TECORUNDUM) is provided between the refractory bricks 9 and 11. 12, 1
Insert 2 'through. Heating rod 1 between refractory bricks 9 and 11
The ceramic boat 13 insulates the space between 2, 2 'and the inner cylinder 6, and the heating rods 12, 12' are electrically connected. In the drawing, reference numeral 7 denotes a cover, 14 denotes a crucible installation port 8 and a crucible installed in a notch, 15 denotes a support base installed on the control box 1, and 16 denotes a collection container supported by the support base 15. is there.

【0008】以上の構成について、以下、その動作と共
に更に詳細に説明する。本発明を利用して貴金属細工細
残屑より金を抽出するには、先ず、覆蓋体7の蓋7′を
開いて内筒体6の耐火セメント、又はセラミック材等の
耐火煉瓦9に形成された坩堝設置口8に坩堝14を設置
し、この坩堝14に貴金属細工細残屑を細かく粉砕して
入れ、電気を供給すれば加熱体である加熱棒(本発明に
おいては商品名:テコランダムを使用した)12、1
2′は加熱される。電気炉4の温度はコントロールボッ
クス1の温度センサとコントロール回路により約1,3
00℃以上程度に調整加熱することにより、坩堝14内
の貴金属細工細残屑中の金以外の他の不純物は全て焼却
されてしまう。
The above configuration will be described in more detail below together with its operation. To extract gold from precious metalwork fines using the present invention, first, the lid 7 'of the cover 7 is opened to form the refractory cement 9 of the inner cylinder 6 or the refractory brick 9 of ceramic material or the like. The crucible 14 is set in the crucible setting port 8, fine noble metal work fines are finely crushed and put into the crucible 14, and when electricity is supplied, a heating rod as a heating body (in the present invention, the product name is Tecorundum. Used) 12, 1
2 'is heated. The temperature of the electric furnace 4 is about 1,3 by the temperature sensor of the control box 1 and the control circuit.
By adjusting and heating to about 00 ° C. or more, all impurities other than gold in the precious metal work fine debris in the crucible 14 are incinerated.

【0009】このとき、電気炉4内の熱が内筒体6と加
熱棒12、12′間の断熱体であるセラミックボート1
3により加熱棒12、12′にて発生する熱を内筒体6
外に発散されないように熱を遮断させ、坩堝14側のみ
を加熱させるので、熱効率を増大化させることができ
る。
At this time, the heat in the electric furnace 4 causes the ceramic boat 1 serving as a heat insulator between the inner cylinder 6 and the heating rods 12 and 12 '.
3, heat generated by the heating rods 12, 12 'is transferred to the inner cylinder 6
Since the heat is blocked so as not to be radiated to the outside and only the crucible 14 side is heated, the thermal efficiency can be increased.

【0010】このようにして不純物の焼却が完了すれ
ば、電源を遮断して坩堝14を引き出し、これに残って
いる金灰を回収することができる。更に坩堝設置口8に
坩堝14を嵌め込み、この坩堝14で焼却させた残りの
金灰を入れて薬品を添加して電気炉4に電源を供給する
ことにより、加熱体である加熱棒12、12′が加熱さ
れつつ電気炉4の温度がコントロールボックス1のコン
トロール回路により前記焼却時と同じ温度に調整加熱さ
れ、坩堝14内には金灰と薬品が作用して金を溶解させ
ることができる。
[0010] When the incineration of the impurities is completed in this way, the power is turned off, the crucible 14 is pulled out, and the gold ash remaining in the crucible 14 can be recovered. Further, the crucible 14 is fitted into the crucible installation port 8, the remaining gold ash incinerated in the crucible 14 is added, a chemical is added, and power is supplied to the electric furnace 4, so that the heating rods 12, 12 While the ′ is being heated, the temperature of the electric furnace 4 is adjusted and heated by the control circuit of the control box 1 to the same temperature as at the time of the incineration, and gold ash and chemicals act in the crucible 14 to melt the gold.

【0011】このように金が溶融すれば電源を遮断して
図3に示すように電気炉4を回動支持台2、2′の回動
棒3により回動させることにより、支持台15上の回収
容器へ坩堝14内の溶融された状態の金を正常に回収す
ることができる。
When the gold melts, the power is cut off and the electric furnace 4 is rotated by the rotating rods 3 of the rotating supports 2 and 2 'as shown in FIG. The molten gold in the crucible 14 can be normally recovered to the recovery container of the above.

【0012】又、万一、加熱溶融時に坩堝14が割れて
この割れ目から溶融された金が漏出しても、この漏出す
る溶融した金は耐火セメント、又はセラミック材等の耐
火煉瓦11に形成された非常収納溝10へ集合させるこ
とができ、坩堝14が割れても金を回収することができ
る。
Also, even if the crucible 14 breaks during heating and melting, and the melted gold leaks from the cracks, the leaked melted gold is formed on the refractory brick 11 such as a refractory cement or a ceramic material. Can be collected in the emergency storage groove 10, and even if the crucible 14 is broken, gold can be collected.

【0013】一方、金を用いて合金、又は鋳物を製造す
る時には、加熱棒12、12′の加熱部位の長さだけの
長さを持つ坩堝14を電気炉4の内筒体6内に嵌め込
み、この坩堝14へ合金、又は鋳物を製造すべき材料を
入れて電気炉4の温度を1,300℃以下にセッティン
グして電源をONすれば、加熱棒12、12′により加
熱されて合金、又は鋳物を製造すべき材料は容易に溶融
できる。
On the other hand, when an alloy or a casting is manufactured using gold, a crucible 14 having a length corresponding to the length of a heating portion of the heating rods 12 and 12 ′ is fitted into the inner cylinder 6 of the electric furnace 4. If an alloy or a material to be cast is put into the crucible 14, the temperature of the electric furnace 4 is set to 1,300 ° C. or less, and the power is turned on, the alloy is heated by the heating rods 12, 12 ′. Alternatively, the material from which the casting is to be produced can be easily melted.

【0014】このとき、坩堝14の長さが加熱棒12、
12′の加熱部位の長さと同じであるから坩堝14内の
位置による上下の温度偏差が無く、どの位置においても
設定温度を維持できるので、合金時の温度偏差による合
金偏差を減らすことができ、又、坩堝14に合金、又は
鋳物を製造すべき材料を入れて密閉された状態にて溶融
するので、金の含量も減少しないことになる。
At this time, the length of the crucible 14 is
Since it is the same as the length of the heating portion 12 ', there is no vertical temperature deviation due to the position in the crucible 14, and the set temperature can be maintained at any position, so that the alloy deviation due to the temperature deviation at the time of alloying can be reduced. Further, since the alloy or the material to be cast is put into the crucible 14 and melted in a sealed state, the content of gold does not decrease.

【0015】又、合金、鋳物製造時には合金、又は鋳物
を製造すべき材料が溶融すれば本発明の電気炉4を回動
させずに坩堝14をニッパ等にて引き出し、次の工程に
移行する。
When the alloy or the material to be cast is melted during the production of the alloy or casting, the crucible 14 is pulled out with a nipper or the like without rotating the electric furnace 4 of the present invention, and the process proceeds to the next step. .

【0016】[0016]

【発明の効果】以上説明したように本発明によれば、電
気炉により貴金属細工時金細残屑を高温加熱溶融して不
純物を焼却除去し、良質の金を回収するようにし、化学
薬品である強酸を使用しないので、環境汚染をなくし、
又、作業者の安全を期し、事故を防止することができ
る。又、合金、又は鋳物製造時にも金含量の減少や温度
偏差による合金偏差が発生しない等、多くの利点を有す
る。
As described above, according to the present invention, gold fine debris is heated and melted at a high temperature during precious metal processing by an electric furnace to incinerate and remove impurities, and high-quality gold is recovered. Eliminates environmental pollution by not using certain strong acids
In addition, accidents can be prevented while ensuring worker safety. In addition, there are many advantages such as a reduction in gold content and no occurrence of alloy deviation due to temperature deviation during the production of alloys or castings.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の一実施の形態による金製錬用電気炉を
示し、一部を切開した分解斜視図
FIG. 1 is an exploded perspective view showing an electric furnace for gold smelting according to an embodiment of the present invention, with a part cut away.

【図2】同金製錬用電気炉を示し、一部破断側面図FIG. 2 is a partially broken side view showing the electric furnace for smelting gold.

【図3】同金製錬用電気炉を示し、回動動作説明用の一
部破断側面図
FIG. 3 shows the electric furnace for smelting gold, and is a partially broken side view for explaining a rotating operation.

【符号の説明】[Explanation of symbols]

1 コントロールボックス 2、2′ 回動支持台 3 回動棒 4 電気炉 5 外筒体 6 内筒体 7 覆蓋体 8 投入口 9 耐火煉瓦 10 収納溝 11 耐火煉瓦 12、12′ 加熱棒 13 セラミックボート DESCRIPTION OF SYMBOLS 1 Control box 2 and 2 'rotation support stand 3 rotation rod 4 Electric furnace 5 Outer cylinder 6 Inner cylinder 7 Cover lid 8 Input port 9 Firebrick 10 Storage groove 11 Firebrick 12, 12' Heating rod 13 Ceramic boat

Claims (1)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 コントロールボックス1上に回動支持台
2、2′を設け、回動支持台2、2′間に回動棒3を軸
着して、これに電気炉4を回動できるように設置し、電
気炉4は外筒体5と内筒体6、覆蓋体7を以って構成
し、内筒体6の内側上部には坩堝設置口8が設けられ、
且つ一側が切欠された耐火セメント、又はセラミック材
等から成る耐火煉瓦9を内設し、下部には収納溝10が
形成された耐火セメント、又はセラミック材等から成る
耐火煉瓦11を内設し、耐火煉瓦9、11間には加熱棒
12、12′を貫通挿入させ、耐火煉瓦9、11間の加
熱棒12、12′と内筒体6との間をセラミックボート
13にて断熱させるようにし、加熱棒12、12′を電
気的に結線することを特徴とする金製錬用電気炉。
1. A rotating support 2, 2 'is provided on a control box 1, and a rotating rod 3 is pivotally mounted between the rotating supports 2, 2', on which an electric furnace 4 can be rotated. The electric furnace 4 is constituted by an outer cylinder 5, an inner cylinder 6, and a cover 7, and a crucible installation port 8 is provided on the upper inside of the inner cylinder 6.
A firebrick 9 made of a refractory cement or a ceramic material or the like with a cutout on one side is installed therein, and a firebrick 11 made of a refractory cement or a ceramic material or the like in which a storage groove 10 is formed is provided at a lower portion, Heating rods 12 and 12 'are inserted between the refractory bricks 9 and 11 so that the ceramic rod 13 insulates between the heating rods 12 and 12' between the refractory bricks 9 and 11 and the inner cylinder 6. An electric furnace for smelting gold, wherein the heating rods 12 and 12 'are electrically connected.
JP9240216A 1996-12-13 1997-08-22 Electric furnace for gold smelting Expired - Lifetime JP2925521B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1996U50732 1996-12-13
KR2019960050732U KR19980037691U (en) 1996-12-13 1996-12-13 Smelting furnace

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JPH10185438A JPH10185438A (en) 1998-07-14
JP2925521B2 true JP2925521B2 (en) 1999-07-28

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101025985B1 (en) 2009-01-22 2011-03-30 김일두 Combustion apparatus of filter for gilding solution
CN107192264A (en) * 2016-03-15 2017-09-22 雷贝卡(天津)金属制品有限公司 Aluminum melting holding furnace
CN106440786A (en) * 2016-09-22 2017-02-22 长春黄金研究院 Pouring type industrial high-temperature heating furnace and usage method thereof

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KR19980037691U (en) 1998-09-15

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