JP2022509685A - マイクロカプセル - Google Patents
マイクロカプセル Download PDFInfo
- Publication number
- JP2022509685A JP2022509685A JP2021531142A JP2021531142A JP2022509685A JP 2022509685 A JP2022509685 A JP 2022509685A JP 2021531142 A JP2021531142 A JP 2021531142A JP 2021531142 A JP2021531142 A JP 2021531142A JP 2022509685 A JP2022509685 A JP 2022509685A
- Authority
- JP
- Japan
- Prior art keywords
- oil
- weight
- microcapsules
- precondensate
- polymer layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003094 microcapsule Substances 0.000 title claims abstract description 52
- 239000002775 capsule Substances 0.000 claims abstract description 85
- 229920000642 polymer Polymers 0.000 claims abstract description 78
- -1 aromatic polyol Chemical class 0.000 claims abstract description 72
- 239000005011 phenolic resin Substances 0.000 claims abstract description 42
- 229920001568 phenolic resin Polymers 0.000 claims abstract description 35
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229920005862 polyol Polymers 0.000 claims abstract description 24
- 239000013543 active substance Substances 0.000 claims abstract description 23
- CQOZJDNCADWEKH-UHFFFAOYSA-N 2-[3,3-bis(2-hydroxyphenyl)propyl]phenol Chemical compound OC1=CC=CC=C1CCC(C=1C(=CC=CC=1)O)C1=CC=CC=C1O CQOZJDNCADWEKH-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims description 43
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 41
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 34
- 229920000877 Melamine resin Polymers 0.000 claims description 26
- 229920000768 polyamine Polymers 0.000 claims description 23
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 21
- 150000001299 aldehydes Chemical group 0.000 claims description 20
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 18
- 229920003180 amino resin Polymers 0.000 claims description 17
- 239000002304 perfume Substances 0.000 claims description 17
- JPYHHZQJCSQRJY-UHFFFAOYSA-N Phloroglucinol Natural products CCC=CCC=CCC=CCC=CCCCCC(=O)C1=C(O)C=C(O)C=C1O JPYHHZQJCSQRJY-UHFFFAOYSA-N 0.000 claims description 16
- 229960001553 phloroglucinol Drugs 0.000 claims description 16
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 15
- QCDYQQDYXPDABM-UHFFFAOYSA-N phloroglucinol Chemical compound OC1=CC(O)=CC(O)=C1 QCDYQQDYXPDABM-UHFFFAOYSA-N 0.000 claims description 15
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 14
- 239000003205 fragrance Substances 0.000 claims description 13
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 10
- 239000004202 carbamide Substances 0.000 claims description 9
- 239000012071 phase Substances 0.000 claims description 9
- 235000019253 formic acid Nutrition 0.000 claims description 8
- 239000002002 slurry Substances 0.000 claims description 8
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 7
- 230000015572 biosynthetic process Effects 0.000 claims description 7
- 239000000839 emulsion Substances 0.000 claims description 7
- 239000003381 stabilizer Substances 0.000 claims description 7
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 6
- 238000006116 polymerization reaction Methods 0.000 claims description 6
- 235000015165 citric acid Nutrition 0.000 claims description 5
- 239000002537 cosmetic Substances 0.000 claims description 5
- 238000004132 cross linking Methods 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 5
- IXJJELULBDAIMY-UHFFFAOYSA-N 1,2,5,6-tetrahydrotriazine Chemical compound C1CC=NNN1 IXJJELULBDAIMY-UHFFFAOYSA-N 0.000 claims description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 4
- GZVHEAJQGPRDLQ-UHFFFAOYSA-N 6-phenyl-1,3,5-triazine-2,4-diamine Chemical compound NC1=NC(N)=NC(C=2C=CC=CC=2)=N1 GZVHEAJQGPRDLQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000008346 aqueous phase Substances 0.000 claims description 3
- 235000010323 ascorbic acid Nutrition 0.000 claims description 3
- 239000011668 ascorbic acid Substances 0.000 claims description 3
- 229960005070 ascorbic acid Drugs 0.000 claims description 3
- 239000003995 emulsifying agent Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000002845 discoloration Methods 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 230000000977 initiatory effect Effects 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 239000003599 detergent Substances 0.000 claims 2
- ZNZYKNKBJPZETN-WELNAUFTSA-N Dialdehyde 11678 Chemical compound N1C2=CC=CC=C2C2=C1[C@H](C[C@H](/C(=C/O)C(=O)OC)[C@@H](C=C)C=O)NCC2 ZNZYKNKBJPZETN-WELNAUFTSA-N 0.000 claims 1
- 239000003921 oil Substances 0.000 description 80
- 235000019198 oils Nutrition 0.000 description 80
- 239000010410 layer Substances 0.000 description 73
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 239000000463 material Substances 0.000 description 10
- 229920005989 resin Polymers 0.000 description 10
- 239000011347 resin Substances 0.000 description 10
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 9
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 9
- 239000000243 solution Substances 0.000 description 9
- 238000003756 stirring Methods 0.000 description 9
- 238000006068 polycondensation reaction Methods 0.000 description 8
- 238000009833 condensation Methods 0.000 description 7
- 230000005494 condensation Effects 0.000 description 7
- 238000009792 diffusion process Methods 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- NUJGJRNETVAIRJ-UHFFFAOYSA-N octanal Chemical compound CCCCCCCC=O NUJGJRNETVAIRJ-UHFFFAOYSA-N 0.000 description 6
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 235000007173 Abies balsamea Nutrition 0.000 description 5
- 239000004857 Balsam Substances 0.000 description 5
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 5
- 244000018716 Impatiens biflora Species 0.000 description 5
- 235000010654 Melissa officinalis Nutrition 0.000 description 5
- 244000062730 Melissa officinalis Species 0.000 description 5
- 150000002148 esters Chemical class 0.000 description 5
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical group O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 description 5
- WPFVBOQKRVRMJB-UHFFFAOYSA-N hydroxycitronellal Chemical compound O=CCC(C)CCCC(C)(C)O WPFVBOQKRVRMJB-UHFFFAOYSA-N 0.000 description 5
- 239000000865 liniment Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- VAJVDSVGBWFCLW-UHFFFAOYSA-N 3-Phenyl-1-propanol Chemical compound OCCCC1=CC=CC=C1 VAJVDSVGBWFCLW-UHFFFAOYSA-N 0.000 description 4
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 4
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
- AMIMRNSIRUDHCM-UHFFFAOYSA-N Isopropylaldehyde Chemical compound CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- IWLBIFVMPLUHLK-UHFFFAOYSA-N azane;formaldehyde Chemical compound N.O=C IWLBIFVMPLUHLK-UHFFFAOYSA-N 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 4
- 239000003431 cross linking reagent Substances 0.000 description 4
- KSMVZQYAVGTKIV-UHFFFAOYSA-N decanal Chemical compound CCCCCCCCCC=O KSMVZQYAVGTKIV-UHFFFAOYSA-N 0.000 description 4
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 4
- FXHGMKSSBGDXIY-UHFFFAOYSA-N heptanal Chemical compound CCCCCCC=O FXHGMKSSBGDXIY-UHFFFAOYSA-N 0.000 description 4
- JARKCYVAAOWBJS-UHFFFAOYSA-N hexanal Chemical compound CCCCCC=O JARKCYVAAOWBJS-UHFFFAOYSA-N 0.000 description 4
- 150000002576 ketones Chemical class 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- GYHFUZHODSMOHU-UHFFFAOYSA-N nonanal Chemical compound CCCCCCCCC=O GYHFUZHODSMOHU-UHFFFAOYSA-N 0.000 description 4
- 150000002989 phenols Chemical class 0.000 description 4
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- YHQGMYUVUMAZJR-UHFFFAOYSA-N α-terpinene Chemical compound CC(C)C1=CC=C(C)CC1 YHQGMYUVUMAZJR-UHFFFAOYSA-N 0.000 description 4
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000011149 active material Substances 0.000 description 3
- 229930016911 cinnamic acid Natural products 0.000 description 3
- 235000013985 cinnamic acid Nutrition 0.000 description 3
- 239000000084 colloidal system Substances 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000002979 fabric softener Substances 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 description 3
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 description 3
- 125000002444 phloroglucinyl group Chemical group [H]OC1=C([H])C(O[H])=C(*)C(O[H])=C1[H] 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- JSNRRGGBADWTMC-UHFFFAOYSA-N (6E)-7,11-dimethyl-3-methylene-1,6,10-dodecatriene Chemical compound CC(C)=CCCC(C)=CCCC(=C)C=C JSNRRGGBADWTMC-UHFFFAOYSA-N 0.000 description 2
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 2
- YGFGZTXGYTUXBA-UHFFFAOYSA-N (±)-2,6-dimethyl-5-heptenal Chemical compound O=CC(C)CCC=C(C)C YGFGZTXGYTUXBA-UHFFFAOYSA-N 0.000 description 2
- SPEUIVXLLWOEMJ-UHFFFAOYSA-N 1,1-dimethoxyethane Chemical compound COC(C)OC SPEUIVXLLWOEMJ-UHFFFAOYSA-N 0.000 description 2
- OHBQPCCCRFSCAX-UHFFFAOYSA-N 1,4-Dimethoxybenzene Chemical compound COC1=CC=C(OC)C=C1 OHBQPCCCRFSCAX-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- DOJDQRFOTHOBEK-UHFFFAOYSA-N 1-Octen-3-yl acetate Chemical compound CCCCCC(C=C)OC(C)=O DOJDQRFOTHOBEK-UHFFFAOYSA-N 0.000 description 2
- BTQAJGSMXCDDAJ-UHFFFAOYSA-N 2,4,6-trihydroxybenzaldehyde Chemical group OC1=CC(O)=C(C=O)C(O)=C1 BTQAJGSMXCDDAJ-UHFFFAOYSA-N 0.000 description 2
- MZZRKEIUNOYYDF-UHFFFAOYSA-N 2,4-dimethylcyclohex-3-ene-1-carbaldehyde Chemical compound CC1C=C(C)CCC1C=O MZZRKEIUNOYYDF-UHFFFAOYSA-N 0.000 description 2
- DGXAGETVRDOQFP-UHFFFAOYSA-N 2,6-dihydroxybenzaldehyde Chemical group OC1=CC=CC(O)=C1C=O DGXAGETVRDOQFP-UHFFFAOYSA-N 0.000 description 2
- LSKONYYRONEBKA-UHFFFAOYSA-N 2-Dodecanone Natural products CCCCCCCCCCC(C)=O LSKONYYRONEBKA-UHFFFAOYSA-N 0.000 description 2
- PETRWTHZSKVLRE-UHFFFAOYSA-N 2-Methoxy-4-methylphenol Chemical compound COC1=CC(C)=CC=C1O PETRWTHZSKVLRE-UHFFFAOYSA-N 0.000 description 2
- RYRVJGWVZYTKAO-UHFFFAOYSA-N 2-[bis(2-hydroxyethyl)amino]ethanol;formaldehyde Chemical group O=C.OCCN(CCO)CCO RYRVJGWVZYTKAO-UHFFFAOYSA-N 0.000 description 2
- ZPVFWPFBNIEHGJ-UHFFFAOYSA-N 2-octanone Chemical compound CCCCCCC(C)=O ZPVFWPFBNIEHGJ-UHFFFAOYSA-N 0.000 description 2
- PRNCMAKCNVRZFX-UHFFFAOYSA-N 3,7-dimethyloctan-1-ol Chemical compound CC(C)CCCC(C)CCO PRNCMAKCNVRZFX-UHFFFAOYSA-N 0.000 description 2
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- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- UXFSPRAGHGMRSQ-UHFFFAOYSA-N 3-isobutyl-2-methoxypyrazine Chemical compound COC1=NC=CN=C1CC(C)C UXFSPRAGHGMRSQ-UHFFFAOYSA-N 0.000 description 2
- YYPNJNDODFVZLE-UHFFFAOYSA-N 3-methylbut-2-enoic acid Chemical compound CC(C)=CC(O)=O YYPNJNDODFVZLE-UHFFFAOYSA-N 0.000 description 2
- ALHUZKCOMYUFRB-UHFFFAOYSA-N 3-methylcyclopentadecan-1-one Chemical compound CC1CCCCCCCCCCCCC(=O)C1 ALHUZKCOMYUFRB-UHFFFAOYSA-N 0.000 description 2
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- GNKZMNRKLCTJAY-UHFFFAOYSA-N 4'-Methylacetophenone Chemical compound CC(=O)C1=CC=C(C)C=C1 GNKZMNRKLCTJAY-UHFFFAOYSA-N 0.000 description 2
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- JVJFIQYAHPMBBX-UHFFFAOYSA-N 4-hydroxynonenal Chemical compound CCCCCC(O)C=CC=O JVJFIQYAHPMBBX-UHFFFAOYSA-N 0.000 description 2
- NTPLXRHDUXRPNE-UHFFFAOYSA-N 4-methoxyacetophenone Chemical compound COC1=CC=C(C(C)=O)C=C1 NTPLXRHDUXRPNE-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
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- 241000717739 Boswellia sacra Species 0.000 description 2
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- 239000002253 acid Substances 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- XCPQUQHBVVXMRQ-UHFFFAOYSA-N alpha-Fenchene Natural products C1CC2C(=C)CC1C2(C)C XCPQUQHBVVXMRQ-UHFFFAOYSA-N 0.000 description 2
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 2
- 150000003927 aminopyridines Chemical class 0.000 description 2
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- NPFVOOAXDOBMCE-UHFFFAOYSA-N trans-3-hexenyl acetate Natural products CCC=CCCOC(C)=O NPFVOOAXDOBMCE-UHFFFAOYSA-N 0.000 description 1
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 1
- XJPBRODHZKDRCB-UHFFFAOYSA-N trans-alpha-ocimene Natural products CC(=C)CCC=C(C)C=C XJPBRODHZKDRCB-UHFFFAOYSA-N 0.000 description 1
- DKZBBWMURDFHNE-UHFFFAOYSA-N trans-coniferylaldehyde Natural products COC1=CC(C=CC=O)=CC=C1O DKZBBWMURDFHNE-UHFFFAOYSA-N 0.000 description 1
- BJIOGJUNALELMI-UHFFFAOYSA-N trans-isoeugenol Natural products COC1=CC(C=CC)=CC=C1O BJIOGJUNALELMI-UHFFFAOYSA-N 0.000 description 1
- HFFLGKNGCAIQMO-UHFFFAOYSA-N trichloroacetaldehyde Chemical compound ClC(Cl)(Cl)C=O HFFLGKNGCAIQMO-UHFFFAOYSA-N 0.000 description 1
- WKSPQBFDRTUGEF-UHFFFAOYSA-N tridec-2-enenitrile Chemical compound CCCCCCCCCCC=CC#N WKSPQBFDRTUGEF-UHFFFAOYSA-N 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 235000016788 valerian Nutrition 0.000 description 1
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 1
- 235000012141 vanillin Nutrition 0.000 description 1
- 239000001846 viola odorata l. leaf absolute Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000009637 wintergreen oil Substances 0.000 description 1
- QRPLZGZHJABGRS-UHFFFAOYSA-N xi-5-Dodecanolide Chemical compound CCCCCCCC1CCCC(=O)O1 QRPLZGZHJABGRS-UHFFFAOYSA-N 0.000 description 1
- WGPCZPLRVAWXPW-UHFFFAOYSA-N xi-Dihydro-5-octyl-2(3H)-furanone Chemical compound CCCCCCCCC1CCC(=O)O1 WGPCZPLRVAWXPW-UHFFFAOYSA-N 0.000 description 1
- PHXATPHONSXBIL-UHFFFAOYSA-N xi-gamma-Undecalactone Chemical compound CCCCCCCC1CCC(=O)O1 PHXATPHONSXBIL-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/20—After-treatment of capsule walls, e.g. hardening
- B01J13/22—Coating
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
- A01N25/28—Microcapsules or nanocapsules
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/14—Polymerisation; cross-linking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/20—After-treatment of capsule walls, e.g. hardening
- B01J13/206—Hardening; drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D20/00—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00
- F28D20/02—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00 using latent heat
- F28D20/023—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00 using latent heat the latent heat storage material being enclosed in granular particles or dispersed in a porous, fibrous or cellular structure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/14—Thermal energy storage
Abstract
Description
(a)少なくとも1つのアクティブなコアと
(b)カプセル壁と、を含むマイクロカプセルに関する。
カプセル壁は少なくとも3つのポリマー層からなり、これらのポリマー層の少なくとも1つは第1のフェノール樹脂からなり、第1のフェノール樹脂は少なくとも1つの芳香族ポリオールに由来する部分の3重量%~50重量%を含む。少なくとも1つのさらなるポリマー層は、第2のフェノール樹脂からなり、第2のフェノール樹脂は、少なくとも1つのトリフェノールに由来する部分の3重量%~50重量%を含む。
(a)少なくとも1つの活性物質を含むコア、および
(b)カプセル壁、
で構成され、カプセル壁は、少なくとも3つのポリマー層からなり、これらポリマー層の少なくとも1つは、少なくとも1つの芳香族ポリオールと少なくとも1つのアルデヒドの縮合に由来する部分を含み、少なくとも1つのさらなるポリマーは、少なくともトリフェノールと少なくとも1つのアルデヒドからの縮合である。
ポリアミン/予備縮合物
活性物質
例えば3-カレン、a-ピネン、ベータピネン、α-テルピネン、ガンマテルピネン、p-シメン、ビサボレン、カンフェン、カリオフィレン、セドレン、ファルネセン、リモネン、ロンギホレン、ミルセン、オシメン、バレンセン、(E,Z)-1,3,5-ウンデカトリエン。
例えばヘキサノール、オクタノール、3-オクタノール、2,6-ジメチルヘプタノール、2-メチルヘプタノール、2-メチルオクタノール、(E)-2-ヘキセノール、(E)-および(Z)-3-ヘキセノール、1-オクテン-3-オール、3,4,5,6,6-ペンタメチル-3/4-ヘプテン-2-オールと3,5,6,6-テトラメチル-4-メチレンヘプタン-2-オールとの混合物、(E,Z)-2,6-ノナジエノール、3,7-ジメチル-7-メトキシオクタン-2-オール、9-デセノール、10-ウンデセノール、4-メチル-3-デセン-5-オール。
例えばヘキサナール、ヘプタナール、オクタナール、ノナナール、デカナール、ウンデカナール、ドデカナール、トリデカナール、2-メチルオクタナール、2-メチルノナナール、(E)-2-ヘキセナール、(Z)-4-ヘプタナール、2,6-ジメチル-5-ヘプテナール、10-アンデセナル、(E)-4-デセナル、2-ドデセナル、2,6,10-トリメチル-5,9-ウンデカジエナール、ヘプタナールジエチルアセタール、1,1-ジメトキシ-2,2,5-トリメチル-4-ヘキセン、シトロネリルオキシアセトアルデヒド。
例えば2-ヘプタノン、2-オクタノン、3-オクタノン、2-ノナノン、5-メチル-3-ヘプタノン、5-メチル-3-ヘプタノオキシム、2,4,4,7-テトラメチル-6-オクテン-3-オン。
例えば3-メチルチオヘキサノール、3-メチルチオヘキシルアセテート、3-メルカプトヘキサノール、3-メルカプトヘキシルアセテート、3-メルカプトヘキシルブチレート、3-アセチルチオヘキシルアセテート、1-メンテン-8-チオール。
例えば2?ノネノニトリル、2-トリデセノニトリル、2,12-トリデセノニトリル、3,7-ジメチル-2,6-オクタジエノニトリル、3,7-ジメチル-6-オクテノニトリル。
例えば、(E)-および(Z)-3-ヘキセニルギ酸塩、アセト酢酸エチル、酢酸イソアミル、酢酸ヘキシル、3,5,5-トリメチルヘキシルアセテート、3-メチル-2-ブテニルアセテート、(E)-2-ヘキセニルアセテート、(E)-および(Z)-3-ヘキセニルアセテート、酢酸オクチル、3-オクチルアセテート、1-オクテン-3-イルアセテート、酪酸エチル、酪酸ブチル、酪酸イソアミル、酪酸ヘキシル、(E)-および(Z)-3-ヘキセニルイソブチレート、クロトン酸ヘキシル、イソ吉草酸エチル、エチル-2-メチルペンタノエート、エチルヘキサノエート、アリルヘキサノエート、ヘプタン酸エチル、ヘプタン酸アリル、オクタン酸エチル、(E,Z)-2,4-デカジエン酸エチル、2-オクチン酸メチル、2-ノニン酸メチル、アリル2-イソアミルオキシアセテート、メチル3,7-ジメチル-2,6-オクタジエノエート。
例えばシトロネロール、ゲラニオール、ネロール、リナロール、ラバデュロール、ネロリドール、ファルネソール、テトラヒドロリナロール、テトラヒドロゲラニオール、2,6-ジメチル-7-オクテン-2-オール、2,6-ジメチルオクタン-2-オール、2-メチル-6-メチレン-7-オクテン-2-オール、2,6-ジメチル-5,7-オクタジエン-2-オール、2,6-ジメチル-3,5-オクタジエン-2-オール、3,7-ジメチル-4,6-オクタジエン-3-オール、3,7-ジメチル-1,5,7-オクタトリエン-3-オール、2,6-ジメチル-2,5,7-オクタトリエン-1-オール、およびそれらのギ酸塩、酢酸塩、プロピオン酸塩、イソ酪酸塩、酪酸塩、イソ吉草酸塩、ペンタノエート、ヘキサノエート、クロトネート、チグリネート、およびそれらの3-メチル-2-ブテノエート。
例えばゲラニアール、ネラル、シトロネラール、7-ヒドロキシ-3,7-ジメチルオクタナール、7-メトキシ-3,7-ジメチルオクタナール、2,6,10-トリメチル-9-ウンデセナール、ゲラニルアセトン、ゲラニアール、ネラル、および7-ヒドロキシ-3,7-ジメチルオクタナールのジメチルおよびジエチルアセタール。
例えばメントール、イソプレゴール、α-テルピネオール、テルピネン-4、メンタン-8-オール、メンタン-1-オール、メンタン-7-オール、ボルネオール、イソボルネオール、リナロールオキシド、ノポール、セドロール、アンブリノール、ベチベロール、グアイオール、およびそれらのギ酸塩、酢酸塩、プロピオン酸塩、イソ酪酸塩、酪酸塩、イソ吉草酸塩、ペンタノエート、ヘキサノエート、クロトネート、チグリネート、およびそれらの3-メチル-2-ブテノエート。
例えばメントン、イソメントン、8-メルカプトメンタン-3-オン、カルボン、樟脳、フェンコン、a-イオノン、ベータイオノン、a-n-メチルイオノン、ベータ-n-メチルイオノン、α-イソメチルイオノン、ベータ-イソメチルイオノン、a-irone、ダマスコン、ベータダマスコン、ベータダマセノン、アルファダマスコン、d-ダマスコン、1-(2,4,4-トリメチル-2-シクロヘキセノン-1-イル)-2-ブテン-1-オン、1,3,4,6,7,8a-ヘキサヒドロ-1,1,5,5-テトラメチル-2H-2,4a-メタノナフタレン-8(5H)-オン、ヌートカトン、ジヒドロヌートカトン、a-sinensal、ベータサイン、アセチル化シダーウッドオイル(メチルセドリルケトン)。
例えば4-tert-ブチルシクロヘキサノール、3,3,5-トリメチルシクロヘキサノール、3-イソカンフィルシクロヘキサノール、2,6,9-トリメチル-(Z2,Z5,E9)-シクロドデカトリエン-1-オール、2-イソブチル-4-メチルテトラヒドロ-2H-ピラン-4-オール、
例えばシネオール、セドリルメチルエーテル、シクロドデシルメチルエーテル、(エトキシメトキシ)シクロドデカン、α-セドレンエポキシド、3a,6,6,9a-テトラメチルドデカヒドロナフト[2,1-b]フラン、3a-エチル-6,6,9a-トリメチルドデカヒドロナフト[2,1-b]フラン、1,5,9-トリメチル-13-オキサビシクロ[10.1.0]トリデカ-4,8-ジエン、ローズオキシド、2-(2,4-ジメチル-3-シクロヘキセン-1-イル)-5-メチル-5-(1-メチルプロピル)-1,3-ジオキサン。
例えば4-tert-ブチルシクロヘキサノン、2,2,5-トリメチル-5-ペンチルシクロペンタノン、2-ヘプチルシクロペンタノン、2-ペンチルシクロペンタノン、2-ヒドロキシ-3-メチル-2-シクロペンテン-1-オン、3-メチル-シス-2-ペンテン-1-イル-2-シクロペンテン-1-オン、3-メチル-2-ペンチル-2-シクロペンテン-1-オン、3-メチル-4-シクロペンタデセノン、3-メチル-5-シクロペンタデセノン、3-メチルシクロペンタデカノン、4-(1-エトキシビニル)-3,3,5,5-テトラメチルシクロヘキサノン、4-tert-ペンチルシクロヘキサノン、5-シクロヘキサデセン-1-オン、6,7-ジヒドロ-1,1,2,3,3-ペンタメチル-4(5H)-インダノン、9-シクロヘプタ-デセン-1-オン、シクロペンタデカノン、シクロヘキサデカノン。
例えば2,4-ジメチル-3-シクロヘキセンカルバルデヒド、2-メチル-4-(2,2,6-トリメチルシクロヘキセン-1-イル)-2-ブテナール、4-(4-ヒドロキシ-4-メチルペンチル)-3-シクロヘキセンカルバルデヒド、4-(4-メチル-3-ペンテン-1-イル)-3-シクロヘキセンカルバルデヒド。
例えば1-(3,3-ジメチルシクロヘキシル)-4-ペンテン-1-オン、1-(5,5-ジメチル-1-シクロヘキセン-1-イル)-4-ペンテン-1-オン、2,3,8,8-テトラメチル-1,2,3,4,5,6,7,8-オクタヒドロ-2-ナフタレニルメチルケトン、メチル2,6,10-トリメチル-2,5,9-シクロドデカトリエニルケトン、tert-ブチル 2,4-ジメチル-3-シクロヘキセン-1-イル ケトン。
例えば2-tert-ブチルシクロヘキシルアセテート、4-tert-ブチルシクロヘキシルアセテート、2-tert-ペンチルシクロヘキシルアセテート、4-tert-ペンチルシクロヘキシルアセテート、デカヒドロ-2-ナフチルアセテート、3-ペンチルテトラヒドロ-2H-ピラン-4-イルアセテート、デカヒドロ-2,5,5,8a-テトラメチル-2-ナフチルアセテート、4,7-メタノ-3a,4,5,6,7,7a-ヘキサヒドロ-5-または-6-インデニルアセテート、4,7-メタノ-3a,4,5,6,7,7a-ヘキサヒドロ-5-または-6-インデニルプロピオネート、4,7-メタノ-3a,4,5,6,7,7a-ヘキサヒドロ-5-または-6-インデニルイソブチレート、4,7-メタノオクタヒドロ-5-または-6-インデニルアセテート。
例えばアリル3?シクロヘキシルプロピオネート、アリルシクロヘキシルオキシアセテート、メチルジヒドロジャスモネート、ジャスモン酸メチル、メチル2-ヘキシル-3-オキソシクロペンタンカルボキシレート、2-エチル-6,6-ジメチル-2-シクロヘキセンカルボン酸エチル、2,3,6,6-テトラメチル-2-シクロヘキセンカルボン酸エチル、2-メチル-1,3-ジオキソラン-2-酢酸エチル。
例えばスチレンおよびジフェニルメタン。
例えばベンジルアルコール、1-フェネチルアルコール、2-フェネチルアルコール、3-フェニルプロパノール、2-フェニルプロパノール、2-フェノキシエタノール、2,2-ジメチル-3-フェニルプロパノール、2,2-ジメチル-3-(3-メチルフェニル)プロパノール、1,1-ジメチル-2-フェネチルアルコール、1,1-ジメチル-3-フェニルプロパノール、1-エチル-1-メチル-3-フェニルプロパノール、2-メチル-5-フェニルペンタノール、3-メチル-5-フェニルペンタノール、3-フェニル-2-プロペン-1-オール、4-メトキシベンジルアルコール、1-(4-イソプロピルフェニル)エタノール。
例えば酢酸ベンジル、プロピオン酸ベンジル、ベンジルイソブチレート、ベンジルイソ吉草酸、2-フェネチルアセテート、2-フェネチルプロピオン酸、2-フェネチルイソブチレート、2-フェネチルイソバレレート、1-フェネチルアセテート、a-トリクロロメチルベンジルアセテート、a,a-ジメチルフェネチルアセテート、a,a-ジメチルフェネチルブチレート、酢酸シンナミル、2-フェノキシエチルイソブチレート、4-メトキシベンジルアセテート。
例えば2-フェネチルメチルエーテル、2-フェネチルイソアミルエーテル、2-フェネチル1-エトキシエチルエーテル、フェニルアセトアルデヒドジメチルアセタール、フェニルアセトアルデヒド ジエチルアセタール、水和性アルデヒドジメチルアセタール、フェニルアセトアルデヒドグリセロールアセタール、2,4,6-トリメチル-4-フェニル-1,3-ジオキサン、4,4a,5,9b-テトラヒドロインデノ[1,2-d]-m-ダイオキシン、4,4a,5,9b-テトラヒドロ-2,4-ジメチルインデノ[1,2-d]-m-ダイオキシン。
例えばベンズアルデヒド。フェニルアセトアルデヒド、3-フェニルプロパナール、水和性アルデヒド、4-メチルベンズアルデヒド、4-メチルフェニルアセトアルデヒド、3-(4-エチルフェニル)-2,2-ジメチルプロパナール、2-メチル-3-(4-イソプロピルフェニル)プロパナール、2-メチル-3-(4-tert-ブチルフェニル)プロパナール、3-(4-tert-ブチルフェニル)プロパナール、シンナムアルデヒド、α-ブチルシンナムアルデヒド、α-アミルシンナムアルデヒド、α-ヘキシルシンナムアルデヒド、3-メチル-5-フェニルペンタナール、4-メトキシ-ベンズアルデヒド、4-ヒドロキシ-3-メトキシベンズアルデヒド、4-ヒドロキシ-3-エトキシベンズアルデヒド、3,4-メチレンジオキシベンズアルデヒド、3,4-ジメトキシベンズアルデヒド、2-メチル-3-(4-メトキシ-フェニル)プロパナール、2-メチル-3-(4-メチレンジオキシフェニル)プロパナール。
例えばアセトフェノン。4-メチルアセトフェノン、4-メトキシアセトフェノン、4-tert-ブチル-2,6-ジメチルアセトフェノン、4-フェニル-2-ブタノン、4-(4-ヒドロキシフェニル)-2-ブタノン、1-(2-ナフタレニル)エタノン、ベンゾフェノン、1,1,2,3,3,6-ヘキサメチル-5-インダニルメチルケトン、6-tert-ブチル-1,1-ジメチル-4-インダニルメチルケトン、1-[2,3-ジヒドロ-1,1,2,6-テトラメチル-3-(1-メチルエチル)-1H-5-インデニル]エタノン、5’,6’,7’,8’-テトラヒドロ-3’,5’,5’,6’,8’,8’-ヘキサメチル-2-アセトナフトン。
例えば安息香酸、フェニル酢酸、安息香酸メチル、安息香酸エチル、安息香酸ヘキシル、安息香酸ベンジル、メチルフェニルアセテート、酢酸エチルフェニル、ゲラニルフェニルアセテート、フェネチルフェニルアセテート、ケイ皮酸メチル、ケイ皮酸エチル、ケイ皮酸ベンジル、ケイ皮酸フェニルエチル、桂皮酸シンナミル、アリルフェノキシアセテート、サリチル酸メチル、サリチル酸イソアミル、サリチル酸ヘキシル、サリチル酸シクロヘキシル、サリチル酸シス-3-ヘキセニル、サリチル酸ベンジル、サリチル酸フェニルエチル、2,4-ジヒドロキシ-3,6-ジメチル安息香酸メチル、エチル3-フェニルグリシデート、エチル3-メチル-3-フェニルグリシデート。
例えば、2,4,6-トリニトロ-1,3-ジメチル-5-tert-ブチルベンゼン、3,5-ジニトロ-2,6-ジメチル-4-tert-ブチルアセトフェノン、シンナモニトリル、5-フェニル-3-メチル-2-ペンテノニトリル、5-フェニル-3-メチルペンタノニトリル、アントラニル酸メチル、N-メチルアントラニル酸メチル、7-ヒドロキシ-3,7-ジメチルオクタナールを含むアントラニル酸メチルのシッフ塩基、2-メチル-3-(4-tert-ブチルフェニル)プロパナールまたは2,4-ジメチル-3-シクロヘキセン-カルバルデヒド、6-イソプロピルキノリン、6-イソブチルキノリン、6-sec-ブチルキノリン、インドール、スカトール、2-メトキシ-3-イソプロピルピラジン、2-イソブチル-3-メトキシピラジン、4-(4,8-ジメチル-3,7-ノナジエニル)ピリジン。
例えばエストラゴール。アネトール、オイゲノール、オイゲニルメチルエーテル、イソオイゲノール、イソオイゲニルメチルエーテル、チモール、カルバクロール、ジフェニルエーテル、ベータナフトールメチルエーテル、ベータナフチルエチルエーテル、ベータ-ナフチルイソブチルエーテル、1,4-ジメトキシベンゼン、オイゲニルアセテート、2-メトキシ-4-メチルフェノール、2-エトキシ-5-(1-プロペニル)フェノール、p-クレシルフェニルアセテート。
例えば1,4-オクタノライド、3-メチル-1,4-オクタノライド、1,4-ノナリド、1,4-デカノライド、8-デセン-1,4-オリド、1,4-ウンデカノライド、1,4-ドデカノライド、1,5-デカノライド、1,5-ドデカノライド、1,15-ペンタデカノライド、シス-およびトランス-11-ペンタデセン-1,15-オリド、シス-およびトランス-12-ペンタデセン-1,15-オリド、1,16-ヘキサデカノリド、9-ヘキサデセン-1,16-オリド、10-オキサ-1,16-ヘキサデカノライド、11-オキサ-1,16-ヘキサデカノライド、12-オキサ-1,16-ヘキサデカノリド、エチレン-1,12-ドデカンジオエート、エチレン-1,13-トリデカンジオエート、クマリン、2,3-ジヒドロクマリン、オクタヒドロクマリン。
安定剤と保護コロイド
製造方法
(a)少なくとも1つのアルデヒドまたは少なくとも1つのポリアミン予備縮合物を含む第1の水性製剤を提供する工程。
(b) カプセル化される活性物質および少なくとも1つの芳香族ポリオールを含む油相を提供する工程。
(c) 少なくとも1つの乳化剤および/または安定剤の存在下で水相を油相と混合して、エマルションを形成する工程。
(d) 重合を開始する工程。
(e) 少なくとも1つのポリアミンまたはポリアミン予備縮合物を添加する工程。
(f) 40~70℃で40~80分間静置する工程。
(g) 少なくとも1つのトリフェノールを加える工程。
(h) 少なくとも1つのアルデヒドまたは少なくとも1つのポリアミン予備縮合物を添加する工程。
(i) 混合物を40~70℃で40~80分間静置する工程。
(j) 得られたマイクロカプセルの架橋および硬化する工程。および必要に応じて、
(k)分散液からマイクロカプセルを分離し、乾燥させる工程。
以下、本発明のカプセルの製造について説明する。これには、次の手順が含まれる。
最初のポリマー層の形成:
1. 芳香族ポリオール、好ましくはレゾルシノールを香料の油相に溶解し、ホルムアルデヒドを水相に添加する。
2. ギ酸またはギ酸の混合物、クエン酸およびアスコルビン酸でpH3~5に酸性化して重合を開始し、呈色反応をブロックする。
3.60°C~70°Cに加熱する。
4. 必要に応じて、反応をCO2でブランケティングする。
第2ポリマー層の形成:
5. 水に溶解したポリアミン、好ましくはメラミン-ホルムアルデヒドまたはLuracollSDを添加する。
6. Lupasol PA140保護コロイドを水に溶解する。
7. 60℃で60分間静置する。
8. 必要に応じて、pHを調整するために酸性化する。
3番目のポリマー層の形成:
9. 少なくとも1つのトリフェノール、好ましくはフロログルシノールを添加する。
10. ホルムアルデヒドまたはLuracollSDを追加する。
11. 60℃で60分間静置する。
12. 必要に応じて、80°C~90°Cに加熱する。
13. その後、35℃まで冷却する。
14. 必要に応じて、カプセルをさらに硬化させるためにさらに物質を追加する。
Claims (15)
- (a)少なくとも1つの活性物質を含むコアと、
(b)カプセル壁、を備え、
前記カプセル壁が少なくとも3つのポリマー層からなり、
これらポリマー層の少なくとも1つが第1のフェノール樹脂で構成され、前記第1のフェノール樹脂が少なくとも1つの芳香族ポリオールに由来する部分を3重量%~50重量%含み、
少なくとも1つのさらなるポリマー層は、第2のフェノール樹脂からなり、前記第2のフェノール樹脂は、少なくとも1つのトリフェノールに由来する部分を3重量%~50重量%含む、マイクロカプセル。 - 前記少なくとも3つのポリマー層が交互構造を有し、フェノール樹脂からなるポリマー層がアミノ樹脂からなるポリマー層によってそれぞれ分離されている、請求項1に記載のマイクロカプセル。
- 芳香族ポリオール部分がレゾルシノールに由来する、請求項1または請求項2に記載のマイクロカプセル。
- 前記トリフェノール部分がフロログルシノールに由来する、請求項1から請求項3のいずれか一項に記載のマイクロカプセル。
- スラリーに基づくカプセル壁含有量が、0.3重量%~3重量%である、請求項1から請求項4のいずれか一項に記載のマイクロカプセル。
- 請求項1に記載のマイクロカプセルを生成する方法であって、
(a)少なくとも1つのアルデヒドまたは少なくとも1つのポリアミン予備縮合物を含む第1の水性製剤を提供する工程と、
(b)カプセル化される活性物質および少なくとも1つの芳香族ポリオールを含む油相を提供する工程と、
(c)少なくとも1つの乳化剤および/または安定剤の存在下で水相を油相と混合して、エマルションを形成する工程と、
(d)重合を開始する工程と、
(e)少なくとも1つのポリアミンまたはポリアミン予備縮合物を添加する工程と、
(f)40~70℃で40~80分間静置する工程と、
(g)少なくとも1つのトリフェノールを加える工程と、
(h)少なくとも1つのアルデヒドまたは少なくとも1つのポリアミン予備縮合物を添加する工程と、
(i)混合物を40~70℃で40~80分間静置する工程と、
(j)工程(f)で得られたマイクロカプセルの架橋および硬化する工程と、任意で、
(k)分散液からマイクロカプセルを分離し、乾燥させる工程と、
を備える、方法。 - 前記工程(c)の後に、CO2による反応のブランケティングが続く、請求項6に記載の方法。
- CO2による反応のブランケティングが、芳香族ポリオールによって引き起こされるマイクロカプセルの変色を少なくとも低減する、請求項7に記載の方法。
- 前記アルデヒドおよび/またはポリアミン予備縮合物が、任意にアルキル化されたモノおよびポリメチロール尿素、またはモノおよびポリメチロールメラミン予備縮合物、部分的にメチル化されたモノ-およびポリメチロール-1,3,5-トリアミノ-2,4,6-トリアジン予備縮合物、モノおよびポリアルキロールベンゾグアナミン予備縮合物、およびモノおよびポリアルキロールグリコールウリル予備縮合物、ジアルデヒド、ホルムアルデヒドおよびそれらの混合物によって形成される群から選択され、使用される、
請求項6から請求項8のうちの少なくとも一項に記載の方法。 - 前記カプセル化される活性物質が香油である、請求項6から請求項9のうち少なくとも一項に記載の方法。
- 前記工程(i)の直後に、外側ポリマー層を形成するために、混合物を80℃~90℃に加熱する、請求項6から請求項10の少なくとも一項に記載の方法。
- 前記トリフェノールがフロログルシノールである、請求項6から請求項11のいずれか一項に記載の方法。
- 前記重合が、芳香族ポリオールの呈色反応をブロックするために、ギ酸またはギ酸、クエン酸およびアスコルビン酸の混合物を添加してpHを3~5の値に下げることにより、工程(d)で開始される、請求項6から請求項12のいずれか一項に記載の方法
- 工程(b)における少なくとも1つの芳香族ポリオールの添加および工程(f)における少なくとも1つのトリフェノールの前記添加が、薄いカプセル壁の形成を可能にする、請求項7から請求項13のいずれか一項に記載の方法。
- 化粧用調合物または香料組成物が、請求項1から請求項5の少なくとも1つに記載、または請求項6から請求項14の少なくとも1つに記載の方法により得られるマイクロカプセルを含む、洗浄剤または洗浄剤組成物。
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