JP2021522184A - 農薬乳剤の散布ドリフト制御のためのレオロジー改質剤 - Google Patents
農薬乳剤の散布ドリフト制御のためのレオロジー改質剤 Download PDFInfo
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- JP2021522184A JP2021522184A JP2020557286A JP2020557286A JP2021522184A JP 2021522184 A JP2021522184 A JP 2021522184A JP 2020557286 A JP2020557286 A JP 2020557286A JP 2020557286 A JP2020557286 A JP 2020557286A JP 2021522184 A JP2021522184 A JP 2021522184A
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- WWJZWCUNLNYYAU-UHFFFAOYSA-N temephos Chemical compound C1=CC(OP(=S)(OC)OC)=CC=C1SC1=CC=C(OP(=S)(OC)OC)C=C1 WWJZWCUNLNYYAU-UHFFFAOYSA-N 0.000 description 1
- IROINLKCQGIITA-UHFFFAOYSA-N terbutryn Chemical compound CCNC1=NC(NC(C)(C)C)=NC(SC)=N1 IROINLKCQGIITA-UHFFFAOYSA-N 0.000 description 1
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- 235000010296 thiabendazole Nutrition 0.000 description 1
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- 125000004305 thiazinyl group Chemical group S1NC(=CC=C1)* 0.000 description 1
- XSKZXGDFSCCXQX-UHFFFAOYSA-N thiencarbazone-methyl Chemical compound COC(=O)C1=CSC(C)=C1S(=O)(=O)NC(=O)N1C(=O)N(C)C(OC)=N1 XSKZXGDFSCCXQX-UHFFFAOYSA-N 0.000 description 1
- YFNCATAIYKQPOO-UHFFFAOYSA-N thiophanate Chemical compound CCOC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OCC YFNCATAIYKQPOO-UHFFFAOYSA-N 0.000 description 1
- QGHREAKMXXNCOA-UHFFFAOYSA-N thiophanate-methyl Chemical compound COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC QGHREAKMXXNCOA-UHFFFAOYSA-N 0.000 description 1
- ILERPRJWJPJZDN-UHFFFAOYSA-N thioquinox Chemical compound C1=CC=C2N=C(SC(=S)S3)C3=NC2=C1 ILERPRJWJPJZDN-UHFFFAOYSA-N 0.000 description 1
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- NKNFWVNSBIXGLL-UHFFFAOYSA-N triazamate Chemical compound CCOC(=O)CSC1=NC(C(C)(C)C)=NN1C(=O)N(C)C NKNFWVNSBIXGLL-UHFFFAOYSA-N 0.000 description 1
- AMFGTOFWMRQMEM-UHFFFAOYSA-N triazophos Chemical compound N1=C(OP(=S)(OCC)OCC)N=CN1C1=CC=CC=C1 AMFGTOFWMRQMEM-UHFFFAOYSA-N 0.000 description 1
- IQGKIPDJXCAMSM-UHFFFAOYSA-N triazoxide Chemical compound N=1C2=CC=C(Cl)C=C2[N+]([O-])=NC=1N1C=CN=C1 IQGKIPDJXCAMSM-UHFFFAOYSA-N 0.000 description 1
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- WCLDITPGPXSPGV-UHFFFAOYSA-N tricamba Chemical compound COC1=C(Cl)C=C(Cl)C(Cl)=C1C(O)=O WCLDITPGPXSPGV-UHFFFAOYSA-N 0.000 description 1
- NFACJZMKEDPNKN-UHFFFAOYSA-N trichlorfon Chemical compound COP(=O)(OC)C(O)C(Cl)(Cl)Cl NFACJZMKEDPNKN-UHFFFAOYSA-N 0.000 description 1
- HSMVPDGQOIQYSR-KGENOOAVSA-N triflumizole Chemical compound C1=CN=CN1C(/COCCC)=N/C1=CC=C(Cl)C=C1C(F)(F)F HSMVPDGQOIQYSR-KGENOOAVSA-N 0.000 description 1
- XAIPTRIXGHTTNT-UHFFFAOYSA-N triflumuron Chemical compound C1=CC(OC(F)(F)F)=CC=C1NC(=O)NC(=O)C1=CC=CC=C1Cl XAIPTRIXGHTTNT-UHFFFAOYSA-N 0.000 description 1
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- WCJYTPVNMWIZCG-UHFFFAOYSA-N xylylcarb Chemical compound CNC(=O)OC1=CC=C(C)C(C)=C1 WCJYTPVNMWIZCG-UHFFFAOYSA-N 0.000 description 1
- 239000005943 zeta-Cypermethrin Substances 0.000 description 1
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Abstract
【選択図】図1
Description
(A)は、式Iのα,βエチレン性不飽和カルボン酸モノマーであり、
(B)は、式IIの非イオン性の共重合性α,βエチレン性不飽和モノマーであり、
(C)は、式IIIの疎水的に改質されたα、βエチレン性不飽和カルボン酸モノマーであり、
式中、R’は、H、−COOH、またはCH3であり、R”は、H、CH3、−COOH、または−CH2COOHであり、Zは、上記の式IIIに示される疎水性残基である。
ならびにそのC1−C12アルキルまたは例えば、ベンジルエステルなどのC7−C12アリールアルキルエステルまたは塩誘導体などの、オーキシン除草剤が含まれる。
カノーラ油(Crisco(登録商標)ブランド)−植物油
Atlox(商標)DP13/6(Croda)−リン酸エステル界面活性剤
Atlox(商標)4912(Croda)−高分子界面活性剤
DOWANOL(商標)DPM(The Dow Chemical Company)−アルキレングリコールエーテル
ACRYSOL(商標)ASE−60(The Dow Chemical Company)−酸含有架橋アクリル乳剤コポリマー。
ACRYSOL(商標)TT−615(The Dow Chemical Company)−疎水性アクリル酸エステルモノマーで形成された三級ポリマー。
ACRYSOL(商標)2020−NPR(The Dow Chemical Company)−非イオン性の疎水的に改質されたエチレンオキシドウレタン。
グアーガム(Sigma Aldrich、製品番号G4129)は、グアーまたはガバール豆の胚乳から単離された糖であるガラクトースおよびマンノースから構成される多糖類である。
乳剤濃縮物1は、200g/kgのカノーラ油、200g/kgのAtlox(商標)DP13/6、25g/kgのAtlox(商標)4912、および575g/kgのDOWANOL(商標)DPMを含有する。室温(23℃)で57.5gのDOWANOL(商標)DPM、20gのカノーラ油、20グラムのAtlox(商標)DP13/6、および2.5gのAtlox(商標)4912を混和して、乳剤濃縮物1を調製する。混和物を軽い振とうまたは磁気撹拌によって混和し、100gの乳剤濃縮物1を提供する。乳剤濃縮物1を脱イオン水中で0.1から1.0重量%の濃度に希釈し、手でゆっくり振とうすることによって乳剤1を調製する。
例えば、表1に示す実施例1〜5に示されているレオロジー改質剤を、表1に示す量で乳剤1に添加し、手で軽く振とうして混合する。最終製剤のpHを、濃縮水酸化アンモニウム水溶液(Fisher Scientific、米国ペンシルベニア州ピッツバーグ)で調整し、これを滴下し、混合物をマグネチックスターラーでかき混ぜた。
水で希釈して散布溶液を調製する実施例および比較例を表1に示す。表1に示すように、0.5および5mLの実施例および比較例をそれぞれ499.5および495mLの脱イオン水で希釈することによって、0.1および1.0重量%の実施例または比較実施例を含有する水中油型乳剤を調製する。各実施例および比較例のpHを表1に示す値(23℃で測定)に調整する。全ての水中油型乳剤を、各々が均一になるまで手で軽く振とうした。
Claims (24)
- 農薬乳剤であって、
乳剤プレミックス濃縮物であって、
40〜70重量パーセント(重量%)のアルキレングリコールエーテル、
10〜40重量%の植物油、および
界面活性剤であって、前記界面活性剤の重量%が、前記植物油の重量%の0.5〜2倍の重量%であり、前記重量%値が、前記乳剤プレミックス濃縮物の総重量に基づき、前記アルキレングリコールエーテル、前記植物油、および前記界面活性剤の前記重量%が、合計で、前記乳剤プレミックス濃縮物の100重量%である、界面活性剤、を含む、乳剤プレミックス濃縮物と、
アクリレート系コポリマーであって、前記アクリレート系コポリマーが、50〜150万の重量平均分子量を有する、アクリレート系コポリマーと、
水系農薬組成物であって、前記農薬乳剤が、0.05〜5重量パーセント(重量%)の前記乳剤プレミックス濃縮物、0.05〜5重量%の前記アクリレート系コポリマー、および90〜99.9重量%の前記水系農薬組成物を含む、水系農薬組成物と、を含む、農薬乳剤。 - 前記アクリレート系コポリマーが、モノマー(A)、(B)、および(C)で形成されたアクリレート系ランダムコポリマーであり、モノマー(A)が、α,βエチレン性不飽和カルボン酸モノマーであり、モノマー(B)が、非イオン性の共重合性α,βエチレン性不飽和モノマーであり、モノマー(C)が、疎水的に改質されたα,βエチレン性不飽和カルボン酸モノマーである、請求項1に記載の農薬乳剤。
- モノマー(A)、(B)、および(C)の前記アクリレート系ランダムコポリマーが、30〜60重量%のモノマー(A)、30〜50重量%のモノマー(B)、および0〜15重量%のモノマー(C)で形成され、前記重量%が、前記アクリレート系ランダムコポリマーの総重量に基づき、前記モノマー(A)、(B)、および(C)が、合計で100重量%である、請求項2に記載の農薬乳剤。
- モノマー(A)が、メタクリル酸またはアクリル酸、モノマー(B)が、アクリル酸エチル、メタクリル酸メチル、またはアクリル酸ブチルであり、モノマー(C)が、10〜22個の炭素を有する疎水的に改質されたメタクリル化アルキルEO/POエステルである、請求項2〜3のいずれか一項に記載の農薬乳剤。
- 前記アルキレングリコールエーテルが、プロピレングリコールn−ブチルエーテル、ジプロピレングリコールメチルエーテル、ジプロピレングリコールn−プロピルエーテル、プロピレングリコールn−プロピルエーテル、ジプロピレングリコールn−ブチルエーテル、エチレングリコールモノヘキシルエーテル、エチレングリコールモノ−n−プロピルエーテル、ジエチレングリコールモノヘキシルエーテル、エチレングリコールモノ−n−プロピルエーテル、ジエチレングリコールモノヘキシルエーテル、ジエチレングリコールモノブチルエーテル、トリエチレングリコールモノブチルエーテル、またはそれらの組み合わせからなる群から選択される、請求項1〜4のいずれか一項に記載の農薬乳剤。
- 前記アルキレングリコールエーテルが、ジプロピレングリコールメチルエーテルである、請求項5に記載の農薬乳剤。
- 前記植物油が、アーモンド油、カノーラ油、大豆油、菜種油、オリーブ油、ヒマシ油、ヒマワリ種子油、ココナッツ油、コーン油、綿実油、亜麻仁油、パーム油、ピーナッツ油、サフラワー油、ゴマ油、桐油、またはそれらの組み合わせからなる群から選択される、請求項1〜6のいずれか一項に記載の農薬乳剤。
- 前記植物油が、メチル化植物油である、請求項1〜7のいずれか一項に記載の農薬乳剤。
- 前記界面活性剤が、リン酸エステル界面活性剤、高分子界面活性剤、またはそれらの組み合わせである、請求項1〜8のいずれか一項に記載の農薬乳剤。
- 前記水系農薬組成物が、除草剤、殺虫剤、殺菌剤、またはそれらの組み合わせを含有する、請求項1〜9のいずれか一項に記載の農薬乳剤。
- 前記農薬乳剤が、23℃の温度で測定された5〜9.5のpHを有する、請求項1〜10のいずれか一項に記載の農薬乳剤。
- タンクミックス添加剤濃縮物であって、
乳剤プレミックス濃縮物であって、
40〜70重量パーセント(重量%)のアルキレングリコールエーテル、
10〜40重量%の植物油、および
界面活性剤であって、前記界面活性剤の重量%が、前記植物油の重量%の0.5〜2倍の重量%であり、
前記乳剤プレミックス濃縮物の前記重量%値が、前記乳剤プレミックス濃縮物の総重量に基づき、前記アルキレングリコールエーテル、前記植物油、および前記界面活性剤の前記重量%が、合計で、前記乳剤プレミックス濃縮物の100重量%である、界面活性剤、を含む、乳剤プレミックス濃縮物と、
アクリレート系コポリマーであって、前記アクリレート系コポリマーが、50〜150万の重量平均分子量を有する、アクリレート系コポリマーと、を含み、
前記タンクミックス添加剤濃縮物が、前記アクリレート系コポリマーに対する前記乳剤プレミックス濃縮物の1:1〜1:10の重量比を含み、前記タンクミックス添加剤濃縮物が、水系農薬組成物中で希釈すると農薬組成物を形成する、タンクミックス添加剤濃縮物。 - 前記アクリレート系コポリマーが、モノマー(A)、(B)、および(C)で形成されたアクリレート系ランダムコポリマーであり、モノマー(A)が、α,βエチレン性不飽和カルボン酸モノマーであり、モノマー(B)が、非イオン性の共重合性α,βエチレン性不飽和モノマーであり、モノマー(C)が、疎水的に改質されたα,βエチレン性不飽和カルボン酸モノマーである、請求項12に記載のタンクミックス添加剤濃縮物。
- モノマー(A)、(B)、および(C)の前記アクリレート系ランダムコポリマーが、30〜60重量%のモノマー(A)、30〜50重量%のモノマー(B)、および0〜15重量%のモノマー(C)で形成され、前記重量%が、前記アクリレート系ランダムコポリマーの総重量に基づき、前記モノマー(A)、(B)、および(C)が、合計で100重量%である、請求項13に記載のタンクミックス添加剤濃縮物。
- モノマー(A)が、メタクリル酸またはアクリル酸、モノマー(B)が、アクリル酸エチル、メタクリル酸メチル、またはアクリル酸ブチルであり、モノマー(C)が、メタクリル化アルキルEO/POエステルある、請求項13〜14のいずれか一項に記載のタンクミックス添加剤濃縮物。
- 前記アルキレングリコールエーテルが、プロピレングリコールn−ブチルエーテル、ジプロピレングリコールメチルエーテル、ジプロピレングリコールn−プロピルエーテル、プロピレングリコールn−プロピルエーテル、ジプロピレングリコールn−ブチルエーテル、エチレングリコールモノヘキシルエーテル、エチレングリコールモノ−n−プロピルエーテル、ジエチレングリコールモノヘキシルエーテル、エチレングリコールモノ−n−プロピルエーテル、ジエチレングリコールモノヘキシルエーテル、ジエチレングリコールモノブチルエーテル、トリエチレングリコールモノブチルエーテル、またはそれらの組み合わせからなる群から選択される、請求項12〜15のいずれか一項に記載のタンクミックス添加剤。
- 前記アルキレングリコールエーテルが、ジプロピレングリコールメチルエーテルである、請求項16に記載のタンクミックス添加剤。
- 前記植物油が、アーモンド油、カノーラ油、大豆油、菜種油、オリーブ油、ヒマシ油、ヒマワリ種子油、ココナッツ油、コーン油、綿実油、亜麻仁油、パーム油、ピーナッツ油、サフラワー油、ゴマ油、桐油、またはそれらの組み合わせからなる群から選択される、請求項12〜17のいずれか一項に記載のタンクミックス添加剤。
- 前記植物油が、メチル化植物油である、請求項12〜18のいずれか一項に記載のタンクミックス添加剤。
- 前記界面活性剤が、リン酸エステル界面活性剤、高分子界面活性剤、またはそれらの組み合わせである、請求項12〜19のいずれか一項に記載のタンクミックス添加剤。
- 前記水系農薬組成物が、除草剤、殺虫剤、殺菌剤、またはそれらの組み合わせを含有する、請求項12〜20のいずれか一項に記載のタンクミックス添加剤。
- 前記タンクミックス添加剤濃縮物が、23℃の温度で測定された5〜8のpHを有する、請求項12〜21のいずれか一項に記載のタンクミックス添加剤。
- 農薬組成物散布適用中の散布ドリフトを低減する方法であって、
請求項12〜22のいずれか一項に記載のタンクミックス添加剤濃縮物を提供することと、
前記タンクミックス添加剤濃縮物を、水系農薬組成物を含む散布タンクに添加して農薬乳剤を形成することと、
前記農薬乳剤を散布器から散布することと、を含む、方法。 - 前記水系農薬組成物が、除草剤、殺虫剤、殺菌剤、またはそれらの組み合わせを含む、請求項23に記載の方法。
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