JP2021519784A - ポリガラクトマナンを含むヘアスタイリング組成物およびその使用方法 - Google Patents
ポリガラクトマナンを含むヘアスタイリング組成物およびその使用方法 Download PDFInfo
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Abstract
Description
方法を提供する。
(i)約40〜約1100KDaの範囲の分子量を有する約0.1重量%〜約2重量%のグアーヒドロキシプロピルトリモニウムクロリド;(ii)約0.1重量%〜約10重量%のポリビニルピロリドン/酢酸ビニルコポリマー、ビニルピロリドン/2−(ジメチルアミノ)エチルメタクリレートコポリマー、メチルビニルエーテル/無水マレイン酸コポリマーのエチルエステルまたはポリイミド−1;および(iii)保存剤、α−ヒドロキシカルボン酸およびそれらの混合物からなる、約0.1重量%〜約25重量%の少なくとも1つの化粧品成分を含み、保存剤がフェノキシエチルアルコール、カプリロイルグリコールまたはそれらの混合物を含み、α−ヒドロキシカルボン酸が乳酸、クエン酸およびリンゴ酸からなる群から選択される、ヘアスタイリングジェル組成物を提供する。
VP:ビニルピロリドン
PVP:ポリビニルピロリドン
VA:酢酸ビニル
DMAEMA:2−(ジメチルアミノ)エチルメタクリレート
PQ−55:ポリクオタニウム−55
PQ−11:ポリクオタニウム−11(ビニルピロリドンと第4級ジメチルミノエチルメタクリレートのコポリマー)
実施例
実験は、実施例5で調製した組成物のフォーム促進性、カール保持性、粘性、耐湿性および分布審美性を試験するために実施した。その結果を図4に示すが、試験データからは、300Kのカチオン変性グアーを含むヘアスタイリング組成物は、他の分子重量範囲に比べて著しく優れた結果をもたらすことが示された。
実施例1のムース0.5gを湿ったカーリーヘアトレス(International Hair Importers;Mulatto Type B、3.5g、幅1.75インチ、長さ6.5インチ)に適用し、スクランチしてカールを強調し、拡散乾燥し、カール形成について評価し、高湿度に60分間曝してカール保持性について評価した。トレスを高湿度(90%相対湿度、27oC)に60分間曝し、カール維持性(カールおよびフリッツ形成の幅/頻度の変化)を評価した。図1およびテーブル1は、グアーヒドロキシプロピルトリモニウムクロリドを添加すると、より明確なカール(より小さな波数とより大きな幅によって目視で確認される)が得られ、高湿度への暴露でカールが維持されることを示す試験結果を示している。
実施例1のムース0.30gを、清浄な湿ったトレス(International Hair Importers;暗褐色ヨーロッパ、2.0g、幅1.0インチ、長さ6.5インチ)に適用し、0.625インチローラーで斜めにロールし、拡散熱下で乾燥させ、40%相対湿度、25oCに平衡化し、ローラーを外し、トレスを0.25インチ区画に印をつけた水平線ボードに掛け、高湿度環境(90%相対湿度、27oC)に置いた。トレス長の開始時(初期)読み取り値をカールの底部で測定した。追加の測定値を24時間かけて測定し、図2に示す。耐湿性は次の式で計算した:
(Lo−Lt/Lo−Li)×100時間t
ここで、
Lo=完全に伸びた髪の長さ
Li=曝す前の毛の長さ(開始時)
Lt=曝した時間後の毛の長さ(t)。
実施例1のエアロゾルムース2.0グラムを並べて分注し、経時的に観察した。炭化水素、水QS、ポリマー1〜5%、炭化水素6〜15%などの推進剤を添加した単純な濃縮液から定性的評価を行った。マウス弁:精度マウス(Precision Mousse)弁、S90逆w/テールピース4スロット、標準スティックスパウト(Standard Stick Spout)。実験結果を図3に示す。
耐湿性‐0.30gムースを清浄な湿ったトレス(International Hair Importers;ダークブラウン欧州、2.0g、1.0インチ幅、6.5インチ長)に適用し、0.625インチローラーで斜めにロールし、拡散熱下で乾燥し、40RH、25oC、に均衡させた。ローラーを外し、トレスを0.25インチ区画に印をつけた水平線付きボードに掛け、高湿度環境に置いた(90RH、27oC)。トレス長の開始時読み取り値をカールの底部で測定した。追加の測定値は24時間にわたって取得され、図2に示されている。耐湿性は次の式で計算された。(図5)
(Lo−Lt/Lo−Li)×100時間t
ここで、
Lo=完全に伸びた髪の長さ
Li=曝す前の毛の長さ(開始時)
Lt=曝した時間後の毛の長さ(t)。
F1およびF10−第1および第10変形における最大の力。
F10/F1−剛性の第10および第1変形表示耐久性における最大力の比率。
Claims (36)
- i.約40〜約1100KDaの範囲の重量平均分子量を有する少なくとも1つのカチオン変性ポリガラクトマンナンと、
ii.少なくとも1つの化粧品成分と、
を含む、ヘアスタイリング組成物。 - 前記カチオン変性ポリガラクトマンナンが、カチオン変性カシアガムおよびカチオン変性グアーからなる群より選択される、請求項1に記載のヘアスタイリング組成物。
- 前記カチオン変性グアーが、グアーヒドロキシプロピルトリモニウムクロリドである、請求項2に記載のヘアスタイリング組成物。
- 前記カチオン変性ポリガラクトマンナンが、約150〜約700KDaの範囲の重量平均分子量(Mw)を有する、請求項1〜3のいずれか1項に記載のヘアスタイリング組成物。
- 前記カチオン変性ポリガラクトマンナンが、約200〜約400KDaの範囲の重量平均分子量(Mw)を有する、請求項1〜4のいずれか1項に記載のヘアスタイリング組成物。
- 前記カチオン変性グアーが、0.001単位を超えるカチオン置換度(Cat−DS)を有する、請求項2〜6のいずれか一項に記載のヘアスタイリング組成物。
- 少なくとも1つの第4級アンモニウム化合物をさらに含む、請求項1〜6のいずれか一項に記載のヘアスタイリング組成物。
- ビニルピロリドンのコポリマー、ポリビニルピロリドン(PVP)のコポリマー、無水マレイン酸のコポリマー、およびポリイミドのうちの少なくとも1種をさらに含む、請求項1〜7のいずれか一項に記載のヘアスタイリング組成物。
- 前記少なくとも1つの第4級アンモニウム化合物が、ポリクオタニウム−55(PQ−55)、およびポリクオタニウム−11(PQ−11)からなる群より選択される、請求項7に記載のヘアスタイリング組成物。
- 前記ビニルピロリドンのコポリマーがビニルピロリドン/2−(ジメチルアミノ)エチルメタクリレートであり、前記ポリビニルピロリドン(PVP)のコポリマーがポリビニルピロリドン/酢酸ビニルコポリマーであり、前記無水マレイン酸のコポリマーがメチルビニルエーテル/無水マレイン酸コポリマーのエチルエステルであり、前記ポリイミドがポリイミド−1である、請求項8に記載のヘアスタイリング組成物。
- 前記少なくとも1つの化粧品成分が、脂肪性物質、ゲル化剤、増粘剤、界面活性剤、保湿剤、軟化剤、親水性または親油性の活性剤、酸化防止剤、封鎖剤、保存剤、酸性化剤または塩基性化剤、フレグランス、フィラー、染料、乳化剤、溶剤、UV‐AまたはUV‐Bブロッカー/フィルタ、植物抽出物、保湿剤、タンパク質、ペプチド、中和剤、シリコン、酸化剤、推進剤、スタイリングポリマー、機能性ポリマー、オルガノシリコン、ふけ防止剤、ビタミン、脱イオン水、有機酸、α‐ヒドロキシカルボン酸、および還元剤からなる群より選択される、請求項1〜10のいずれか一項に記載のヘアスタイリング組成物。
- 毛髪の固定またはトリートメント、毛髪の矯正またはヘアスタイリングのために使用される、請求項1〜11のいずれか一項に記載のヘアスタイリング組成物。
- pHが約3〜約13の範囲である、請求項1〜12のいずれか1項に記載のヘアスタイリング組成物。
- エアロゾル、乳剤、ローション、ジェル、ベシクル分散液、ペースト、クリーム、固形スティック、ムース、シャンプー、またはスプレーとして配合される、請求項13に記載のヘアスタイリング組成物。
- 毛髪の矯正またはヘアスタイリングの配合組成に使用される組成物量が、配合組成物の全重量を基準として約0.01重量%〜約10.0重量%の範囲である、請求項1〜14のいずれか一項に記載のヘアスタイリング組成物。
- 前記界面活性剤が、両性界面活性剤,アニオン性界面活性剤,ノニオン性界面活性剤、両性イオン界面活性剤、およびそれらの混合物からなる群から選択される、請求項11に記載のヘアスタイリング組成物。
- 毛髪をスタイリングまたはストレートにする方法であって、
(a)シャンプーにより毛髪を洗浄し、
(b)乾燥または湿った毛髪を得るために、工程(a)の毛髪の水分を除去または低減し、
(c)請求項1〜16のいずれか1項に記載のヘアスタイリング組成物を工程(b)の乾燥または湿った毛髪に適用することによって毛髪をトリートメントし、
(d)約15〜約30分間、トリートメントした毛髪をそのままにし、
(e)工程(d)のトリートメントされた毛髪を機械的にスタイリング、カールまたはストレートにすることによりホットエアで乾燥し、
(f)約375〜450°Fに予熱したフラットアイロンを用いて、工程(e)の毛髪を約4〜8回アイロンし、
(g)工程(f)の毛髪を約15〜約20分間そのままにして、ストレートにされた、またはスタイリングされた毛髪を得る、
方法。 - (i)約40〜約1100KDaの範囲の重量平均分子量を有する、約0.1重量%〜約2重量%の少なくとも1つのカチオン変性ポリガラクトマンナンと、
(ii)約0.1重量%〜約25重量%の少なくとも1つの化粧品成分と、
を含む、ヘアスタイリング組成物。 - 約0.1重量%〜約10重量%の少なくとも1つの第4級アンモニウム化合物をさらに含む、請求項18に記載のヘアスタイリング組成物。
- ポリビニルピロリジン(PVP)の少なくとも1つのコポリマー、ビニルピロリドンのコポリマー、無水マレイン酸およびポリイミドのコポリマーを約0.1重量%〜約10重量%さらに含む、請求項18または19に記載のヘアスタイリング組成物。
- (i)約40〜約1100KDaの範囲の重量平均分子量を有する約0.1重量%〜約2重量%のグアーヒドロキシプロピルトリモニウムクロリドと、
(ii)約0.1重量%〜約25重量%の少なくとも1つの化粧品成分と、
を含む、エアロゾルヘアスタイリングムース組成物。 - 約0.1重量%〜約10重量%のポリクオタニウム−55(PQ−55)またはポリクオタニウム−11(PQ−11)をさらに含む、請求項21に記載のエアロゾルヘアスタイリングムース組成物。
- 約0.1重量%〜約10重量%のポリビニルピロリドン/酢酸ビニルコポリマー、ビニルピロリドン/2−(ジメチルアミノ)エチルメタクリレートコポリマー、メチルビニルエーテル/無水マレイン酸コポリマーのエチルエステル、またはポリイミド−1をさらに含む、請求項21または22に記載のエアロゾルヘアスタイリングムース組成物。
- 前記少なくとも1つの化粧品成分が、防腐剤、α−ヒドロキシカルボン酸、カチオン性界面活性剤、推進剤およびそれらの混合物からなる群から選択される、請求項21〜23のいずれか1項に記載のエアロゾルヘアスタイリングムース組成物。
- 前記防腐剤が、フェノキシエチルアルコール、カプリロイルグリコールまたはそれらの混合物を含む、請求項24に記載のエアロゾルヘアスタイリングムース組成物。
- 前記α−ヒドロキシカルボン酸が、乳酸、クエン酸およびリンゴ酸からなる群から選択される、請求項24に記載のエアロゾルヘアスタイリングムース組成物。
- 前記カチオン性界面活性剤が塩化セトリモニウムである、請求項24に記載のエアロゾルヘアスタイリングムース組成物。
- 前記推進剤が、ジメチルエーテル、イソブタンまたはプロパンを含む、請求項24に記載のエアロゾルヘアスタイリングムース組成物。
- 90%湿度および80°Fで24時間にわたって約80%〜約100%のカール保持性を示す、請求項21〜28のいずれかに記載のエアロゾルヘアスタイリングムース組成物。
- (i)約40〜約1100KDaの範囲の重量平均分子量を有する約0.1重量%〜約2重量%のグアーヒドロキシプロピルトリモニウムクロリドと、
(ii)約0.1重量%〜約25重量%少なくとも1つの化粧品成分と、
を含む、ヘアスタイリングジェル組成物。 - 約0.1重量%〜約10重量%のポリビニルピロリドン/酢酸ビニルコポリマー、ビニルピロリドン/2−(ジメチルアミノ)エチルメタクリレートコポリマー、メチルビニルエーテル/無水マレイン酸コポリマーのエチルエステル、またはポリイミド−1をさらに含む、請求項30に記載のヘアスタイリングジェル組成物。
- 前記少なくとも1つの化粧品成分が、防腐剤、α−ヒドロキシカルボン酸およびそれらの混合物からなる群から選択される、請求項30および31のいずれか1項に記載のヘアスタイリングジェル組成物。
- 前記防腐剤が、フェノキシエチルアルコール、カプリロイルグリコールまたはそれらの混合物を含む、請求項32に記載のヘアスタイリングジェル組成物。
- 前記α−ヒドロキシカルボン酸が、乳酸、クエン酸およびリンゴ酸からなる群から選択される、請求項32に記載のヘアスタイリングジェル組成物。
- 90%湿度および80°Fで24時間にわたって約80%〜約100%のカール保持性を示す、請求項30〜34のいずれかに記載のヘアスタイリングジェル組成物。
- 耐湿性、剛性、保持の持続性、低滑り性、フォーム促進性、およびカール保持性を増強する際に使用するためのヘアスタイリング組成物であって、
(i)約40〜約1100KDaの範囲の重量平均分子量を有する少なくとも1つのカチオン変性ポリガラクトマンナンと、
(i)少なくとも1つの第4級アンモニウム化合物と、
(iii)ビニルピロリドンのコポリマー、ポリビニルピロリドン(PVP)のコポリマー、無水マレイン酸のコポリマー、およびポリイミドのうちの少なくとも1つと、
(iv)少なくとも1つの化粧品成分と、
を含む、ヘアスタイリング組成物。
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