JP2018501210A5 - - Google Patents
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- Publication number
- JP2018501210A5 JP2018501210A5 JP2017527873A JP2017527873A JP2018501210A5 JP 2018501210 A5 JP2018501210 A5 JP 2018501210A5 JP 2017527873 A JP2017527873 A JP 2017527873A JP 2017527873 A JP2017527873 A JP 2017527873A JP 2018501210 A5 JP2018501210 A5 JP 2018501210A5
- Authority
- JP
- Japan
- Prior art keywords
- chlorine
- compound
- group
- thiol
- bromine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 12
- -1 terphenyl lithium compound Chemical class 0.000 claims 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 4
- 229910052801 chlorine Inorganic materials 0.000 claims 4
- 239000000460 chlorine Substances 0.000 claims 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 3
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 3
- 229910052794 bromium Inorganic materials 0.000 claims 3
- 239000007800 oxidant agent Substances 0.000 claims 3
- BMCNAHBDZUYGJG-UHFFFAOYSA-N 4-phenyldibenzothiophene Chemical compound C1=CC=CC=C1C1=CC=CC2=C1SC1=CC=CC=C12 BMCNAHBDZUYGJG-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- NHKJPPKXDNZFBJ-UHFFFAOYSA-N phenyllithium Chemical compound [Li]C1=CC=CC=C1 NHKJPPKXDNZFBJ-UHFFFAOYSA-N 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 229910052717 sulfur Inorganic materials 0.000 claims 2
- 239000011593 sulfur Substances 0.000 claims 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 150000001335 aliphatic alkanes Chemical class 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 125000001033 ether group Chemical group 0.000 claims 1
- 150000002170 ethers Chemical class 0.000 claims 1
- 150000002431 hydrogen Chemical class 0.000 claims 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims 1
- 229910052740 iodine Inorganic materials 0.000 claims 1
- 239000011630 iodine Substances 0.000 claims 1
- 238000005580 one pot reaction Methods 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462091119P | 2014-12-12 | 2014-12-12 | |
| US62/091,119 | 2014-12-12 | ||
| PCT/US2015/063237 WO2016094135A1 (en) | 2014-12-12 | 2015-12-01 | Process for the preparation of 4-phenyldibenzothiophene |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018501210A JP2018501210A (ja) | 2018-01-18 |
| JP2018501210A5 true JP2018501210A5 (https=) | 2018-12-27 |
| JP6793643B2 JP6793643B2 (ja) | 2020-12-02 |
Family
ID=55024252
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017527873A Expired - Fee Related JP6793643B2 (ja) | 2014-12-12 | 2015-12-01 | 4−フェニルジベンゾチオフェンの調製のためのプロセス |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9951037B2 (https=) |
| EP (1) | EP3230271B1 (https=) |
| JP (1) | JP6793643B2 (https=) |
| CN (1) | CN107001314B (https=) |
| CA (1) | CA2967439A1 (https=) |
| TW (1) | TWI691492B (https=) |
| WO (1) | WO2016094135A1 (https=) |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20110129766A (ko) | 2010-05-26 | 2011-12-02 | 덕산하이메탈(주) | 오원자 헤테로고리를 포함하는 화합물 및 이를 이용한 유기전기소자, 그 단말 |
| KR101887003B1 (ko) * | 2011-07-21 | 2018-08-13 | 롬엔드하스전자재료코리아유한회사 | 신규한 유기 발광 화합물 및 이를 채용하고 있는 유기 전계 발광 소자 |
| KR102026824B1 (ko) | 2012-06-27 | 2019-10-01 | 삼성디스플레이 주식회사 | 신규한 축합환 화합물 및 이를 포함하는 유기 발광 소자 |
| KR102154705B1 (ko) * | 2013-04-25 | 2020-09-11 | 삼성디스플레이 주식회사 | 헤테로고리 화합물 및 이를 포함한 유기 발광 소자 |
-
2015
- 2015-11-23 TW TW104138677A patent/TWI691492B/zh not_active IP Right Cessation
- 2015-12-01 WO PCT/US2015/063237 patent/WO2016094135A1/en not_active Ceased
- 2015-12-01 CA CA2967439A patent/CA2967439A1/en not_active Abandoned
- 2015-12-01 EP EP15816597.7A patent/EP3230271B1/en not_active Not-in-force
- 2015-12-01 JP JP2017527873A patent/JP6793643B2/ja not_active Expired - Fee Related
- 2015-12-01 CN CN201580067301.9A patent/CN107001314B/zh not_active Expired - Fee Related
- 2015-12-01 US US15/525,492 patent/US9951037B2/en active Active
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