JP2018199872A - Method for producing laminated pulp mold and apparatus for producing the same - Google Patents

Method for producing laminated pulp mold and apparatus for producing the same Download PDF

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JP2018199872A
JP2018199872A JP2017104087A JP2017104087A JP2018199872A JP 2018199872 A JP2018199872 A JP 2018199872A JP 2017104087 A JP2017104087 A JP 2017104087A JP 2017104087 A JP2017104087 A JP 2017104087A JP 2018199872 A JP2018199872 A JP 2018199872A
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mold
paper
pulp
pulp mold
layer
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正雄 栗原
Masao Kurihara
正雄 栗原
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KURIHARA SHIZAI KK
Nippon Paper Industries Co Ltd
Jujo Paper Co Ltd
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KURIHARA SHIZAI KK
Nippon Paper Industries Co Ltd
Jujo Paper Co Ltd
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Priority to JP2017104087A priority Critical patent/JP2018199872A/en
Priority to PCT/JP2018/018674 priority patent/WO2018216544A1/en
Priority to TW107116666A priority patent/TW201900983A/en
Publication of JP2018199872A publication Critical patent/JP2018199872A/en
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    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/16—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only modified by a particular after-treatment
    • D21H11/18—Highly hydrated, swollen or fibrillatable fibres
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21J—FIBREBOARD; MANUFACTURE OF ARTICLES FROM CELLULOSIC FIBROUS SUSPENSIONS OR FROM PAPIER-MACHE
    • D21J5/00—Manufacture of hollow articles by transferring sheets, produced from fibres suspensions or papier-mâché by suction on wire-net moulds, to couch-moulds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
    • B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
    • B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
    • C08B15/08—Fractionation of cellulose, e.g. separation of cellulose crystallites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B16/00—Regeneration of cellulose

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Paper (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

To provide a method and an apparatus for producing a laminated pulp mold in which the produced pulp mold has large mechanical strength and can be easily released from the mold.SOLUTION: A method for producing a laminated pulp mold of this invention comprises: forming a first pulp mold layer by a pulp molding method in a waste paper-regenerated pulp slurry containing 0-5 mass% cellulose nanofibers; then dehydrating a pulp mold intermediate; subsequently forming a second pulp mold layer on the surface of the first pulp mold layer by the pulp molding method in a cellulose nanofiber slurry containing 1-30 mass% waste paper-regenerated pulp slurry; and finally dewatering and drying the formed layers to obtain the laminated pulp mold.SELECTED DRAWING: Figure 1

Description

本発明は、パルプモールドの製造方法および製造装置に関し、更に詳細には、積層パルプモールドの製造方法および装置に関する。   The present invention relates to a method and apparatus for manufacturing a pulp mold, and more particularly to a method and apparatus for manufacturing a laminated pulp mold.

例えば特開２０１２−２１４９４３号公報に開示されているように、セルロースナノファイバを含有した紙や抄紙方法が盛んに研究されている。また、セルロースナノファイバを含有した樹脂材料を用いた航空機部材、自動車部材等の研究も進められている。   For example, as disclosed in JP2012-214943A, paper and papermaking methods containing cellulose nanofibers are actively studied. In addition, research on aircraft members, automobile members, and the like using resin materials containing cellulose nanofibers is also underway.

本件特許出願人は、先の特許出願（特願２０１６−１９０５６８）で、所定量のセルロースナノファイバを含有し、強度が向上したパルプモールドを提供することを目的とした下記のパルプモールドを提案した。
先の特許出願で提案したパルプモールドは、固形分として０．０１質量％以上のセルロースナノファイバと、固形分としての残部が主として古紙再生パルプとからなるパルプモールドである。 The present applicant of the present patent has proposed the following pulp mold in order to provide a pulp mold containing a predetermined amount of cellulose nanofiber and having improved strength in a previous patent application (Japanese Patent Application No. 2014-190568). .
The pulp mold proposed in the previous patent application is a pulp mold composed of cellulose nanofibers with a solid content of 0.01% by mass or more and the remainder as the solid content mainly made of recycled paper.

前記のパルプモールドは、セルロースナノファイバの含有量が多いほど強度が増して行くが、セルロースナノファイバの含有量が固形分で３０質量％を越えると、成形物が金型から離型し難くなり、無理をして離型すると、亀裂が入ってしまう等の問題が生じていた。   The pulp mold increases in strength as the content of cellulose nanofibers increases. However, if the content of cellulose nanofibers exceeds 30% by mass, the molded product is difficult to release from the mold. When it was forced to release, there were problems such as cracks.

特開２０１２−２１４９４３号公報JP 2012-214943 A

そこで、本発明は、出来上がったパルプモールドの強度が大きく、しかも離型しやすい積層パルプモールドの製造方法および製造装置を提供することを目的とする。   Then, an object of this invention is to provide the manufacturing method and manufacturing apparatus of a laminated pulp mold with which the strength of the completed pulp mold is large and it is easy to release.

前記目的は、下記（１）〜（４）の構成の本発明の積層パルプモールドの製造方法および製造装置により達成できる。
（１）
セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリー中でパルプモールド法によりパルプモールド第１層を形成し、次いでパルプモールド中間体を脱水し、続けて、古紙再生パルプを１〜３０質量％含有するセルロースナノファイバスラリー中で、パルプモールド法により、前記パルプモールド第１層の表面にパルプモールド第２層を形成し、最後に脱水、乾燥を行って積層パルプモールドを製造する積層パルプモールドの製造方法。
（２）
第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた前記（１）の積層パルプモールドの製造方法。
（３）
表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第１抄型と、この第１抄型を支持し、該抄型の内部を吸引するための第１モールダーと、セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリーを収容した第１容器と、前記第１抄型とこれを支持した第１モールダーを、前記古紙再生パルプスラリーの表面の上方の不作用位置と、前記古紙再生パルプスラリー内に浸漬した作用位置との間で昇降させる第１昇降手段とを備え、前記第１抄型の網体上にパルプモールド第１層を抄造する第１抄造ステージ、
表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第２抄型と、この第２抄型を支持し、該抄型の内部を吸引するための第２モールダーと、セルロースナノファイバを１〜３０質量％含有するセルロースナノファイバスラリーを収容した第２容器と、前記第２抄型とこれを支持した第２モールダーを、前記セルロースナノファイバスラリーの表面の上方の不作用位置と、前記セルロースナノファイバスラリー内に浸漬した作用位置との間で昇降させる第２昇降手段とを備え、前記パルプモールド第１層の表面にパルプモールド第２層を抄造する第２抄造ステージ、
乾燥手段、
前記第１、第２抄型上のパルプモールド中間体を吸引することによって、離型させる上型、
この上型を昇降させるだめの第２昇降手段、および
前記上型を第１抄造構造体、第２抄造構造体、乾燥手段の順に移送手段
を備えていることを特徴とするパルプモールド製造装置。
（４）
第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた前記（３）の積層パルプモールド製造装置。 The said objective can be achieved by the manufacturing method and manufacturing apparatus of the laminated pulp mold of this invention of the structure of following (1)-(4).
(1)
A pulp mold first layer is formed by a pulp mold method in a recycled paper slurry containing 0 to 5% by mass of cellulose nanofibers, and then a pulp mold intermediate is dehydrated, followed by 1 to 30 mass of recycled paper pulp. In a cellulose nanofiber slurry containing 1% by weight, a pulp mold method is used to form a pulp mold second layer on the surface of the pulp mold first layer, and finally dehydrated and dried to produce a laminated pulp mold. Manufacturing method.
(2)
The method for producing a laminated pulp mold according to (1), wherein a part of the first recycled paper and / or the second recycled paper is replaced with a waste fiber such as resin, rubber, or coffee candy or tea husk.
(3)
A first paper mold having a net provided on the front surface and having a number of suction ports penetrating from the front surface to the back surface, and a first paper for supporting the first paper mold and sucking the inside of the paper mold A molder, a first container containing used paper recycled pulp slurry containing 0 to 5% by mass of cellulose nanofibers, the first papermaking mold and a first molder supporting the first paper mold, above the surface of the used paper recycled pulp slurry. A first lifting means for moving up and down between the inactive position and the operating position immersed in the recycled paper slurry of the waste paper, and the first layer of the pulp mold is made on the first paper making type net. 1 paper making stage,
A second paper mold having a net provided on the front surface and having a plurality of suction ports penetrating from the front surface to the back surface, and a second paper for supporting the second paper mold and sucking the inside of the paper mold A molder, a second container containing a cellulose nanofiber slurry containing 1 to 30% by mass of cellulose nanofibers, a second paper mold and a second molder supporting the second paper mold, above the surface of the cellulose nanofiber slurry. A second raising / lowering means for raising and lowering between the non-acting position and the acting position immersed in the cellulose nanofiber slurry, and forming a pulp mold second layer on the surface of the pulp mold first layer. Paper making stage,
Drying means,
An upper mold to be released by sucking the pulp mold intermediate on the first and second papermaking molds;
A pulp mold manufacturing apparatus comprising: a second lifting and lowering means for raising and lowering the upper mold; and a transfer means for the upper mold in the order of the first papermaking structure, the second papermaking structure, and the drying means.
(4)
The laminated pulp mold manufacturing apparatus according to the above (3), wherein a part of the first recycled paper and / or the second recycled paper recycled pulp is replaced with waste fibers such as resin, rubber or the like, coffee cake, and tea shells.

本発明の積層パルプモールドの製造方法においては、上記したように、セルロースナノファイバの含有量が比較的少ない原料スラリーを用いて初層を抄造し、次いでこの初層上に、セルロースナノファイバの含有量が比較的多い原料スラリーを用いて第２層を形成してパルプモールドを抄造するようにしたので、パルプモールド中間体の離型が容易で有り、しかも出来上がったパルプモールドの強度が高い。
また、本発明のパルプモールドのパルプには、古紙再生パルプを用いているので、自然環境や地球資源の保全・保護も行えるという利点もある。 In the method for producing a laminated pulp mold of the present invention, as described above, an initial layer is made using a raw slurry having a relatively small content of cellulose nanofibers, and then the cellulose nanofibers are contained on the initial layer. Since the pulp layer is made by forming the second layer using a relatively large amount of raw material slurry, the release of the pulp mold intermediate is easy and the strength of the finished pulp mold is high.
Moreover, since the recycled paper pulp is used for the pulp of the pulp mold of the present invention, there is an advantage that the natural environment and earth resources can be preserved and protected.

本発明の実施形態による積層パルプモールド製造装置の概略図である。It is the schematic of the laminated pulp mold manufacturing apparatus by embodiment of this invention. 本発明の実施形態による、図１に示した積層パルプモールド製造装置を用いた積層パルプモールドの製造方法の工程を示す説明図である。It is explanatory drawing which shows the process of the manufacturing method of a laminated pulp mold using the laminated pulp mold manufacturing apparatus shown in FIG. 1 by embodiment of this invention. 本発明の実施形態による積層パルプモールド製造装置で用いる抄型の断面図である。It is sectional drawing of the papermaking type | mold used with the laminated pulp mold manufacturing apparatus by embodiment of this invention.

以下、本発明の実施形態による積層パルプモールド製造装置について説明する。
積層パルプモールド製造装置１０は、第１抄造ステージ１２およびこの第１抄造ステージ１２の下流側に配置された第２抄造ステージ５０を備えている。
前記第１抄造ステージ１２は、所定の外部形状（抄造面）を有する第１抄型１４（図１５参照）を備えており、この第１抄型１４の抄型本体１６には、該本体全体に等間隔で設けられ、その表面（内面）から裏面（外面）に貫通する多数の吸引口１８が形成されている。また、前記抄型本体１６上には、網体２０が配置されている。 Hereinafter, the laminated pulp mold manufacturing apparatus by embodiment of this invention is demonstrated.
The laminated pulp mold manufacturing apparatus 10 includes a first papermaking stage 12 and a second papermaking stage 50 disposed on the downstream side of the first papermaking stage 12.
The first papermaking stage 12 includes a first papermaking mold 14 (see FIG. 15) having a predetermined external shape (papermaking surface). The papermaking body 16 of the first papermaking mold 14 includes the entire body. Are formed at equal intervals, and a plurality of suction ports 18 penetrating from the front surface (inner surface) to the rear surface (outer surface) are formed. A net 20 is disposed on the papermaking main body 16.

前記第１抄型１４は、第１モールダー２２上に固定支持されている。以下、第１抄型とモールダーとの組み合わせを第１抄型構造体２４と称する。前記第１モールダー２２は、図示していない吸引ポンプにより内部が吸引されるようになっている。第１抄造ステージ１２の下部には、セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリーを収容した第１容器２６が配置されている。前記古紙再生パルプスラリー中の古紙再生パルプの一部は、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えることができる。   The first paper mold 14 is fixedly supported on the first molder 22. Hereinafter, the combination of the first papermaking mold and the molder is referred to as a first papermaking structure 24. The inside of the first molder 22 is sucked by a suction pump (not shown). A first container 26 containing used paper recycled pulp slurry containing 0 to 5% by mass of cellulose nanofibers is disposed below the first papermaking stage 12. A part of the recycled paper pulp in the recycled paper pulp slurry can be replaced with resin, rubber or the like, or waste fiber such as coffee cake or tea husk.

前記第１抄型構造体２４は、例えば油圧シリンダーにより構成される第１昇降手段２８により、前記第１抄型１４が、第１容器２６内に収容された古紙再生パルプスラリーの表面の上方に位置する不作用位置（図１等参照）と、前記古紙再生パルプスラリー内に浸漬した作用位置（例えば、図２参照）との間で昇降される。以上の構造の第１抄造ステージ１２により、前記第１抄型１４の網体２０上にパルプモールド第１層を抄造する。   The first papermaking structure 24 is formed above the surface of the used paper recycled pulp slurry accommodated in the first container 26 by the first elevating means 28 composed of, for example, a hydraulic cylinder. It is moved up and down between the inactive position (see FIG. 1 and the like) and the active position (see, for example, FIG. 2) immersed in the used paper recycled pulp slurry. A pulp mold first layer is made on the mesh body 20 of the first paper making mold 14 by the first paper making stage 12 having the above structure.

前記第２抄造ステージ５０は、前記第１抄型１４と同一の構造で有り、所定の外部形状（抄造面）を有する第２抄型５２（図１５参照）を備えており、この第４抄型５２の抄型本体５４には、該本体全体に等間隔で設けられ、その表面（内面）から裏面（外面）に貫通する多数の吸引口５６が形成されている。また、前記抄型本体１６上には、網体５８が配置されている。   The second papermaking stage 50 has the same structure as that of the first papermaking mold 14, and includes a second papermaking mold 52 (see FIG. 15) having a predetermined external shape (papermaking surface). The papermaking main body 54 of the mold 52 is provided with a plurality of suction ports 56 that are provided at equal intervals throughout the main body and penetrate from the front surface (inner surface) to the rear surface (outer surface). A net 58 is disposed on the paper making body 16.

前記第２抄型５２は、第１モールダー６０上に固定支持されている。以下、第抄型とモールダーとの組み合わせを第２抄型構造体６２と称する。前記第２モールダー６０は、図示していない吸引ポンプにより内部が吸引されるようになっている。第２抄造ステージ５０の下部には、セルロースナノファイバを１〜３０質量％含有するセルロースナノファイバスラリーを収容した第２容器６４が配置されている。前記古紙再生パルプスラリー中の古紙再生パルプの一部は、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えることができる。   The second papermaking mold 52 is fixedly supported on the first molder 60. Hereinafter, the combination of the first papermaking mold and the molder is referred to as a second papermaking structure 62. The inside of the second molder 60 is sucked by a suction pump (not shown). A second container 64 containing a cellulose nanofiber slurry containing 1 to 30% by mass of cellulose nanofibers is disposed below the second papermaking stage 50. A part of the recycled paper pulp in the recycled paper pulp slurry can be replaced with resin, rubber or the like, or waste fiber such as coffee cake or tea husk.

前記第２抄型構造体６２は、例えば油圧シリンダーにより構成される第２昇降手段６６により、前記第２抄型５２が、第２容器６４内に収容された古紙再生パルプスラリーの表面の上方に位置する不作用位置（図１等参照）と、前記古紙再生パルプスラリー内に浸漬した作用位置（例えば、図９参照）との間で昇降される。以上の構造の第２抄造ステージ５０により、第２抄型５２の網体５８上の前記パルプモールド第１層上にパルプモールド第２層を抄造して、製品の構造をしたパルプモールドを完成する。   The second papermaking structure 62 is formed by, for example, a second lifting / lowering means 66 constituted by a hydraulic cylinder so that the second papermaking paper 52 is placed above the surface of the used paper recycled pulp slurry stored in the second container 64. It is moved up and down between the inactive position (see FIG. 1 and the like) and the active position (see, for example, FIG. 9) immersed in the recycled paper slurry. By the second papermaking stage 50 having the above structure, the pulp mold second layer is made on the pulp mold first layer on the net body 58 of the second papermaking mold 52 to complete a pulp mold having a product structure. .

前記第２抄造ステージ５０の下流側には、乾燥設備７０が設けられている。この乾燥設備７０は、何らかの構造のヒーター（図示せず）を備えた乾燥設備本体７２，及びこの乾燥設備本体７２に前記第２抄造ステージ５０からのパルプモールドを移送する移送手段（コンベア）７４を備えている。   A drying facility 70 is provided on the downstream side of the second papermaking stage 50. The drying equipment 70 includes a drying equipment main body 72 having a heater (not shown) of some structure, and a transfer means (conveyor) 74 for transferring the pulp mold from the second papermaking stage 50 to the drying equipment main body 72. I have.

前記第１抄造ステージ１２の上部には、前記第１抄型１４上のパルプモールド中間体（パルプモールド第１層）を吸引することによって、離型させる上型８０が設けられている。このため、上型８０は、図示しない吸引ポンプを備えている。この上型８０は、例えば油圧シリンダーである第２昇降手段８２により昇降させられる。   Above the first papermaking stage 12, there is provided an upper die 80 for releasing the pulp mold intermediate (pulp mold first layer) on the first papermaking die 14 by suction. For this reason, the upper mold 80 includes a suction pump (not shown). The upper mold 80 is raised and lowered by the second raising / lowering means 82 that is, for example, a hydraulic cylinder.

前記上型８０にはまた、移送モータ８４を備えた移送手段８６が設けられており、この移送手段８６により、レール８８に沿って、第１抄造ステージ１２、第２抄造ステージ５０、乾燥設備手段７２の順に移送されるようになっている。   The upper mold 80 is also provided with a transfer means 86 having a transfer motor 84, by which the first paper making stage 12, the second paper making stage 50, and the drying equipment means along the rail 88. 72 is transferred in this order.

次に、以上の構造の積層パルプモールド製造装置１０を用いての積層パルプモールドの製造方法について説明する。
先ず、前記第１抄造ステージ１２において、第１抄型構造体２４を図１の状態から図２の作用位置に下降させて、第１抄型１４を第１容器２６内の古紙再生パルプスラリー内に浸漬させ、第１モールダー２２を介して吸引し、第１抄型の網体２０（図１５参照）上に、古紙再生パルプスラリー中の固形分を堆積させ、パルプモールド第１層を形成する。吸引は、１〜３０秒程度行い、厚さ１〜５ｍｍ程度の未脱水状態のパルプモールド第１層を形成する。 Next, the manufacturing method of the laminated pulp mold using the laminated pulp mold manufacturing apparatus 10 of the above structure is demonstrated.
First, in the first papermaking stage 12, the first papermaking structure 24 is lowered from the state shown in FIG. 1 to the operation position shown in FIG. 2, and the first papermaking 14 is placed in the recycled paper recycled pulp slurry in the first container 26. And is sucked through the first molder 22 to deposit the solid content in the recycled paper slurry of the used paper on the first papermaking type mesh body 20 (see FIG. 15) to form a pulp mold first layer. . Suction is performed for about 1 to 30 seconds to form a non-dehydrated pulp mold first layer having a thickness of about 1 to 5 mm.

未脱水状態のパルプモールド第１層が形成された後、第１抄型構造体２４を図３の不作用位置に上昇させ、この状態で第１モールダー２４を介してパルプモールド第１層を吸引して、脱水を行う。この脱水は、５〜６０秒程度行い、パルプモールド第１層の含水量を５〜８０％程度とする。この脱水後のパルプモールド第１層の厚さは、１〜５ｍｍ程度となる。 After the undehydrated pulp mold first layer is formed, the first papermaking structure 24 is raised to the inactive position of FIG. 3, and the pulp mold first layer is sucked through the first molder 24 in this state. Then, dehydration is performed. This dehydration is performed for about 5 to 60 seconds, and the water content of the pulp mold first layer is about 5 to 80%. The thickness of the pulp mold first layer after dehydration is about 1 to 5 mm.

この脱水後、図４に示すように上型８０を下降し、第１抄型１４上のパルプモールド第１層上に被せ、この上型８０を吸引することにより、パルプモールド第１層を第１抄型１４から離型させ、該上型８０内に吸引保持させる。   After the dehydration, the upper mold 80 is lowered as shown in FIG. 4 and placed on the pulp mold first layer on the first papermaking mold 14, and the upper mold 80 is sucked to remove the pulp mold first layer. 1 The mold is released from the papermaking mold 14 and sucked and held in the upper mold 80.

この後、図５に示すように、上型８０を上昇させ、次いで図６に示すように、上型８０を第２抄造ステージ５０に移送する。この後、上型８０を図６の位置から図７の位置に下降させ、第２抄型５２上に被せ、この状態で第２モールダー６０を介して、上型８０に保持されているパルプモールド第１層を第２抄型５２上に吸引させる。   Thereafter, the upper die 80 is raised as shown in FIG. 5, and then the upper die 80 is transferred to the second papermaking stage 50 as shown in FIG. 6. Thereafter, the upper mold 80 is lowered from the position of FIG. 6 to the position of FIG. 7 and is put on the second papermaking mold 52. In this state, the pulp mold held by the upper mold 80 via the second molder 60. The first layer is sucked onto the second papermaking mold 52.

次いで、上型８０を図８に示すように上昇させ、この後、第２抄型構造体６２を図９に示すように下降させて、第２抄型５２を第２容器６４内のセルロースナノファイバスラリー内に浸漬させ、第２モールダー６０を介して吸引し、第２抄型の網体５８（図１５参照）上のパルプモールド第１層上に、セルロースナノファイバスラリー中の固形分を堆積させ、パルプモールド第２層を形成する。吸引は、５〜６０秒程度行い、厚さ１〜５ｍｍ程度の未脱水状態のパルプモールド第２層を形成する。   Next, the upper mold 80 is raised as shown in FIG. 8, and then the second papermaking structure 62 is lowered as shown in FIG. 9 to bring the second papermaking mold 52 into the cellulose nano-particles in the second container 64. It is immersed in the fiber slurry, sucked through the second molder 60, and the solid content in the cellulose nanofiber slurry is deposited on the pulp mold first layer on the second papermaking type net 58 (see FIG. 15). To form a pulp mold second layer. Suction is performed for about 5 to 60 seconds to form a non-dehydrated pulp mold second layer having a thickness of about 1 to 5 mm.

未脱水状態のパルプモールド第２層が形成された後、第２抄型構造体６２を図１０の不作用位置に上昇させ、この状態で第２モールダー６２を介してパルプモールド第１、第２層を吸引して、脱水を行う。この脱水は、５〜６０秒程度行い、パルプモールド第１、第２層の含水量を１０〜８０％程度とする。この脱水後のパルプモールド第１、第２層のトータル厚さは、１〜５ｍｍ程度となる。 After the non-dehydrated pulp mold second layer is formed, the second papermaking structure 62 is raised to the inoperative position of FIG. 10, and in this state, the pulp mold first and second are passed through the second molder 62. The layer is aspirated and dehydrated. This dehydration is performed for about 5 to 60 seconds, and the water content of the pulp mold first and second layers is about 10 to 80%. The total thickness of the pulp mold first and second layers after dehydration is about 1 to 5 mm.

この脱水後、図１１に示すように上型８０を下降し、第２抄型５２上のパルプモールド第１、第２層上に被せ、この上型８０を吸引することにより、パルプモールド第１、第２層を第２抄型５２から離型させ、該上型８０内に吸引保持させる。   After this dehydration, the upper mold 80 is lowered as shown in FIG. 11 and placed on the pulp mold first and second layers on the second papermaking mold 52, and the upper mold 80 is sucked to obtain the pulp mold first. Then, the second layer is released from the second papermaking mold 52 and is sucked and held in the upper mold 80.

この後、図１２に示すように、上型８０を上昇させ、次いで図１３に示すように、乾燥設備７０移送手段（コンベア）７４上に移送し、次いで、ブローにより、図１４に示したように、乾燥前パルプモールドＰを移送手段（コンベア）７４上に下ろし、乾燥設備本体７２に移送して乾燥し、パルプモールドを完成させる。   Thereafter, as shown in FIG. 12, the upper die 80 is raised, and then, as shown in FIG. 13, it is transferred onto the drying equipment 70 transfer means (conveyor) 74, and then blown as shown in FIG. Then, the pulp mold P before drying is lowered onto a transfer means (conveyor) 74, transferred to the drying equipment main body 72, and dried to complete the pulp mold.

パルプモールド第１層用として、セルロースナノファイバを含まない古紙再生パルプスラリーを用い、第２層用として固形分としてセルロースナノファイバを１質量％含んだ古紙再生パルプスラリーを用い、前記の製造方法で。実施例のパルプモールドＰ−１を製造した。一方、第１層は実施例のものと同じで、また、前記第２層用の固形分としてセルロースナノファイバを１質量％含んだ古紙再生パルプスラリーを、今度は、第１層上に刷毛塗りして、乾燥させたものを比較例のパルプモールドＰ−２を製造した。
なお、古紙再生パルプスラリーは、先ず、古紙（機密文書や新聞紙、段ボール等）をパルパーにより溶解し、その後、異物除去装置により、原料から製品に適さないゴミ等の異物を除き、次いで、出来上がったパルプモールドにおいて、セルロースナノファイバの含有量が１質量％となるようにセルロースナノファイバを添加するとともに、スラリーの濃度調節を行い、セルロースナノファイバ添加古紙再生パルプスラリーを得た。 For the pulp mold first layer, used paper recycled pulp slurry that does not contain cellulose nanofibers, and for the second layer, used paper recycled pulp slurry containing 1% by mass of cellulose nanofibers as the solid content, . The pulp mold P-1 of the example was manufactured. On the other hand, the first layer is the same as that of the example, and the recycled pulp slurry of used paper containing 1% by mass of cellulose nanofibers as the solid content for the second layer is brushed on the first layer. Then, a dried pulp mold P-2 of a comparative example was manufactured.
Waste paper recycled pulp slurry was first made by dissolving waste paper (confidential documents, newspapers, cardboard, etc.) with a pulper, and then removing foreign substances such as unsuitable dust from the raw material with a foreign matter removing device. In the pulp mold, the cellulose nanofiber was added so that the content of the cellulose nanofiber was 1% by mass, and the concentration of the slurry was adjusted to obtain a cellulose nanofiber-added waste paper recycled pulp slurry.

以上の実施例および比較例からのサンプルを切り出し、それを用いて、サンプルの引張強さおよび破裂強さを測定した。
その結果は、実施例のものでは、引張強さ：２７６Ｎおよび破裂強さ：４５６ｋＰａであり、比較例では、引張強さ：２５４Ｎおよび破裂強さ：３８６ｋＰａであった。 Samples from the above examples and comparative examples were cut out and used to measure the tensile strength and burst strength of the samples.
The results were tensile strength: 276 N and burst strength: 456 kPa in the examples, and tensile strength: 254 N and burst strength: 386 kPa in the comparative example.

試験方法
両試験は、20℃、65%RHに設定された恒温恒湿室内にて実施した。

引張強さ試験
定速伸長形引張試験機（(株)エイ・アンド・デイ製 RTF-1250）を使用
試験片の幅：50mm
つかみ間隔：200mm
引張速度：200mm/min
試験回数：3回

破裂強さ試験
ミューレン破裂試験機（高圧型）（(株)東洋精機製作所製 M2-HD）を使用
測定面：ゴム隔膜に接触している面
（網目面から凹凸面へ破裂させた。）
試験回数：10回

以上の試験から、本発明の効果が明瞭である。 Test Method Both tests were conducted in a constant temperature and humidity room set at 20 ° C. and 65% RH.

Tensile strength test Using a constant speed extension type tensile tester (RTF-1250 manufactured by A & D Co., Ltd.) Specimen width: 50 mm
Grasp interval: 200mm
Tensile speed: 200mm / min
Number of tests: 3

Burst strength test Uses a Müren burst tester (high pressure type) (M2-HD manufactured by Toyo Seiki Seisakusho Co., Ltd.)
Measurement surface: Surface in contact with rubber diaphragm
(Ruptured from a mesh surface to an uneven surface.)
Number of tests: 10

From the above test, the effect of the present invention is clear.

また、各サンプルの離型の容易さを観察したところ、実施例および比較例ともに良好であった。
すなわち、本発明によれば、離型の容易さを確保しつつ、強度の大きな積層パルプモールドを製造することができる。 Moreover, when the ease of mold release of each sample was observed, both the examples and comparative examples were good.
That is, according to the present invention, it is possible to produce a laminated pulp mold having a high strength while ensuring ease of release.

１０ 積層パルプモールド製造装置
１２ 第１抄造ステージ
１４ 第１抄型
１６ 抄型本体
１８ 吸引口
２０ 網体
２２ 第１モールダー
２４ 第１抄型構造体
２６ 容器 DESCRIPTION OF SYMBOLS 10 Laminated pulp mold manufacturing apparatus 12 1st papermaking stage 14 1st papermaking 16 Papermaking main body 18 Suction port 20 Net body 22 1st molder 24 1st papermaking structure 26 Container

前記目的は、下記（１）〜（４）の構成の本発明の積層パルプモールドの製造方法および製造装置により達成できる。
（１）
セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリー中でパルプモールド法によりパルプモールド第１層を形成し、次いでパルプモールド中間体を脱水し、続けて、セルロースナノファイバを１〜３０質量％含有する古紙再生パルプスラリー中で、パルプモールド法により、前記パルプモールド第１層の表面にパルプモールド第２層を形成し、最後に脱水、乾燥を行って積層パルプモールドを製造する積層パルプモールドの製造方法。
（２）
第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた前記（１）の積層パルプモールドの製造方法。
（３）
表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第１抄型と、この第１抄型を支持し、該抄型の内部を吸引するための第１モールダーと、セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリーを収容した第１容器と、前記第１抄型とこれを支持した第１モールダーを、前記古紙再生パルプスラリーの表面の上方の不作用位置と、前記古紙再生パルプスラリー内に浸漬した作用位置との間で昇降させる第１昇降手段とを備え、前記第１抄型の網体上にパルプモールド第１層を抄造する第１抄造ステージ、
表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第２抄型と、この第２抄型を支持し、該抄型の内部を吸引するための第２モールダーと、セルロースナノファイバを１〜３０質量％含有するセルロースナノファイバスラリーを収容した第２容器と、前記第２抄型とこれを支持した第２モールダーを、前記セルロースナノファイバスラリーの表面の上方の不作用位置と、前記セルロースナノファイバスラリー内に浸漬した作用位置との間で昇降させる第２昇降手段とを備え、前記パルプモールド第１層の表面にパルプモールド第２層を抄造する第２抄造ステージ、
乾燥手段、
前記第１、第２抄型上のパルプモールド中間体を吸引することによって、離型させる上型、
この上型を昇降させるだめの第２昇降手段、および
前記上型を第１抄造構造体、第２抄造構造体、乾燥手段の順に移送手段
を備えていることを特徴とするパルプモールド製造装置。
（４）
第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた前記（３）の積層パルプモールド製造装置。
The said objective can be achieved by the manufacturing method and manufacturing apparatus of the laminated pulp mold of this invention of the structure of following (1)-(4).
(1)
A pulp mold first layer is formed by a pulp molding method in a recycled paper slurry containing 0 to 5% by mass of cellulose nanofibers, and then the pulp mold intermediate is dehydrated, followed by 1 to 30 masses of cellulose nanofibers. % waste paper regenerated pulp slurry containing, by pulp molding method, the the surface of the pulp mold the first layer to form a pulp mold second layer, and finally dried, laminated pulp mold for manufacturing a laminated pulp mold and dried Manufacturing method.
(2)
The method for producing a laminated pulp mold according to (1), wherein a part of the first recycled paper and / or the second recycled paper is replaced with a waste fiber such as resin, rubber, or coffee candy or tea husk.
(3)
A first paper mold having a net provided on the front surface and having a number of suction ports penetrating from the front surface to the back surface, and a first paper for supporting the first paper mold and sucking the inside of the paper mold A molder, a first container containing used paper recycled pulp slurry containing 0 to 5% by mass of cellulose nanofibers, the first papermaking mold and a first molder supporting the first paper mold, above the surface of the used paper recycled pulp slurry. A first lifting means for moving up and down between the inactive position and the operating position immersed in the recycled paper slurry of the waste paper, and the first layer of the pulp mold is made on the first paper making type net. 1 paper making stage,
A second paper mold having a net provided on the front surface and having a plurality of suction ports penetrating from the front surface to the back surface, and a second paper for supporting the second paper mold and sucking the inside of the paper mold A molder, a second container containing a cellulose nanofiber slurry containing 1 to 30% by mass of cellulose nanofibers, a second paper mold and a second molder supporting the second paper mold, above the surface of the cellulose nanofiber slurry. A second raising / lowering means for raising and lowering between the non-acting position and the acting position immersed in the cellulose nanofiber slurry, and forming a pulp mold second layer on the surface of the pulp mold first layer. Paper making stage,
Drying means,
An upper mold to be released by sucking the pulp mold intermediate on the first and second papermaking molds;
A pulp mold manufacturing apparatus comprising: a second lifting and lowering means for raising and lowering the upper mold; and a transfer means for the upper mold in the order of the first papermaking structure, the second papermaking structure, and the drying means.
(4)
The laminated pulp mold manufacturing apparatus according to the above (3), wherein a part of the first recycled paper and / or the second recycled paper recycled pulp is replaced with waste fibers such as resin, rubber or the like, coffee cake, and tea shells.

Claims (4)

セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリー中でパルプモールド法によりパルプモールド第１層を形成し、次いでパルプモールド中間体を脱水し、続けて、古紙再生パルプを１〜３０質量％含有するセルロースナノファイバスラリー中で、パルプモールド法により、前記パルプモールド第１層の表面にパルプモールド第２層を形成し、最後に脱水、乾燥を行って積層パルプモールドを製造する積層パルプモールドの製造方法。   A pulp mold first layer is formed by a pulp mold method in a recycled paper slurry containing 0 to 5% by mass of cellulose nanofibers, and then a pulp mold intermediate is dehydrated, followed by 1 to 30 mass of recycled paper pulp. In a cellulose nanofiber slurry containing 1% by weight, a pulp mold method is used to form a pulp mold second layer on the surface of the pulp mold first layer, and finally dehydrated and dried to produce a laminated pulp mold. Manufacturing method. 第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた請求項１の積層パルプモールドの製造方法。   The method for producing a laminated pulp mold according to claim 1, wherein a part of the first recycled paper and / or the second recycled paper is replaced with a waste fiber such as resin, rubber or the like, coffee cake, tea husk or the like. 表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第１抄型と、この第１抄型を支持し、該抄型の内部を吸引するための第１モールダーと、セルロースナノファイバを０〜５質量％含有する古紙再生パルプスラリーを収容した第１容器と、前記第１抄型とこれを支持した第１モールダーを、前記古紙再生パルプスラリーの表面の上方の不作用位置と、前記古紙再生パルプスラリー内に浸漬した作用位置との間で昇降させる第１昇降手段とを備え、前記第１抄型の網体上にパルプモールド第１層を抄造する第１抄造ステージ、
表面に設けられた網体を有し、表面から裏面に貫通する多数の吸引口を有する第２抄型と、この第２抄型を支持し、該抄型の内部を吸引するための第２モールダーと、セルロースナノファイバを１〜３０質量％含有するセルロースナノファイバスラリーを収容した第２容器と、前記第２抄型とこれを支持した第２モールダーを、前記セルロースナノファイバスラリーの表面の上方の不作用位置と、前記セルロースナノファイバスラリー内に浸漬した作用位置との間で昇降させる第２昇降手段とを備え、前記パルプモールド第１層の表面にパルプモールド第２層を抄造する第２抄造ステージ、
乾燥手段、
前記第１、第２抄型上のパルプモールド中間体を吸引することによって、離型させる上型、
この上型を昇降させるだめの第２昇降手段、および
前記上型を第１抄造構造体、第２抄造構造体、乾燥手段の順に移送手段
を備えていることを特徴とするパルプモールド製造装置。 A first paper mold having a net provided on the front surface and having a number of suction ports penetrating from the front surface to the back surface, and a first paper for supporting the first paper mold and sucking the inside of the paper mold A molder, a first container containing used paper recycled pulp slurry containing 0 to 5% by mass of cellulose nanofibers, the first papermaking mold and a first molder supporting the first paper mold, above the surface of the used paper recycled pulp slurry. A first lifting means for moving up and down between the inactive position and the operating position immersed in the recycled paper slurry of the waste paper, and the first layer of the pulp mold is made on the first paper making type net. 1 paper making stage,
A second paper mold having a net provided on the front surface and having a plurality of suction ports penetrating from the front surface to the back surface, and a second paper for supporting the second paper mold and sucking the inside of the paper mold A molder, a second container containing a cellulose nanofiber slurry containing 1 to 30% by mass of cellulose nanofibers, a second paper mold and a second molder supporting the second paper mold, above the surface of the cellulose nanofiber slurry. A second raising / lowering means for raising and lowering between the non-acting position and the acting position immersed in the cellulose nanofiber slurry, and forming a pulp mold second layer on the surface of the pulp mold first layer. Paper making stage,
Drying means,
An upper mold to be released by sucking the pulp mold intermediate on the first and second papermaking molds;
A pulp mold manufacturing apparatus comprising: a second lifting and lowering means for raising and lowering the upper mold; and a transfer means for the upper mold in the order of the first papermaking structure, the second papermaking structure, and the drying means. 第１古紙再生パルプおよび／または第２古紙再生パルプの一部を、樹脂、ゴム等またはコーヒー滓、茶殻等の廃棄物のファイバーで置き換えた請求項３の積層パルプモールド製造装置。   The laminated pulp mold manufacturing apparatus according to claim 3, wherein a part of the first recycled paper and / or the second recycled paper pulp is replaced with resin, rubber or the like, or waste fibers such as coffee cake or tea husk.
JP2017104087A 2017-05-26 2017-05-26 Method for producing laminated pulp mold and apparatus for producing the same Pending JP2018199872A (en)

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