JP2016029028A - Powder cosmetic - Google Patents
Powder cosmetic Download PDFInfo
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- JP2016029028A JP2016029028A JP2015126197A JP2015126197A JP2016029028A JP 2016029028 A JP2016029028 A JP 2016029028A JP 2015126197 A JP2015126197 A JP 2015126197A JP 2015126197 A JP2015126197 A JP 2015126197A JP 2016029028 A JP2016029028 A JP 2016029028A
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- powder
- oil
- powder cosmetic
- impregnated
- cosmetic
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- 239000000843 powder Substances 0.000 title claims abstract description 66
- 239000002537 cosmetic Substances 0.000 title claims abstract description 28
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 abstract description 9
- 230000000704 physical effect Effects 0.000 abstract description 4
- 238000013329 compounding Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 23
- 235000019198 oils Nutrition 0.000 description 23
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 238000002156 mixing Methods 0.000 description 7
- 238000002360 preparation method Methods 0.000 description 7
- 239000000049 pigment Substances 0.000 description 5
- 239000003755 preservative agent Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 230000002335 preservative effect Effects 0.000 description 4
- 239000004408 titanium dioxide Substances 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000003086 colorant Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- 239000004606 Fillers/Extenders Substances 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- 240000002871 Tectona grandis Species 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- XJNUECKWDBNFJV-UHFFFAOYSA-N hexadecyl 2-ethylhexanoate Chemical compound CCCCCCCCCCCCCCCCOC(=O)C(CC)CCCC XJNUECKWDBNFJV-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229940057995 liquid paraffin Drugs 0.000 description 2
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 2
- 230000001333 moisturizer Effects 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 239000010696 ester oil Substances 0.000 description 1
- 210000004709 eyebrow Anatomy 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- -1 for example Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000007542 hardness measurement Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 235000019359 magnesium stearate Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
Description
本発明は、しっとりとする、肌へののびが良いといった使用性を有する粉体化粧料に関し、より詳しくはシリカに油分を予め混合することで、粉体化粧料の硬度や色味を変化させることなく優れた使用性（しっとり感、肌上の伸び易さ）を付与できる粉体化粧料に関するものである。 TECHNICAL FIELD The present invention relates to a powder cosmetic that is moist and has good usability of spreading on the skin. More specifically, the hardness and color of the powder cosmetic are changed by premixing oil in silica. The present invention relates to a powder cosmetic that can impart excellent usability (moist feeling, ease of elongation on the skin) without any problems.
ファンデーション類は基本的には粉末、油剤、水の３成分のうち２種または３種を組み合わせて作られ、目的に応じて薬剤、乳化剤、保湿剤等を添加する。剤型はルースパウダー、プレストパウダーなどの粉末化粧料型やリキッドファンデーションやクリームファンデーションなどの乳化型など様々である。中でも粉末化粧料型は乳化型に比べて、粉末配合量が多く、べたつきにくくカバー力に優れるが、油分が少ないことから粉感を強く感じる。そのため、乾燥肌タイプの消費者はリキッドファンデーションなどの乳化型を好む傾向にあり、乾燥期の秋や冬でも同様に乳化型が好まれる傾向にある。さらに、プレストファンデーションに油性感を強めるために油分を多く配合した場合、成型後の硬度が上昇し、ケーキングといった問題を起こし易くなる。 Foundations are basically made by combining two or three of the three components of powder, oil and water, and add chemicals, emulsifiers, moisturizers and the like according to the purpose. There are various dosage forms, such as powder cosmetic types such as loose powder and pressed powder, and emulsified types such as liquid foundation and cream foundation. In particular, the powder cosmetic type has a larger amount of powder and is less sticky and has better covering power than the emulsified type, but has a strong feeling of powder because it contains less oil. For this reason, consumers with dry skin types tend to prefer emulsified types such as liquid foundations, and emulsified types also tend to be preferred in autumn and winter in the dry season. Furthermore, when a large amount of oil is added to the pressed foundation in order to enhance the oily feeling, the hardness after molding rises and problems such as caking are likely to occur.
そこで、粉体化粧料の粉感を低減する技術として、アミノ変性シリコーンや脂肪酸により疎水化処理した体質顔料を粉体化粧料中に配合することでしっとりした感触を得る技術（特許文献１、特開２０１４−５２７９）やシリコーンエラストマーなどのシリコーン粉末を配合することできしみ感を低減する方法（特許文献２、特開１９９６−２６９３２）などが一般的であるが、油分配合量を多く配合する技術ではなく、その効果は満足のいくものではなかった。また、水溶性高分子などの保湿剤を配合することでしっとり感を付与する技術（特許文献３、特開２０１０−３７２１６）があるが、処理が複雑であり簡便に使用できるものではなかった。 Therefore, as a technique for reducing the powdery feeling of the powder cosmetic, a technique for obtaining a moist feel by blending an extender pigment hydrophobized with amino-modified silicone or fatty acid into the powder cosmetic (Patent Document 1, Special). Open 2014-4279) and a method of reducing the squeaky feeling by blending silicone powder such as silicone elastomer (Patent Document 2, JP-A-1996-26932), etc., but a technique for blending a large amount of oil. But the effect was not satisfactory. Moreover, although there exists a technique (patent document 3, Unexamined-Japanese-Patent No. 2010-37216) which gives a moist feeling by mix | blending moisturizing agents, such as water-soluble polymer, a process is complicated and cannot be used easily.
本発明は、優れた使用性（しっとり感、肌上の伸び易さ）を有する粉体化粧料を提供することにある。 An object of the present invention is to provide a powder cosmetic having excellent usability (moist feeling, ease of elongation on the skin).
本課題を解決すべく鋭意検討を加えたところ、予め多孔質シリカに対して油剤を１０〜７０質量％含浸させた粉体を、化粧料全体に対して１〜３０質量％配合した粉体化粧料に上記課題を解決する特性を見出したものである。 As a result of intensive studies to solve this problem, powder cosmetics in which 1 to 30% by mass of a powder obtained by impregnating porous silica with an oil agent in an amount of 10 to 70% by mass is preliminarily incorporated. The characteristic which solves the said subject to a material was discovered.
本発明品は、吸油性に優れた多孔質シリカなどの粉体に予め油剤を含浸させた粉体を粉体化粧料に配合することで、配合しない場合と比較して、硬度や色味をほぼ変化させることなく優れた使用性（しっとり感、肌上の伸び易さ）を付与することが簡便にできる。 The product of the present invention has a hardness and color as compared with the case where it is not blended by blending a powder such as porous silica excellent in oil absorption with a powder that is pre-impregnated with an oil agent. It is possible to easily provide excellent usability (moist feeling, ease of elongation on the skin) without substantially changing.
以下に、本発明について詳述する。
本発明で用いられる油含浸多孔質粉体は、多孔質粉体としてシリカを用いることが好ましく、予め油を含浸させる方法としては特に限定されるものではない。本発明に用いられる多孔質粉体は、特に限定はされないが、平均粒子径は１〜５０μｍ、比表面積は２５０〜１０００ｍ2/ｇ、細孔容積は５ｍL/ｇ以下、細孔直径は３〜５０ｎｍ、吸油量は１００〜４００ｍL/１００ｇであれば好ましく、このような多孔質粉体の市販品としてはサンスフェアＨシリーズなどがある。さらに、多孔質粉体質量に対して１０〜７０質量％の油剤を含浸させることが好ましい。含浸させる油剤には特に限定はなく、化粧品原料として汎用的に使用される油剤、例えば、炭化水素油、エステル油、植物油、シリコーン油などが挙げられる。
The present invention is described in detail below.
In the oil-impregnated porous powder used in the present invention, silica is preferably used as the porous powder, and the method of impregnating oil in advance is not particularly limited. The porous powder used in the present invention is not particularly limited, but the average particle diameter is 1 to 50 μm, the specific surface area is 250 to 1000 m 2 / g, the pore volume is 5 mL / g or less, and the pore diameter is 3 to 3. It is preferable if the oil absorption is 50 nm and the oil absorption is 100 to 400 mL / 100 g, and a commercial product of such a porous powder includes Sunsphere H series. Furthermore, it is preferable to impregnate 10-70 mass% of oil agent with respect to porous powder mass. The oil agent to be impregnated is not particularly limited, and examples thereof include oil agents that are generally used as cosmetic raw materials, such as hydrocarbon oils, ester oils, vegetable oils, and silicone oils.
本発明における油含浸多孔質粉体の配合量は、粉体化粧料全量に対して１．０〜３０．０質量％であるが、好ましくは３．０〜１５.０質量％である。この範囲であれば、化粧料塗布時に十分なしっとり感や肌上への伸び易さを得ることができる。
本発明の粉体化粧料には、前記本発明の効果を損なわない範囲において、一般に化粧料に配合される各種任意成分、例えば油剤、保湿剤、増粘剤、防腐剤、乳化剤、顔料、その他の粉体、ｐＨ調整剤、薬効成分、紫外線吸収剤、抗酸化剤、香料等を適宜配合することができる。
The blending amount of the oil-impregnated porous powder in the present invention is 1.0 to 30.0% by mass, preferably 3.0 to 15.0% by mass, based on the total amount of the powder cosmetic. If it is this range, sufficient moist feeling at the time of cosmetics application and the easiness to extend on skin can be acquired.
In the powder cosmetics of the present invention, various optional ingredients generally incorporated in cosmetics, for example, oils, moisturizers, thickeners, preservatives, emulsifiers, pigments, etc., within a range that does not impair the effects of the present invention. Powders, pH adjusters, medicinal components, ultraviolet absorbers, antioxidants, fragrances, and the like can be appropriately blended.
本発明の粉体化粧料を調製する際は、粉体用ミキサーやプレス装置など通常の製造装置が使用できる。調製方法は、粉体用ミキサーで顔料やその他の粉体を攪拌混合し、必要であれば予め加温溶解したバインダーを加え、均一になるまで十分に攪拌し、必要であれば型に入れプレス成型する方法などが挙げられる。 When preparing the powder cosmetic of the present invention, a normal production apparatus such as a powder mixer or a press apparatus can be used. The preparation method involves stirring and mixing pigments and other powders in a powder mixer, adding a pre-warmed binder if necessary, stirring well until uniform, and if necessary, placing in a mold and pressing Examples include a molding method.
さらに本発明の粉体化粧料とは、前述の油含浸多孔質粉体を必須成分として配合するものであり、形態としては特に限定されず、プレストパウダー、ルースパウダーのいずれも該当する。また用途としても特に限定されず、ボディパウダー、フェイスパウダー、ファンデーション、チーク、アイシャドウ、アイブロウなどが挙げられる。
次に本発明をより多くの実施例で詳述するが、本発明はこれにより限定されるものではない。
Furthermore, the powder cosmetic of the present invention contains the aforementioned oil-impregnated porous powder as an essential component, and the form is not particularly limited, and both pressed powder and loose powder are applicable. Also, the use is not particularly limited, and examples thereof include body powder, face powder, foundation, teak, eye shadow, and eyebrow.
Next, the present invention will be described in more detail with reference to more examples, but the present invention is not limited thereto.
（１）油含浸多孔質粉体の調製
表１に示す処方に従って、多孔質粉体シリカと油剤をあらかじめ混合し含浸させた油含浸多孔質粉体（製造例１〜５）を調製した。
（２）プレストファンデーションの調製
表２、３に示す処方に従ってプレストファンデーションを作製した。各成分をミキサーにて均一に混合し、メッシュを通した後にプレス成型することでプレストファンデーションを得た。
(2) Preparation of Presto Foundation Presto Foundation was prepared according to the formulations shown in Tables 2 and 3. Each component was uniformly mixed with a mixer, passed through a mesh, and press molded to obtain a pressed foundation.
（３）使用感評価
化粧品専門パネラー１０名を用いて、調製したプレストファンデーションの使用感（しっとり感、肌上への伸び易さ）を評価した。評価は以下の４段階の基準に分類した。
◎：１０名中８名以上が良好と感じた
○：１０名中６〜７名が良好と感じた
△：１０名中４〜５名が良好と感じた
×：１０名中３名以下が良好と感じた
(3) Usability Evaluation Using 10 cosmetic panelists, the feeling of use of the prepared pressed foundation (moist feeling, ease of extension on the skin) was evaluated. Evaluation was classified into the following four criteria.
◎: 8 or more out of 10 felt good ○: 6-7 out of 10 felt good △: 4-5 out of 10 felt good ×: 3 or less out of 10 Felt good
（４）硬度測定
オルゼン型硬度計を用いて、プレスト表面５点の平均値を測定した。
（５）色測定
色差計を用いて、L*、a*、b*および比較品１に対するΔE*abを測定した。
(5) Color measurement L *, a *, b * and ΔE * ab for Comparative Product 1 were measured using a color difference meter.
（６）結果
予め油剤を多孔質粉体に含浸させたものを体質顔料であるセリサイトと置き換えて粉体化粧料に配合した場合（発明品１〜７）、比較品１と比べ、使用感が向上し、物性値の変化は硬度において±１０％以内、ΔＥは目視で差が分かるとされる１．５より低い値であり影響はほとんどみられなかった。また、多孔質粉体に油量を変更し含浸させた製造例１〜３の油含浸多孔質粉体を用いたプレストファンデーション（発明品１〜３）の物性に大きな差はなかった。
(6) Results When the oil powder previously impregnated with porous powder is replaced with sericite, which is an extender pigment, and blended into powder cosmetics (Invention products 1 to 7), the usability compared to Comparative product 1 As a result, the change in physical properties was within ± 10% in hardness, and ΔE was a value lower than 1.5, which is considered to be a visual difference, and there was almost no effect. Moreover, there was no big difference in the physical property of the pressed foundation (invention products 1-3) using the oil-impregnated porous powder of Production Examples 1 to 3 in which the porous powder was impregnated with the oil amount changed.
ルースパウダー
マイカ １００．０に調整（質量％）
製造例２の油含浸多孔質粉体 １０．０
酸化亜鉛 ５．０
顔料級二酸化チタン １０．０
ベンガラ １．５
黄酸化鉄 ４．５
黒酸化鉄 ０．３
防腐剤 適量
（調製方法）各成分をミキサーにて均一に混合し、メッシュを通した後にプレス成型した。
（結果）肌上への伸びやすさ、しっとり感に優れていた。
Adjust to loose powder mica 100.0 (mass%)
Oil impregnated porous powder of Production Example 2 10.0
Zinc oxide 5.0
Pigment grade titanium dioxide 10.0
Bengala 1.5
Yellow iron oxide 4.5
Black iron oxide 0.3
Preservative Appropriate amount (preparation method) Each component was uniformly mixed with a mixer, passed through a mesh, and press molded.
(Results) Excellent stretchability on skin and moist feeling.
チークパウダー
タルク １００．０に調整（質量％）
製造例４の油含浸多孔質粉体 １０．０
セリサイト ２０．０
マイカ ５．０
二酸化チタン ５．０
ステアリン酸マグネシウム ３．０
流動パラフィン ４．０
２−エチルヘキサン酸セチル １．５
着色料 適量
防腐剤 適量
（調製方法）各成分をミキサーにて均一に混合し、メッシュを通した後にプレス成型した。
（結果）肌上への伸びやすさ、しっとり感に優れていた。
Teak powder talc adjusted to 100.0 (mass%)
Oil impregnated porous powder of Production Example 4 10.0
Sericite 20.0
Mica 5.0
Titanium dioxide 5.0
Magnesium stearate 3.0
Liquid paraffin 4.0
Cetyl 2-ethylhexanoate 1.5
Colorant Appropriate amount Preservative Appropriate amount (preparation method) Each component was uniformly mixed with a mixer, passed through a mesh, and press-molded.
(Results) Excellent stretchability on skin and moist feeling.
アイシャドウ
タルク １００．０に調整（質量％）
製造例５の油含浸多孔質粉体 １０．０
セリサイト ２０．０
マイカ １５．０
二酸化チタン ３．０
ステアリン酸亜鉛 ３．０
流動パラフィン ４．０
２−エチルへキサン酸セチル ２．５
着色料 適量
防腐剤 適量
（調製方法）各成分をミキサーにて均一に混合し、メッシュを通した後にプレス成型した。
（結果）肌上への伸びやすさ、しっとり感に優れていた。
Eye shadow talc adjusted to 100.0 (mass%)
Oil impregnated porous powder of Production Example 5 10.0
Sericite 20.0
Mica 15.0
Titanium dioxide 3.0
Zinc stearate 3.0
Liquid paraffin 4.0
Cetyl 2-ethylhexanoate 2.5
Colorant Appropriate amount Preservative Appropriate amount (preparation method) Each component was uniformly mixed with a mixer, passed through a mesh, and press molded.
(Results) Excellent stretchability on skin and moist feeling.
粉おしろい
タルク １００．０に調整（質量％）
製造例１の油含浸多孔質粉体 １０．０
セリサイト １０．０
カオリン ５．０
二酸化チタン ５．０
ステアリン酸亜鉛 ５．０
炭酸マグネシウム ５．０
着色料 適量
防腐剤 適量
（調製方法）各成分をミキサーにて均一に混合し、メッシュを通した後に充填した。
（結果）肌上への伸びやすさ、しっとり感に優れていた。
Adjust to 100.0 powder talc (mass%)
Oil impregnated porous powder of Production Example 1 10.0
Sericite 10.0
Kaolin 5.0
Titanium dioxide 5.0
Zinc stearate 5.0
Magnesium carbonate 5.0
Colorant Appropriate amount Preservative Appropriate amount (preparation method) Each component was uniformly mixed with a mixer, passed through a mesh, and filled.
(Results) Excellent stretchability on skin and moist feeling.
Claims (4)
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20190023455A (en) * | 2017-08-29 | 2019-03-08 | 코스맥스 주식회사 | A Stick-form Cosmetic Composition Comprising Porous Powder And A Preparing Method Thereof |
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| JP6644485B2 (en) | 2020-02-12 |
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