JP2013060610A - Method of controlling the atmosphere of continuous heat treatment furnace - Google Patents

Method of controlling the atmosphere of continuous heat treatment furnace Download PDF

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JP2013060610A
JP2013060610A JP2011197843A JP2011197843A JP2013060610A JP 2013060610 A JP2013060610 A JP 2013060610A JP 2011197843 A JP2011197843 A JP 2011197843A JP 2011197843 A JP2011197843 A JP 2011197843A JP 2013060610 A JP2013060610 A JP 2013060610A
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furnace
atmosphere
gas
temperature
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JP5733121B2 (en
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Motoki Takada
基樹 高田
Hideyuki Takahashi
秀行 高橋
Takamasa Fujii
貴将 藤井
Nobuyuki Sato
伸行 佐藤
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JFE Steel Corp
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  • Heat Treatment Of Strip Materials And Filament Materials (AREA)
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Abstract

PROBLEM TO BE SOLVED: To provide a method for lowering a dew point of the furnace atmosphere, while suppressing the decrease of local temperature in a furnace because a local decrease of temperature in the furnace cannot be prevented without an additional charge of a quantity of heat, when lowering the dew point in the furnace of a continuous annealing furnace by a refiner.SOLUTION: The method of controlling the atmosphere of the continuous annealing furnace includes taking a gas that is a portion of the furnace atmosphere into the refiner 8 installed outside the furnace to dehumidify and deacidify, and injecting it into the furnace again. The gas after dehumidification and deacidification out from the refiner 8 is heat exchanged with a gas to be taken into the refiner 8 by a heat exchanger 7 installed outside the furnace, subsequently heat-exchanged with the furnace atmosphere by an in-furnace heat exchanger 11 installed in the furnace, and then injected in the furnace.

Description

本発明は、連続熱処理炉の炉内雰囲気調整方法に関し、詳しくは、連続焼鈍炉の炉内雰囲気ガスの露点を低減し、めっき付着が良好な鋼板を有利に生産するための、連続熱処理炉の炉内雰囲気調整方法に関する。   The present invention relates to a method for adjusting the in-furnace atmosphere of a continuous heat treatment furnace. More specifically, the present invention relates to a continuous heat treatment furnace for reducing the dew point of the in-furnace atmosphere gas of a continuous annealing furnace and advantageously producing a steel sheet with good plating adhesion. The present invention relates to a furnace atmosphere adjustment method.

鋼板(詳しくは、帯状の鋼板)に連続的に熱処理を施す連続焼鈍炉において、熱処理後の鋼板の化成処理性向上および高張力鋼板のめっき性を向上させるために炉内雰囲気ガスの露点は−45℃以下が目標とされることが知られている。
連続焼鈍炉において、炉立上げ時の炉内は大気雰囲気で充満されており、炉内および炉壁耐火物内部には、大気中の水分が浸透している。かかる水分は炉を運転することによって徐々に除去されていくが、炉内が鋼板製造可能な露点範囲になるには十数時間から数日の運転が必要で非効率的である。この理由としては、炉立上げ後、耐火物内部に浸透していた水分が徐々に炉内へ供給されることによって炉内の露点が下がるまでに時間を要するということが挙げられる。従来の炉内雰囲気調整方法の一つとして特許文献1のように炉内空間に直接雰囲気ガスを供給するとともに、炉壁耐火物の最外面側から炉内空間に向けて50℃〜120℃の低温の雰囲気ガスを送給する方法が知られている。
In a continuous annealing furnace that continuously heat-treats a steel plate (specifically, a strip-shaped steel plate), the dew point of the atmosphere gas in the furnace is − in order to improve the chemical conversion treatment property of the steel plate after heat treatment and the plating property of the high-tensile steel plate. It is known that 45 ° C. or lower is targeted.
In the continuous annealing furnace, the interior of the furnace when the furnace is started up is filled with an atmospheric atmosphere, and moisture in the atmosphere permeates into the furnace and the inside of the furnace wall refractory. Such moisture is gradually removed by operating the furnace, but it is inefficient because it requires an operation of several tens of hours to several days to reach the dew point range in which the steel sheet can be produced. The reason for this is that it takes time until the dew point in the furnace is lowered by gradually supplying moisture that has penetrated into the refractory after the furnace is started up. As one of the conventional furnace atmosphere adjustment methods, atmospheric gas is directly supplied to the furnace space as in Patent Document 1, and 50 ° C. to 120 ° C. from the outermost surface side of the furnace wall refractory toward the furnace space. A method of supplying a low-temperature atmospheric gas is known.

特開平07−173526号公報Japanese Patent Application Laid-Open No. 07-173526

連続焼鈍炉において、炉内雰囲気の低露点化の為に、炉内の高温の雰囲気の一部であるガスを、脱湿・脱酸装置であるリファイナーに取り込み、脱湿・脱酸処理を行った後、炉内に吹き込む方法を採る場合、脱湿・脱酸処理を行う為に前記の取り込んだ高温のガスはこれを一旦常温近くまで冷却する必要がある。その常温近くまで冷却された脱湿・脱酸処理後のガスをそのまま炉内へ吹き込むと、炉内温度が過剰に低下し、鋼板の品質劣化に繋がる事になる。そこで、前記常温近くまで冷却された脱湿・脱酸処理後のガスは、これを炉内に吹き込む前に、前記取り込んだ高温のガスと熱交換させる事によって昇温させる方法が採られている。   In a continuous annealing furnace, in order to lower the dew point in the furnace atmosphere, gas that is part of the high-temperature atmosphere in the furnace is taken into a refiner that is a dehumidifying / deoxidizing device, and dehumidified / deoxidized. After that, when the method of blowing into the furnace is employed, it is necessary to once cool the taken-in high-temperature gas to near normal temperature in order to perform dehumidification / deoxidation treatment. If the dehumidified and deoxidized gas that has been cooled to near normal temperature is blown into the furnace as it is, the temperature inside the furnace will be excessively lowered, leading to deterioration of the quality of the steel sheet. Therefore, a method is employed in which the gas after dehumidification / deoxidation treatment cooled to near room temperature is heated by exchanging heat with the incorporated high-temperature gas before blowing it into the furnace. .

然しながら、前記取り込んだ高温のガスと前記常温近くまで冷却された脱湿・脱酸処理後のガスとの熱交換では、熱交換後のガス温度は精々両者の中間程度の温度までしか昇温せず、前記熱交換後の温度が炉温よりも低くて、これを炉内へ吹き込むと局所的な炉温低下が生じるから、これを防ぐ為に、追加の熱量を投じる必要があった。
つまり、従来、リファイナーで連続焼鈍炉の炉内低露点化を図る場合、熱量の追加投入無しでは炉内温度の局所的低下を防ぎ得ないという課題があった。
However, in the heat exchange between the taken-in high-temperature gas and the dehumidified / deoxidized gas cooled to near room temperature, the temperature of the gas after the heat exchange can be raised only to an intermediate temperature between them. First, since the temperature after the heat exchange is lower than the furnace temperature and blowing it into the furnace, a local decrease in the furnace temperature occurs. Therefore, in order to prevent this, it is necessary to apply an additional amount of heat.
In other words, conventionally, when reducing the in-furnace dew point of a continuous annealing furnace with a refiner, there has been a problem that a local decrease in the in-furnace temperature cannot be prevented without additional input of heat.

発明者らは前記課題を解決するために鋭意検討し、その結果、前記熱交換後のガスを、更に炉内雰囲気との熱交換にて昇温させて炉内へ吹き込む事で、熱量の追加投入無しでも炉内温度の局所的低下が防げる事を知見し、本発明を成した。
即ち、本発明は、連続焼鈍炉の炉内雰囲気の低露点化のために前記炉内雰囲気の一部であるガスを炉外に設けたリファイナーに取り込んで脱湿・脱酸した後、再び炉内へ吹き込む、連続焼鈍炉の炉内雰囲気調整方法において、前記リファイナーを出た脱湿・脱酸後のガスを、炉外に設けた熱交換器にて前記リファイナーに取り込むガスと熱交換させ、次いで、炉内に設けた炉内熱交換器にて炉内雰囲気と熱交換させた後、炉内へ吹き込むことを特徴とする連続焼鈍炉の炉内雰囲気調整方法である。
The inventors have intensively studied to solve the above problems, and as a result, the heat-exchanged gas is further heated by heat exchange with the furnace atmosphere and blown into the furnace to add heat. It was found that local reduction of the furnace temperature could be prevented without charging, and the present invention was made.
That is, the present invention relates to a dehumidification / deoxidation after taking a gas that is a part of the furnace atmosphere into a refiner provided outside the furnace in order to lower the dew point in the furnace atmosphere of the continuous annealing furnace, In the in-furnace atmosphere adjustment method of the continuous annealing furnace, the gas after dehumidification / deoxidation that exits the refiner is heat exchanged with the gas taken into the refiner by a heat exchanger provided outside the furnace, Next, after the heat exchange with the furnace atmosphere is performed in the furnace heat exchanger provided in the furnace, the furnace atmosphere adjustment method of the continuous annealing furnace is characterized by blowing into the furnace.

本発明によれば、リファイナーで脱湿・脱酸したガスを、炉外に設けた熱交換器にてリファイナーに取り込むガスと熱交換して昇温させ、次いで、炉内に設けた炉内熱交換器にて炉内雰囲気と熱交換させて更に昇温させてから炉内へ吹き込むようにしたことから、熱量の追加投入無しで、炉内吹き込みガス温度を炉内温度に近づけることができ、以て、炉温の局所的低下を抑えつつ、炉内雰囲気の低露点化を図ることができる。   According to the present invention, the gas dehumidified and deoxidized by the refiner is heated by exchanging heat with the gas taken into the refiner by a heat exchanger provided outside the furnace, and then the furnace heat provided in the furnace. Since the heat was exchanged with the furnace atmosphere in the exchanger and the temperature was further raised and then blown into the furnace, the gas temperature in the furnace could be brought close to the furnace temperature without additional input of heat. Thus, it is possible to achieve a low dew point in the furnace atmosphere while suppressing a local decrease in the furnace temperature.

本発明の一実施形態を示す模式図である。It is a schematic diagram which shows one Embodiment of this invention.

図1は、本発明の一実施形態を示す模式図であり、該図において、1は鋼板、2は焼鈍炉第1加熱帯、3は焼鈍炉第2加熱帯、4は炉内ロール、5は取り出し配管、6は送風機、7は熱交換器、8はリファイナー(脱湿・脱酸装置)、9は熱交換器繋ぎ込み配管、10は炉内熱交換器供給配管、11は炉内熱交換器、12は吹き込み配管である。
図示の様に、第1加熱帯2と第2加熱帯3とに分けられた連続焼鈍炉において、鋼板1が炉内ロール4にて連続通板されつつ連続焼鈍される場合、第2加熱帯3から取り出し配管5を介して炉内雰囲気の一部であるガスが取り出される。該取り出されたガスは送風機6により熱交換器7へ送られ、熱交換器7の高温側熱媒とされ、熱交換器7の低温側熱媒との熱交換により抜熱された後、リファイナー8へ導かれ、リファイナー8内で常温近くまで冷却され、脱湿・脱酸される。リファイナー8を出た常温に近いガスは、熱交換器繋ぎ込み配管9を経由して熱交換器7の低温側熱媒とされ、熱交換器7の高温側熱媒とされた前記取り出されたガスとの熱交換により加熱されて、両者の温度の中間程度の温度に昇温したガスとなる。
FIG. 1 is a schematic view showing an embodiment of the present invention, in which 1 is a steel plate, 2 is an annealing furnace first heating zone, 3 is an annealing furnace second heating zone, 4 is an in-furnace roll, Is a take-out pipe, 6 is a blower, 7 is a heat exchanger, 8 is a refiner (dehumidification / deoxidation device), 9 is a heat exchanger connection pipe, 10 is a heat exchanger supply pipe in the furnace, and 11 is heat in the furnace An exchanger 12 is a blowing pipe.
As shown in the drawing, in the continuous annealing furnace divided into the first heating zone 2 and the second heating zone 3, when the steel plate 1 is continuously annealed while being continuously passed through the in-furnace roll 4, the second heating zone is used. A gas which is a part of the furnace atmosphere is taken out from 3 through a take-out pipe 5. The extracted gas is sent to the heat exchanger 7 by the blower 6, used as the high temperature side heat medium of the heat exchanger 7, and removed by heat exchange with the low temperature side heat medium of the heat exchanger 7. 8 is cooled to near normal temperature in the refiner 8 and dehumidified and deoxidized. The gas close to room temperature exiting the refiner 8 is taken as the low temperature side heat medium of the heat exchanger 7 via the heat exchanger connecting pipe 9 and is taken out as the high temperature side heat medium of the heat exchanger 7. It is heated by heat exchange with the gas, and becomes a gas whose temperature has been raised to an intermediate temperature between the two.

熱交換器7を出たガスは、炉内熱交換器供給配管10を経由して炉内熱交換器11に導かれ、炉内熱交換器11の低温側熱媒とされる。炉内熱交換器11は第1加熱帯2内に設置されており、その高温側熱媒は第1加熱帯2の炉内雰囲気である。従って、熱交換器7を出たガスは炉内熱交換器11内で炉内雰囲気との熱交換により加熱され、炉内雰囲気温度により近い温度まで昇温されたガスとなって、吹き込み配管12経由で第2加熱帯3内へ吹き込まれる。   The gas exiting the heat exchanger 7 is guided to the in-furnace heat exchanger 11 via the in-furnace heat exchanger supply pipe 10 and is used as a low-temperature side heat medium for the in-furnace heat exchanger 11. The in-furnace heat exchanger 11 is installed in the first heating zone 2, and the high temperature side heat medium is the in-furnace atmosphere of the first heating zone 2. Therefore, the gas exiting the heat exchanger 7 is heated by heat exchange with the furnace atmosphere in the furnace heat exchanger 11 and becomes a gas heated to a temperature closer to the furnace atmosphere temperature, and the blow pipe 12 It is blown into the second heating zone 3 via.

炉内熱交換器11の設置箇所としては、本例の如く、吹き込み箇所(本例では第2加熱帯3)から離れた箇所で且つ多少炉温が低下しても問題のない箇所,即ち炉の加熱能力に余力のある箇所(本例では第1加熱帯2)を選択することが、炉温の局所的低下をより良く抑える観点から好ましい。   As the location where the in-furnace heat exchanger 11 is installed, as in this example, the location away from the blowing location (second heating zone 3 in this example) and the location where there is no problem even if the furnace temperature drops somewhat, that is, the furnace It is preferable from the viewpoint of better suppressing the local decrease in the furnace temperature to select a portion having sufficient heating capacity (first heating zone 2 in this example).

本発明例として、図1において、第1加熱帯2と第2加熱帯3の燃焼機器の負荷状態を夫々一定に保持して炉温を800℃に設定した条件下で、リファイナー8の処理ガス流量(=吹き込み流量)を200Nm/hとして、図1のガス経路に沿ってガス吹込みを行い、吹き込む直前のガス温度(略して、吹き込みガス温度)と、該ガス吹き込み後の第2加熱帯3の炉温(略して、吹き込み後第2加熱帯炉温)とを測定した。一方、比較例として、図1において、炉内熱交換器11を使用せず熱交換器7で昇温されたガスを直接第2加熱帯3へ吹き込み、これ以外は本発明例と同様とし、同様の測定を行った。その結果を表1に示す。 As an example of the present invention, in FIG. 1, the processing gas of the refiner 8 is maintained under the condition that the load conditions of the combustion devices in the first heating zone 2 and the second heating zone 3 are kept constant and the furnace temperature is set to 800 ° C. A gas flow is performed along the gas path of FIG. 1 with a flow rate (= injection flow rate) of 200 Nm 3 / h, the gas temperature just before the injection (abbreviated gas temperature for short), and the second pressure after the gas injection. Tropical 3 furnace temperature (abbreviated, second heating zone furnace temperature after blowing) was measured. On the other hand, as a comparative example, in FIG. 1, without using the in-furnace heat exchanger 11, the gas heated in the heat exchanger 7 was directly blown into the second heating zone 3, and other than this, the same as in the present invention example, Similar measurements were made. The results are shown in Table 1.

表1より、本発明例では、吹き込みガス温度が比較例のそれに比して格段に高く、吹き込み後第2加熱帯3の炉温がそれに比して格段に高く、設定炉温(800℃)からの温度低下が大幅に軽減できた。   From Table 1, in the example of the present invention, the blowing gas temperature is much higher than that of the comparative example, and the furnace temperature of the second heating zone 3 after blowing is much higher than that of the comparative example, and the set furnace temperature (800 ° C.). The temperature drop from can be greatly reduced.

Figure 2013060610
Figure 2013060610

1 鋼板(詳しくは、帯状の鋼板)
2 焼鈍炉第1加熱帯
3 焼鈍炉第2加熱帯
4 炉内ロール
5 取り出し配管
6 送風機
7 熱交換器
8 脱湿・脱酸装置(リファイナー)
9 熱交換器繋ぎ込み配管
10 炉内熱交換器供給配管
11 炉内熱交換器
12 吹き込み配管
1 Steel plate (For details, strip steel plate)
2 Annealing furnace 1st heating zone 3 Annealing furnace 2nd heating zone 4 In-furnace roll 5 Extraction piping 6 Blower 7 Heat exchanger 8 Dehumidification / deoxidation equipment (refiner)
9 Heat exchanger connecting pipe 10 Furnace heat exchanger supply pipe 11 Furnace heat exchanger 12 Blowing pipe

Claims (1)

連続焼鈍炉の炉内雰囲気の低露点化のために前記炉内雰囲気の一部であるガスを炉外に設けたリファイナーに取り込んで脱湿・脱酸した後、再び炉内へ吹き込む、連続焼鈍炉の炉内雰囲気調整方法において、前記リファイナーを出た脱湿・脱酸後のガスを、炉外に設けた熱交換器にて前記リファイナーに取り込むガスと熱交換させ、次いで、炉内に設けた炉内熱交換器にて炉内雰囲気と熱交換させた後、炉内へ吹き込むことを特徴とする連続焼鈍炉の炉内雰囲気調整方法。   In order to lower the dew point in the furnace atmosphere of a continuous annealing furnace, the gas that is part of the furnace atmosphere is taken into a refiner provided outside the furnace, dehumidified and deoxidized, and then blown into the furnace again. In the furnace atmosphere adjustment method of the furnace, the dehumidified / deoxidized gas exiting the refiner is heat-exchanged with the gas taken into the refiner by a heat exchanger provided outside the furnace, and then provided in the furnace. A method for adjusting the in-furnace atmosphere of a continuous annealing furnace, wherein the heat is exchanged with the in-furnace atmosphere by using an in-furnace heat exchanger and then blown into the furnace.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115190A1 (en) * 2013-01-28 2014-07-31 Jfeスチール株式会社 Method for adjusting in-furnace atmosphere of continuous heat-treating furnace
CN105018714A (en) * 2014-04-17 2015-11-04 宝山钢铁股份有限公司 Method for humidifying atmosphere in continuous annealing furnace
CN111484023A (en) * 2019-12-23 2020-08-04 浙江精功新材料技术有限公司 Horizontal deacidification furnace for producing high-temperature steam based on hydrogen combustion method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115190A1 (en) * 2013-01-28 2014-07-31 Jfeスチール株式会社 Method for adjusting in-furnace atmosphere of continuous heat-treating furnace
CN105018714A (en) * 2014-04-17 2015-11-04 宝山钢铁股份有限公司 Method for humidifying atmosphere in continuous annealing furnace
CN111484023A (en) * 2019-12-23 2020-08-04 浙江精功新材料技术有限公司 Horizontal deacidification furnace for producing high-temperature steam based on hydrogen combustion method
CN111484023B (en) * 2019-12-23 2022-10-11 浙江精功新材料技术有限公司 Horizontal deacidification furnace for producing high-temperature steam based on hydrogen combustion method

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