JP2013005750A - Animal feed including cereal bran or cereal ground product subjected to modification treatment - Google Patents
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Abstract
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本発明は、改質処理した穀類糠或いは穀類粉砕物を配合することにより、動物の有用な飼料原料である穀類糠或いは穀類粉砕物を増大した量で有効に利用することを可能とした動物飼料を提供すること、特に、反芻動物のような動物の飼料として穀類糠或いは穀類粉砕物を増大した量で有効に利用するために障害となる穀類糠或いは穀類粉砕物中の有機態リンを除去、減少させることによって穀類糠或いは穀類粉砕物を改質処理し、該飼料原料を増大した量で有効に利用することを可能とした動物飼料を提供すること、及び、該穀類糠或いは穀類粉砕物の改質処理手段として、飼料製造に際して実用的に適用できる手段を提供することに関する。 The present invention provides an animal feed that can effectively use an increased amount of cereal meal or cereal pulverized material, which is a useful feed material for animals, by blending the modified cereal meal or cereal cereal. In particular, removing organic phosphorus in the cereal meal or cereal grind which is an obstacle to effectively use the increased amount of cereal meal or cereal grind as animal feed such as ruminants, To provide an animal feed capable of effectively using the feed raw material in an increased amount by modifying the cereal meal or the cereal meal by reducing the amount of the cereal meal or the pulverized cereal The present invention relates to providing means that can be practically applied during feed production as modification processing means.
穀類等の植物種子は、食品や飼料等として広く利用されている材料であり、これらの植物種子にはリンが豊富に含まれている。該植物種子に含有されているリンの大部分はフィチン態として存在している。リンは全ての生物の生育に必須の元素であるが、反芻動物のように胃内に共生する微生物によって食餌を分解して消化する動物と相違して、ヒトや、豚、鶏等の家畜のような単胃動物ではフィチンを分解できないため、植物種子由来の食品や飼料を摂取しても、含有されるフィチン態リンを全く利用できない。また、食品や飼料中のフィチン態リンは、栄養源として利用されていないだけでなく、フィチン酸は、タンパク質と結合し、消化酵素の働きを阻害したり、カルシウム、亜鉛、マグネシウム、鉄等のミネラルをキレートし、栄養的に重要なミネラルの吸収を妨げる等の栄養学的な面からの問題も引き起こす。そこで、従来より、これらの問題を解決するために、植物種子由来の食品や飼料中のフィチン酸を除去する各種の方法が検討されている。 Plant seeds such as cereals are materials that are widely used as foods and feeds, and these plant seeds are rich in phosphorus. Most of the phosphorus contained in the plant seed exists as a phytin state. Phosphorus is an essential element for the growth of all living organisms, but unlike animals that decompose and digest food by microorganisms that coexist in the stomach, such as ruminants, humans, pigs, chickens and other livestock In such a monogastric animal, phytin cannot be decomposed. Therefore, even if food or feed derived from plant seeds is ingested, the contained phytic phosphorus cannot be used at all. In addition, phytic phosphorus in food and feed is not used as a nutrient source, but phytic acid binds to proteins and inhibits the action of digestive enzymes, and calcium, zinc, magnesium, iron, etc. It also causes nutritional problems such as chelating minerals and preventing the absorption of nutritionally important minerals. In order to solve these problems, various methods for removing phytic acid in plant seed-derived foods and feeds have been studied.
穀類等の植物種子を、食品や飼料等として利用するに際して、フィチン酸を除去する方法としては、フィターゼのような酵素や、微生物を用いてフィチン酸を無機リン酸塩に分解する方法が知られている。例えば、特表２００１−５１４８６９号公報、特表２００２−５２３０２６号公報には、フィターゼを用いて、穀類等の植物種子中に含まれるフィチン態リンを無機リン酸塩に分解し、食品や飼料として利用する方法が開示されている。特開平６−３１９５３９号公報には、アスペルギルス（Aspergillus）属由来のフィターゼを用いて、及び、特開平１１−１６４号公報には、ペニシリウム（Penicillum）属由来のフィターゼを用いて、飼料や食品中に含まれるフィチンを分解し、遊離したリン酸を有効に利用する方法が開示されている。 As a method for removing phytic acid when using plant seeds such as cereals as food or feed, a method of decomposing phytic acid into inorganic phosphate using an enzyme such as phytase or a microorganism is known. ing. For example, in Japanese translations of PCT publication No. 2001-514869 and JP 2002-523026 A, phytase phosphorus contained in plant seeds such as cereals is decomposed into inorganic phosphate using phytase, and used as food or feed. A method of using is disclosed. JP-A-6-319539 uses a phytase derived from the genus Aspergillus, and JP-A-11-164 uses a phytase derived from the genus Penicillium in feeds and foods. Discloses a method of effectively decomposing phytin contained in the phosphine and using the liberated phosphoric acid effectively.
また、特開平７−２３６４３９号公報、特開平８−２１４８２２号公報には、穀類に麹菌を接種して、製麹することにより、穀類中のフィチン酸を分解し、低減することが、及び、特開平５−４９４０７号公報には、米糠やふすまを、バチルス・ナットーで好気的に発酵させて、飼料中に多量に含まれる有機態リンの弊害を解消することが開示されている。 JP-A-7-236439, JP-A-8-214822 discloses that phytic acid in cereals is decomposed and reduced by inoculating cereals with koji mold and koji making, and Japanese Patent Laid-Open No. 5-49407 discloses that rice bran and bran are fermented aerobically with Bacillus natto to eliminate the harmful effects of organic phosphorus contained in a large amount in the feed.
穀類等の植物種子を、食品や飼料等として利用するに際して、フィチン酸の除去に、フィターゼのような酵素や、微生物を用いる以外の方法としては、樹脂を用いるものや、飼料中に含まれるフィチン酸を高温、高圧下で加水分解する方法などが知られている。例えば、特開２００１−１６３８００号公報には、穀類や豆類等の植物タンパク質に結合しているフィチン酸又はその塩を、アニオン交換樹脂と接触させることにより、除去する方法が、特開２０１０−１３６６８３号公報には、飼料中のフィチン酸態リンを、水分を共存させた状態で、温度１５０〜２６０℃、圧力０．４〜３０ＭＰａ、液固比１：１〜１００：１の条件で、１〜１８０分間保持することにより加水分解する方法が、それぞれ開示されている。 When plant seeds such as cereals are used as foods, feeds, etc., methods other than using an enzyme such as phytase or a microorganism to remove phytic acid include those using resins and phytin contained in feed A method of hydrolyzing an acid at high temperature and high pressure is known. For example, Japanese Patent Laid-Open No. 2001-163800 discloses a method for removing phytic acid or a salt thereof bound to plant proteins such as cereals and beans by contacting with an anion exchange resin. In the publication, phytic acid phosphorus in feed is 1 in the condition of a temperature of 150 to 260 ° C., a pressure of 0.4 to 30 MPa, and a liquid-solid ratio of 1: 1 to 100: 1 in the presence of moisture. Methods of hydrolyzing by holding for ˜180 minutes are each disclosed.
これらの方法は、穀類等のフィチン酸を含有する植物材料を食品や飼料に用いるに際して、ヒトや、豚、鶏等の家畜のような単胃動物では利用できないフィチン酸を分解して、除去したり、或いは無機リン酸塩として有効に利用することを目的としたものであるが、いずれの方法も、その処理の複雑さ等の問題があり、動物飼料として用いられる穀類糠や、穀類粉砕物等の大量の処理に実用的に用いることができる、有効で、簡便かつ安価な処理手段としては、適用の難しいものであった。 When using plant materials containing phytic acid such as cereals for food and feed, these methods decompose and remove phytic acid that cannot be used in monogastric animals such as humans, domestic animals such as pigs and chickens. Or any of these methods have problems such as the complexity of the treatment, and cereal straws used as animal feed and pulverized cereals. As an effective, simple, and inexpensive processing means that can be used practically for a large amount of processing, it has been difficult to apply.
ところで、穀類糠や、穀類粉砕物等のフィチン酸を含有する植物材料を反芻動物用の飼料に用いるに際しては、特殊な事情が発生する。すなわち、反芻動物は胃内に共生する微生物によって食餌を分解し、それを利用して体成分を再構築する。これによって、微生物が分解できる全ての有機物を利用することが可能である。反芻動物胃内微生物はフィチン酸を分解するフィターゼも有するため、反芻動物は他の哺乳類には利用できないフィチン酸態リンを有効に利用することができる。しかしながら、フィチン酸などの有機態リンを多く含む穀類又は穀類糠を反芻動物に多量に投与するとリンの摂取量が過多となり、尿石症や体内カルシウムの排出増大による骨格形成障害が起こる危険性が高くなるという問題がある。したがって、飼料としての投与量は制限せざるを得ないのが現状である。 By the way, when using plant materials containing phytic acid such as cereal meal and pulverized cereal for feed for ruminants, special circumstances arise. In other words, ruminants decompose food by microorganisms symbiotic in the stomach and use it to reconstruct body components. This makes it possible to use all organic substances that can be decomposed by microorganisms. Ruminant gastric microorganisms also have a phytase that degrades phytic acid, so that ruminants can effectively utilize phytate-phosphorus that is not available to other mammals. However, if a large amount of cereals or cereal meals containing a large amount of organic phosphorus such as phytic acid is administered to ruminants, the intake of phosphorus will be excessive, and there is a risk of urolithiasis and skeletal formation disorder due to increased excretion of calcium in the body. There is a problem of becoming higher. Therefore, at present, the dosage as feed must be limited.
小麦、大麦、米、大豆、トウモロコシ等の穀類の加工処理では、胚芽やふすま、糠などの副産物が多量に生じるが、これらの副産物の主成分はデンプン及びセルロースであり、反芻動物の有効な飼料となる。したがって、穀類産業副産物の有効利用と反芻動物の飼養効率を増大するためには、これらの副産物の最大限の利用が望まれる。しかし、これらの副産物には、上記のようにフィチン酸態リンが多く含まれるために、現状では、これらの穀類の反芻動物飼料への添加配合量は、最大でも１０％程度まであり、それ以上の有効利用はできないのが現状である。したがって、穀類産業副産物として大量に発生する、穀類糠や、穀類粉砕物等の有効利用と反芻動物の飼養効率の増大を図り、反芻動物飼料への増大した添加配合を可能とするためには、穀類糠や、穀類粉砕物等からのフィチン酸態リンの除去や低減化を図る必要があり、かつ、該穀類糠や、穀類粉砕物等の改質を飼料の製造現場で実用的に適用できる、有効で、簡便かつ安価な処理手段を開発する必要がある。 In the processing of cereals such as wheat, barley, rice, soybeans, and corn, by-products such as germs, bran, and straw are produced in large quantities. The main components of these by-products are starch and cellulose, which is an effective feed for ruminants. It becomes. Therefore, in order to increase the effective use of cereal industry by-products and the breeding efficiency of ruminants, the maximum use of these by-products is desired. However, since these by-products contain a large amount of phytic acid phosphorus as described above, the amount of these cereals added to ruminant feed is at most about 10%, more than that. Currently, it is not possible to effectively use. Therefore, in order to increase the effective use of cereal meal and crushed cereals and the efficiency of ruminant feeding that occur in large quantities as a cereal industry by-product, and to allow increased addition to ruminant feed, It is necessary to remove or reduce phytic acid phosphorus from cereal meal and pulverized cereals, and the modification of cereal meal and pulverized cereals can be applied practically at the production site of feed. There is a need to develop effective, simple and inexpensive processing means.
本発明の課題は、改質処理した穀類糠或いは穀類粉砕物を配合することにより、動物の有用な飼料原料である穀類糠或いは穀類粉砕物を増大した量で有効に利用することを可能とした動物飼料を提供すること、特に、反芻動物のような動物飼料として穀類糠或いは穀類粉砕物を増大した量で有効に利用することを図る上で障害となる穀類糠或いは穀類粉砕物中の有機態リンを除去、減少させることによって穀類糠或いは穀類粉砕物を改質処理し、該飼料原料を増大した量で有効に利用することを可能とした動物飼料を提供すること、及び、該穀類糠或いは穀類粉砕物の改質処理手段として、飼料製造に際して実用的に適用できる有効で、簡便かつ安価な処理手段を提供することにある。 An object of the present invention is to enable effective use of an increased amount of cereal meal or cereal pulverized material, which is a useful feed material for animals, by blending the modified cereal meal or cereal pulverized product. The organic state in cereal meal or pulverized grains that hinders the provision of animal feed, in particular the effective use of increased amounts of cereal meal or cereal grains as animal feed such as ruminants Providing an animal feed that can effectively use the feed raw material in an increased amount by modifying and modifying the cereal meal or the pulverized cereal by removing and reducing phosphorus, and the cereal meal or An object of the present invention is to provide an effective, simple and inexpensive processing means that can be applied practically in the production of feed as a modification processing means for pulverized cereals.
本発明者は、上記課題を解決すべく、動物飼料原料として用いる穀類糠或いは穀類粉砕物中の有機態リンを除去、減少させるための飼料製造現場で実用的に適用できる有効な処理手段について鋭意検討する中で、穀類糠或いは穀類粉砕物を飼料製造原料として利用するに際して、該穀類糠或いは穀類粉砕物を水洗浄することにより、穀類糠或いは穀類粉砕物中の有機態リンを除去、減少させることができることを見出し、更に、該洗浄をカルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液で行うことにより、効果的に有機態リンを除去、減少させることができることを見出し、本発明を完成するに至った。 In order to solve the above-mentioned problems, the present inventor has earnestly devised an effective treatment means that can be practically applied at a feed production site for removing and reducing organic phosphorus in cereal meal or cereal pulverized material used as an animal feed raw material. During the study, when using the cereal meal or the pulverized cereal as a feed production raw material, the organic phosphat in the cereal meal or the pulverized cereal is removed and reduced by washing the cereal meal or the pulverized cereal with water. Further, it was found that organic phosphorus can be effectively removed and reduced by performing the washing with an aqueous solution containing a chelate compound composed of a carboxylic acid or a carboxylate, and the present invention It came to be completed.
すなわち、本発明は穀類糠或いは穀類粉砕物を動物飼料用原料として用いるに際し、穀類糠或いは穀類粉砕物を水、又は、カルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液で洗浄処理することにより、穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させ、飼料への添加量増大を可能とした動物飼料用穀類糠或いは穀類粉砕物を製造する方法からなる。この方法によって改質された動物飼料用穀類糠或いは穀類粉砕物は、特に、反芻動物用の飼料用原料として有利に利用することができ、該飼料用原料の飼料への添加量を増大することを可能として、該飼料用原料の動物飼料への添加配合量を、動物飼料全量に対して、１０重量％以上とすることを可能として、該飼料用原料の利用を大幅に増進することができる。 That is, in the present invention, when using cereal meal or pulverized cereal as a raw material for animal feed, the cereal meal or pulverized cereal is washed with water or an aqueous solution containing a chelate compound composed of carboxylic acid or carboxylate. Thus, the organic phosphorus in the cereal meal or the pulverized cereal is removed and reduced, and the cereal meal or the pulverized cereal for animal feed that can increase the amount added to the feed is produced. The cereal meal for animal feed modified by this method or the pulverized cereal can be advantageously used as a feed ingredient for ruminants, and increase the amount of the feed ingredient added to the feed. The amount of the feed raw material added to the animal feed can be 10% by weight or more based on the total amount of the animal feed, and the use of the feed raw material can be greatly enhanced. .
本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法において、穀類糠或いは穀類粉砕物中の有機体リンの除去、減少のための洗浄処理に用いられカルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液のキレート化合物としては、クエン酸、コハク酸、フタル酸、或いはＥＤＴＡ、又はそれらの塩を挙げることができる。また、本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法における動物飼料用穀類糠或いは穀類粉砕物の具体例としては、小麦、大麦、米、大豆、或いはトウモロコシのふすま或いは糠、又は胚芽或いは該穀類の粉砕物等を挙げることができる。なお、前記米は、玄米や分搗き米等、表面に糠が残存している状態の方が好ましい。 Chelate compound comprising carboxylic acid or carboxylic acid salt used for washing treatment for removal and reduction of organic phosphorus in cereal meal or cereal cereal product in the method for producing cereal meal or cereal product for animal feed of the present invention Examples of the chelate compound of the aqueous solution containing citrate, citric acid, succinic acid, phthalic acid, EDTA, or salts thereof. In addition, as specific examples of the cereal meal for animal feed or the pulverized cereal for the animal feed in the method for producing cereal meal for animal feed or the cereal of the present invention, wheat, barley, rice, soybean, corn bran or straw, or germ Or the ground material etc. of this grain can be mentioned. The rice is preferably in a state in which rice bran remains on the surface, such as brown rice or brewed rice.
本発明は、本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法によって製造された穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させた動物飼料用穀類糠或いは穀類粉砕物自体の発明を包含する。該改質された動物飼料用穀類糠或いは穀類粉砕物は、特に、反芻動物用の飼料用原料として有利に用いることができ、該飼料用原料の利用を大幅に増進することを可能とする。更に、本発明は、本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法によって改質された動物飼料用穀類糠或いは穀類粉砕物を配合し、製造した動物飼料自体の発明を包含する。該動物飼料は、特に反芻動物用の飼料として有利に調製することができ、動物飼料用穀類糠或いは穀類粉砕物を、動物飼料全量に対して、１０重量％以上配合した反芻動物用の飼料として、製品化することを可能とする。 The present invention provides animal feed cereals or cereals obtained by removing organic phosphorus in the cereals or cereals produced by the method for producing animal feed cereals or cereals according to the present invention. It includes its own invention. The modified animal feed cereal meal or pulverized cereal can be advantageously used as a feed ingredient for ruminants, and can greatly enhance the utilization of the feed ingredient. Furthermore, the present invention includes an invention of an animal feed itself produced by blending an animal feed cereal meal or cereal pulverized product modified by the method for producing an animal feed cereal meal or cereal crushed product of the present invention. The animal feed can be advantageously prepared particularly as a ruminant feed. As a feed for ruminants, 10% by weight or more of animal meal cereal meal or cereal pulverized material is blended with respect to the total amount of animal feed. , Making it possible to commercialize.
すなわち具体的には本発明は、［１］穀類糠或いは穀類粉砕物を動物飼料用原料として用いるに際し、穀類糠或いは穀類粉砕物を水、又は、カルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液で洗浄処理することにより、穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させたことを特徴とする飼料への添加量増大を可能とした動物飼料用穀類糠或いは穀類粉砕物の製造方法や、［２］カルボン酸或いはカルボン酸塩からなるキレート化合物が、クエン酸、コハク酸、フタル酸、或いはＥＤＴＡ、又はそれらの塩からなることを特徴とする前記［１］記載の動物飼料用穀類糠或いは穀類粉砕物の製造方法や、［３］飼料への添加量の増大が、動物飼料全量に対して、１０重量％以上であることを特徴とする前記［１］又は［２］記載の動物飼料用穀類糠或いは穀類粉砕物の製造方法や、［４］穀類糠或いは穀類粉砕物が、小麦、大麦、米、大豆、或いはトウモロコシのふすま或いは糠、又は胚芽或いは該穀類の粉砕物であることを特徴とする前記［１］〜［３］のいずれか記載の動物飼料用穀類糠或いは穀類粉砕物の製造方法からなる。 That is, the present invention specifically relates to [1] when using cereal meal or crushed cereal as a raw material for animal feed, the cereal meal or pulverized cereal contains water, or a chelate compound composed of carboxylic acid or carboxylate. Cereal meal or cereal pulverization for animal feed that enables increased addition to feed, characterized by removing and reducing organic phosphorus in cereal meal or cereal cereals [2] The method for producing a product, or [2] the chelate compound comprising a carboxylic acid or a carboxylate salt comprises citric acid, succinic acid, phthalic acid, EDTA, or a salt thereof. The method for producing a cereal meal for animal feed or a pulverized cereal, and [3] The increase in the amount added to the feed is 10% by weight or more with respect to the total amount of the animal feed. ] Or [2] the method for producing animal meal cereal meal or pulverized cereal, or [4] cereal meal or cereal pulverized product is wheat, barley, rice, soybean, corn bran or cocoon, or germ or It consists of a method for producing a cereal meal for animal feed or a pulverized cereal according to any one of the above [1] to [3], which is a pulverized cereal.
また本発明は、［５］前記［１］〜［４］のいずれか記載の動物飼料用穀類糠或いは穀類粉砕物の製造方法によって製造された穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させた動物飼料用穀類糠或いは穀類粉砕物や、［６］動物飼料用穀類糠或いは穀類粉砕物が、反芻動物用の飼料用原料であることを特徴とする前記［５］記載の動物飼料用穀類糠或いは穀類粉砕物や、［７］前記［５］記載の動物飼料用穀類糠或いは穀類粉砕物を配合したことを特徴とする動物飼料や、［８］動物飼料が、前記［５］記載の動物飼料用穀類糠或いは穀類粉砕物を、動物飼料全量に対して、１０重量％以上配合した反芻動物用の飼料であることを特徴とする動物飼料用穀類糠或いは穀類粉砕物の配合量を増大した前記［７］記載の動物飼料からなる。 [5] The present invention also removes organic phosphorus in a cereal meal or cereal pulverized product produced by the method for producing a cereal meal or cereal cereal for animal feed according to any one of [1] to [4]. The reduced cereal meal or ground cereal for animal feed, or [6] cereal meal or cereal ground for animal feed, which is a raw material for feed for ruminants, Animal feed cereal meal or pulverized cereal, [7] Animal feed cereal meal or cereal crushed cereal according to [5] above, [8] Animal feed 5] An animal feed cereal meal or pulverized cereal, wherein the animal meal cereal meal or pulverized cereal is 10% by weight or more based on the total amount of animal feed. From the animal feed according to [7], wherein the blending amount is increased. That.
本発明は、穀類の加工処理で多量に発生する胚芽やふすま、糠などの副産物の動物飼料への有効利用と飼養効率を増大する方法を提供し、該飼料原料を増大した量で有効に利用する方法を提供する。本発明の改質された動物飼料用穀類糠或いは穀類粉砕物の製造方法は、特に、反芻動物用飼料の製造に有利に適用することができ、穀類糠や、穀類粉砕物等の有効利用と反芻動物の飼養効率の増大を図り、反芻動物用飼料への増大した添加配合を可能とした動物飼料を提供することができる。本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法は、飼料製造に際して実用的に適用できることができ、本発明は、穀類糠或いは穀類粉砕物の改質処理手段として有効で、簡便かつ安価な処理手段を提供する。 The present invention provides a method for increasing the use efficiency and feeding efficiency of by-products such as germs, bran, and straw, which are generated in large quantities in the processing of cereals, and effectively using the feed material in an increased amount Provide a way to do it. The method for producing a modified cereal meal for animal feed or crushed cereal of the present invention can be advantageously applied particularly to the production of feed for ruminants, and can be effectively used for cereal meal, crushed cereal, etc. It is possible to provide an animal feed capable of increasing the feeding efficiency of ruminants and enabling an increased addition to the ruminant feed. The method for producing a cereal meal for animal feed or pulverized cereal of the present invention can be applied practically in the production of feed, and the present invention is effective, simple and inexpensive as a means for modifying the cereal meal or crushed cereal. Providing a simple processing means.
本発明は、穀類糠或いは穀類粉砕物を動物飼料用原料として用いるに際し、穀類糠或いは穀類粉砕物を水、又は、カルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液で洗浄処理することにより、穀類糠或いは穀類粉砕物中の有機体リンを除去、減少させ、飼料への添加量増大を可能とした改質された動物飼料用穀類糠或いは穀類粉砕物を製造することからなる。本発明における穀類糠或いは穀類粉砕物としては、デンプンやセルロースを主成分とする穀類糠或いは穀類粉砕物を用いることができ、特に限定されないが、小麦、大麦、米、大豆、或いはトウモロコシのふすま或いは糠、又は胚芽或いは該穀類の粉砕物を挙げることができる。これらのものは、穀類の加工に際して、副産物として多量に発生するものであり、該副産物を動物飼料用原料として有効に利用することができる。 In the present invention, when using cereal meal or cereal pulverized material as a raw material for animal feed, the cereal meal or pulverized cereal is washed with water or an aqueous solution containing a chelate compound composed of carboxylic acid or carboxylate. The present invention comprises producing a modified cereal meal or cereal pulverized product for animal feed that can remove and reduce organic phosphorus in the cereal meal or cereal pulverized product and increase the amount added to the feed. As the cereal meal or cereal pulverized product in the present invention, a cereal meal or cereal pulverized product mainly composed of starch or cellulose can be used, although not particularly limited, wheat, barley, rice, soybean, corn bran or Mention may be made of cocoons, germs or pulverized products of the grains. These products are produced in large quantities as by-products in the processing of cereals, and the by-products can be effectively used as raw materials for animal feed.
本発明において、穀類糠或いは穀類粉砕物中の有機体リンを除去、減少させるための処理は、水、又は、カルボン酸或いはカルボン酸塩からなるキレート化合物を含有する水溶液で、穀類糠或いは穀類粉砕物を洗浄処理することよりなる。かかるキレート化合物としては、クエン酸、コハク酸、フタル酸、或いはＥＤＴＡ、又はそれらの塩を用いることができる。該キレート化合物を含有する水溶液を洗浄液として用いる場合の水溶液中のキレート化合物の濃度としては、キレート化合物によって多少の相違はあるが、おおむね０．１〜２０ｍＭの濃度で用いることができる。穀類糠或いは穀類粉砕物中の有機体リンの除去は、水洗浄によってもかなりの部分を除去することができるが、水溶液中に該キレート化合物を含有させることにより、その洗浄除去効果を著しく高めることができる。その理由は、水溶液中のキレート化合物により、穀類糠或いは穀類粉砕物中のフィチン酸などの有機体リンが、カルシウム、亜鉛、マグネシウム、鉄等のミネラルのイオンと結合して不溶性の沈殿を形成するのを阻止するためであると推測される。該キレート化合物としては、特に限定はないが、該化合物が飼料中に残存することを考慮すると、クエン酸、コハク酸のようなキレート化合物が特に好ましい。なお、本発明で使用する水又は水溶液の温度は高いほど好ましいが、穀類粉砕物に含まれる澱粉のα化を防ぐために６０度を超えない温度の高温水又は高温の水溶液とするのがよい。 In the present invention, the treatment for removing and reducing organic phosphorus in the cereal meal or cereal pulverized product is water or an aqueous solution containing a chelate compound consisting of carboxylic acid or carboxylic acid salt, and cereal meal or cereal pulverization. It consists of washing the object. As such a chelate compound, citric acid, succinic acid, phthalic acid, EDTA, or a salt thereof can be used. When the aqueous solution containing the chelate compound is used as a cleaning solution, the concentration of the chelate compound in the aqueous solution may vary depending on the chelate compound, but it can be generally used at a concentration of 0.1 to 20 mM. The removal of organic phosphorus in cereal meal or pulverized cereals can remove a significant portion even by washing with water, but by containing the chelate compound in an aqueous solution, the washing removal effect can be remarkably enhanced. Can do. The reason for this is that organic phosphorus such as phytic acid in cereal meal or pulverized cereals binds to ions of minerals such as calcium, zinc, magnesium, and iron to form an insoluble precipitate by a chelate compound in an aqueous solution. It is presumed to prevent this. The chelate compound is not particularly limited, but a chelate compound such as citric acid and succinic acid is particularly preferable in consideration that the compound remains in the feed. In addition, although the temperature of the water or aqueous solution used by this invention is so preferable that it is high, in order to prevent the gelatinization of the starch contained in a grain ground material, it is good to set it as the high temperature water or the high temperature aqueous solution of the temperature which does not exceed 60 degree | times.
本発明において、穀類糠或いは穀類粉砕物中の有機体リンの除去のための洗浄処理は、穀類糠或いは穀類粉砕物を、本発明における洗浄液と混合処理し、洗浄した後、洗浄液を分離・除去することにより行われる。該洗浄処理における洗浄液の混合量は、その洗浄処理の効果及び操作の容易性を考慮して、被洗浄対象ごとに適宜決定することができるが、通常、被洗浄対象の容量に対して、３〜１０倍の洗浄液を混合して、３０ｒｐｍで３分間以上撹拌して洗浄処理を行うことが好ましい。洗浄回数は、複数回行うことができるが、通常、１〜３回の洗浄で効果的なリンの除去を行うことができる。洗浄処理後の洗浄液の分離は、適宜の手段により行うことができる。例えば、ろ過や、遠心分離、或いはそれらを併用して実施することができる。 In the present invention, the washing treatment for removing organic phosphorus in the cereal meal or the pulverized cereal is performed by mixing the cereal meal or the pulverized cereal with the washing liquid in the present invention, washing, and then separating and removing the washing liquid. Is done. The mixing amount of the cleaning liquid in the cleaning process can be appropriately determined for each object to be cleaned in consideration of the effect of the cleaning process and the ease of operation. It is preferable to perform a cleaning treatment by mixing 10 to 10 times the cleaning liquid and stirring at 30 rpm for 3 minutes or more. The number of washings can be performed a plurality of times, but in general, effective phosphorus removal can be performed by 1 to 3 washings. Separation of the cleaning liquid after the cleaning treatment can be performed by an appropriate means. For example, filtration, centrifugation, or a combination thereof can be performed.
本発明において、洗浄処理により穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させた動物飼料用穀類糠或いは穀類粉砕物は、改質された動物飼料製造用の原料として調製することができる。該動物飼料製造用の原料として調製するに際して、該動物飼料製造用の原料は、洗浄処理後の洗浄液を分離した（半乾燥）状態で、或いは、更に、脱水、乾燥した状態の調整品として、調製することができる。洗浄液を分離した（半乾燥）状態のものは、該動物飼料用穀類糠或いは穀類粉砕物を、直接、動物飼料製造のための発酵原料として供することができる。 In the present invention, the organic phosphorus in the cereal meal or cereal pulverized product is removed by washing treatment, and the reduced cereal meal or cereal cereal product for animal feed is prepared as a modified raw material for animal feed production. Can do. When preparing as a raw material for the production of animal feed, the raw material for the production of animal feed is in a state where the washing liquid after the washing treatment is separated (semi-dry), or further, as an adjusted product in a dehydrated and dried state, Can be prepared. In the separated (semi-dry) state of the washing liquid, the animal feed cereal meal or cereal pulverized product can be directly used as a fermentation raw material for animal feed production.
本発明の穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させ改質した動物飼料用穀類糠或いは穀類粉砕物は、該飼料原料を用いて動物用の飼料として調製することができる。特に、穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させ改質した動物飼料用原料は、反芻動物用の飼料として有利に調製することができ、動物飼料用穀類糠或いは穀類粉砕物を、動物飼料全量に対して、１０重量％以上配合した反芻動物用の飼料として、製品化することができる。本発明において、本発明の方法により、穀類糠或いは穀類粉砕物中の有機体リンを除去し、減少させ改質した動物飼料用穀類糠或いは穀類粉砕物を飼料原料として用いて、動物用飼料を調製するに際しては、該飼料原料を用いるほか、適宜、動物用飼料の調製に際して配合或いは添加されている公知の配合成分及び添加剤を配合或いは添加することができる。 The cereal meal or cereal pulverized product for animal feed, which is obtained by removing and reducing organic phosphorus in the cereal meal or cereal pulverized product of the present invention, can be prepared as animal feed using the feed material. . In particular, animal feed ingredients that have been modified by removing and reducing organic phosphorus in cereal meal or cereal cereals can be advantageously prepared as feed for ruminants. The product can be commercialized as a ruminant feed containing 10% by weight or more based on the total amount of animal feed. In the present invention, the method according to the present invention removes organic phosphorus in cereal meal or cereal pulverized material, and uses the reduced cereal meal or cereal pulverized product for animal feed as a feed raw material. In preparation, in addition to using the feed raw material, known blending components and additives that are blended or added when preparing animal feed can be blended or added as appropriate.
以下、実施例により本発明をより具体的に説明するが、本発明の技術的範囲はこれらの例示に限定されるものではない。 EXAMPLES Hereinafter, although an Example demonstrates this invention more concretely, the technical scope of this invention is not limited to these illustrations.
［各種洗浄液を用いた飼料中の有機態リン化合物の除去効果］ [Removal effect of organic phosphorus compounds in feed using various cleaning solutions]
＜試験方法＞
米糠に、重量比で３倍量の下記の組成の溶液を添加し、３０ｒｐｍで３分間攪拌して吸引ろ過を行い、再度同じ溶液を添加して攪拌及びろ過を行った。得られた残渣を１１０℃で５時間加熱し、完全に乾燥した。得られた乾燥物から１００ｍｇを採取し、濃硫酸−濃硝酸−過塩素酸存在下で湿式灰化を行った。完全に湿式灰化された試料についてFiske and Subbarow法に従って全リン含量を測定した。
水；
０．１ｍＭ ＥＤＴＡ ３Ｋ水溶液；
１ｍＭ ＥＤＴＡ ３Ｋ水溶液；
１０ｍＭ ＥＤＴＡ ３Ｋ水溶液；
５ｍＭ クエン酸ナトリウム水溶液；
２０ｍＭ クエン酸ナトリウム水溶液。
<Test method>
To the rice bran, a solution having the following composition in a weight ratio of 3 times was added, stirred at 30 rpm for 3 minutes, subjected to suction filtration, added again with the same solution, and stirred and filtered. The resulting residue was heated at 110 ° C. for 5 hours and dried completely. 100 mg was collected from the obtained dried product and wet ashed in the presence of concentrated sulfuric acid-concentrated nitric acid-perchloric acid. The total phosphorus content was measured according to Fiske and Subbarow method on the fully wet ashed sample.
water;
0.1 mM EDTA 3K aqueous solution;
1 mM EDTA 3K aqueous solution;
10 mM EDTA 3K aqueous solution;
5 mM aqueous sodium citrate solution;
20 mM sodium citrate aqueous solution.
＜結果＞
図１（米糠における水および種々の濃度のＥＤＴＡ水溶液およびクエン酸ナトリウム水溶液によるリン除去効果）に示すように、３倍量の水で２回洗浄するだけで米糠中の全リン含量は半分以下に低下した。ＥＤＴＡ水溶液及びクエン酸ナトリウム水溶液ではその効果が著しく増大し、また各水溶液の濃度上昇に伴って効果が増大した。フィチン酸などの有機態リン化合物がカルシウムイオンや鉄イオンなどと不溶性の沈殿を形成するのを抑止したため、効果的にリンが除去されたと推測される。
<Result>
As shown in Fig. 1 (phosphorus removal effect of water and various concentrations of EDTA aqueous solution and sodium citrate aqueous solution in rice bran), the total phosphorus content in rice bran can be reduced to less than half simply by washing twice with 3 times the amount of water. Declined. The effect of EDTA aqueous solution and sodium citrate aqueous solution increased remarkably, and the effect increased with increasing concentration of each aqueous solution. It is presumed that phosphorus was effectively removed because organic phosphorus compounds such as phytic acid were prevented from forming insoluble precipitates with calcium ions and iron ions.
［洗浄回数による飼料中の有機態リン化合物の除去効果への影響］ [Effects of the number of washings on the removal effect of organic phosphorus compounds in feed]
＜試験方法＞
洗浄液の洗浄回数による飼料中の有機態リン化合物の除去効果への影響について検討した。５ｍＭクエン酸ナトリウム水溶液で、１回から５回まで洗浄し、実施例１の方法により、残存全リン含量を測定した。
<Test method>
The effect of the number of washings on the removal of organic phosphorus compounds in the feed was examined. Washing was performed 1 to 5 times with a 5 mM sodium citrate aqueous solution, and the residual total phosphorus content was measured by the method of Example 1.
＜結果＞
結果を、図２（５ｍＭクエン酸ナトリウム水溶液による洗浄回数が米糠中の残存全リン含量に及ぼす影響）及び表１（多重比較検定）に示す。図２に示されるように、洗浄回数の増大によって米糠中の残存全リン含量は低下した。表１に示されるようにTukeyの多重比較検定によると、３回洗浄とそれ以上の４回及び５回洗浄との間で有意差が見られなくなることから、洗浄回数は３回で十分な効果が得られるものと考えられた。
<Result>
The results are shown in FIG. 2 (influence of the number of washings with 5 mM sodium citrate aqueous solution on the residual total phosphorus content in rice bran) and Table 1 (multiple comparison test). As shown in FIG. 2, the total phosphorus content in the rice bran decreased as the number of washings increased. As shown in Table 1, according to Tukey's multiple comparison test, there is no significant difference between 3 washings and 4 or 5 washings. Was considered to be obtained.
本発明は、穀類の加工処理で多量に発生する胚芽やふすま、糠などの副産物の動物飼料への有効利用と飼養効率を増大する方法を提供し、該飼料原料を増大した量で有効に利用する方法を提供する。本発明の改質された動物飼料用穀類糠或いは穀類粉砕物の製造方法は、特に、反芻動物用飼料の製造に有利に適用することができ、穀類糠や、穀類粉砕物等の有効利用と反芻動物の飼養効率の増大を図り、反芻動物用飼料への増大した添加配合を可能とした動物飼料を提供することができる。本発明の動物飼料用穀類糠或いは穀類粉砕物の製造方法は、飼料製造に際して実用的に適用することができ、本発明は、穀類糠或いは穀類粉砕物の改質処理手段として有効で、簡便かつ安価な処理手段を提供する。
The present invention provides a method for increasing the use efficiency and feeding efficiency of by-products such as germs, bran, and straw, which are generated in large quantities in the processing of cereals, and effectively using the feed material in an increased amount Provide a way to do it. The method for producing a modified cereal meal for animal feed or crushed cereal of the present invention can be advantageously applied particularly to the production of feed for ruminants, and can be effectively used for cereal meal, crushed cereal, etc. It is possible to provide an animal feed capable of increasing the feeding efficiency of ruminants and enabling an increased addition to the ruminant feed. The method for producing a cereal meal or cereal pulverized product for animal feed according to the present invention can be applied practically during the production of feed, and the present invention is effective, simple and effective as a modification treatment means for cereal meal or cereal cereal. Provide inexpensive processing means.
Claims (8)
The animal feed is a ruminant feed comprising 10% by weight or more of the animal feed cereal meal or the cereal pulverized product according to claim 5 based on the total amount of the animal feed. Or the animal feed of Claim 7 which increased the compounding quantity of the grain ground material.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019139210A1 (en) * | 2018-01-09 | 2019-07-18 | 김순태 | Extruded rice bran puffs for supplementary animal feed, and method for producing same |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4848268A (en) * | 1971-10-18 | 1973-07-09 | ||
| JPS5016278B1 (en) * | 1970-10-12 | 1975-06-11 | ||
| JPH0423958A (en) * | 1990-05-17 | 1992-01-28 | Nippon Flour Mills Co Ltd | Bran-processed food and production thereof |
| JPH05336907A (en) * | 1992-06-05 | 1993-12-21 | Nippon Flour Mills Co Ltd | Production of processed wheat bran |
| JPH09121780A (en) * | 1995-10-31 | 1997-05-13 | Morinaga & Co Ltd | Production of soybean protein |
| US5853779A (en) * | 1993-05-11 | 1998-12-29 | Nichimo Co., Ltd. | Process for preparing grain product |
| US6774288B1 (en) * | 1997-07-07 | 2004-08-10 | Basf Plant Science L.L.C. | Animal feed with low phytic acid, oil, burdened and protein laden grain |
| JP2005515763A (en) * | 2002-01-24 | 2005-06-02 | カーギル・インコーポレーテッド | Animal feed with low phosphorus concentration and method for producing the same |
| JP2006217900A (en) * | 2005-02-14 | 2006-08-24 | J-Oil Mills Inc | Soybean embryo protein composition |
| JP2010136683A (en) * | 2008-12-12 | 2010-06-24 | Toyohashi Univ Of Technology | Method for producing feed |
-
2011
- 2011-06-24 JP JP2011140036A patent/JP2013005750A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5016278B1 (en) * | 1970-10-12 | 1975-06-11 | ||
| JPS4848268A (en) * | 1971-10-18 | 1973-07-09 | ||
| JPH0423958A (en) * | 1990-05-17 | 1992-01-28 | Nippon Flour Mills Co Ltd | Bran-processed food and production thereof |
| JPH05336907A (en) * | 1992-06-05 | 1993-12-21 | Nippon Flour Mills Co Ltd | Production of processed wheat bran |
| US5853779A (en) * | 1993-05-11 | 1998-12-29 | Nichimo Co., Ltd. | Process for preparing grain product |
| JPH09121780A (en) * | 1995-10-31 | 1997-05-13 | Morinaga & Co Ltd | Production of soybean protein |
| US6774288B1 (en) * | 1997-07-07 | 2004-08-10 | Basf Plant Science L.L.C. | Animal feed with low phytic acid, oil, burdened and protein laden grain |
| JP2005515763A (en) * | 2002-01-24 | 2005-06-02 | カーギル・インコーポレーテッド | Animal feed with low phosphorus concentration and method for producing the same |
| JP2006217900A (en) * | 2005-02-14 | 2006-08-24 | J-Oil Mills Inc | Soybean embryo protein composition |
| JP2010136683A (en) * | 2008-12-12 | 2010-06-24 | Toyohashi Univ Of Technology | Method for producing feed |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019139210A1 (en) * | 2018-01-09 | 2019-07-18 | 김순태 | Extruded rice bran puffs for supplementary animal feed, and method for producing same |
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