JP2011251860A - Granular organic fertilizer and method for manufacturing the same - Google Patents

Granular organic fertilizer and method for manufacturing the same Download PDF

Info

Publication number
JP2011251860A
JP2011251860A JP2010125486A JP2010125486A JP2011251860A JP 2011251860 A JP2011251860 A JP 2011251860A JP 2010125486 A JP2010125486 A JP 2010125486A JP 2010125486 A JP2010125486 A JP 2010125486A JP 2011251860 A JP2011251860 A JP 2011251860A
Authority
JP
Japan
Prior art keywords
organic fertilizer
granulation
weight
leather powder
granular organic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2010125486A
Other languages
Japanese (ja)
Other versions
JP5610517B2 (en
Inventor
Eiji Fujisawa
英司 藤澤
Teppei Komiyama
鉄兵 小宮山
Masayuki Setagawa
正之 瀬田川
Katsu Iijima
克 飯島
Naoto Togashi
直人 冨樫
Miyuki Iizuka
美由紀 飯塚
Takao Ikeda
隆夫 池田
Tomotaka Asano
智孝 浅野
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
National Federation of Agricultural Cooperative Associations
Asahi Sangyo Co Ltd
Asahi Industries Co Ltd
Original Assignee
National Federation of Agricultural Cooperative Associations
Asahi Sangyo Co Ltd
Asahi Industries Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Federation of Agricultural Cooperative Associations, Asahi Sangyo Co Ltd, Asahi Industries Co Ltd filed Critical National Federation of Agricultural Cooperative Associations
Priority to JP2010125486A priority Critical patent/JP5610517B2/en
Publication of JP2011251860A publication Critical patent/JP2011251860A/en
Application granted granted Critical
Publication of JP5610517B2 publication Critical patent/JP5610517B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses

Abstract

PROBLEM TO BE SOLVED: To provide a granular organic compound fertilizer having sufficient physical and chemical properties to endure mechanical fertilizing etc., while it is mainly made from steamed leather powder as a raw material at a low cost by making it possible to compound the steamed leather powder as a raw material of the granular organic compound fertilizer much higher than current use (30-40% to the total raw material).SOLUTION: This granular organic fertilizer is manufactured by mixing 50-75 wt.% steamed leather powder, 15-48 wt.% organic fertilizer and 2-10 wt.% granulation accelerator, granulating and drying. The steamed leather powder has bulk specific gravity of not smaller than 0.8 and a maximum water content of not higher than 450 wt.%.

Description

この発明は粒状有機肥料及びその製造方法に関し、特に低コスト高蛋白質有機原料である蒸製皮革粉を主な原料とした粒状有機肥料及びその製造法に関する。   The present invention relates to a granular organic fertilizer and a method for producing the same, and more particularly to a granular organic fertilizer mainly using steamed leather powder, which is a low-cost, high-protein organic raw material, and a method for producing the same.

消費者の安全・安心な作物への要望から、有機農産物、特別栽培農産物など、有機肥料を主体にした肥料による作物生産が増加している。また低コスト複合肥料の生産方式として採用されている粒状配合肥料工場においても、有機入り複合肥料の原料として、配合適性に合致した物理化学性を保有し、低コストな粒状有機肥料が求められている。このような有機肥料に関しては本願出願人も既に多数の提案を行っているところである(例えば、特許文献1)。   Due to consumer demand for safe and secure crops, crop production using fertilizers mainly composed of organic fertilizers such as organic farm products and specially grown farm products is increasing. In addition, granular compound fertilizer factories that have been adopted as production methods for low-cost compound fertilizers also require low-cost granular organic fertilizers that possess physicochemical properties that match compounding suitability as raw materials for organic-containing compound fertilizers. Yes. With regard to such organic fertilizers, the present applicant has already made many proposals (for example, Patent Document 1).

一方有機原料の状況としては、BSE、鶏インフルエンザなど海外畜産病害発生による畜産関連商品の輸入規制やバイオエタノールなどの穀物生産物の燃料向けへの需要増加、また中国・発展途上国における穀物系食料から畜産物系食料への移行による飼料原料の需要増により、特に肥料向け有機原料は非常にタイトな状況にある。   On the other hand, regarding organic raw materials, import restrictions on livestock-related products due to the occurrence of overseas livestock diseases such as BSE and poultry influenza, increased demand for fuel for cereal products such as bioethanol, and cereal foods in China and developing countries Due to the increase in demand for feed raw materials due to the shift from livestock to livestock products, organic raw materials for fertilizers are particularly tight.

その様な状況の中、動物系有機原料の一つである蒸製皮革粉は、皮革産業における皮革屑を原料に生産され、飼料用には使用されないことから、高蛋白でありながら低コストな有機質肥料として評価されている。本願出願人も、粒状配合肥料の製造にあたって蒸製皮革粉を原材料に使用することを例示している(例えば、特許文献2)。   Under such circumstances, steamed leather powder, one of animal organic raw materials, is produced from leather scraps in the leather industry and is not used for feed. It is evaluated as a fertilizer. The present applicant also exemplifies the use of steamed leather powder as a raw material in the production of a granular compound fertilizer (for example, Patent Document 2).

しかしながら、蒸製皮革粉は繊維状蛋白質であることから粉砕性・凝集性に欠け、粒状有機肥料の原料としては使用しにくく、粒状有機肥料に要求される造粒性や、製品の物性確保の制約から、原料全体に対して3〜4割の配合が使用限界であると認識されていた。   However, steamed leather powder is a fibrous protein, so it lacks pulverization and agglomeration and is difficult to use as a raw material for granular organic fertilizers. Therefore, it was recognized that 30 to 40% of the total amount of raw materials was the use limit.

特開平3−237084号公報JP-A-3-237084 特開2007−290948号公報JP 2007-290948 A

そこで、この発明は、従来、粒状有機肥料に要求される造粒性や、製品の物性確保の制約から、原料全体に対して3〜4割の配合が使用限界であると認識されていた蒸製皮革粉を粒状有機複合肥料の原料として従来より多く配合して使用することを可能にし、蒸製皮革粉を原料の主体にしていながら機械施肥等に耐えうる充分な物理化学性を備えた粒状有機複合肥料を低コストで提供することを目的にしている。   Therefore, this invention has been conventionally recognized as a steaming that has been recognized as the use limit of 30 to 40% of the total raw materials due to the granulation properties required for the granular organic fertilizer and the constraints of ensuring the physical properties of the product. Granular organic composite with sufficient physicochemical properties that can withstand mechanical fertilization, etc., while allowing leather powder to be blended and used more as a raw material for granular organic composite fertilizer than ever before The purpose is to provide fertilizer at low cost.

本願の請求項1記載の発明は、
蒸製皮革粉50〜75重量%と、有機質肥料15〜48重量%と、造粒促進材2〜10重量%とを混合し、造粒、乾燥させてなる粒状有機肥料
である。
The invention according to claim 1 of the present application is
It is a granular organic fertilizer obtained by mixing 50 to 75% by weight of steamed leather powder, 15 to 48% by weight of organic fertilizer and 2 to 10% by weight of a granulation accelerator, granulating and drying.

請求項2記載の発明は、
前記蒸製皮革粉は、嵩比重0.8以上で、最大容水量450重量%以下であることを特徴とする請求項1記載の粒状有機肥料
である。
The invention according to claim 2
2. The granular organic fertilizer according to claim 1, wherein the steamed leather powder has a bulk specific gravity of 0.8 or more and a maximum water capacity of 450% by weight or less.

請求項3記載の発明は、
蒸製皮革粉、有機質肥料、造粒促進材を混合した後、粉砕して粒度を500ミクロン通過割合で40%以上70%以下に調整した後に造粒することを特徴とする請求項1又は2記載の粒状有機肥料
である。
The invention described in claim 3
3. The steamed leather powder, the organic fertilizer, and the granulation accelerator are mixed and then pulverized to adjust the particle size to 40% or more and 70% or less at a passage rate of 500 microns, and then granulated. Of granular organic fertilizer.

請求項4記載の発明は、
窒素全量を9%以上含有することを特徴とする請求項1乃至3のいずれか一項記載の粒状有機肥料
である。
The invention according to claim 4
The granular organic fertilizer according to any one of claims 1 to 3, wherein the total amount of nitrogen is 9% or more.

請求項5記載の発明は、
蒸製皮革粉50〜75重量%と、有機質肥料15〜48重量%と、造粒促進材2〜10重量%とを混合し、造粒、乾燥を行う粒状有機肥料の製造方法
である。
The invention according to claim 5
It is the manufacturing method of the granular organic fertilizer which mixes 50-75 weight% of steamed leather powder, 15-48 weight% of organic fertilizer, and 2-10 weight% of granulation promoters, and performs granulation and drying.

請求項6記載の発明は、
前記蒸製皮革粉は、嵩比重0.8以上で、最大容水量450重量%以下であることを特徴とする請求項5記載の粒状有機肥料の製造方法
である。
The invention described in claim 6
6. The method for producing a granular organic fertilizer according to claim 5, wherein the steamed leather powder has a bulk specific gravity of 0.8 or more and a maximum water capacity of 450% by weight or less.

請求項7記載の発明は、
蒸製皮革粉、有機質肥料、造粒促進材を混合した後、粉砕して粒度を500ミクロン通過割合で40%以上70%以下に調整した後に造粒することを特徴とする請求項5又は6記載の粒状有機肥料の製造方法
である。
The invention described in claim 7
7. The steamed leather powder, the organic fertilizer and the granulation accelerator are mixed and then pulverized to adjust the particle size to 40% or more and 70% or less at a passage rate of 500 microns, and then granulated. This is a method for producing granular organic fertilizer.

請求項8記載の発明は、
前記造粒工程の前に、混練工程を実施し、水分率35%以下で造粒することを特徴とする請求項5乃至7のいずれか一項記載の粒状有機肥料の製造方法
である。
The invention described in claim 8
The method for producing a granular organic fertilizer according to any one of claims 5 to 7, wherein a kneading step is performed before the granulation step and granulation is performed at a moisture content of 35% or less.

請求項9記載の発明は、
造粒工程後に、高速転動整粒又は解砕転動整粒からなる整粒工程を組み合わせることを特徴とする請求項5乃至8のいずれか一項記載の粒状有機肥料
である。
The invention according to claim 9
The granular organic fertilizer according to any one of claims 5 to 8, wherein a granulating step is combined with a granulating step comprising high-speed rolling sizing or pulverizing rolling sizing.

この発明によれば、従来、粒状有機肥料に要求される造粒性や、製品の物性確保の制約から、原料全体に対して3〜4割の配合が使用限界であると認識されていた蒸製皮革粉を粒状有機複合肥料の原料として従来より多く配合して使用することを可能にし、蒸製皮革粉を原料の主体にしていながら機械施肥等に耐えうる充分な物理化学性を備えた粒状有機複合肥料を低コストで提供することができる。   According to this invention, from the past, the granulation required for granular organic fertilizer and the restriction of securing the physical properties of the product, steaming that was recognized as 30 to 40% of the total raw material was the use limit Granular organic composite with sufficient physicochemical properties that can withstand mechanical fertilization, etc., while allowing leather powder to be blended and used more as a raw material for granular organic composite fertilizer than ever before Fertilizer can be provided at low cost.

本発明の製造方法の一例の概略工程を説明する流れ図。The flowchart explaining the outline process of an example of the manufacturing method of this invention.

本願発明は、蒸製皮革粉50〜75重量%と、有機質肥料15〜48重量%と、造粒促進材2〜10重量%とを混合し、造粒、乾燥を行うことにより粒状有機肥料を製造するものである。   In the present invention, 50 to 75% by weight of steamed leather powder, 15 to 48% by weight of organic fertilizer and 2 to 10% by weight of granulation accelerator are mixed, and granulated and dried to produce a granular organic fertilizer. To do.

従来から、蒸製皮革粉は、高蛋白(窒素成分含有率が高い)でありながら低コストな有機質肥料として評価されていた。しかし、繊維状蛋白質であることから粉砕性・凝集性に欠け、粒状有機肥料の原料としては使用しにくく、粒状有機肥料に要求される造粒性や、製品の物性確保の制約から、蒸製皮革粉は原料全体に対して3〜4割の配合が使用限界であると認識されていた。本発明は、蒸製皮革粉を原料の50〜75重量%配合して粒状有機肥料を製造したものである。これによって、高成分な粒状有機複合肥料を提供することができる。   Conventionally, steamed leather powder has been evaluated as a low-cost organic fertilizer with high protein (high nitrogen content). However, since it is a fibrous protein, it lacks pulverization and cohesion, is difficult to use as a raw material for granular organic fertilizer, and is a steamed leather due to the granulation properties required for granular organic fertilizer and the restrictions on securing physical properties of products. It was recognized that the blending of 30 to 40% of the powder was the use limit with respect to the whole raw material. In the present invention, a granular organic fertilizer is produced by blending steamed leather powder in an amount of 50 to 75% by weight of the raw material. Thereby, a high-component granular organic composite fertilizer can be provided.

本発明の粒状有機肥料は、肥料取締法上の有機質肥料を混合し、粒状化した有機複合肥料であり、肥料取締法上は、混合有機質肥料の範疇となるものである。そこで、前記において配合する有機質肥料は、肥料取締法に基づき普通肥料として公定規格で定められているものであればいかなるものでも使用することができる。   The granular organic fertilizer of the present invention is an organic composite fertilizer that is granulated by mixing organic fertilizers according to the fertilizer control method, and falls under the category of mixed organic fertilizers under the fertilizer control method. Therefore, any organic fertilizer to be blended in the above can be used as long as it is defined in the official standard as a normal fertilizer based on the Fertilizer Control Law.

本発明に使用する蒸製皮革粉は、「製革工場及び皮革加工業者より廃出される皮革くずを加圧・蒸解して粉砕したもの」(「ポケット肥料要覧」の肥料用語の解説より)である。生皮のなめし方法により、タンニンなめし、クロムなめしの蒸製皮革粉ができる。タンニンなめしものは6.0〜7.5%、クロムなめしものは、11.0〜12.5%の窒素を含み、通常皮粉(かわこ)と称されているものである。   The steamed leather powder used in the present invention is “pulverized by pressurizing and digesting leather scraps discarded from a leather factory and a leather processor” (from the explanation of fertilizer terms in the “Pocket Fertilizer Manual”). Steamed leather powder with tannin and chrome tanning can be produced by tanning the raw leather. Tannin tanned products contain 6.0-7.5% nitrogen, and chrome tanned products contain 11.0-12.5% nitrogen and are usually referred to as skin powder (kawako).

蒸製皮革粉の配合が使用原料の50重量%未満では皮粉使用によるコスト低減効果が充分でなく(これまでも30〜40%であれば使用可能であった)、高窒素成分を確保出来ないので望ましくない。一方、75重量%を越えると凝集力を与える為の加水量が増加してしまい、生産性低下、エネルギーコスト等の悪化となり、コスト改善効果が十分でなくなるので望ましくない。   If the content of steamed leather powder is less than 50% by weight of the raw material used, the cost reduction effect due to the use of the skin powder is not sufficient (it could be used if it was 30-40% so far), and a high nitrogen component cannot be secured. So undesirable. On the other hand, if it exceeds 75% by weight, the amount of water added to give cohesive force increases, resulting in a decrease in productivity, energy cost, etc., and the cost improvement effect becomes insufficient, which is not desirable.

前記において、バインダーの配合割合を2重量%以上としているのは、これより少ない場合、原料結着力の確保が難しくなるという観点からであり、10重量%以下としているのは、これを越えると肥料成分の確保が難しく、コストアップにもなるという観点からである。   In the above, the blending ratio of the binder is set to 2% by weight or more from the viewpoint that it is difficult to secure the raw material binding force when the content is less than this, and 10% by weight or less is the fertilizer. This is because it is difficult to secure the components and the cost is increased.

使用するバインダーの種類としては、有機入り粒状肥料で使用される一般的バインダーであれば特に限定されるものでない。一例としては、デンプンまたはα化でんぷん、リグニン、ベントナイトやゼオライトなどの粘土鉱物、こんにゃく芋を粉末化する際に副生されるこんにゃくとび粉などを使用することができる。   The type of binder to be used is not particularly limited as long as it is a general binder used for organic fertilizers containing organic matter. As an example, clay minerals such as starch or pregelatinized starch, lignin, bentonite and zeolite, and konjac powder produced as a by-product when konjac flour is pulverized can be used.

前記において、蒸製皮革粉は、嵩比重0.8以上で、最大容水量450重量%以下のものを選抜して使用することが望ましい。   In the above, it is desirable to select and use steamed leather powder having a bulk specific gravity of 0.8 or more and a maximum water capacity of 450% by weight or less.

蒸製皮革粉は、さまざま加工条件で生産される。そこで、蒸製皮革粉として市場に流通しているものであっても、その物性には違いがある。   Steamed leather powder is produced under various processing conditions. Therefore, even if it is in the market as steamed leather powder, there are differences in its physical properties.

通常の皮粉では、成分の安定性、蒸製処理の加工適性からなめし工程で発生するシェービング屑が好んで使用されるが、物性的にスポンジの様に柔らかく比重が軽いという特長がある。そこで、凝集力を付与する為には多量の加水を必要とするのが一般的である。この為、一般的傾向とし蒸製処理後の蒸製皮革粉は嵩比重が低く、保水力が高い。   In normal skin powder, shaving scraps generated in the tanning process are preferably used because of the stability of the components and the suitability for processing in the steaming process. However, the physical properties are soft and light in specific gravity like a sponge. Therefore, a large amount of water is generally required to impart cohesive force. For this reason, as a general tendency, steamed leather powder after steaming has low bulk specific gravity and high water retention.

本願の発明者等は、市場に流通している各生産工場より入手した蒸製皮革粉を物性面で分類し、造粒試験を行うことにより、比重が高く、保水力が低いものが粒状加工的に有利であることを見出した。そして、特定の物性を示す蒸製皮革粉を用いることにより、蒸製皮革粉を原料の主体にしていながら機械施肥等に耐えうる充分な物理化学性を備えた粒状有機複合肥料を提供できるという有効性を確認し、本願発明を完成させたものである。   The inventors of the present application classify steamed leather powder obtained from each production factory distributed in the market in terms of physical properties and conduct a granulation test, so that those with high specific gravity and low water retention are granular processing Has been found to be advantageous. And, by using steamed leather powder showing specific physical properties, it is possible to provide a granular organic composite fertilizer with sufficient physicochemical properties that can withstand mechanical fertilization while using steamed leather powder as the main ingredient. This was confirmed and the present invention was completed.

この特定の物性が前述したように、嵩比重で0.8以上、土壌分析で用いられる最大容水量%で450以下である。   As described above, this specific physical property is 0.8 or more in bulk specific gravity and 450 or less in maximum water content% used in soil analysis.

嵩比重が0.8未満であると、凝集性、粘りが弱まる為、製品硬度が低下し、粉化率が高まる。このため、粒状有機肥料として必要な物理性を確保出来なくなるため好ましくない。   If the bulk specific gravity is less than 0.8, the cohesiveness and stickiness are weakened, so that the product hardness is lowered and the powdering rate is increased. For this reason, since it becomes impossible to ensure physical properties required as a granular organic fertilizer, it is not preferable.

また、最大容水量が450重量%を超えると、原料の吸水力が高まるので、凝集性を与える為の造粒水分が高まり、乾燥工程でエネルギーコストが大きくなるため望ましくない。   On the other hand, when the maximum water volume exceeds 450% by weight, the water absorption capacity of the raw material is increased, so that granulated moisture for imparting cohesiveness is increased, and the energy cost is increased in the drying step, which is not desirable.

なお、本発明において嵩比重は、サンプル約400gを500mLメスシリンダーに入れ、メスシリンダーの底を軽く3回たたき、容積を目盛りで読み取り、重量は中味を自動天秤で量るという操作を3回行い、平均を求めることにより求めている。   In the present invention, the bulk specific gravity is measured three times by putting about 400 g of a sample into a 500 mL measuring cylinder, tapping the bottom of the measuring cylinder lightly three times, reading the volume with a scale, and measuring the weight with an automatic balance. By seeking the average.

また、本発明において最大容水量%は、土壌の測定で使用されるヒルガード法に準じて、次のようにして測定している。容器の底面に穴を開け、評価対象の蒸製皮革粉(絶乾品)を容器に充填し、底面より自然給水させ、容器に充填した蒸製皮革粉にまんべんなく給水されるのを確認し、30分放置させて十分に給水させ、給水量と評価対象の蒸製皮革粉(絶乾品)との比率を求めるものである。   In the present invention, the maximum water content% is measured in the following manner according to the Hilgard method used in soil measurement. Make a hole in the bottom of the container, fill the container with the steamed leather powder to be evaluated (absolutely dried product), let it water naturally from the bottom, and check that the steamed leather powder filled in the container is evenly fed, 30 minutes It is allowed to stand for sufficient water supply, and the ratio between the amount of water supply and the steamed leather powder (an absolute dry product) to be evaluated is determined.

前記の配合の原料は混合した後、適宜加水しながら造粒するが、図1の概略工程図に示されているように、蒸製皮革粉、有機質肥料、造粒促進材を混合した後、粉砕して粒度を500ミクロン通過割合で40%以上70%以下に調整した後に造粒することが望ましい。   The raw materials of the above blending are mixed and then granulated while appropriately adding water. As shown in the schematic process diagram of FIG. 1, steamed leather powder, organic fertilizer, and granulation accelerator are mixed and then pulverized. Then, it is desirable to granulate after adjusting the particle size to 40% or more and 70% or less at a passage rate of 500 microns.

本願の発明等が更に検討を進めたところ、本願発明の粒状有機肥料は、その製造工程において特定の条件で粒状化することがより有利であることが認められた。この特定の条件の一つが、造粒工程の前に、混合した蒸製皮革粉、有機質肥料及び、造粒促進材を粉砕し、粒度を500ミクロン通過割合で40%以上70%以下に調整するものであある。   As a result of further investigation by the invention of the present application, it was recognized that it is more advantageous to granulate the granular organic fertilizer of the present invention under specific conditions in the production process. One of these specific conditions is that the mixed steamed leather powder, organic fertilizer and granulation accelerator are pulverized before the granulation step, and the particle size is adjusted to 40% or more and 70% or less at a passage rate of 500 microns. It is.

500ミクロン通過割合で40%未満の場合、原料粒子の結着力が弱まり、歩留り及び生産性の低下となり、コスト悪化となる。また、品質面でも硬度の低下、粉化率の高まりなど、粒状有機肥料として必要な品質を確保することが難しくなるので望ましくない。   If the passing rate of 500 microns is less than 40%, the binding force of the raw material particles is weakened, the yield and productivity are lowered, and the cost is deteriorated. Further, in terms of quality, it is not desirable because it becomes difficult to ensure the quality necessary for the granular organic fertilizer, such as a decrease in hardness and an increase in the powdering rate.

一方、500ミクロン通過割合で70%より高いと保水力が高まり、造粒適性水分が上昇し、乾燥コストの悪化につながる。また、乾燥前粒状品の硬度が低下し、乾燥工程での粉化が高まり、生産性低下、コストアップのおそれがある。更に、製品品質面でも硬度の低下が起こるおそれがあることから望ましくない。   On the other hand, if it is higher than 70% at a passage rate of 500 microns, the water holding power is increased, the water suitable for granulation is increased, and the drying cost is deteriorated. In addition, the hardness of the granular product before drying is lowered, and powdering in the drying process is increased, which may reduce productivity and increase costs. Further, the product quality is not desirable because hardness may decrease.

前記のように混合した配合原料を粉砕し、粉砕品粒度を500ミクロン通過割合で40%以上70%以下に調整する際に使用する粉砕機としては、奈良式、ハンマーミル、レイモンドミル、パルペライザーなど、一般に使用される粉砕機を使用することができ、特に限定されるものではない。   Nara type, hammer mill, Raymond mill, pulverizer, etc. are used as pulverizers for pulverizing the blended raw materials mixed as described above and adjusting the particle size of the pulverized product to 40% or more and 70% or less at a passage rate of 500 microns A commonly used crusher can be used and is not particularly limited.

本発明においては、上述した配合原料を混合した後、あるいは、上述したように、混合後に粉砕、粒度調整を行った後、図1で概略工程を説明しているように、造粒加工する。   In the present invention, after mixing the above-described blended raw materials, or after pulverization and particle size adjustment after mixing as described above, granulation is performed as described in the schematic steps in FIG.

造粒加工では原料に加水し、ドラム造粒機等で転動し原料の粘りを活用することにより1〜6mm程度の粒径の粒状にする。造粒方式は、特に限定されるものではなく、転動式、押出造粒、圧縮造粒いずれでも可能である。   In the granulation process, water is added to the raw material, and it is rolled with a drum granulator or the like to make use of the viscosity of the raw material to form particles having a particle diameter of about 1 to 6 mm. The granulation method is not particularly limited, and any of rolling type, extrusion granulation, and compression granulation can be used.

この際、引き続く乾燥工程でのエネルギーコストを考慮して、水分率35%以下で造粒することが望ましい。   At this time, it is desirable to granulate with a moisture content of 35% or less in consideration of the energy cost in the subsequent drying step.

また、粒状化する際、図1の概略工程に示したように、前処理として混練すると、より粘りを強くする等の粘度調整ができ、これによって成形性を向上させ、粒状化を促進させることにより生産性、造粒歩留まりを向上させ、また、製品品質を向上させることができるので有利である。   Moreover, when granulating, as shown in the schematic process of FIG. 1, when kneading as a pretreatment, viscosity adjustment such as increasing the viscosity can be performed, thereby improving the moldability and promoting granulation. This is advantageous because it can improve the productivity and the granulation yield, and can improve the product quality.

混練の方法は、有機原料に練り効果を与える機器であれば特に限定されるものでなく、ニーダー、ホイール型混練機、パグミキサーなどを使用することができる。   The kneading method is not particularly limited as long as it is a device that gives a kneading effect to the organic raw material, and a kneader, a wheel-type kneader, a pug mixer, or the like can be used.

なお、一般の粒状肥料で求められる物性値(物理化学性)は、粒度2〜4mmが95%以上、硬度1kgf以上、粉化率1.0%%以下、安息角38度以下、堆積時の固結性がないというものである。   In addition, the physical property value (physicochemical property) calculated | required with a general granular fertilizer is the particle size 2-4mm 95% or more, hardness 1kgf or more, a powdering rate 1.0 %% or less, an angle of repose 38 degrees or less, There is no caking property.

本願では、これらの物性値(物理化学性)を満たすことにより一般の粒状肥料と同等に機械施肥対応や粒状配合肥料の原料として使用することが可能な粒状有機肥料であって、高品質なものを、低コストで提供するようにしている。   In this application, by satisfying these physical property values (physicochemical properties), it is a granular organic fertilizer that can be used as a raw material for mechanical fertilization and granular compound fertilizer as well as general granular fertilizer, and has high quality At low cost.

そこで、前述したように、水分率35%以下で造粒する、好ましくは、混練工程の後に水分率35%以下で造粒することが、製品品質(硬度1kgf以上、粉化率1.0%%以下)を満たす上で望ましい。   Therefore, as described above, granulation is performed at a moisture content of 35% or less, preferably granulation at a moisture content of 35% or less after the kneading step to improve product quality (hardness of 1 kgf or more, powdering rate of 1.0%). % Or less) is desirable.

なお、製品品質(機械施肥特性)を向上させる観点から、圧縮造粒・解砕転動整粒、湿式押出造粒・高速転動整粒などの造粒工程後の整粒工程を組み合わせることが好ましい。   In addition, from the viewpoint of improving product quality (mechanical fertilization characteristics), combining granulation processes after granulation processes such as compression granulation / disintegration rolling sizing, wet extrusion granulation / high speed rolling sizing, etc. preferable.

造粒工程後、必要があれば、図1の概略工程に示したように、整粒を行い、その後、乾燥させて、本発明の粒状有機肥料を製造することができる。   After the granulation step, if necessary, the granulated organic fertilizer of the present invention can be produced by sizing and then drying as shown in the schematic step of FIG.

なお、乾燥させて製造した粒状有機肥料は、図1の概略工程に示したように冷却後、篩別し、包装して製品出荷する。篩別では、篩別機により粒度を2〜4mmに調整する。   The granular organic fertilizer produced by drying is cooled, sieved, packaged and shipped as shown in the schematic process of FIG. In sieving, the particle size is adjusted to 2 to 4 mm with a sieving machine.

乾燥工程では、造粒品を水分率5%以下に乾燥させる。乾燥には、例えば、従来公知の火力乾燥機を用いることができる。水分率を5%以下にすることにより、製品のカビ発生等の防止、物理性硬度を確保し、保存時の変質防止、機械施肥対応時の流動性、粉化防止等の物理性を確保する。   In the drying step, the granulated product is dried to a moisture content of 5% or less. For example, a conventionally known thermal power dryer can be used for drying. By controlling the moisture content to 5% or less, it is possible to prevent the occurrence of mold, etc., and ensure physical hardness, to ensure physical properties such as alteration during storage, fluidity during mechanical fertilization, and prevention of powdering. .

本発明によれば、高蛋白(窒素成分含有率が高い)な蒸製皮革粉を原料成分に50〜75重量%配合しているため、高成分(窒素全量で9%以上)であって、機械施肥特性(製品品質で硬度1kgf以上、粉化率1.0%%以下)を備えた粒状有機肥料を提供することができる。   According to the present invention, 50 to 75% by weight of high-protein (high nitrogen component content) steamed leather powder is blended in the raw material component, so that the high-component (9% or more of the total amount of nitrogen) It is possible to provide a granular organic fertilizer having fertilization characteristics (product quality, hardness of 1 kgf or more, powdering rate of 1.0% or less).

発明者等が検討したところによれば、蒸製皮革粉を原料成分に50〜75重量%配合している本発明では、窒素全量で9%以上、なおかつ、燐酸全量で1%以上という高成分な粒状有機肥料を製造することができた。   According to a study by the inventors, in the present invention in which steamed leather powder is blended in the raw material components in an amount of 50 to 75% by weight, the total amount of nitrogen is 9% or more, and the total amount of phosphoric acid is 1% or more. Granular organic fertilizer could be produced.

なお、本発明において、窒素全量(TN)、燐酸全量(TP)は、肥料取締法に基づき、普通肥料の公定規格を定める件に記載されている保証成分で、肥料分析法(参考資料1:農林水産省農業環境技術研究所 日本肥料検定協会発行、4.1.1 窒素全量、4.2.3 燐酸全量)に記載されている定量方法で算出したものである。   In the present invention, the total amount of nitrogen (TN) and the total amount of phosphoric acid (TP) are guaranteed components described in the official standards for ordinary fertilizer based on the Fertilizer Control Law, and the fertilizer analysis method (reference material 1: Calculated by the quantitative method described in Agricultural Environmental Technology Research Institute, Ministry of Agriculture, Forestry and Fisheries, Japan Fertilizer Examination Association, 4.1.1 Total amount of nitrogen, 4.2.3 Total amount of phosphoric acid).

市販されている蒸製皮革粉(クロムなめしの蒸製皮革粉を用いた)について上述した要領で嵩比重、最大容水量%を測定したところ、表1の通常皮粉の欄に記載されているように、嵩比重:0.7、最大容水量595重量%であった。これを比較対象品として原料に使用した。   When the bulk specific gravity and the maximum water content% were measured in the manner described above for commercially available steamed leather powder (using chrome-tanned steamed leather powder), as described in the normal skin powder column of Table 1. The bulk specific gravity was 0.7, and the maximum water capacity was 595% by weight. This was used as a comparative product in the raw material.

次に、市販されている蒸製皮革粉(クロムなめしの蒸製皮革粉を用いた)ついて上述した要領で嵩比重、最大容水量を測定し、嵩比重0.8以上で、最大容水量450重量%以下であるものを選抜したところ、表1の選抜皮粉の欄に記載されているように、嵩比重:0.82、最大容水量424重量%のものを選抜でき、これを本発明の粒状有機肥料を製造する原料に使用した。

Figure 2011251860
Next, the bulk specific gravity and the maximum water volume were measured as described above for the commercially available steamed leather powder (using chrome-tanned steamed leather powder), the bulk specific gravity was 0.8 or more, and the maximum water volume was 450% by weight. When the following were selected, as described in the column of selected skin powder in Table 1, one having a bulk specific gravity of 0.82 and a maximum water content of 424% by weight can be selected. Used as raw material to produce organic fertilizer.
Figure 2011251860

有機質肥料として油粕、蒸製毛粉、副産植物質肥料、菌体肥料、骨粉を用い、バインダーとしてこんにゃくとび粉を用いた。   Oil cake, steamed hair flour, by-product vegetable fertilizer, fungus body fertilizer, and bone powder were used as organic fertilizers, and konjac flying powder was used as a binder.

各原料を図1の製造工程概略図に示されているように計量し、表2の配合割合(重量%)で合計5kgとなるように配合し、窒素全量を10%以上、燐酸全量は1%以上となるように設計した。

Figure 2011251860
Each raw material is weighed as shown in the schematic diagram of the manufacturing process of FIG. 1, and is blended so that the total proportion is 5 kg in the blending ratio (% by weight) shown in Table 2. Designed to be at least%.
Figure 2011251860

配合原料を混合した後、奈良式粉砕機にて全量を通過させて粉砕した。粉砕粒度は表3に記載の通りである。   After mixing the blended raw materials, the entire amount was passed through a Nara type pulverizer and pulverized. The pulverized particle size is as shown in Table 3.

次いで、混練工程を経ずに、皿形造粒機(径1m、21rpm)に配合原料を投入し、動力噴霧器にて造粒状況を確認しながら加水噴霧し、造粒した。   Next, without passing through the kneading step, the blended raw materials were put into a dish-type granulator (diameter 1 m, 21 rpm), and sprayed with water while confirming the granulation status with a power sprayer, and granulated.

次いで、粒状品を通風棚乾燥機にて、80度熱風で3時間乾燥させた後、2mm、4mmの篩いを使用し2〜4mmの造粒歩留まりを測定し、製品について硬度を木屋式硬度計で測定した。   Next, after drying for 3 hours with hot air at 80 degrees in a ventilation shelf dryer, the granular product is measured for 2 to 4 mm granulation yield using a 2 mm and 4 mm sieve, and the hardness of the product is measured by a Kiyama hardness tester. Measured with

なお、本発明において、硬度は、いずれも、木屋式硬度計で15粒の硬度を測定し、平均を求めたものである。   In the present invention, the hardness is obtained by measuring the hardness of 15 grains with a Kiyama hardness tester and calculating the average.

結果は表3の通りであった。

Figure 2011251860
The results are shown in Table 3.
Figure 2011251860

<嵩比重、最大容水量(重量%)>
表3の結果から、嵩比重:0.7、最大容水量595重量%の通常皮粉が使用されていたもの(試験No.1−1〜1−3)では、製品に対する皮粉使用割合が30%以下の場合(試験No.1−1)では良好な造粒性となったが、皮粉使用割合50%以上では(試験No.1−2及び試験No.1−3)、造粒水分が48%以上と高くなり、造粒歩留、硬度は目標値を大きく低下し、粒状化は困難と考えられた。
<Bulk specific gravity, maximum water volume (% by weight)>
From the results shown in Table 3, in the case where normal skin powder having a bulk specific gravity of 0.7 and a maximum water volume of 595% by weight was used (Test Nos. 1-1 to 1-3), the ratio of skin powder used to the product was In the case of 30% or less (Test No. 1-1), good granulation property was obtained, but in the case where the skin powder was used at 50% or more (Test No. 1-2 and Test No. 1-3), granulation was performed. The moisture content was as high as 48% or more, and the granulation yield and hardness were greatly reduced from the target values, and granulation was considered difficult.

一方、嵩比重:0.82、最大容水量424重量%の選抜皮粉では、皮粉使用割合50%以上でも(試験No.1−4−1)、やや造粒水分は高めとなったが、歩留及び硬度は目標値をクリアし、造粒可能であった。     On the other hand, in the selected skin powder having a bulk specific gravity of 0.82 and a maximum water content of 424% by weight, the granulated water was slightly increased even when the skin powder was used at 50% or more (Test No. 1-4-1). The yield and hardness cleared the target values and could be granulated.

この結果、嵩比重:0.7、最大容水量595重量%の蒸製皮革粉が原料に使用される場合、配合割合が50%を越えると造粒歩留、硬度が目標値を大きく低下し、粒状化が困難になるが、嵩比重:0.82、最大容水量424重量%の蒸製皮革粉では、原料への配合割合が50%を越えても造粒可能であることを確認できた。   As a result, when steamed leather powder having a bulk specific gravity of 0.7 and a maximum water volume of 595% by weight is used as the raw material, if the blending ratio exceeds 50%, the granulation yield and hardness greatly decrease the target value, Although granulation becomes difficult, it was confirmed that the steamed leather powder having a bulk specific gravity of 0.82 and a maximum water content of 424% by weight can be granulated even if the blending ratio to the raw material exceeds 50%.

<粉砕粒度>
この実施例では、粉砕粒度は、粉砕機通過速度により調整し、500ミクロン篩通過割合を粉砕割合として試験No.1−4区を3段階に調整した。
<Grinding particle size>
In this example, the pulverization particle size is adjusted by the pulverizer passing speed, and the test No. The 1-4 district was adjusted to 3 stages.

表3の結果にあるように、500ミクロン通過割合が76.0%と多い1−4−2区では、保水量アップ゜により造粒水分が増加し、造粒歩留まりはやや良化したが、整粒後粒が柔らかめとなり、製品硬度が低下した。     As shown in the results of Table 3, in the 1-4-2 district where the 500 micron passage ratio is as high as 76.0%, the granulation moisture increased due to the increased water retention amount, and the granulation yield was slightly improved. The grain after sizing became softer and the product hardness decreased.

一方、500ミクロン通過割合が37.70%と粉砕粒度を粗めに調整した1−4−3区では、保水量の低下により造粒水分は低下したが、粒のまとまりが悪化し、造粒歩留が悪化した。また、硬度も低下した。     On the other hand, in the 1-4-3 section in which the crushed particle size was coarsely adjusted to 37.70% with a passage of 500 microns, the granulated moisture decreased due to the decrease in the water retention amount, but the grain size deteriorated, and the granulation Yield deteriorated. Moreover, the hardness also decreased.

発明者等が他に行った検討も踏まえると、粒度調整は、500ミクロンパス割合で40%以上、70%以下が良好であると認められた。     In light of other studies conducted by the inventors, it was recognized that the particle size adjustment was good at 40% or more and 70% or less at a 500 micron pass rate.

<バインダーの配合割合>
バインダーの効果確認として、添加区(試験No.1−4−1)と、無添加区(試験No.1−5)を比較した。バインダーを添加しないと造粒性は悪化し、各目標値をやや悪化する結果となり、所望の造粒性及び製品品質を達成する上でバインダーが必要であることが確認された。
<Binder compounding ratio>
As a confirmation of the effect of the binder, an added group (Test No. 1-4-1) and an additive-free group (Test No. 1-5) were compared. If the binder is not added, the granulation property is deteriorated, and each target value is slightly deteriorated. It was confirmed that the binder is necessary for achieving the desired granulation property and product quality.

市販されている2種類の蒸製皮革粉(いずれもクロムなめしの蒸製皮革粉)について上述した要領で嵩比重、最大容水量を測定したところ、表4の通常皮粉の欄A、Bに記載されているように、それぞれ、嵩比重:0.7で最大容水量%599、嵩比重:0.69で最大容水量483重量%であった。これらをそれぞれ比較対象品として原料に使用した。   When the bulk specific gravity and the maximum water volume were measured in the same manner as described above for two types of steamed leather powders that were marketed (both steamed leather powders of chrome tanning), they were listed in columns A and B of Table 4 for normal skin powders. As shown, the bulk specific gravity was 0.7 and the maximum water content was 599%, and the bulk specific gravity was 0.69 and the maximum water content was 483% by weight. These were used as raw materials for comparison.

次に、市販されている蒸製皮革粉ついて上述した要領で嵩比重、最大容水量を測定し、嵩比重0.8以上で、最大容水量450重量%以下であるものを2種類(いずれもクロムなめしの蒸製皮革粉)選抜したところ、表4の選抜皮粉の欄C、Dに記載されているように、嵩比重:0.82で最大容水量431重量%、嵩比重:0.82で最大容水量407重量%のものを選抜でき、これらをそれぞれ本発明の粒状有機肥料を製造する原料に使用した。

Figure 2011251860
Next, for the steamed leather powder commercially available, the bulk specific gravity and the maximum water volume were measured in the manner described above, and two kinds of those having a bulk specific gravity of 0.8 or more and a maximum water volume of 450 wt% or less (both of which were chromium) Tanned steamed leather powder) When selected, as shown in the selected skin powder columns C and D of Table 4, the bulk specific gravity is 0.82, the maximum water capacity is 431 wt%, and the bulk specific gravity is 0.82. Those having a maximum water capacity of 407% by weight can be selected and used as raw materials for producing the granular organic fertilizer of the present invention.
Figure 2011251860

有機質肥料として油粕、蒸製毛粉、副産植物質肥料、菌体肥料、骨粉を用い、バインダーとしてこんにゃくとび粉を用いた。   Oil cake, steamed hair flour, by-product vegetable fertilizer, fungus body fertilizer, and bone powder were used as organic fertilizers, and konjac flying powder was used as a binder.

各原料を図1の製造工程概略図に示されているように計量し、表5の配合割合(重量%)で合計7kgとなるように配合した。窒素全量、燐酸全量はそれぞれ表5記載の通りであった。

Figure 2011251860
Each raw material was weighed as shown in the production process schematic diagram of FIG. 1 and blended so that the blending ratio (% by weight) in Table 5 was 7 kg in total. The total amount of nitrogen and the total amount of phosphoric acid were as shown in Table 5, respectively.
Figure 2011251860

配合原料を混合した後、奈良式粉砕機にて全量を通過させて粉砕した。粉砕粒度は粉砕機通過速度により調整し、500ミクロン通過割合を60%になるように調整した。実測の粉砕粒度はそれぞれ表6、表7記載の通りであった。   After mixing the blended raw materials, the entire amount was passed through a Nara type pulverizer and pulverized. The pulverized particle size was adjusted by the pulverizer passing speed, and the 500 micron passing rate was adjusted to 60%. The actually measured pulverized particle sizes were as shown in Tables 6 and 7, respectively.

次に、混練機を使用し、練り状況を確認しながら適宜加水し、2分間混練りを行った。この後、造粒を行ったが、造粒水分率はそれぞれ表6、表7記載の通りであった。   Next, using a kneader, water was added appropriately while confirming the kneading situation, and kneading was performed for 2 minutes. Thereafter, granulation was performed, and the granulation moisture percentages were as shown in Tables 6 and 7, respectively.

造粒については、全ての試験区について湿式押出造粒機で成型後、整粒機で整粒した(表6)。また、この他に、試験No.2−1、2−3については、ブリケット造粒機にて圧縮造粒した後、整粒機で整粒した(表7)。実施例1で採用した皿形方式等の転動造粒だけでは、有機原料の凝集力を加水のみに依存している為、粒度調整、混練りによる粒状化改善を検討したものである。   For granulation, all test sections were molded with a wet extrusion granulator and then sized with a granulator (Table 6). In addition, test No. About 2-1 and 2-3, after carrying out compression granulation with a briquette granulator, it granulated with the granulator (Table 7). Only the rolling granulation of the dish type method etc. employed in Example 1 relies on only water for cohesion of organic raw materials, and therefore, improvement of granulation by particle size adjustment and kneading was examined.

次いで、造粒品を通風棚乾燥機で80度熱風により3時間乾燥した後、2mm、4mmの篩いで2〜4mmの製品歩留まりを測定し、製品硬度を実施例1と同じようにして木屋式硬度計にて測定した。   Next, the granulated product was dried with hot air at 80 ° C. for 3 hours in a ventilation shelf dryer, and then the product yield of 2 to 4 mm was measured with a 2 mm and 4 mm sieve, and the product hardness was set in the same manner as Example 1 Measured with a hardness meter.

結果は表6、表7の通りであった。

Figure 2011251860
The results are shown in Tables 6 and 7.
Figure 2011251860

表6の結果の通り、嵩比重0.8以上で、最大容水量%450以下の蒸製皮革粉を原料に用いた場合、皮粉使用割合55〜75%で粒状肥料としての生産性、物性を確保出来ることを確認できた。     As shown in Table 6, when steamed leather powder having a bulk specific gravity of 0.8 or more and a maximum water volume of 450% or less is used as a raw material, the productivity and physical properties as granular fertilizer are used at a skin powder usage rate of 55 to 75%. It was confirmed that it could be secured.

なお、この実施例及び、本発明においては、安息角、粉化率はそれぞれ次のようにして測定している。   In this example and the present invention, the angle of repose and the powdering rate are measured as follows.

<安息角>
三輪式安息角測定器(筒井理化学製)で測定。測定操作を2回行い、平均値を求めた。
<Repose angle>
Measured with a three-wheel repose angle measuring instrument (manufactured by Tsutsui Riken). The measurement operation was performed twice to obtain an average value.

<粉化率>
あらかじめサンプルを2.0mmの篩いでふるい、2.0mm未満の粉を除去する。2.0mm未満の粉を除去したサンプル250gを500mlのスチロール棒瓶に入れ、蓋をした後、往復振とう機(TAITEC製 RECIPRO SHAKER SR−2W、振とう設定:300min−1)で15分間振とうする。振とう後のサンプルを再び2.0mmの篩いでふるい、篩下部分の比率を求め(重量%)とする。

Figure 2011251860
<Powdering rate>
The sample is sieved in advance with a 2.0 mm sieve to remove powder less than 2.0 mm. 250 g of sample from which powder less than 2.0 mm has been removed is placed in a 500 ml styrol stick bottle, covered, and shaken for 15 minutes with a reciprocating shaker (TAITEC's RECIPRO SHAKER SR-2W, shake setting: 300 min −1 ). I will. The sample after shaking is sieved again with a 2.0 mm sieve, and the ratio of the portion under the sieve is determined (% by weight).
Figure 2011251860

表7の結果の通り、試験No.2−1、試験No.2−3とも皮粉使用割合55重量%であったが、嵩比重0.8以上で、最大容水量%450以下の蒸製皮革粉を原料に用いると(試験No.2−3)造粒状況が改善され、製品品質も目標値を達成することができた。一方、この嵩比重、最大容水量%の条件を満たさないとき(試験No.2−1)には、造粒不可であった。   As shown in Table 7, test no. 2-1, test no. In both cases, the percentage of skin powder used was 55% by weight, but when steamed leather powder having a bulk specific gravity of 0.8 or more and a maximum water capacity of 450 or less was used as a raw material (Test No. 2-3) As a result, the product quality was able to achieve the target value. On the other hand, when the conditions of the bulk specific gravity and the maximum water capacity% were not satisfied (Test No. 2-1), granulation was impossible.

すなわち、ブリケット造粒機にて圧縮造粒した場合にも、嵩比重0.8以上で、最大容水量%450以下の蒸製皮革粉を原料に用いた場合、皮粉使用割合55〜75%で粒状肥料としての生産性、物性を確保出来ることを確認できた。   That is, even when compression granulation is performed with a briquette granulator, when steamed leather powder having a bulk specific gravity of 0.8 or more and a maximum water capacity of 450 or less is used as a raw material, the skin powder usage rate is 55 to 75%. It was confirmed that productivity and physical properties as granular fertilizer can be secured.

以上、本発明の好ましい実施形態、実施例を説明したが、本発明はかかる実施形態、実施例に限定されるものではなく、特許請求の範囲の記載から把握される技術的範囲において種々に変更可能である。     The preferred embodiments and examples of the present invention have been described above. However, the present invention is not limited to these embodiments and examples, and various modifications can be made within the technical scope grasped from the description of the claims. Is possible.

Claims (9)

蒸製皮革粉50〜75重量%と、有機質肥料15〜48重量%と、造粒促進材2〜10重量%とを混合し、造粒、乾燥させてなる粒状有機肥料。   A granular organic fertilizer obtained by mixing 50 to 75% by weight of steamed leather powder, 15 to 48% by weight of organic fertilizer, and 2 to 10% by weight of a granulation accelerator, granulating and drying. 前記蒸製皮革粉は、嵩比重0.8以上で、最大容水量450重量%以下であることを特徴とする請求項1記載の粒状有機肥料。   The granular organic fertilizer according to claim 1, wherein the steamed leather powder has a bulk specific gravity of 0.8 or more and a maximum water capacity of 450% by weight or less. 蒸製皮革粉、有機質肥料、造粒促進材を混合した後、粉砕して粒度を500ミクロン通過割合で40%以上70%以下に調整した後に造粒することを特徴とする請求項1又は2記載の粒状有機肥料。   3. The steamed leather powder, the organic fertilizer, and the granulation accelerator are mixed and then pulverized to adjust the particle size to 40% or more and 70% or less at a passage rate of 500 microns, and then granulated. Granular organic fertilizer. 窒素全量を9%以上含有することを特徴とする請求項1乃至3のいずれか一項記載の粒状有機肥料。   The granular organic fertilizer according to any one of claims 1 to 3, wherein the total amount of nitrogen is 9% or more. 蒸製皮革粉50〜75重量%と、有機質肥料15〜48重量%と、造粒促進材2〜10重量%とを混合し、造粒、乾燥を行う粒状有機肥料の製造方法。   A method for producing granular organic fertilizer in which 50 to 75% by weight of steamed leather powder, 15 to 48% by weight of organic fertilizer, and 2 to 10% by weight of a granulation accelerator are mixed and granulated and dried. 前記蒸製皮革粉は、嵩比重0.8以上で、最大容水量450重量%以下であることを特徴とする請求項5記載の粒状有機肥料の製造方法。   6. The method for producing a granular organic fertilizer according to claim 5, wherein the steamed leather powder has a bulk specific gravity of 0.8 or more and a maximum water capacity of 450% by weight or less. 蒸製皮革粉、有機質肥料、造粒促進材を混合した後、粉砕して粒度を500ミクロン通過割合で40%以上70%以下に調整した後に造粒することを特徴とする請求項5又は6記載の粒状有機肥料の製造方法。   7. The steamed leather powder, the organic fertilizer and the granulation accelerator are mixed and then pulverized to adjust the particle size to 40% or more and 70% or less at a passage rate of 500 microns, and then granulated. Production method of granular organic fertilizer. 前記造粒工程の前に、混練工程を実施し、水分率35%以下で造粒することを特徴とする請求項5乃至7のいずれか一項記載の粒状有機肥料の製造方法。   The method for producing a granular organic fertilizer according to any one of claims 5 to 7, wherein a kneading step is performed before the granulation step and granulation is performed at a moisture content of 35% or less. 造粒工程後に、高速転動整粒又は解砕転動整粒からなる整粒工程を組み合わせることを特徴とする請求項5乃至8のいずれか一項記載の粒状有機肥料。   The granular organic fertilizer according to any one of claims 5 to 8, wherein a granulation step comprising high-speed rolling granulation or pulverization rolling granulation is combined after the granulation step.
JP2010125486A 2010-06-01 2010-06-01 Granular organic fertilizer and method for producing the same Active JP5610517B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2010125486A JP5610517B2 (en) 2010-06-01 2010-06-01 Granular organic fertilizer and method for producing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2010125486A JP5610517B2 (en) 2010-06-01 2010-06-01 Granular organic fertilizer and method for producing the same

Publications (2)

Publication Number Publication Date
JP2011251860A true JP2011251860A (en) 2011-12-15
JP5610517B2 JP5610517B2 (en) 2014-10-22

Family

ID=45416144

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2010125486A Active JP5610517B2 (en) 2010-06-01 2010-06-01 Granular organic fertilizer and method for producing the same

Country Status (1)

Country Link
JP (1) JP5610517B2 (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04317487A (en) * 1991-04-11 1992-11-09 Koopu Chem Kk Spherical granular body of manure and granulating method thereof
JPH04317486A (en) * 1991-04-11 1992-11-09 Koopu Chem Kk Granulating method of manure
JPH05262591A (en) * 1992-03-16 1993-10-12 Ube Ind Ltd Granular organic fertilizer composition

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04317487A (en) * 1991-04-11 1992-11-09 Koopu Chem Kk Spherical granular body of manure and granulating method thereof
JPH04317486A (en) * 1991-04-11 1992-11-09 Koopu Chem Kk Granulating method of manure
JPH05262591A (en) * 1992-03-16 1993-10-12 Ube Ind Ltd Granular organic fertilizer composition

Also Published As

Publication number Publication date
JP5610517B2 (en) 2014-10-22

Similar Documents

Publication Publication Date Title
US8979970B2 (en) Fertilizer composition incorporating fibrous material for enhanced particle integrity
KR101668454B1 (en) Integrated manufacturing system for powder compost or pellet compost
CN101575222B (en) Method for producing ammonium sulphate grain products by using inorganic caking agent
CN107614463A (en) Granular fertilizer with micronizing sulphur
US20020011087A1 (en) Homogeneous granules of slow-release fertilizer and method of making the same
JP6540094B2 (en) Granular fertilizer composition and method for producing granular fertilizer composition
WO2017156610A1 (en) Method for producing organic or organic-mineral fertilizers in granule form, and fertilizers obtained by this method
JP2008239382A (en) Method for producing granular compound fertilizer
Zafari et al. Management and reduction of chemical nitrogen consumption in agriculture
JP5610517B2 (en) Granular organic fertilizer and method for producing the same
CN102485017A (en) Mixed feed of straws and plants
US11432570B2 (en) Method for producing an extruded feed containing fibres
CN108936033A (en) A kind of pet rabbit U.S. hair extruding grain and preparation method thereof
Kibret et al. Pan pelletization of bone char fertilizer: An evaluation of process parameters and their effect on granule strength
RU2174971C1 (en) Complex organomineral fertilizer and method of production thereof
CN102845460B (en) Phosethyl-aluminum water dispersible granules and preparation method thereof
KR100608444B1 (en) The method of granular a soil conditioner making from the by-product of slag and a gypsum
JP2017132659A (en) Granular nitrogen fertilizer, and method for producing the granular nitrogen fertilizer
JP7430379B2 (en) Method for producing granular organic fertilizer
KR101346599B1 (en) Processing method of organic fertilizer of pellet type
JPH0397684A (en) Production of fertilizer containing organic substance
JP5057541B2 (en) Production method of granular salt
KR101623640B1 (en) Processing method of complex fertilizer that has much more organic matter
JP3226937B2 (en) Granulation method of granular fertilizer
CN101744103A (en) Method for processing floral disc of sunflower into feed

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130426

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140422

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140613

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140701

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140828

R150 Certificate of patent or registration of utility model

Ref document number: 5610517

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313115

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250