JP2009255107A - Method of preventing crack in rolling caused by change of set temperature of heating furnace in 18-8 stainless steel - Google Patents

Method of preventing crack in rolling caused by change of set temperature of heating furnace in 18-8 stainless steel Download PDF

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JP2009255107A
JP2009255107A JP2008105224A JP2008105224A JP2009255107A JP 2009255107 A JP2009255107 A JP 2009255107A JP 2008105224 A JP2008105224 A JP 2008105224A JP 2008105224 A JP2008105224 A JP 2008105224A JP 2009255107 A JP2009255107 A JP 2009255107A
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Tatsuji Hiraishi
達二 平石
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Sanyo Special Steel Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method of preventing the generation of cracks by changing a hot rolling temperature by properly changing the set temperature of a heating furnace corresponding to the residence time in the heating furnace of a bloom to be heated for hot-rolling 18-8 stainless steel and suppressing the production of ferrite in the corner parts of the bloom in hot rolling. <P>SOLUTION: When the residence time in the heating furnace for heating in order to the hot-rolling of the bloom of the 18-8 stainless steel is ≥2.5 to <3.5h, the set temperature of the heating furnace is taken as 1,160-1,180°C in the preheating zone, as 1,330-1,350°C in the heating zone and as 1,330-1,340°C in the soaking zone. When the residence time is 3.5-6.0h, the preset temperature is taken as the same as the above in the preheating zone, but as 1,320-1,340°C in the heating zone and as 1,320-1,330°C in the soaking zone. By lowering the each temperature of the heating zone and the soaking zone downward by 10°C as compared with the case where the residence time is <3.5 hr, the cracks in the corner parts of the bloom in the hot rolling are prevented. <P>COPYRIGHT: (C)2010,JPO&INPIT

Description

この出願は、オーステナイト系ステンレス鋼である18−8系ステンレス鋼における加熱炉における設定温度を低く変更することにより、ブルームコーナー部のフェライトの生成量を抑えることで、熱間圧延時の割れ疵の発生の防止方法に関する。   In this application, by changing the set temperature in the heating furnace in the 18-8 stainless steel, which is an austenitic stainless steel, to lower the generation amount of ferrite in the bloom corner portion, The present invention relates to an occurrence prevention method.

従来、連続鋳造によるオーステナイト系ステンレス鋼のブルームは、熱間圧延のために加熱炉で加熱される。その加熱の際の加熱炉の設定温度は、予熱帯で1160℃〜1180℃、均熱帯で1330℃〜1350℃、均熱帯で1330℃〜1340℃とされ、加熱炉への装入から抽出までのブルームの在炉時間は2.5時間以上から6.0時間以下とされていた。しかし、ブルームの加熱炉への装入から抽出までの在炉時間が3.5時間以上に長くなると、ブルームコーナー部においてフェライトの生成量が増加し、このために熱間圧延時に割れが発生する問題があった。   Conventionally, blooms of austenitic stainless steel by continuous casting are heated in a heating furnace for hot rolling. The set temperature of the heating furnace at the time of heating is 1160 ° C to 1180 ° C in the pretropical zone, 1330 ° C to 1350 ° C in the soaking zone, and 1330 ° C to 1340 ° C in the soaking zone. The blooming time of the bloom of No. 1 was 2.5 hours or more and 6.0 hours or less. However, if the in-furnace time from charging to extraction in the heating furnace of the bloom becomes longer than 3.5 hours, the amount of ferrite generated in the bloom corner increases, which causes cracks during hot rolling. There was a problem.

一方、従来のオーステナイトステンレス鋼の鋳片スラブの加熱温度と加熱時間を規定する操業条件では、δ−フェライトが1%以上残留し、熱間圧延時に加工割れが発生して、ヘゲ疵の発生の原因になるとし、これを回避する方法として、鋼片の加熱温度を1200℃〜1260℃に維持すると共に、鋼片温度が1200℃以上となった状態で40分以上保定することにより、残存する鋼片内のδ−フェライトを消滅させてから熱間圧延する方法が提案されている(例えば、特許文献1参照。)。しかし、この方法は予熱帯の温度を高めに設定していた従来技術を生産性を向上のために変更するものであり、従来のように1260℃以上に加熱して保定すると延性が劣化し熱間加工性が劣化するとするので、それを改良するものであった。ところで、この提案の先行技術の方法は、加熱炉の在炉時間によって加熱帯や均熱帯のヒートパターンを変更する方法ではなかった。   On the other hand, under the operating conditions that stipulate the heating temperature and heating time of the conventional slab slab of austenitic stainless steel, 1% or more of δ-ferrite remains and work cracks occur during hot rolling, resulting in the occurrence of whipping. As a method of avoiding this, the heating temperature of the steel slab is maintained at 1200 ° C. to 1260 ° C., and the steel slab temperature is maintained at 1200 ° C. or higher for 40 minutes or more, thereby remaining. A method of hot rolling after eliminating δ-ferrite in the steel slab is proposed (for example, see Patent Document 1). However, this method changes the conventional technology, which has been set to a high pretropical temperature, in order to improve productivity. When heated and maintained at 1260 ° C. or higher as in the prior art, the ductility deteriorates and the heat is reduced. Since the inter-workability deteriorated, it was an improvement. By the way, the proposed prior art method is not a method of changing the heating zone or the soaking zone heat pattern according to the in-furnace time of the heating furnace.

特開2004−137540号公報JP 2004-137540 A

一般に、18−8系ステンレス鋼の熱間圧延のためのブルームの加熱炉の設定温度は、予熱帯を1160℃〜1180℃、加熱帯を1330℃〜1350℃、均熱帯を1330℃〜1340℃とし、加熱炉への装入から抽出までの鋼材の在炉時間を2.5時間以上6.0時間以下に制限していた。しかし、在炉時間が3.5時間以上となる鋼材においては、熱間圧延時にブルームコーナー部でフェライト生成量が増加し、このために圧延時に割れが発生するという問題がある。   In general, the preset temperature of the Bloom heating furnace for hot rolling of 18-8 stainless steel is 1160 ° C to 1180 ° C in the pretropical zone, 1330 ° C to 1350 ° C in the heating zone, and 1330 ° C to 1340 ° C in the soaking zone. In addition, the in-furnace time of the steel material from charging to extraction in the heating furnace was limited to 2.5 hours or more and 6.0 hours or less. However, in steel materials whose in-furnace time is 3.5 hours or more, there is a problem that the amount of ferrite generated increases at the bloom corner portion during hot rolling, and cracks occur during rolling.

そこで、本発明が解決しようとする課題は、18−8系ステンレス鋼の熱間圧延のために加熱するブルームの加熱炉の在炉時間に対応して、加熱炉における設定温度を適切に変更することにより熱間圧延温度を変更し、熱間圧延時のブルームコーナー部のフェライト生成量を抑えることで割れの発生を防止する方法を提供することである。   Therefore, the problem to be solved by the present invention is to appropriately change the set temperature in the heating furnace in accordance with the in-furnace time of the Bloom heating furnace heated for hot rolling of 18-8 stainless steel. It is providing the method of preventing generation | occurrence | production of a crack by changing hot rolling temperature by this and suppressing the ferrite production amount of the bloom corner part at the time of hot rolling.

上記の課題を解決するための本発明の手段は、請求項1の発明では、18−8系ステンレス鋼のブルームを熱間圧延するために加熱する加熱炉中の在炉時間に対応して加熱炉の設定温度を変更することにより熱間圧延温度を低く抑制することを特徴とするブルームコーナー部の熱間圧延時の割れ疵防止方法である。   The means of the present invention for solving the above-mentioned problems is as follows. In the invention of claim 1, heating is performed according to the in-furnace time in the heating furnace for heating the 18-8 stainless steel bloom in order to hot-roll. This is a cracking prevention method during hot rolling of a bloom corner portion, characterized in that the hot rolling temperature is suppressed low by changing the set temperature of the furnace.

請求項2の発明では、加熱炉中の在炉時間に対応して加熱炉の設定温度を変更する方法は、18−8系ステンレス鋼のブルームの加熱炉への装入から抽出までの在炉時間が2.5時間以上から3.5時間未満の場合は、加熱炉の設定温度を予熱帯で1160℃〜1180℃、加熱帯を1330℃〜1350℃、均熱帯を1330℃〜1340℃とするが、在炉時間が3.5時間以上から6.0時間以下の場合は、予熱帯を1160℃〜1180℃とする点は変更しないが、加熱帯を1320℃〜1340℃とし、均熱帯を1320℃〜1330℃として加熱帯及び均熱帯の温度を在炉時間の3.5時間未満の場合に比してそれぞれ10℃ずつ下方に下げることを特徴とする請求項1の手段のブルームコーナー部の熱間圧延時の割れ疵防止方法である。   In the invention of claim 2, the method of changing the set temperature of the heating furnace in accordance with the in-furnace time in the heating furnace is the in-furnace from charging to extraction of the 18-8 series stainless steel bloom to the extraction furnace. When the time is 2.5 hours or more and less than 3.5 hours, the set temperature of the heating furnace is 1160 ° C to 1180 ° C in the pretropical zone, the heating zone is 1330 ° C to 1350 ° C, and the soaking zone is 1330 ° C to 1340 ° C. However, when the in-furnace time is 3.5 hours or more to 6.0 hours or less, the point where the pre-tropical zone is 1160 ° C to 1180 ° C is not changed, but the heating zone is 1320 ° C to 1340 ° C, The temperature of the heating zone and the soaking zone is lowered by 10 ° C. each by 10 ° C. compared to the case where the temperature in the furnace is less than 3.5 hours. To prevent cracks during hot rolling A.

本発明の上記の手段としたことで、18−8系ステンレス鋼において、熱間圧延されたブルームコーナー部のフェライトの生成量を押さえることにより、熱間圧延時の割れ疵の発生を防止して圧延材の品質の向上を図ることができ、特に加熱炉における在炉時間が3.5時間以上から6.0時間以下の場合に、加熱炉の加熱帯および均熱帯の温度をそれぞれ3.5時間未満の場合に比して10℃ずつ低下して、熱間圧延されたブルームコーナー部のフェライトの生成量を押さえることにより、熱間圧延時の割れ疵の発生を防止して圧延材の品質の向上を図ることができ、本発明は従来にない優れた効果を奏する方法である。   By using the above-described means of the present invention, in 18-8 stainless steel, by suppressing the amount of ferrite produced in the hot-rolled bloom corner portion, generation of cracks during hot rolling can be prevented. The quality of the rolled material can be improved. Especially when the in-furnace time in the heating furnace is 3.5 hours or more and 6.0 hours or less, the heating zone of the heating furnace and the temperature of the soaking zone are set to 3.5 respectively. Reduced by 10 ° C as compared to the case of less than the time, suppressing the generation of ferrite in the hot-rolled bloom corner, thereby preventing the occurrence of cracks during hot rolling and the quality of the rolled material Therefore, the present invention is a method that exhibits an excellent effect that has never been achieved.

本発明を実施するための最良の形態について、表を参照して以下に説明する。これに先立ち、18−8系ステンレス鋼であるJIS規格のSUS304からなるブルームを熱間圧延するために、熱間圧延温度に加熱するための加熱炉の設定温度およびブルームの装入から抽出までの在炉時間によって、熱間圧延したブルームのコーナー部の疵の発生状況を実験して調査した。   The best mode for carrying out the present invention will be described below with reference to the table. Prior to this, in order to hot-roll a bloom made of JIS standard SUS304, which is 18-8 stainless steel, from the setting temperature of the heating furnace for heating to the hot rolling temperature and from the charging to the extraction of the bloom Experiments were conducted to investigate the occurrence of flaws at the corners of the hot-rolled bloom, depending on the in-furnace time.

先ず、従来方法である加熱炉におけるブルームの在炉時間を、2.5時間以上〜3.0時間未満、3.0時間以上〜3.5時間未満、3.5時間以上〜6.0時間以下の3段階に区分し、圧延時のブルームのコーナー部の温度を、2.5時間以上〜3.0時間未満では1120℃とし、3.0時間以上〜3.5時間未満では1120℃とし、3.5時間以上〜6.0時間以下では1135℃としてブルームを加熱した。さらに、圧延時の面中央温度を、2.5時間以上〜3.0時間未満では1115℃とし、3.0時間以上〜3.5時間未満では1117℃とし、3.5時間以上〜6.0時間以下では1125℃としてブルームを加熱した。次いで、これらのブルームを熱間圧延し、熱間圧延したブルーム1本あたりに発生した疵個数(N=10とするときの数)を調査した。その結果、ブルームの在炉時間が2.5時間以上〜3.0時間未満では、疵個数は2.4個であった。ブルームの在炉時間が3.0時間以上〜3.5時間未満では、疵個数は2.5個であった。ブルームの在炉時間が3.5時間以上〜6.0時間以下では、疵個数は5.4個であった。なお、この在炉時間が3.5時間以上の場合、ブルームコーナー部ではフェライト生成量が増加して割れが増加したものと考えられる。これらの発生した疵の個数による評価を、疵3個未満で〇、疵3〜5個を△、疵5個以上を×とし、表1に示した。   First, the in-furnace time of the bloom in the conventional heating furnace is 2.5 hours to less than 3.0 hours, 3.0 hours to less than 3.5 hours, 3.5 hours to 6.0 hours. The temperature at the corner of the bloom during rolling is 1120 ° C. for 2.5 hours to less than 3.0 hours, and 1120 ° C. for 3.0 hours to less than 3.5 hours. The bloom was heated to 1135 ° C. for 3.5 hours to 6.0 hours. Furthermore, the surface center temperature during rolling is 1115 ° C. for 2.5 hours to less than 3.0 hours, 1117 ° C. for 3.0 hours to less than 3.5 hours, and 3.5 hours to 6. Below 0 hours, the bloom was heated to 1125 ° C. Next, these blooms were hot-rolled, and the number of wrinkles generated per one hot-rolled bloom (the number when N = 10) was investigated. As a result, when the in-furnace time of the bloom was 2.5 hours or more and less than 3.0 hours, the number of soot was 2.4. When the in-furnace time of the bloom was 3.0 hours or more and less than 3.5 hours, the number of soot was 2.5. When the bloom time in the bloom was 3.5 hours to 6.0 hours, the number of soot was 5.4. In addition, when this in-furnace time is 3.5 hours or more, it is thought that the amount of ferrite generation increased and the cracks increased in the bloom corner portion. The evaluation based on the number of the generated wrinkles is shown in Table 1, with less than 3 wrinkles being ◯, 3 to 5 wrinkles being Δ, and five or more wrinkles being ×.

Figure 2009255107
Figure 2009255107

次いで、ブルームの在炉時間3.5時間以上において、加熱炉の設定温度を下げて加熱したブルームを圧延テストした。すなわち、加熱炉の加熱帯および均熱帯の温度を10℃下げ、圧延時のブルームコーナー部温度を1120℃とし、圧延時の面中央部の温度は1114℃とした。この場合の、圧延によりブルーム1本あたりに発生した、疵個数(N=10とするときの数)は2.5個で、評価は〇であった。   Next, a rolling test was performed on the bloom that had been heated by lowering the set temperature of the heating furnace at a blooming time of 3.5 hours or longer. That is, the temperature of the heating zone and the soaking zone of the heating furnace was lowered by 10 ° C., the bloom corner temperature during rolling was 1120 ° C., and the temperature at the center of the surface during rolling was 1114 ° C. In this case, the number of ridges (number when N = 10) generated per bloom by rolling was 2.5, and the evaluation was ◯.

さらに、加熱炉の加熱帯および均熱帯の温度を20℃下げ、圧延時のブルームコーナー部温度を1102℃とし、圧延時の面中央部の温度を1098℃とした。この場合の、圧延によりブルーム1本あたりに発生した、疵個数(N=10とするときの数)は5.5個で、評価は×であった。   Furthermore, the heating zone of the heating furnace and the soaking zone temperature were lowered by 20 ° C., the bloom corner temperature during rolling was set to 1102 ° C., and the temperature at the center of the surface during rolling was set to 1098 ° C. In this case, the number of ridges (number when N = 10) generated per bloom by rolling was 5.5, and the evaluation was x.

さらに、加熱炉の加熱帯および均熱帯の温度を30℃下げ、圧延時のブルームコーナー部温度を1099℃とし、圧延時の面中央部の温度を1089℃とした。この場合の、圧延によりブルーム1本あたりに発生した、疵個数(N=10とするときの数)は7.0個で、評価は×であった。   Further, the temperature of the heating zone and the soaking zone of the heating furnace was lowered by 30 ° C., the bloom corner temperature during rolling was set to 1099 ° C., and the temperature at the center of the surface during rolling was set to 1089 ° C. In this case, the number of ridges (number when N = 10) generated per bloom by rolling was 7.0, and the evaluation was x.

これらのテストにおいて、加熱炉の加熱帯および均熱帯の温度を20℃以上に下げた場合には、上記の在炉時間が3.5時間以上の場合にブルームコーナー部でフェライト生成量が増加して割れが増加したものと異なり、圧延されるブルームの温度低下が著しくなるために熱間加工性が悪化し、特に圧延により割れが発生したと推測される。これらのテスト結果を表2に示す。   In these tests, when the heating zone of the heating furnace and the temperature of the soaking zone are lowered to 20 ° C or higher, the amount of ferrite produced increases at the bloom corner when the above furnace time is 3.5 hours or more. Unlike the case in which cracks increase, the temperature drop of the rolled bloom becomes remarkable, so that hot workability deteriorates, and it is speculated that cracks are generated particularly by rolling. These test results are shown in Table 2.

Figure 2009255107
Figure 2009255107

以上のテスト結果を踏まえて、本発明では、ブルームの加熱炉による予熱帯、加熱帯、および均熱帯のそれぞれの加熱温度およびそれらの帯域在炉時間を変更し、さらに、ブルームコーナー部のフェライト生成量を抑えることで、熱間圧延時の割れ疵の発生を防止する方法である。そのためには、18−8系ステンレス鋼からなるブルームを加熱および均熱するために装入する加熱炉中のブルームの在炉時間に応じて、加熱炉の温度を変更する方法である。   Based on the above test results, the present invention changes the heating temperature and the time in the zone of the pre-tropics, heating zone, and soaking zone in the Bloom heating furnace, and further generates ferrite in the bloom corner portion. This is a method for preventing the occurrence of cracks during hot rolling by suppressing the amount. For that purpose, it is a method of changing the temperature of the heating furnace according to the in-furnace time of the bloom in the heating furnace to be charged in order to heat and soothe the bloom made of 18-8 stainless steel.

この本発明の方法の最良の実施の形態では、表3における、材炉時間制限が、2.5hr≦在炉<3.5hrである、新1の場合には、その予熱帯、加熱帯および均熱帯の加熱温度を、従来の在炉時間制限が2.5hr≦在炉≦6.0hrである、旧の場合の予熱帯、加熱帯および均熱帯の加熱温度と全く同じとし、それぞれの加熱温度は、予熱帯が1160℃〜1180℃、加熱帯が1330℃〜1350℃、均熱帯が1330℃〜1340℃とした。   In the best mode of the method of the present invention, in Table 3, when the material furnace time limit is 2.5 hr ≦ in-furnace <3.5 hr, the pre-tropical zone, the heating zone and The heating temperature in the soaking zone is exactly the same as the heating temperature in the pretropical zone, heating zone, and soaking zone in the old case where the conventional in-furnace time limit is 2.5 hr ≦ in-furnace ≦ 6.0 hr. The temperatures were 1160 ° C to 1180 ° C in the pretropical zone, 1330 ° C to 1350 ° C in the heating zone, and 1330 ° C to 1340 ° C in the soaking zone.

しかし、表3における、在炉時間制限が3.5hr≦在炉≦6.0hrである、新2の場合には、予熱帯の温度は新1および旧の温度と同じ1160℃〜1180℃としたが、加熱帯の温度は1320℃〜1340℃とし、均熱帯の温度は1320℃〜1330℃とし、これらの加熱帯および均熱帯の温度は新1および旧の温度に比してそれぞれ10℃ずつシフトして低く制御した。この結果、新1および新2の方法において、ブルームコーナー部の割れ疵の発生はいずれも3個未満に抑制できた。   However, in Table 3, in the case of the new 2 in which the in-furnace time limit is 3.5 hr ≦ in-furnace ≦ 6.0 hr, the temperature of the pretropical zone is 1160 ° C. to 1180 ° C. which is the same as the new 1 and old temperatures. However, the temperature of the heating zone is 1320 ° C to 1340 ° C, the temperature of the soaking zone is 1320 ° C to 1330 ° C, and the temperature of the heating zone and soaking zone is 10 ° C compared to the new 1 and the old temperature, respectively. Shifted gradually and controlled low. As a result, in the new 1 and new 2 methods, it was possible to suppress the occurrence of cracks in the bloom corner portion to less than three.

Figure 2009255107
Figure 2009255107

Claims (2)

18−8系ステンレス鋼のブルームを熱間圧延するために加熱する加熱炉中の在炉時間に対応して加熱炉の設定温度を変更することにより熱間圧延温度を低く抑制することを特徴とするブルームコーナー部の熱間圧延時の割れ疵防止方法。   It is characterized by suppressing the hot rolling temperature low by changing the set temperature of the heating furnace corresponding to the in-furnace time in the heating furnace heated to hot-roll the bloom of 18-8 stainless steel. How to prevent cracks during hot rolling at the bloom corner. 加熱炉中の在炉時間に対応して加熱炉の設定温度を変更する方法は、18−8系ステンレス鋼のブルームの加熱炉への装入から抽出までの在炉時間が2.5時間以上3.5時間未満の場合は、加熱炉の設定温度を予熱帯で1160℃〜1180℃、加熱帯を1330℃〜1350℃、均熱帯を1330℃〜1340℃とするが、在炉時間が3.5時間以上6.0時間以下の場合は、予熱帯の温度を1160℃〜1180℃とする点は変更しないが、加熱帯を1320℃〜1340℃とし、均熱帯を1320℃〜1330℃として加熱帯及び均熱帯の温度を在炉時間の3.5時間未満の場合に比してそれぞれ10℃ずつ下方に下げることを特徴とする請求項1に記載のブルームコーナー部の熱間圧延時の割れ疵防止方法。   The method of changing the set temperature of the heating furnace corresponding to the in-furnace time in the heating furnace is that the in-furnace time from charging to extraction of the 18-8 stainless steel bloom into the heating furnace is 2.5 hours or more. In the case of less than 3.5 hours, the set temperature of the heating furnace is 1160 ° C to 1180 ° C in the pretropical zone, the heating zone is 1330 ° C to 1350 ° C, the soaking zone is 1330 ° C to 1340 ° C, but the in-furnace time is 3 In the case of 5 hours or more and 6.0 hours or less, the temperature of the pretropical zone is not changed, but the heating zone is set to 1320 ° C to 1340 ° C, and the soaking zone is set to 1320 ° C to 1330 ° C. The temperature of the heating zone and the soaking zone is lowered by 10 ° C respectively in comparison with the case where the in-furnace time is less than 3.5 hours, and at the time of hot rolling of the bloom corner portion according to claim 1, How to prevent cracks.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101528065B1 (en) * 2013-12-18 2015-06-10 주식회사 포스코 Heating method for hot rolling of stainless steel
CN114273431A (en) * 2021-11-13 2022-04-05 中南大学 Method for reducing heating schedule of micro-alloy steel thermal cracks

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101528065B1 (en) * 2013-12-18 2015-06-10 주식회사 포스코 Heating method for hot rolling of stainless steel
CN114273431A (en) * 2021-11-13 2022-04-05 中南大学 Method for reducing heating schedule of micro-alloy steel thermal cracks

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