JP2009155157A - Device of producing preform for optical fiber - Google Patents

Device of producing preform for optical fiber Download PDF

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Publication number
JP2009155157A
JP2009155157A JP2007334799A JP2007334799A JP2009155157A JP 2009155157 A JP2009155157 A JP 2009155157A JP 2007334799 A JP2007334799 A JP 2007334799A JP 2007334799 A JP2007334799 A JP 2007334799A JP 2009155157 A JP2009155157 A JP 2009155157A
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optical fiber
preform
insulating material
heat insulating
soot preform
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Takahiro Hamada
貴弘 濱田
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Fujikura Ltd
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Fujikura Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/014Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/01446Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering
    • C03B37/0146Furnaces therefor, e.g. muffle tubes, furnace linings

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
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  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide a device of producing a preform for an optical fiber which can improve the heat efficiency of a heating furnace, and can sinter a soot preform at lower output. <P>SOLUTION: In the device where a soot preform is stored at the inside of a furnace core pipe, and is heated, so as to produce a preform for an optical fiber, a heat shield disk comprising a heat insulating material is set in the upper part of the soot preform. The heat shield disk set in the upper part of the soot preform preferably has a structure where the heat insulating material is stored in the inside of a glass vessel. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は、光ファイバ母材の品質を維持しつつ、炉心管内の断熱を効率的に行うための光ファイバ母材製造装置に関する。   The present invention relates to an optical fiber preform manufacturing apparatus for efficiently performing heat insulation in a furnace core tube while maintaining the quality of the optical fiber preform.

光ファイバ母材を製造するためには、VAD法、OVD法などでからなる多孔質ガラス微粒子積層体(以下、スートプリフォームと記す。)を形成し、該スートプリフォームを脱水し、焼結して透明化する必要がある。これらの、脱水、透明化のため、スートプリフォームを収容する炉心管を備えた加熱炉が使用される。図1は、従来の加熱炉を例示する概略構成図であり、この図中、符号1はスートプリフォーム、2は光ファイバ母材、3は炉心管、4はダミー棒、6はヒータである。この炉心管3の材質としては、主に石英ガラスが使われている。   In order to manufacture an optical fiber preform, a porous glass particulate laminate (hereinafter referred to as a soot preform) formed by a VAD method, an OVD method, or the like is formed, and the soot preform is dehydrated and sintered. Need to be transparent. For these dehydration and transparency, a heating furnace equipped with a furnace core tube for containing a soot preform is used. FIG. 1 is a schematic configuration diagram illustrating a conventional heating furnace, in which reference numeral 1 is a soot preform, 2 is an optical fiber preform, 3 is a core tube, 4 is a dummy rod, and 6 is a heater. . Quartz glass is mainly used as the material of the core tube 3.

スートプリフォームの脱水・透明化は、スートプリフォームの下端から上端に向かって行われる。このとき、上端部に近づくほど、熱が上方に拡散するため、加熱炉出力を高くする必要があり、エネルギーコストが高くなってしまう。この課題に対し、特許文献1に開示された従来技術では、光ファイバ多孔質母材(スートプリフォーム)の上端に接するように、遮蔽板を取り付けて熱拡散の改善を行っている。
特開2003−321235号公報
The soot preform is dehydrated and made transparent from the lower end to the upper end of the soot preform. At this time, the closer to the upper end, the more the heat diffuses upward, so the heating furnace output needs to be increased, and the energy cost increases. In response to this problem, in the conventional technique disclosed in Patent Document 1, a heat shield is attached to improve the thermal diffusion so as to be in contact with the upper end of the optical fiber porous preform (soot preform).
JP 2003-321235 A

しかしながら、特許文献1の従来技術では、遮蔽板として石英板を用いているが、石英板はカーボンなどの断熱材に比べると断熱効果及び遮熱効果は高いとは言えない。また、不透明化した石英板であっても同様である。
また、カーボンなどの遮熱板を使用した場合には、熱により劣化したカーボンの粉塵により母材品質の悪化が懸念される。
However, in the prior art of Patent Document 1, a quartz plate is used as a shielding plate. However, it cannot be said that the quartz plate has a higher heat insulating effect and heat shielding effect than a heat insulating material such as carbon. The same applies to an opaque quartz plate.
Further, when a heat shield such as carbon is used, there is a concern that the quality of the base material is deteriorated due to carbon dust deteriorated by heat.

本発明は、前記事情に鑑みてなされ、加熱炉の熱効率を向上でき、より低出力でスートプリフォームの焼結が可能となる光ファイバ母材製造装置の提供を目的とする。   The present invention has been made in view of the above circumstances, and an object of the present invention is to provide an optical fiber preform manufacturing apparatus that can improve the thermal efficiency of a heating furnace and can sinter a soot preform with a lower output.

前記目的を達成するため、本発明は、スートプリフォームを炉心管内部に収容し、加熱して光ファイバ母材を製造する加熱炉を有する光ファイバ母材製造装置において、
スートプリフォームの上部に、断熱材を含む遮熱円盤を設置したことを特徴とする光ファイバ母材製造装置を提供する。
In order to achieve the above object, the present invention provides an optical fiber preform manufacturing apparatus having a heating furnace in which a soot preform is accommodated in a furnace tube and heated to manufacture an optical fiber preform.
Provided is an optical fiber preform manufacturing apparatus in which a heat shield disk including a heat insulating material is installed on an upper portion of a soot preform.

本発明の光ファイバ母材製造装置において、スートプリフォームの上部に設置した遮熱円盤が、ガラス容器内に断熱材を収容した構造であることが好ましい。   In the optical fiber preform manufacturing apparatus of the present invention, it is preferable that the heat shield disk installed on the upper portion of the soot preform has a structure in which a heat insulating material is accommodated in a glass container.

本発明の光ファイバ母材製造装置において、スートプリフォームの上部に設置した遮熱円盤が、カーボン製断熱材を含むことが好ましい。   In the optical fiber preform manufacturing apparatus of the present invention, it is preferable that the heat shield disk installed on the upper portion of the soot preform includes a carbon heat insulating material.

本発明の光ファイバ母材製造装置において、スートプリフォームの上部に設置した遮熱円盤が、グラスウール製断熱材を含むことが好ましい。   In the optical fiber preform manufacturing apparatus of the present invention, it is preferable that the heat shield disk installed on the upper portion of the soot preform includes a glass wool heat insulating material.

本発明の光ファイバ母材製造装置は、スートプリフォームの上部に、断熱材を含む遮熱円盤を設置した構成としたので、スートプリフォームの脱水・透明化においてスートプリフォーム上方側への熱の拡散を抑制でき、加熱炉の熱効率を向上でき、より低出力でスートプリフォームの焼結が可能となる。
また、カーボン製断熱材などの断熱材を石英ガラス製の容器に密封し、又は石英ガラスで覆うことで、断熱材の加熱時の発塵を抑えることができるので、光ファイバ母材の品質の悪化を防ぐことができる。
The optical fiber preform manufacturing apparatus of the present invention has a structure in which a heat shield disk including a heat insulating material is installed on the upper portion of the soot preform. Diffusion can be suppressed, the thermal efficiency of the heating furnace can be improved, and the soot preform can be sintered at a lower output.
In addition, by sealing a heat insulating material such as a carbon heat insulating material in a quartz glass container or covering it with quartz glass, dust generation during heating of the heat insulating material can be suppressed, so that the quality of the optical fiber preform can be improved. Deterioration can be prevented.

以下、図面を参照して本発明の実施形態を説明する。
図2は、本発明の光ファイバ母材製造装置の一実施形態を示す図である。本実施形態の光ファイバ母材製造装置10は、スートプリフォーム1(透明化後は光ファイバ母材2)を収容する炉心管3と、そのスートプリフォーム1を加熱するためのヒータ4と、スートプリフォーム1の上部に設置された断熱材を含む遮熱円盤5とを備えて構成されている。
Hereinafter, embodiments of the present invention will be described with reference to the drawings.
FIG. 2 is a diagram showing an embodiment of the optical fiber preform manufacturing apparatus of the present invention. An optical fiber preform manufacturing apparatus 10 according to this embodiment includes a furnace core tube 3 that houses a soot preform 1 (an optical fiber preform 2 after being transparent), a heater 4 for heating the soot preform 1, A heat shield disk 5 including a heat insulating material installed on the upper portion of the soot preform 1 is configured.

このスートプリフォーム1は、その上端に設けられたダミー棒4を、図示していない移動軸に固定し、この移動軸の上下動によって炉心管3内を上下方向に移動し、ヒータ6との相対位置を変更可能になっている。炉心管3は、石英ガラスによって作られている。   The soot preform 1 has a dummy rod 4 provided at the upper end thereof fixed to a moving shaft (not shown), and is moved up and down in the core tube 3 by the vertical movement of the moving shaft. The relative position can be changed. The furnace core tube 3 is made of quartz glass.

図3は、スートプリフォーム1の上部に設置された断熱材を含む遮熱円盤5の第1の例を示す断面図である。本例の遮熱円盤5は、石英ガラスからなる蓋付容器状のガラス容器11内に、カーボン製断熱材12を収容し、このガラス容器11を密封状態とし、その中央の貫通孔をスートプリフォーム1のダミー棒4に挿通した構造になっている。   FIG. 3 is a cross-sectional view showing a first example of a heat shield disk 5 including a heat insulating material installed on the upper portion of the soot preform 1. The heat shield disk 5 of the present example accommodates a carbon heat insulating material 12 in a glass container 11 with a lid made of quartz glass, puts the glass container 11 in a sealed state, and inserts a through hole at its center into a soot. It is structured to be inserted through the dummy bar 4 of the reform 1.

ガラス容器11に収容される断熱材としては、カーボンファイバ等のカーボン製断熱材の他、グラスウールなどの無機繊維などを用いることができる。   As a heat insulating material accommodated in the glass container 11, in addition to carbon heat insulating materials such as carbon fibers, inorganic fibers such as glass wool can be used.

この遮熱円盤5を、図2に示すようにスートプリフォーム1の上部に設置し、脱水・透明化を行う場合、スートプリフォーム1をヒータ6により加熱する際に、炉心管3内の熱が上方に拡散するのを遮熱円盤5によって抑制でき、光ファイバ母材製造装置10の加熱炉の熱効率を向上でき、より低出力でスートプリフォーム1を焼結して透明な光ファイバ母材2を製造することができる。
また、カーボン製断熱材などの断熱材12を石英ガラス製の容器11に密封した遮熱円盤5を用いたことで、断熱材12の加熱時の発塵を抑えることができるので、光ファイバ母材の品質の悪化を防ぐことができる。図4に示すように、円盤状のカーボン製断熱材12のみを使用した場合には、高温加熱によりカーボン製断熱材12から発塵が生じ、それが光ファイバ母材2中に混入し、光ファイバ母材の紡糸時に光ファイバの機械強度を悪化させて断線等のトラブルを生じ易くなる。
When the heat shield disk 5 is installed on the upper portion of the soot preform 1 as shown in FIG. 2 to perform dehydration and transparency, the heat in the core tube 3 is heated when the soot preform 1 is heated by the heater 6. Can be suppressed by the heat shield disk 5, the thermal efficiency of the heating furnace of the optical fiber preform manufacturing apparatus 10 can be improved, and the soot preform 1 is sintered at a lower output to obtain a transparent optical fiber preform. 2 can be manufactured.
Further, since the heat shield disk 5 in which the heat insulating material 12 such as the carbon heat insulating material is sealed in the quartz glass container 11 can be used, dust generation at the time of heating the heat insulating material 12 can be suppressed. The deterioration of the quality of the material can be prevented. As shown in FIG. 4, when only the disk-shaped carbon heat insulating material 12 is used, dust is generated from the carbon heat insulating material 12 due to high-temperature heating, which is mixed into the optical fiber preform 2 and light. When the fiber preform is spun, the mechanical strength of the optical fiber is deteriorated to easily cause troubles such as disconnection.

図5は、本発明において用いる遮熱円盤の第2の例を示す断面図である。本例の遮熱円盤は、カーボン製断熱材12をガラス容器13内に完全に封入した構造になっている。
本例では、図3の遮熱円盤5を用いた場合と同様の効果を得ることができる。
FIG. 5 is a cross-sectional view showing a second example of the heat shield disk used in the present invention. The heat shield disk of this example has a structure in which the carbon heat insulating material 12 is completely enclosed in the glass container 13.
In this example, the same effect as the case where the heat shield disk 5 of FIG. 3 is used can be obtained.

(実施例1)
図3に示す円盤型のガラス容器にカーボン製断熱材を収容した遮熱円盤を、図2に示すようにスートプリフォームの上部に設置し、スートプリフォームの透明化を実施した。
本実施例では、円盤を使用しないときと比較して、加熱炉電力を10%程度削減して透明化することが可能であった。
また、この透明化した光ファイバ母材を光ファイバに線引きしたところ、遮熱円盤を使用しない母材と同様の機械強度を示した。
Example 1
As shown in FIG. 2, a soot preform was made transparent by installing a heat shield disc in which a carbon heat insulating material was housed in a disc-shaped glass container shown in FIG. 3.
In this example, it was possible to reduce the heating furnace power by about 10% and make it transparent as compared with the case where no disk was used.
Moreover, when this transparent optical fiber preform was drawn on an optical fiber, it showed the same mechanical strength as that of the preform that did not use a heat shield disk.

(比較例1)
図4に示すカーボン製断熱材12からなる遮熱円盤をスートプリフォームの上部に設置し、スートプリフォームの透明化を実施した。
本比較例では、円盤を使用しないときと比較して、加熱炉電力を10%程度削減して透明化することが可能であった。しかし、この透明化した光ファイバ母材を線引きした光ファイバの機械強度不良発生回数は、合計20回であった。
(Comparative Example 1)
A heat shield disk made of the carbon heat insulating material 12 shown in FIG. 4 was installed on the upper part of the soot preform, and the soot preform was made transparent.
In this comparative example, it was possible to make the heating furnace power transparent by reducing the heating furnace power by about 10% as compared with the case where no disk was used. However, the number of occurrences of mechanical strength defects in the optical fiber obtained by drawing the transparent optical fiber preform was 20 in total.

(実施例2)
図5に示すように、円盤型の密閉したガラス容器にカーボン製断熱材12を含む遮熱円盤を、図2に示すようにスートプリフォームの上部に設置し、スートプリフォームの透明化を実施した。
本実施例では、円盤を使用しないときと比較して、加熱炉電力を10%程度削減して透明化することが可能であった。
また、この透明化した光ファイバ母材を光ファイバに線引きしたところ、遮熱円盤を使用しない母材と同様の機械強度を示した。
この紡糸炉下部開口部を使用して10母材の紡糸を行った。その結果、光ファイバの機械強度不良発生回数は0回と良好であった。
(Example 2)
As shown in FIG. 5, a heat shielding disk including a carbon heat insulating material 12 in a disk-shaped sealed glass container is installed on the upper part of the soot preform as shown in FIG. 2, and the soot preform is made transparent. did.
In this example, it was possible to reduce the heating furnace power by about 10% and make it transparent as compared with the case where no disk was used.
Moreover, when this transparent optical fiber preform was drawn on an optical fiber, it showed the same mechanical strength as that of the preform that did not use a heat shield disk.
Ten base materials were spun using the lower opening of the spinning furnace. As a result, the number of occurrences of mechanical strength defects in the optical fiber was as good as zero.

(実施例3)
図3に示すように、円盤型のガラス容器にグラスウール製断熱材を収容した遮熱円盤を、図2に示すようにスートプリフォームの上部に設置し、スートプリフォームの透明化を実施した。
本実施例では、円盤を使用しないときと比較して、加熱炉電力を10%程度削減して透明化することが可能であった。
また、この透明化した光ファイバ母材を光ファイバに線引きしたところ、遮熱円盤を使用しない母材と同様の機械強度を示した。
(Example 3)
As shown in FIG. 3, a heat shield disc in which a glass wool heat insulating material was housed in a disc-shaped glass container was installed on the upper portion of the soot preform as shown in FIG. 2, and the soot preform was made transparent.
In this example, it was possible to reduce the heating furnace power by about 10% and make it transparent as compared with the case where no disk was used.
Moreover, when this transparent optical fiber preform was drawn on an optical fiber, it showed the same mechanical strength as that of the preform that did not use a heat shield disk.

従来の加熱炉を例示する概略構成図である。It is a schematic block diagram which illustrates the conventional heating furnace. 本発明の光ファイバ母材製造装置の一実施形態を示す概略構成図である。It is a schematic block diagram which shows one Embodiment of the optical fiber preform manufacturing apparatus of this invention. 遮熱円盤の第1の例を示す断面図である。It is sectional drawing which shows the 1st example of a heat insulation disk. 比較例で用いたカーボン製円盤を示す断面図である。It is sectional drawing which shows the carbon disk used in the comparative example. 遮熱円盤の第2の例を示す断面図である。It is sectional drawing which shows the 2nd example of a heat insulation disk.

符号の説明Explanation of symbols

1…スートプリフォーム、2…光ファイバ母材、3…炉心管、4…ダミー棒、5…遮熱円盤、6…ヒータ、10…光ファイバ母材製造装置、11…ガラス容器、12…カーボン製断熱材、13…ガラス容器。   DESCRIPTION OF SYMBOLS 1 ... Soot preform, 2 ... Optical fiber preform | base_material, 3 ... Core tube, 4 ... Dummy rod, 5 ... Heat insulation disk, 6 ... Heater, 10 ... Optical fiber preform manufacturing apparatus, 11 ... Glass container, 12 ... Carbon Heat-insulating material, 13 ... Glass container.

Claims (4)

スートプリフォームを炉心管内部に収容し、加熱して光ファイバ母材を製造する加熱炉を有する光ファイバ母材製造装置において、
スートプリフォームの上部に、断熱材を含む遮熱円盤を設置したことを特徴とする光ファイバ母材製造装置。
In an optical fiber preform manufacturing apparatus having a heating furnace that houses a soot preform in a furnace core tube and heats to produce an optical fiber preform,
An optical fiber preform manufacturing apparatus characterized in that a heat shield disk including a heat insulating material is installed on an upper portion of a soot preform.
スートプリフォームの上部に設置した遮熱円盤が、ガラス容器内に断熱材を収容した構造であることを特徴とする請求項1に記載の光ファイバ母材製造装置。   2. The optical fiber preform manufacturing apparatus according to claim 1, wherein the heat shield disk installed on the upper portion of the soot preform has a structure in which a heat insulating material is accommodated in a glass container. スートプリフォームの上部に設置した遮熱円盤が、カーボン製断熱材を含むことを特徴とする請求項1又は2に記載の光ファイバ母材製造装置。   The optical fiber preform manufacturing apparatus according to claim 1 or 2, wherein the heat shield disk installed on the upper portion of the soot preform includes a carbon heat insulating material. スートプリフォームの上部に設置した遮熱円盤が、グラスウール製断熱材を含むことを特徴とする請求項1又は2に記載の光ファイバ母材製造装置。   The optical fiber preform manufacturing apparatus according to claim 1 or 2, wherein the heat shield disk installed on the upper portion of the soot preform includes a glass wool heat insulating material.
JP2007334799A 2007-12-26 2007-12-26 Device of producing preform for optical fiber Pending JP2009155157A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103214180A (en) * 2012-01-19 2013-07-24 信越化学工业株式会社 Porous glass base material thermal insulating member and sintering method

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CN103214180A (en) * 2012-01-19 2013-07-24 信越化学工业株式会社 Porous glass base material thermal insulating member and sintering method
JP2013147379A (en) * 2012-01-19 2013-08-01 Shin-Etsu Chemical Co Ltd Porous glass base material thermal insulating member and sintering method
US9382148B2 (en) 2012-01-19 2016-07-05 Shin-Etsu Chemical Co., Ltd. Porous glass base material thermal insulating member and sintering method

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