JP2009017874A - Oil-in-water type emulsified oil and fat composition and method for producing the same - Google Patents

Oil-in-water type emulsified oil and fat composition and method for producing the same Download PDF

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JP2009017874A
JP2009017874A JP2008150675A JP2008150675A JP2009017874A JP 2009017874 A JP2009017874 A JP 2009017874A JP 2008150675 A JP2008150675 A JP 2008150675A JP 2008150675 A JP2008150675 A JP 2008150675A JP 2009017874 A JP2009017874 A JP 2009017874A
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oil
fat composition
water
emulsified oil
water emulsified
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JP5398178B2 (en
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Shunsuke Kutari
俊輔 久多里
Takashi Yanagida
崇至 柳田
Akio Sakaki
晃生 榊
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Kaneka Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To provide an oil-in-water type emulsified oil and fat composition having rich flavor (strong taste and strong smell), and fresh feeling, and to provide a new method for producing the composition. <P>SOLUTION: The method for producing the oil-in-water type emulsified oil and fat composition includes a steam-heating step (1) and an indirect cooling step (2) and does not include an evaporative cooling step for regulating a water content. Preferably, the end-point temperature in the steam-heating step (1) is 125-150°C in the method for producing the oil-in-water type emulsified oil and fat composition. The oil-in-water type emulsified oil and fat composition is obtained by the method. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は、水中油型乳化油脂組成物の殺菌方法、製造方法、更にはこれにより得られる水中油型乳化油脂組成物に関する。   The present invention relates to a sterilization method and a production method for an oil-in-water emulsified oil / fat composition, and further to an oil-in-water emulsified oil / fat composition obtained thereby.

ケーキなどのトッピングに使用されるホイップクリームや、パン菓子などに練り込み用途で使用される人工濃縮乳などのような水中油型乳化油脂組成物の製造方法は、通常、原料調整工程、加熱殺菌工程、冷却工程、充填工程の4工程を有している。   The manufacturing method for oil-in-water emulsified oils and fats such as whipped cream used for toppings such as cakes and artificial concentrated milk used for kneading in bread confectionery, etc. is usually the raw material adjustment step, heat sterilization It has four processes, a process, a cooling process, and a filling process.

この内、加熱殺菌工程、特に賞味期限の長い製品を製造するための加熱殺菌方法としては、食品に直接蒸気を作用させる蒸気直接加熱殺菌が多用されている(特許文献1)。この殺菌方法は、短時間で高温に加熱できることから、製品が受ける加熱によるダメージ(風味劣化等)が少なく、フレッシュ感が多い製品が製造可能となる。一方、この方法は蒸気を直接作用させるため、加熱量に応じて系中の水分増加が起こることが多く、加熱殺菌工程の後に設置されたフラッシュタンクにおいて真空引きし、蒸発冷却するのが通常であった。しかし、フラッシュタンクでの真空引きにより、水分と共に原材料の香気成分や高揮発性成分が除去されるため、製品の風味が薄っぺらくなってしまう問題があった。
特開平2−35038号公報
Among these, steam direct heat sterilization, in which steam directly acts on foods, is frequently used as a heat sterilization process, particularly a heat sterilization method for producing a product with a long shelf life (Patent Document 1). Since this sterilization method can be heated to a high temperature in a short time, it is possible to produce a product with little damage (flavor deterioration, etc.) due to heating received by the product and a lot of fresh feeling. On the other hand, since this method uses steam directly, moisture in the system often increases depending on the amount of heating, and it is normal to draw a vacuum in a flash tank installed after the heat sterilization step and evaporate and cool it. there were. However, there is a problem that the flavor of the product becomes thin because the aroma component and the highly volatile component of the raw material are removed together with moisture by evacuation in the flash tank.
JP-A-2-35038

本発明は、風味豊かで(味が強く、においが強い)、フレッシュ感がある水中油型乳化油脂組成物、更にはその新規製造方法、殺菌方法を提供することを目的とする。   An object of the present invention is to provide an oil-in-water emulsified oil composition that is rich in flavor (strong in taste and strong in smell) and has a fresh feeling, and further, a novel production method and a sterilization method thereof.

本発明者らは上記課題を解決するために鋭意研究を重ねた結果、蒸気加熱工程と間接冷却工程を含み、水分調整のための蒸発冷却工程を含まないことを特徴とする水中油型乳化油脂組成物の製造方法を提供した。これによれば、蒸発冷却での香気成分や高揮発性成分の減少を防止し、風味豊かな(味が強く、においが強い)、フレッシュ感がある水中油型乳化油脂組成物を提供することが可能となる。   As a result of intensive studies to solve the above problems, the present inventors have included a steam heating step and an indirect cooling step, and do not include an evaporative cooling step for moisture adjustment. A method for producing the composition was provided. According to this, an oil-in-water emulsified oil and fat composition that prevents aroma components and highly volatile components from being reduced by evaporative cooling, is rich in flavor (strong in taste, strong in smell), and has a fresh feeling. Is possible.

さらに、蒸気加熱工程での到達温度が、125℃〜150℃であることを特徴とする前記の水中油型乳化油脂組成物の製造方法を提供した。   Furthermore, the reached temperature in a steam heating process is 125 degreeC-150 degreeC, The manufacturing method of the said oil-in-water type emulsified oil-fat composition characterized by the above-mentioned was provided.

さらに、高周速の回転式乳化機による乳化工程が含まれることを特徴とする前記の水中油型乳化油脂組成物の製造方法を提供した。これによれば、仕込み時に水分調整したエマルションが不安定になりやすい水中油型乳化油脂組成物であっても、安定なエマルションの風味豊かな(味が強く、においが強い)、フレッシュ感がある水中油型乳化油脂組成物を提供することが可能となる。   Furthermore, the manufacturing method of the said oil-in-water type emulsified oil-fat composition characterized by including the emulsification process by the high-speed peripheral rotary emulsifier was provided. According to this, even if the emulsion whose water content was adjusted at the time of preparation is an oil-in-water emulsified oil composition, the flavor of the stable emulsion is rich (taste is strong and smell is strong), and there is a fresh feeling. It becomes possible to provide an oil-in-water emulsified oil and fat composition.

さらに、蒸気加熱工程に供する水中油型乳化油脂組成物の温度が75℃以上であることを特徴とする前記の水中油型乳化油脂組成物の製造方法を提供した。これによれば、蒸気による加熱温度幅を小さくすることができ、その分、増加水分量を抑制できる。しかも、蒸気加熱以外の加熱方法では加熱によるダメージが通常大きくなるが、その蒸気加熱以外の加熱方法を低温域の加熱に使用することで、加熱によるダメージをも防ぐことが可能となる。その結果、仕込み時での水分調整を容易におこなうことができ、安定なエマルションの風味豊かな(味が強く、においが強い)、フレッシュ感がある水中油型乳化油脂組成物を提供することが可能となる。   Furthermore, the temperature of the oil-in-water type emulsified oil-fat composition used for a steam heating process is 75 degreeC or more, The manufacturing method of the said oil-in-water type emulsified oil-fat composition characterized by the above-mentioned was provided. According to this, the heating temperature range by steam can be reduced, and the amount of increased moisture can be suppressed accordingly. In addition, although heating damage other than steam heating usually increases, heating damage other than steam heating can be prevented by using a heating method other than steam heating for low-temperature heating. As a result, it is possible to easily adjust the water content at the time of preparation, and to provide an oil-in-water emulsified oil / fat composition that is rich in the flavor of a stable emulsion (strong in taste and strong in smell) and has a fresh feeling. It becomes possible.

さらに、前記水中油型乳化油脂組成物の製造方法を用いて製造されたことを特徴とする水中油型乳化油脂組成物を提供した。   Furthermore, the present invention provides an oil-in-water emulsified oil / fat composition produced using the method for producing an oil-in-water emulsified oil / fat composition.

本発明の殺菌方法に従えば、風味豊かで(味が強く、においが強い)、フレッシュ感がある水中油型乳化油脂組成物を製造することが可能となる。   According to the sterilization method of the present invention, it is possible to produce an oil-in-water emulsified fat composition that is rich in flavor (strong in taste and strong in smell) and has a fresh feeling.

以下、本発明につき、さらに詳細に説明する。本発明の水中油型乳化油脂組成物は、通常、油脂を主成分とする油相と、水を主成分とする水相とからなり、水中に油滴が分散した形態であり、牛乳や生クリームといった天然由来の水中油型乳化油脂組成物や、人工の水中油型乳化油脂組成物も含む。水相又は油相中には、各種成分を含有していてもよい。各種成分としては、例えば、蛋白原料、乳化剤、糖類、安定剤・増粘剤、無機塩類などが挙げられ、それらを必要に応じて添加できる。   Hereinafter, the present invention will be described in more detail. The oil-in-water emulsified oil / fat composition of the present invention is usually composed of an oil phase mainly composed of oil and fat and an aqueous phase mainly composed of water, and is a form in which oil droplets are dispersed in water. Naturally derived oil-in-water emulsified oil and fat compositions such as creams and artificial oil-in-water emulsified oil and fat compositions are also included. Various components may be contained in the water phase or the oil phase. Examples of the various components include protein raw materials, emulsifiers, saccharides, stabilizers / thickeners, inorganic salts, and the like, which can be added as necessary.

前記油脂としては、食用であれば特に限定されないが、例えば、大豆油、綿実油、コーン油、サフラワー油、ヒマワリ種子油、オリーブ油、パーム油、パーム核油、ヤシ油、菜種油、ゴマ油、カポック油、落花生油、米糠油、胡麻油、月見草油、シア脂、サル脂、カカオ脂、マンゴー核油、イリッペ脂などの各種植物油脂、乳脂、牛脂、豚脂、魚油、鯨油などの各種動物油脂および、それらの分別、硬化、エステル交換等の処理をして得られる加工油脂、さらには市販のバター、マーガリン、またはショートニングあるいはハードバター等が挙げられ、これらを少なくとも1種用いることができる。   The oil and fat is not particularly limited as long as it is edible. For example, soybean oil, cottonseed oil, corn oil, safflower oil, sunflower seed oil, olive oil, palm oil, palm kernel oil, coconut oil, rapeseed oil, sesame oil, kapok oil Various vegetable oils such as peanut oil, rice bran oil, sesame oil, evening primrose oil, shea fat, monkey fat, cacao fat, mango kernel oil, iripe fat, various fats such as milk fat, beef fat, pork fat, fish oil, whale oil, and Processed fats and oils obtained by processing such as fractionation, curing, and transesterification, and commercially available butter, margarine, shortening, hard butter, and the like can be used, and at least one of them can be used.

前記蛋白原料としては、特に限定されないが、牛乳、脱脂乳、脱脂濃縮乳、加糖練乳、無糖練乳、全脂粉乳、脱脂粉乳、バターミルク、バターミルクパウダー、ホエー、ホエーパウダー、カゼイン、カゼインナトリウム、脂肪球皮膜タンパク、α−ラクトアルブミンやβ−ラクトグロブリン、血清アルブミン、生クリーム等の乳由来の蛋白質、更には卵蛋白質、大豆蛋白質、小麦蛋白質等の乳以外の蛋白質等を使用することができる。卵蛋白質としては、液状あるいは乾燥された卵黄、卵白、全卵及びこれらより分離される単一(単純)蛋白質、例えばオボアルブミン、コンアルブミン、オボムコイド、オボグロブリン、ホスビチン、リベチン、リン糖蛋白質、低密度リポ蛋白質、高密度リポ蛋白質等がある。大豆蛋白質としては、豆乳、脱脂大豆粉、濃縮大豆蛋白、分離大豆蛋白、脱脂豆乳粉末、大豆蛋白加水分解物等がある。小麦蛋白質としては、グリアジン、グルテニン、プロラミン、グルテリン等がある。また、その他動物性及び植物性蛋白質等の蛋白質も使用できる。これらの蛋白質は、目的に応じ少なくとも1種用いることができる。   The protein material is not particularly limited, but milk, skim milk, skim concentrated milk, sweetened condensed milk, sugar-free condensed milk, whole milk powder, skim milk powder, butter milk, butter milk powder, whey, whey powder, casein, casein sodium , Fat globule membrane protein, α-lactalbumin, β-lactoglobulin, serum albumin, milk-derived proteins such as fresh cream, and proteins other than milk such as egg protein, soy protein, wheat protein, etc. it can. Egg proteins include liquid or dried egg yolk, egg white, whole egg and single (simple) proteins separated from these, such as ovalbumin, conalbumin, ovomucoid, ovoglobulin, phosvitin, ribetin, phosphoglycoprotein, low There are density lipoprotein and high density lipoprotein. Examples of soy protein include soy milk, defatted soy flour, concentrated soy protein, separated soy protein, defatted soy milk powder, and soy protein hydrolysate. Wheat proteins include gliadin, glutenin, prolamin, glutelin and the like. In addition, other proteins such as animal and plant proteins can be used. These proteins can be used in accordance with the purpose.

前記乳化剤としては、特に限定されないが、大豆レシチン、卵黄レシチン、または、それらの酵素分解物、脂肪酸とグリセリンのエステル及びその誘導体(グリセリン脂肪酸エステル、酢酸モノグリセリド、乳酸モノグリセリド、クエン酸モノグリセリド、コハク酸モノグリセリド、ジアセチル酒石酸モノグリセリド、ポリグリセリン脂肪酸エステル、ポリグリセリン縮合リシノール酸エステル等)、ソルビタン脂肪酸エステル、プロピレングリコール脂肪酸エステル、ショ糖脂肪酸エステル、ショ糖酢酸イソ酪酸エステル、ステアロイル乳酸カルシウム、ステアロイル乳酸ナトリウム、ポリオキシエチレンソルビタンモノステアレート、ポリオキシエチレンソルビタンモノグリセリド等を挙げることができる。これらは、少なくとも1種用いることができる。   The emulsifier is not particularly limited, but it is soy lecithin, egg yolk lecithin, or an enzyme degradation product thereof, fatty acid and glycerin ester and derivatives thereof (glycerin fatty acid ester, acetic acid monoglyceride, lactic acid monoglyceride, citric acid monoglyceride, succinic acid monoglyceride , Diacetyltartaric acid monoglyceride, polyglycerin fatty acid ester, polyglycerin condensed ricinoleic acid ester, etc.), sorbitan fatty acid ester, propylene glycol fatty acid ester, sucrose fatty acid ester, sucrose acetate isobutyric acid ester, calcium stearoyl lactate, sodium stearoyl lactate, polyoxy Examples thereof include ethylene sorbitan monostearate and polyoxyethylene sorbitan monoglyceride. At least one of these can be used.

前記糖類としては、特に限定されないが、ブドウ糖、果糖、マンノース、キシロース、ショ糖、乳糖、麦芽糖、マルトース、トレハロース、マルトトリオース、オリゴ糖、フラクトオリゴ糖、ガラクトオリゴ糖、大豆オリゴ糖、乳果オリゴ糖、パラチノースオリゴ糖、異性化液糖、ショ糖結合水飴、酵素糖化水飴、還元乳糖、還元澱粉糖化物、還元糖ポリデキストロース、澱粉加水分解物、ソルビトール、マンニトール、マルチトール、エリスリトール、キシリトール、オリゴ糖アルコール、ラフィノース、ラクチュロース、ステビア、アスパルテーム等の糖類が挙げられる。これらは、少なくとも1種用いることができる。   The sugars are not particularly limited, but glucose, fructose, mannose, xylose, sucrose, lactose, maltose, maltose, trehalose, maltotriose, oligosaccharides, fructooligosaccharides, galactooligosaccharides, soybean oligosaccharides, and whey oligosaccharides. , Palatinose oligosaccharide, isomerized liquid sugar, sucrose-linked starch syrup, enzyme saccharified starch syrup, reduced lactose, reduced starch saccharified product, reduced sugar polydextrose, starch hydrolysate, sorbitol, mannitol, maltitol, erythritol, xylitol, oligosaccharide Examples include saccharides such as alcohol, raffinose, lactulose, stevia, and aspartame. At least one of these can be used.

前記安定剤・増粘剤としては、特に限定されないが、プルラン、サイリウム、アラビアガム、カラヤガム、トラガントガム、ジェランガム、グルコマンナン、グアーガム、キサンタンガム、タマリンド種子多糖、カラギーナン、アルギン酸塩、アルギン酸プロピレングリコールエステル、ファーセルラン、ローカストビーンガム、ペクチン、カルボキシメチルセルロース(CMC)、メチルセルロース(MC)、ヒドロキシエチルセルロース(HEC)、結晶セルロース、カードラン及びそれらの低分子化物、澱粉、化工澱粉、各種α化デンプン、ゼラチン、デキストリン、寒天、デキストラン等が挙げられる。これらの安定剤・増粘剤は、少なくとも1種用いることができる。   The stabilizer / thickening agent is not particularly limited. Cellulan, locust bean gum, pectin, carboxymethylcellulose (CMC), methylcellulose (MC), hydroxyethylcellulose (HEC), crystalline cellulose, curdlan and low molecular weight products thereof, starch, modified starch, various pregelatinized starches, gelatin, Examples include dextrin, agar and dextran. These stabilizers and thickeners can be used in at least one kind.

また、前記の蛋白原料、油脂、糖類は、脂質蛋白複合体や蛋白糖複合体などのような複合体を形成して含有させてもよい。   In addition, the protein raw material, fats and oils, and saccharides may be contained by forming a complex such as a lipid protein complex or a protein sugar complex.

前記無機塩類としては、特に限定されないが、食塩、岩塩、海塩、塩化カリウム、ヘキサメタリン酸塩、第2リン酸塩、第1リン酸塩、クエン酸のアルカリ金属塩(カリウム、ナトリウム等)、ポリリン酸塩、重曹等が挙げられる。これらは、少なくとも1種用いることができる。   Examples of the inorganic salts include, but are not limited to, salt, rock salt, sea salt, potassium chloride, hexametaphosphate, second phosphate, first phosphate, alkali metal salt of citric acid (potassium, sodium, etc.), Polyphosphate, baking soda, etc. are mentioned. At least one of these can be used.

この他、抽出物、着香料、調味料、乳製品、酵素処理物、pH調整剤、酵素、食品保存料、日持ち向上剤、酸化防止剤、果実、果汁、コーヒー、ナッツペースト、香辛料、カカオマス、ココアパウダー等を使用することができ、これらは、少なくとも1種用いることができる。   In addition, extracts, flavorings, seasonings, dairy products, enzyme-treated products, pH adjusters, enzymes, food preservatives, shelf life improvers, antioxidants, fruits, fruit juices, coffee, nut paste, spices, cacao mass, Cocoa powder or the like can be used, and at least one of them can be used.

本発明の水中油型乳化油脂組成物の製造方法は、蒸気加熱工程(1)と間接冷却工程(2)を含み、水分調整のための蒸発冷却工程を含まないことを特徴としている。また、高周速の回転式乳化機による乳化工程(3)を有することが好ましく、蒸気による水分の持ち込みを抑えるためには、蒸気加熱工程の前に予備加熱工程(4)を有する方が好ましい。これら以外に原料調整工程、ホールド工程、均質化工程、熟成工程、充填工程などの工程を有していても良い。具体的な製造方法を以下に例示する。   The method for producing an oil-in-water emulsified oil / fat composition of the present invention includes a steam heating step (1) and an indirect cooling step (2), and does not include an evaporative cooling step for moisture adjustment. Moreover, it is preferable to have the emulsification process (3) by the high-speed rotary emulsifier, and in order to suppress the carrying-in of the water | moisture content by a steam, it is more preferable to have a preheating process (4) before a steam heating process. . In addition to these, you may have processes, such as a raw material adjustment process, a holding process, a homogenization process, an aging process, and a filling process. Specific production methods are exemplified below.

<蒸気加熱工程(1)>
油脂を主成分とする油相と水を主成分とする水相を調整した後、それぞれを混合してから好ましくは乳化工程(3)を通してから、蒸気加熱工程(1)に供する。蒸気加熱工程(1)の前には、間接加熱による予備加熱を行うことが好ましい。
<Steam heating process (1)>
After preparing the oil phase which has fats and oils as a main component and the water phase which has water as a main component, after mixing each, Preferably after passing through an emulsification process (3), it uses for a steam heating process (1). Prior to the steam heating step (1), preheating by indirect heating is preferably performed.

本発明の蒸気加熱工程(1)における蒸気加熱とは、蒸気を直接、食品に作用させることで加熱する方法である。方式としては、例えば蒸気吹き込み方式(インジェクション方式)、インフュージョン方式等があり、蒸気加熱工程(1)には少なくとも何れかの方式を用いていればよい。前者は、食品に蒸気を直接吹き込む方式であり、装置としては、例えば、スチームインジェクション(岩井機械(株))がある。後者は、蒸気雰囲気中に食品を入れ込む方式であり、装置としては、例えば、スチームインフュージョンシステム(岩井機械(株))がある。本発明の目的であるフレッシュ感を残すためには、蒸気吹き込み方式がより好ましい。それは、蒸気吹き込み方式は、インフュージョン方式と比較し、高温での保持時間を正確に制御できるため、フレッシュ感を残存させやすい傾向があるからである。   The steam heating in the steam heating step (1) of the present invention is a method of heating by causing steam to act directly on food. Examples of the method include a steam blowing method (injection method) and an infusion method, and at least one of the methods may be used for the steam heating step (1). The former is a system in which steam is directly blown into food, and as an apparatus, for example, there is steam injection (Iwai Kikai Co., Ltd.). The latter is a system in which food is put into a steam atmosphere. As an apparatus, for example, there is a steam infusion system (Iwai Kikai Co., Ltd.). In order to leave the fresh feeling that is the object of the present invention, the steam blowing method is more preferable. This is because the steam blowing method can control the holding time at a high temperature more accurately than the infusion method, so that a fresh feeling tends to remain.

また、蒸気加熱工程(1)において、商業的滅菌を満足させるために、その到達温度が125℃〜150℃まで加熱されていることが好ましいく、より好ましくは140〜150℃で、特に蒸気加熱工程(1)の前に予備加熱工程(4)を行う場合は、予備加熱工程(4)によって加熱された温度より高い温度に到達させることが好ましい。一方、到達温度が150℃を越えると、加熱ダメージが大きくなってしまいフレッシュ感が失われる場合がある。蒸気加熱時間は、上記温度で2〜30秒間ホールドすることが好ましい。   Further, in the steam heating step (1), in order to satisfy commercial sterilization, the ultimate temperature is preferably heated to 125 ° C. to 150 ° C., more preferably 140 to 150 ° C., particularly steam heating. When performing a preheating process (4) before a process (1), it is preferable to make it reach the temperature higher than the temperature heated by the preheating process (4). On the other hand, if the ultimate temperature exceeds 150 ° C., the heat damage increases and the fresh feeling may be lost. The steam heating time is preferably held at the above temperature for 2 to 30 seconds.

<間接冷却工程(2)>
間接冷却工程(2)は、蒸気加熱工程(1)を介した後の高温状態から間接冷却で所望の温度まで冷却する工程で、クリーム等の水中油型乳化油脂組成物の製造に於いては、その結晶性の制御の点から、2〜15℃まで冷却することが好ましい。ここで間接冷却とは、冷却される対象物とそれ以外の物質との熱交換により冷却する方法であり、例えば、プレート式、チューブラー式、多管式、掻き取り式冷却方式や冷たい物質の混合などが挙げられるが、中でも熱交換能力が高い、プレート方式、多管式、掻き取り式冷却方式を用いるのが好ましい。間接冷却によれば、蒸発冷却を行う際とは異なり、香気成分や高揮発性成分が除去されにくく、風味豊かな水中油型乳化油脂組成物を提供することが容易となる。上記間接冷却は、1段階でも良いが、水中油型乳化油脂組成物の粒径を小さくしたい場合などは、1段目の間接冷却の後に2〜25MPaの条件で高圧ホモジナイザーをかけてから、好ましくは1段以上、より好ましくは2段以上の間接冷却を行う。そして、2段目以降の間接冷却工程に供される場合の水中油型乳化油脂組成物の粒径は、3.3μm以下であることが好ましい。間接冷却が終了した水中油型乳化油脂組成物は、タンクに移送される。
<Indirect cooling process (2)>
The indirect cooling step (2) is a step of cooling from the high temperature state after the steam heating step (1) to a desired temperature by indirect cooling, and in the production of an oil-in-water type emulsified oil and fat composition such as cream. From the viewpoint of controlling the crystallinity, it is preferable to cool to 2 to 15 ° C. Here, indirect cooling is a method of cooling by heat exchange between an object to be cooled and other substances, for example, a plate type, a tubular type, a multi-pipe type, a scraping type cooling method or a cold substance. Although mixing etc. are mentioned, it is preferable to use a plate system, a multi-tubular system, and a scraping type cooling system that has a high heat exchange capability. According to indirect cooling, unlike when evaporative cooling is performed, it is difficult to remove aroma components and highly volatile components, and it is easy to provide a flavor-rich oil-in-water emulsified oil and fat composition. The indirect cooling may be performed in one stage. However, when it is desired to reduce the particle size of the oil-in-water emulsified oil / fat composition, it is preferable to apply a high pressure homogenizer under the condition of 2 to 25 MPa after the first stage indirect cooling. Performs indirect cooling of one or more stages, more preferably two or more stages. And it is preferable that the particle size of the oil-in-water type emulsified oil-fat composition in the second and subsequent indirect cooling steps is 3.3 μm or less. The oil-in-water emulsified oil / fat composition after the indirect cooling is transferred to the tank.

<乳化工程(3)>
乳化工程は、一般にエマルションの粒径を微細化する等の方法で、水中油型乳化油脂組成物をより安定化する工程であり、蒸気加熱工程(1)前や1段目の間接冷却の後に設定することが好ましい。本発明の乳化工程においては各種乳化機を使用することが可能であるが、蒸気加熱工程(1)前には、高周速の回転式乳化機(周速が25m/秒以上の回転能力を有する乳化機)を使用することが好ましい。例えば、フィルミックス(プライミクス(株))、キャビトロン(キャビトロン社)、インライン型高せん断分散装置(IKA社)、ハイシェアミキサー(CHARLES ROSS&SON社)、クレアミックス(エム・テクニック(株))などが使用できる。特に本発明の、蒸気加熱工程(1)と間接冷却工程(2)を含み、水分調整のための蒸発冷却工程を含まない水中油型乳化油脂組成物の製造方法では、通常行われる蒸気加熱工程(1)と蒸発冷却工程(直接冷却工程)の組み合わせによる製造方法に比べ、その水中油型乳化油脂組成物の安定性が低下しやすく、この問題を解決する為に、通常の乳化機ではなく、高周速の回転式乳化機を使用することが好ましい。
<Emulsification step (3)>
The emulsification step is generally a step of further stabilizing the oil-in-water emulsified oil / fat composition by a method such as refining the particle size of the emulsion, and before the steam heating step (1) or after the first indirect cooling. It is preferable to set. Various emulsifiers can be used in the emulsification process of the present invention, but before the steam heating process (1), a high-speed rotary emulsifier (with a rotational speed of 25 m / sec or more). It is preferable to use an emulsifier). For example, Philmix (Primics Co., Ltd.), Cavitron (Cabitron Co., Ltd.), Inline type high shear disperser (IKA Co., Ltd.), High shear mixer (CHARLES ROSS & SON Co.), Claremix (M Technique Co., Ltd.) etc. it can. In particular, in the method for producing an oil-in-water emulsified oil composition comprising the steam heating step (1) and the indirect cooling step (2) of the present invention and not including the evaporative cooling step for moisture adjustment, the steam heating step usually performed Compared with the manufacturing method by the combination of (1) and the evaporative cooling process (direct cooling process), the stability of the oil-in-water emulsified oil / fat composition is likely to decrease, and in order to solve this problem, instead of a normal emulsifier It is preferable to use a high-speed rotating emulsifier.

また、前記蒸気加熱工程(1)前の高周速の回転式乳化機による乳化後には、さらに1〜20MPaの条件で高圧ホモジナイザーをかけることが好ましい。そして、前記蒸気加熱工程(1)に供される水中油型乳化油脂組成物の粒径は、3.5μm以下であることが好ましい。   Moreover, after emulsification by a high peripheral speed rotary emulsifier before the steam heating step (1), it is preferable to apply a high-pressure homogenizer under conditions of 1 to 20 MPa. And it is preferable that the particle size of the oil-in-water type emulsified oil-fat composition provided to the said steam heating process (1) is 3.5 micrometers or less.

尚、この乳化工程は、タンクなどを用いてバッチ式でおこなっても、インラインによる連続式でおこなっても良く、それらの組合せであるバッチ連続式でおこなっても良い。バッチ式の場合、含気・含泡の問題を生じやすいため、脱気処理できるタンクなどを用いておこなうことや、満液にしておこなうことが考えられる。この乳化工程を用いれば、安定なエマルションの風味豊かな水中油型乳化油脂組成物を製造することが容易となる。   In addition, this emulsification process may be performed by a batch system using a tank or the like, or may be performed by an in-line continuous system, or by a batch continuous system that is a combination thereof. In the case of a batch type, since problems of aeration and foaming are likely to occur, it can be considered to use a tank that can be degassed or filled up. If this emulsification process is used, it will become easy to manufacture the oil-in-water-type emulsified oil-fat composition with the rich flavor of a stable emulsion.

<予備加熱工程(4)>
本発明の水中油型乳化油脂組成物の製造方法においては、蒸気加熱工程(1)に供する水中油型乳化油脂組成物の温度が75℃以上であることが好ましい。言い換えると、蒸気加熱工程(1)の前に、予め加熱を行う予備加熱工程(4)を有していることが好ましい。予備加熱工程(4)における加熱方式としては、加熱時に水分を増加しない方法であることが特に好ましく、この様な方法としては、プレート式、チューブラー式、多管式や掻き取り式などの間接加熱方式や、通電加熱や電磁波加熱などの内部加熱方式が例示できる。より好ましい方法を具体的に示すと、水中油型乳化油脂組成物が、予備加熱工程(4)で加熱され、蒸気加熱工程(1)で好ましくは125℃〜150℃に、より好ましくは140〜150℃に加熱され、予備加熱工程(4)からの蒸気加熱工程(1)における昇温幅が、5〜75℃となる条件が特に好ましい。
<Preheating step (4)>
In the method for producing an oil-in-water emulsified oil / fat composition of the present invention, the temperature of the oil-in-water emulsified oil / fat composition subjected to the steam heating step (1) is preferably 75 ° C. or higher. In other words, it is preferable to have a preheating step (4) in which heating is performed in advance before the steam heating step (1). The heating method in the preheating step (4) is particularly preferably a method that does not increase moisture during heating. Such methods include indirect methods such as a plate method, a tubular method, a multi-tube method, and a scraping method. Examples of the heating method include internal heating methods such as current heating and electromagnetic wave heating. More specifically, the oil-in-water emulsified oil / fat composition is heated in the preheating step (4), preferably in the steam heating step (1), preferably from 125 ° C to 150 ° C, more preferably from 140 to It is particularly preferable that the heating temperature is 150 ° C., and the temperature increase width in the steam heating step (1) from the preheating step (4) is 5 to 75 ° C.

特に、この様に蒸気加熱工程(1)に供する水中油型乳化油脂組成物の温度が75℃以上、より好ましくは85〜130℃であると、蒸気による加熱温度幅を小さくすることができ、その分、工程中の増加水分量を抑制でき、代わりに仕込み時の水分量を多くすることが可能となって、製造がより容易となる。本来、最終製品の水分量と蒸気加熱工程(1)で増加する水分量を考慮して、仕込み時の水分量を決める必要があるが、蒸気加熱工程(1)で増加する水分量が多いと仕込み時の水分量を減らさざるをえず、油分を含む水中油型乳化油脂組成物において、相対的に仕込み時の油脂濃度が上昇し、エマルションが不安定になりやすい。また、蒸気加熱以外の加熱方法を使用すると、通常加熱によるダメージが大きくなるが、その蒸気加熱以外の加熱方法を低温域の加熱に使用することで、加熱によるダメージをも防ぐことが可能となる。   In particular, when the temperature of the oil-in-water emulsified oil and fat composition to be subjected to the steam heating step (1) is 75 ° C. or higher, more preferably 85 to 130 ° C., the heating temperature range by steam can be reduced, Accordingly, the increased amount of water in the process can be suppressed, and instead, the amount of water at the time of preparation can be increased, and the production becomes easier. Originally, it is necessary to determine the amount of moisture at the time of preparation in consideration of the amount of moisture in the final product and the amount of moisture increased in the steam heating step (1), but if the amount of moisture increased in the steam heating step (1) is large In the oil-in-water emulsified oil / fat composition containing oil, the oil / fat concentration at the time of charging relatively increases and the emulsion tends to become unstable. Further, when a heating method other than steam heating is used, damage due to normal heating is increased, but by using a heating method other than steam heating for heating in a low temperature region, damage due to heating can be prevented. .

本発明の殺菌後の水中油型乳化油脂組成物は、必要により冷蔵(0〜15℃)もしくは冷凍状態(−0℃以下)で保存してもよい。   The oil-in-water emulsified oil / fat composition after sterilization of the present invention may be stored in a refrigerated state (0 to 15 ° C.) or a frozen state (−0 ° C. or lower) as necessary.

本発明の水中油型乳化油脂組成物は、例えば、ホイップ用クリーム、コーヒー用クリーム、調理加工済みソース(ホワイトソース、グラタンなど)用クリーム、アイスクリーム、ソフトクリーム用プレミックス、パン、菓子、デザート、ハム、ソーセージ、食肉、魚肉、練り込み用油脂、マヨネーズ、ドレッシング、チーズ様食品、フラワーペースト、フィリング、トッピング、サンド、スプレッド等の加工食品用途に用いられる。   The oil-in-water emulsified oil / fat composition of the present invention includes, for example, whipped cream, coffee cream, cream for cooked sauce (white sauce, gratin, etc.), ice cream, soft cream premix, bread, confectionery, dessert , Ham, sausage, meat, fish, kneading oil, mayonnaise, dressing, cheese-like food, flower paste, filling, topping, sand, spread, etc.

以下に実施例を示し、本発明をより具体的に説明するが、本発明はこれらの実施例に何ら限定されるものではない。なお、実施例において「部」や「%」は重量基準である。   EXAMPLES Hereinafter, the present invention will be described more specifically with reference to examples. However, the present invention is not limited to these examples. In the examples, “parts” and “%” are based on weight.

<蒸発冷却工程>
比較例1における蒸発冷却工程とは、水分調整のためであり、高温状態にある製品を減圧下にせしめることで、水分を蒸発させ、その気化熱により冷却する工程であり、特に、蒸気加熱工程(1)で増加した水分量の3/4以上の量を低減する工程を意味する。蒸発冷却工程では、陰圧制御可能な(フラッシュタンクorデアレーター)タンクを使用した。
<Evaporative cooling process>
The evaporative cooling process in Comparative Example 1 is for adjusting the water content, and is a process of evaporating the water by letting the product in a high temperature state under reduced pressure, and cooling with the heat of vaporization. It means a step of reducing the amount of water more than 3/4 of the amount of water increased in (1). In the evaporative cooling process, a tank capable of controlling negative pressure (a flash tank or a deaerator) was used.

<官能評価>
実施例及び比較例で得られた水中油型乳化油脂組成物、プリン、ホワイトソース、パンナコッタを熟練した5人のパネラーに食べてもらい、以下の方法で点数化し、その平均点を評価点とした。水中油型乳化油脂組成物に関しては、風味の強さ、においの強さ、フレッシュ感を評価し、プリン、ホワイトソース、パンナコッタについては乳感、濃厚感について評価した。5点:強く感じる、4点:やや強く感じる、3点:やや弱く感じる、2点:弱く感じる、1点:ほとんど感じない。
<Sensory evaluation>
Oil-in-water emulsified oil and fat compositions obtained in Examples and Comparative Examples, pudding, white sauce, panna cotta were eaten by five experienced panelists, scored by the following method, and the average score was used as an evaluation score . With respect to the oil-in-water emulsified oil and fat composition, the strength of flavor, the strength of odor, and the fresh feeling were evaluated, and the pudding, white sauce, and panna cotta were evaluated for milk feeling and rich feeling. 5 points: feel strong, 4 points: feel slightly strong, 3 points: feel slightly weak, 2 points: feel weak, 1 point: hardly feel.

<水中油型乳化油脂組成物の粘度測定>
実施例及び比較例で得られた水中油型乳化油脂組成物を、5℃で2日間保管した後、B型粘度計(型番:BM型、TOKIMEC INC社製)にて測定した。
<Measurement of viscosity of oil-in-water emulsified oil / fat composition>
The oil-in-water emulsified oil / fat compositions obtained in Examples and Comparative Examples were stored at 5 ° C. for 2 days, and then measured with a B-type viscometer (model number: BM type, manufactured by TOKIMEC INC).

(実施例1) 水中油型乳化油脂組成物の作製
表1の配合と最終的に同じになるようにスチームインジェクション(蒸気加熱工程(1))での水分増加量を考慮して、水相と油相を調整し、65℃に温調・撹拌しながら予備乳化した。予備乳化液を調合タンクに投入し、均質化圧力を1.0MPaに調整したホモゲナイザーHV((株)イズミフードマシナリ社製)を用いて送液した。プレート式熱交換機(岩井機械工業(株)製)にて80℃まで予備加熱を行い(予備加熱工程(4))、スチームインジェクション(岩井機械工業(株))での加熱により140℃まで加熱した(蒸気加熱工程(1))。さらに、殺菌保持装置であるホールディングチューブにて140℃で4秒間保持し、チューブラー式熱交換機(岩井機械工業(株)製)により60℃まで冷却した後(間接冷却工程(2))、6.0MPaの均質化圧力の下で均質化処理をおこない、再び、プレート式熱交換機にて5℃まで冷却して(間接冷却工程(2))、水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Example 1) Preparation of oil-in-water emulsified oil / fat composition Considering the amount of water increase in steam injection (steam heating step (1)) so as to be finally the same as the formulation in Table 1, The oil phase was adjusted and pre-emulsified while adjusting the temperature to 65 ° C. and stirring. The pre-emulsified liquid was put into a preparation tank and fed using a homogenizer HV (manufactured by Izumi Food Machinery Co., Ltd.) whose homogenization pressure was adjusted to 1.0 MPa. Preheating was performed up to 80 ° C using a plate heat exchanger (Iwai Machine Industry Co., Ltd.) (preheating step (4)), and heating was performed up to 140 ° C using steam injection (Iwai Machine Industry Co., Ltd.). (Steam heating process (1)). Furthermore, after hold | maintaining at 140 degreeC for 4 second with the holding tube which is a sterilization holding | maintenance apparatus, and cooling to 60 degreeC with a tubular type heat exchanger (Iwai Machine Industry Co., Ltd. product) (indirect cooling process (2)), 6 The mixture was homogenized under a homogenization pressure of 0.0 MPa, and cooled again to 5 ° C. with a plate heat exchanger (indirect cooling step (2)) to obtain an oil-in-water emulsified oil / fat composition. The sensory evaluation and the viscosity after storage of the obtained oil-in-water emulsified oil / fat composition were evaluated, and the results are shown in Table 2.

(比較例1) 水中油型乳化油脂組成物の作製
間接冷却工程(2)において、ホールディングチューブにて140℃で4秒間保持した後、チューブラー式熱交換機の代わりに蒸発冷却器(岩井機械工業(株)製)を用いて80℃まで冷却した(蒸発冷却)以外は、実施例1と同様にして水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Comparative Example 1) Preparation of oil-in-water emulsified oil / fat composition In the indirect cooling step (2), after holding at 140 ° C for 4 seconds in a holding tube, an evaporative cooler (Iwai Kikai Kogyo Co., Ltd.) instead of a tubular heat exchanger The oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 1 except that the product was cooled to 80 ° C. using an evaporative cooling method. The sensory evaluation and the viscosity after storage of the obtained oil-in-water emulsified oil / fat composition were evaluated, and the results are shown in Table 2.

(比較例2) 水中油型乳化油脂組成物の作製
蒸気加熱工程(1)において、スチームインジェクション(岩井機械工業(株))の代わりに、予備加熱工程(4)で用いたプレート式熱交換機(岩井機械工業(株))で140℃まで加熱した以外は、実施例1と同様にして水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Comparative Example 2) Preparation of oil-in-water emulsified oil / fat composition In the steam heating step (1), instead of steam injection (Iwai Kikai Kogyo Co., Ltd.), a plate heat exchanger used in the preheating step (4) ( An oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 1 except that it was heated to 140 ° C. by Iwai Machine Industry Co., Ltd. The sensory evaluation and the viscosity after storage of the obtained oil-in-water emulsified oil / fat composition were evaluated, and the results are shown in Table 2.

(実施例2) 水中油型乳化油脂組成物の作製
予備乳化液を調合タンクとホモジナイザーHVの間に高周速乳化機(クレアミックス(エム・テクニック(株))を設置し、回転数20000rpm(周速31m/s)にて乳化した以外は、実施例1と同様にして水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Example 2) Preparation of oil-in-water emulsified oil / fat composition A pre-emulsified liquid was installed between a preparation tank and a homogenizer HV with a high peripheral speed emulsifier (Clearmix (M Technique Co., Ltd.)) and a rotational speed of 20000 rpm ( Except for emulsification at a peripheral speed of 31 m / s), an oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 1. The obtained oil-in-water emulsified oil / fat composition was subjected to sensory evaluation and viscosity after storage. The results are shown in Table 2.

(実施例3) 水中油型乳化油脂組成物の作製
予備加熱工程(4)において、プレート式熱交換機(岩井機械工業(株)製)での予備加熱を110℃まで加熱した以外は、実施例1と同様にして水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Example 3) Preparation of oil-in-water emulsified oil / fat composition Example in Example 2 except that preheating in plate type heat exchanger (Iwai Machine Industry Co., Ltd.) was heated to 110 ° C in preheating step (4). In the same manner as in No. 1, an oil-in-water emulsified oil / fat composition was obtained. The sensory evaluation and the viscosity after storage of the obtained oil-in-water emulsified oil / fat composition were evaluated, and the results are shown in Table 2.

(実施例4) 水中油型乳化油脂組成物の作製
予備乳化液を調合タンクとホモジナイザーHVの間に高周速乳化機(クレアミックス(エム・テクニック(株))を設置し、回転数20000rpm(周速31m/s)にて乳化した以外は、実施例3と同様にして水中油型乳化油脂組成物を得た。得られた水中油型乳化油脂組成物の官能評価及び保存後の粘度を評価し、その結果を表2に示した。
(Example 4) Preparation of oil-in-water emulsified oil / fat composition A pre-emulsified liquid was installed between a preparation tank and a homogenizer HV with a high peripheral speed emulsifier (Claremix (M Technique Co., Ltd.)), and a rotational speed of 20000 rpm ( Except for emulsification at a peripheral speed of 31 m / s), an oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 3. The resulting oil-in-water emulsified oil / fat composition was subjected to sensory evaluation and viscosity after storage. The results are shown in Table 2.

表2より分かるように、実施例1〜4で得られた水中油型乳化油脂組成物は、比較例1〜2と比較して、味・におい共に強く風味豊かでフレッシュ感のあるものであった。また、2日後の粘度では、実施例1のものは、商品レベルは満たすものの、少し乳化状態が芳しくなく、粘度が高い結果となったが、高周速乳化機の使用や予備加熱温度を上昇させることで、それを改善することができていることがわかった。   As can be seen from Table 2, the oil-in-water emulsified oil / fat compositions obtained in Examples 1 to 4 were stronger and richer in flavor and smell than those in Comparative Examples 1 and 2, and had a fresh feeling. It was. In addition, in the viscosity after 2 days, although the product of Example 1 satisfies the product level, the emulsified state is not good and the viscosity is high, but the use of a high peripheral speed emulsifier and the preheating temperature are increased. It was found that it was possible to improve it.

(実施例5) 水中油型乳化油脂組成物及びプリンの作製
表3の配合と最終的に同じになるようにスチームインジェクション(蒸気加熱工程(1))での水分増加量を考慮して、水相と油相を調整し、65℃に温調・撹拌しながら予備乳化した。予備乳化液を調合タンクに投入し、均質化圧力を5.0MPaに調整したホモゲナイザーHV((株)イズミフードマシナリ社製)を用いて送液した。プレート式熱交換機(岩井機械工業(株)製)にて80℃まで予備加熱を行い(予備加熱工程(4))、スチームインジェクション(岩井機械工業(株))での加熱により140℃まで加熱した(蒸気加熱工程(1))。さらに、殺菌保持装置であるホールディングチューブにて140℃で4秒間保持し、チューブラー式熱交換機(岩井機械工業(株)製)により60℃まで冷却した後(間接冷却工程(2))、15.0MPaの均質化圧力の下で均質化処理をおこない、再び、プレート式熱交換機にて5℃まで冷却して(間接冷却工程(2))、水中油型乳化油脂組成物を得た(表4)。
(Example 5) Preparation of oil-in-water emulsified oil / fat composition and pudding Water in consideration of the amount of water increase in steam injection (steam heating step (1)) so as to be finally the same as the formulation in Table 3 The phase and the oil phase were adjusted and pre-emulsified while adjusting the temperature to 65 ° C. and stirring. The pre-emulsified liquid was put into the preparation tank and fed using a homogenizer HV (manufactured by Izumi Food Machinery Co., Ltd.) whose homogenization pressure was adjusted to 5.0 MPa. Preheating was performed up to 80 ° C using a plate heat exchanger (Iwai Machine Industry Co., Ltd.) (preheating step (4)), and heating was performed up to 140 ° C using steam injection (Iwai Machine Industry Co., Ltd.). (Steam heating process (1)). Furthermore, after hold | maintaining at 140 degreeC with the holding tube which is a disinfection holding | maintenance apparatus for 4 second, and cooling to 60 degreeC with the tubular type heat exchanger (Iwai Machine Industry Co., Ltd. product), (indirect cooling process (2)), 15 A homogenization treatment was performed under a homogenization pressure of 0.0 MPa, and the mixture was again cooled to 5 ° C. with a plate heat exchanger (indirect cooling step (2)) to obtain an oil-in-water emulsified oil / fat composition (Table) 4).

得られた水中油型乳化油脂組成物を用いて、表5の配合で、下記の通りの常法に従い、プリンを作製した。即ち、グラニュー糖と全卵を混ぜ撹拌した後、上記で得た水中油型乳化油脂組成物、水、バニラエッセンスを添加し撹拌後、プリンカップに移し、アルミホイルで覆って150℃、35分湯煎焼きした。その後、アルミホイルを外して150℃で5分湯煎焼きしてプリンを得、その官能評価結果は、表5に示した。   Using the obtained oil-in-water emulsified oil / fat composition, purines were prepared according to the conventional method as shown below with the formulation shown in Table 5. That is, after mixing and stirring granulated sugar and whole egg, the oil-in-water emulsified oil / fat composition obtained above, water and vanilla essence were added, stirred, transferred to a pudding cup, covered with aluminum foil, 150 ° C., 35 minutes Yakisaki. Thereafter, the aluminum foil was removed, and the pudding was obtained by boiling in water at 150 ° C. for 5 minutes. The sensory evaluation results are shown in Table 5.

(比較例3) 水中油型乳化油脂組成物及びプリンの作製
間接冷却工程(2)において、ホールディングチューブにて140℃で4秒間保持した後、チューブラー式熱交換機の代わりに蒸発冷却器(岩井機械工業(株)製)を用いて80℃まで冷却した以外は、実施例5と同様にして水中油型乳化油脂組成物を得た(表4)。得られた水中油型乳化油脂組成物を用いて、実施例5と同様にしてプリンを得、その官能評価結果は、表5に示した。
(Comparative Example 3) Preparation of oil-in-water emulsified oil / fat composition and pudding In an indirect cooling step (2), after holding for 4 seconds at 140 ° C in a holding tube, an evaporative cooler (Iwai) was used instead of a tubular heat exchanger. An oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 5 except that it was cooled to 80 ° C. using a machine industry) (Table 4). Using the obtained oil-in-water emulsified oil and fat composition, pudding was obtained in the same manner as in Example 5, and the sensory evaluation results are shown in Table 5.

表5から明らかなように、実施例5は、比較例3と比較して、乳感、濃厚感共に豊かなものであった。   As is apparent from Table 5, Example 5 was richer in both milkiness and richness than Comparative Example 3.

(実施例6) 水中油型乳化油脂組成物及びホワイトソースの作製
表6の配合とした以外は、実施例5と同様にして水中油型乳化油脂組成物を得た(表7)。得られた水中油型乳化油脂組成物を用いて、表8の配合で、下記の通りの常法に従い、ホワイトソースを作製した。即ち、ホワイトルーを木ベラで伸ばした後、上記で得た水中油型乳化油脂組成物を加え十分に伸ばし、コンソメ、チーズ、レモン果汁、水の順番で材料を添加し、品温が85℃になるまで加熱を続けてホワイトソースを得、その官能評価結果は、表8に示した。
(Example 6) Production of oil-in-water emulsified oil / fat composition and white sauce An oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 5 except that the composition shown in Table 6 was used (Table 7). Using the obtained oil-in-water emulsified oil / fat composition, a white sauce was prepared according to the conventional method shown below with the formulation shown in Table 8. That is, after extending white roux with a wooden spatula, add the oil-in-water emulsified oil and fat composition obtained above, fully extend, add ingredients in the order of consomme, cheese, lemon juice, water, the product temperature is 85 ℃ Heating was continued until a white sauce was obtained, and the sensory evaluation results are shown in Table 8.

(比較例4) 水中油型乳化油脂組成物及びホワイトソースの作製
間接冷却工程(2)において、ホールディングチューブにて140℃で4秒間保持した後、チューブラー式熱交換機の代わりに蒸発冷却器(岩井機械工業(株)製)を用いて80℃まで冷却した以外は、実施例6と同様にして水中油型乳化油脂組成物を得た(表7)。得られた水中油型乳化油脂組成物を用いて、実施例6と同様にしてホワイトソースを得、その官能評価結果は、表8に示した。
(Comparative example 4) Preparation of oil-in-water emulsified oil and fat composition and white sauce In the indirect cooling step (2), after holding at 140 ° C for 4 seconds in a holding tube, an evaporative cooler (instead of a tubular heat exchanger) An oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 6 except that it was cooled to 80 ° C. using Iwai Machine Industry Co., Ltd. (Table 7). Using the obtained oil-in-water emulsified oil / fat composition, white sauce was obtained in the same manner as in Example 6, and the sensory evaluation results are shown in Table 8.

表8から明らかなように、実施例6のホワイトソースは、比較例4のホワイトソースと比較して、乳感、濃厚感共に豊かなものであった。   As is apparent from Table 8, the white sauce of Example 6 was richer in both milkiness and richness than the white sauce of Comparative Example 4.

(実施例7) 水中油型乳化油脂組成物及びパンナコッタの作製
フレッシュクリーム(47%)を65℃に温調した。その後、均質化圧力を0.5MPaに調整したホモゲナイザーHV((株)イズミフードマシナリ社製)を用いて送液した。プレート式熱交換機(岩井機械工業(株)製)にて80℃まで予備加熱を行い(予備加熱工程(4))、スチームインジェクション(岩井機械工業(株))での加熱により140℃まで加熱した(蒸気加熱工程(1))。さらに、殺菌保持装置であるホールディングチューブにて140℃で4秒間保持し、プレート式熱交換機(岩井機械工業(株)製)により60℃まで冷却した後(間接冷却工程(2))、1.0MPaの均質化圧力の下で均質化処理をおこない、再び、プレート式熱交換機にて5℃まで冷却して(間接冷却工程(2))、水中油型乳化油脂組成物を得た(表9)。得られた水中油型乳化油脂組成物を用いて、表10の配合で、下記の通りの常法に従い、パンナコッタを作製した。即ち、上記で得た水中油型乳化油脂組成物、牛乳に、はちみつを添加し加温した。それからゼラチンを加え溶解させた後、バニラエッセンスを加え、冷蔵庫で冷やし固め、パンナコッタを得、その官能評価結果は、表10に示した。
(Example 7) Production of oil-in-water emulsified oil / fat composition and panna cotta Fresh cream (47%) was temperature-controlled at 65 ° C. Then, it liquid-fed using the homogenizer HV (made by Izumi Food Machinery Co., Ltd.) which adjusted the homogenization pressure to 0.5 MPa. Preheating was performed up to 80 ° C using a plate heat exchanger (Iwai Machine Industry Co., Ltd.) (preheating step (4)), and heating was performed up to 140 ° C using steam injection (Iwai Machine Industry Co., Ltd.). (Steam heating process (1)). Furthermore, after holding at 140 ° C. for 4 seconds with a holding tube as a sterilization holding device and cooling to 60 ° C. with a plate heat exchanger (manufactured by Iwai Machine Industry Co., Ltd.) (indirect cooling step (2)), A homogenization treatment was performed under a homogenization pressure of 0 MPa, and the mixture was again cooled to 5 ° C. with a plate heat exchanger (indirect cooling step (2)) to obtain an oil-in-water emulsified oil / fat composition (Table 9). ). Using the obtained oil-in-water emulsified oil / fat composition, a panna cotta was prepared according to a conventional method as shown below with the formulation shown in Table 10. That is, honey was added to the oil-in-water emulsified oil composition and milk obtained above and heated. Then, after gelatin was added and dissolved, vanilla extract was added and cooled and hardened in a refrigerator to obtain a panna cotta. The sensory evaluation results are shown in Table 10.

(比較例5) 水中油型乳化油脂組成物及びパンナコッタの作製
間接冷却工程(2)において、ホールディングチューブにて140℃で4秒間保持した後、チューブラー式熱交換機の代わりに蒸発冷却器(岩井機械工業(株)製)を用いて80℃まで冷却した。その後、実施例7と水分が同じになるように水分調整を行った以外は、実施例7と同様にして水中油型乳化油脂組成物を得た(表9)。得られた水中油型乳化油脂組成物を用いて、実施例7と同様にしてパンナコッタを得、その官能評価結果は、表10に示した。
(Comparative Example 5) Preparation of oil-in-water emulsified oil / fat composition and panna cotta In indirect cooling step (2), after holding at 140 ° C for 4 seconds in a holding tube, an evaporative cooler (Iwai) was used instead of a tubular heat exchanger. The product was cooled to 80 ° C. using a machine industry). Thereafter, an oil-in-water emulsified oil / fat composition was obtained in the same manner as in Example 7 except that the water content was adjusted to be the same as in Example 7 (Table 9). Using the obtained oil-in-water emulsified oil / fat composition, a panna cotta was obtained in the same manner as in Example 7. The sensory evaluation results are shown in Table 10.

表10から明らかなように、実施例7は、比較例5と比較して、乳感、濃厚感共に豊かなものであった。   As is apparent from Table 10, Example 7 was richer in both milkiness and richness than Comparative Example 5.

Claims (7)

蒸気加熱工程(1)と間接冷却工程(2)を含み、水分調整のための蒸発冷却工程を含まないことを特徴とする水中油型乳化油脂組成物の製造方法。   A method for producing an oil-in-water emulsified oil-fat composition comprising a steam heating step (1) and an indirect cooling step (2), and not including an evaporative cooling step for moisture adjustment. 蒸気加熱工程(1)での到達温度が、125℃〜150℃であることを特徴とする請求項1に記載の水中油型乳化油脂組成物の製造方法。   2. The method for producing an oil-in-water emulsified oil / fat composition according to claim 1, wherein an ultimate temperature in the steam heating step (1) is 125 ° C. to 150 ° C. 3. 蒸気加熱工程(1)での加熱方式が、蒸気吹き込み方式及び/又はインフュージョン方式であることを特徴とする請求項1又は2に記載の水中油型乳化油脂組成物の製造方法。   The method for producing an oil-in-water emulsified oil / fat composition according to claim 1 or 2, wherein the heating method in the steam heating step (1) is a steam blowing method and / or an infusion method. 間接冷却工程(2)での冷却方式が、プレート式、チューブラー式、多管式、或いは、掻き取り式冷却方式から選ばれる1以上の冷却方式であることを特徴とする請求項1〜3の何れか一項に記載の水中油型乳化油脂組成物の製造方法。   The cooling method in the indirect cooling step (2) is one or more cooling methods selected from a plate type, a tubular type, a multi-tube type, or a scraping type cooling method. The manufacturing method of the oil-in-water type emulsified oil-fat composition as described in any one of these. 高周速の回転式乳化機による乳化工程(3)が含まれることを特徴とする請求項1〜4の何れか一項に記載の水中油型乳化油脂組成物の製造方法。   The method for producing an oil-in-water emulsified oil / fat composition according to any one of claims 1 to 4, further comprising an emulsification step (3) using a rotary emulsifier at a high peripheral speed. 蒸気加熱工程(1)に供する水中油型乳化油脂組成物の温度が75℃以上であることを特徴とする請求項1〜5の何れか一項に記載の水中油型乳化油脂組成物の製造方法。   The temperature of the oil-in-water type emulsified oil and fat composition to be subjected to the steam heating step (1) is 75 ° C or higher, and the production of the oil-in-water type emulsified oil and fat composition according to any one of claims 1 to 5 Method. 請求項1〜6の何れか一項に記載の製造方法を用いて製造された水中油型乳化油脂組成物。   The oil-in-water type emulsified fat composition manufactured using the manufacturing method as described in any one of Claims 1-6.
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