JP2008266284A - Method for evaluating controlling effect of agent support material on insect harmful to fiber - Google Patents

Method for evaluating controlling effect of agent support material on insect harmful to fiber Download PDF

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JP2008266284A
JP2008266284A JP2007264154A JP2007264154A JP2008266284A JP 2008266284 A JP2008266284 A JP 2008266284A JP 2007264154 A JP2007264154 A JP 2007264154A JP 2007264154 A JP2007264154 A JP 2007264154A JP 2008266284 A JP2008266284 A JP 2008266284A
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product storage
fiber
storage area
textile product
textile
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Masayo Sugano
雅代 菅野
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Sumitomo Chemical Co Ltd
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Sumitomo Chemical Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for evaluating the controlling effect of an agent support material on insects harmful to fiber. <P>SOLUTION: A test space that is composed of a fiber product storage section (A) where an agent support material having an agent that can take the controlling effect on the harmful insects to fiber supported by a substrate and a fiber product are stored in a fiber product container and another fiber product storage section (B) where at least a fiber product is stored in a fiber product container and the agent support material is not stored, is closed so as to prevent the harmful insects to fiber from escaping. The controlling effect of the agent support material on harmful insects to fibers can be evaluated by the method for evaluating the controlling effect of the agent support material on harmful insects to fiber that includes a step and the like for placing the harmful insects to fiber on the outside of the fiber product storage section (A) and the fiber product storage section (B) in the test space. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は、薬剤保持体の繊維害虫に対する防除効力の評価方法に関する。   The present invention relates to a method for evaluating the control effect of a drug carrier against fiber pests.

従来、繊維害虫を防除するために多くの繊維害虫防除剤が開発され実用に供されている。また、繊維害虫を防除する形態としては、殺虫、忌避、孵化阻害及び食害防止等の数多くの形態が存在するため、これらの繊維害虫防除剤の開発においては多くの評価方法が用いられることが知られている。
孵化阻害効力の評価方法としては、例えば、繊維製品（布、衣服等）の収納容器内に、繊維製品及び繊維害虫防除剤を収納し、一定期間経過後に繊維害虫の卵などを併せて収納することにより、その後の供試した卵の観察結果から該繊維害虫防除剤の孵化阻害効力を評価する手法が挙げられる（例えば、特許文献１参照。）。 Conventionally, many fiber pest control agents have been developed and put into practical use for controlling fiber pests. In addition, there are many forms for controlling fiber pests, such as insecticide, repellent, hatching inhibition and food damage prevention, and it is known that many evaluation methods are used in the development of these fiber pest control agents. It has been.
As a method for evaluating the hatching inhibitory effect, for example, a textile product and a textile pest control agent are accommodated in a textile container (cloth, clothes, etc.), and a textile insect pest is stored together after a certain period of time. By this, the technique of evaluating the hatching inhibitory effect of this fiber pest control agent from the observation result of the tested egg after that is mentioned (for example, refer patent document 1).

特開平１０−２３６９０５号公報JP-A-10-236905

本発明は、新たな薬剤保持体の繊維害虫に対する防除効力の評価方法を提供することを課題とする。   This invention makes it a subject to provide the evaluation method of the control effect with respect to the fiber pest of a new chemical | medical agent holder.

本発明者は、新たな薬剤保持体の繊維害虫に対する防除効力の評価方法を見出すべく検討した結果、下記に示される新たな方法を見出し、本発明に到った。
すなわち本発明は、
基材に繊維害虫に対する防除効力を示し得る薬剤が保持されてなる薬剤保持体、及び、繊維製品が繊維製品収納容器に収納されてなる繊維製品収納区（Ａ）
と、
少なくとも繊維製品が繊維製品収納容器に収納されてなり、かつ前記薬剤保持体が収納されていない繊維製品収納区（Ｂ）
とを収容し、繊維害虫が逃亡しないように閉鎖された試験空間において、該試験空間内部のうち、該繊維製品収納区（Ａ）及び該繊維製品収納区（Ｂ）の外部に繊維害虫を供試する工程（Ｉ）、
前記工程（Ｉ）における繊維害虫の供試から一定時間経過後に、該繊維製品収納区（Ａ）と該繊維製品収納区（Ｂ）との各々の繊維製品収納容器内部に存在する繊維害虫の虫数及び卵数のうち少なくとも一方の数値を求める工程（II）、
及び、
前記工程（II）で求められる該繊維製品収納区（Ａ）における数値と該繊維製品収納区（Ｂ）における数値とを対比する工程（III）、
を有してなる薬剤保持体の繊維害虫に対する防除効力の評価方法（以下、本発明評価方法と記す場合もある。）を提供するものである。 As a result of studying to find out a method for evaluating the control effect of a new drug carrier on fiber pests, the present inventor found a new method shown below and arrived at the present invention.
That is, the present invention
A medicine holder in which a medicine capable of exhibiting a pest control effect on fiber pests is held on a base material, and a textile product storage area (A) in which textile products are stored in a textile product storage container
When,
Textile product storage area (B) in which at least the textile product is stored in a textile product storage container and the medicine holder is not stored
In the test space closed so that the fiber pests do not escape, the fiber pests are provided outside the fiber product storage area (A) and the fiber product storage area (B) in the test space. Step (I) to try,
Insects of fiber pests present in the fiber product storage containers of the fiber product storage area (A) and the fiber product storage area (B) after a lapse of a certain time from the test of the fiber pest in the step (I) The step of obtaining at least one of the number and the number of eggs (II),
as well as,
Step (III) for comparing the numerical value in the textile product storage area (A) and the numerical value in the textile product storage area (B) determined in the step (II),
The present invention provides a method for evaluating the control effect of a pharmaceutical carrier having a pest against fiber pests (hereinafter sometimes referred to as the present invention evaluation method).

本発明評価方法により、薬剤保持体の繊維害虫に対する防除効力を評価することができる。   By the evaluation method of the present invention, it is possible to evaluate the control effect of the drug holder against fiber pests.

本発明評価方法とは、下記の工程（Ｉ）、（II）及び（III）を有してなるものである。   The evaluation method of the present invention comprises the following steps (I), (II) and (III).

・工程（Ｉ）
基材に繊維害虫に対する防除効力を示し得る薬剤が保持されてなる薬剤保持体、及び、繊維製品が繊維製品収納容器に収納されてなり、かつ前記薬剤保持体が収納されていない繊維製品収納区（Ａ）と、少なくとも繊維製品が繊維製品収納容器に収納されてなる繊維製品収納区（Ｂ）とを収容し、繊維害虫が逃亡しないように閉鎖された試験空間において、該試験空間内部のうち、該繊維製品収納区（Ａ）及び該繊維製品収納区（Ｂ）の外部に繊維害虫を供試する工程。 ・ Process (I)
A drug holder in which a drug capable of exhibiting a pest control effect on fiber pests is held on a base material, and a fiber product storage area in which a fiber product is stored in a fiber product storage container and the drug holder is not stored (A) and at least a fiber product storage area (B) in which the fiber product is stored in a fiber product storage container, and in a test space closed so that fiber pests do not escape, , A step of testing fiber pests outside the textile product storage area (A) and the textile product storage area (B).

本発明に用いられる繊維害虫に対する防除効力を示し得る薬剤（以下、本薬剤と記す場合もある。）とは、本発明により繊維害虫に対する防除効力を確認しようとするものであれば特に限定されるものではないが、具体的には、例えば２，３，５，６−テトラフルオロ−４−メチルベンジル ３−（１−プロペニル）−２，２−ジメチルシクロプロパンカルボキシラート、２，３，５，６−テトラフルオロ−４−メトキシメチルベンジル ３−（１−プロペニル）−２，２−ジメチルシクロプロパンカルボキシラート、２，３，５，６−テトラフルオロ−４−メトキシベンジル ３−（１−プロペニル）−２，２−ジメチルシクロプロパンカルボキシラート、２，３，５，６−テトラフルオロベンジル ３−（２，２−ジクロロビニル）−２，２−ジメチルシクロプロパンカルボキシラート及びエンペントリン等のピレスロイド化合物を有効成分として含有する薬剤が挙げられる。
本発明の薬剤保持体に用いられる基材とは、本薬剤を保持し得るものであれば特に限定されるものではなく、評価しようとする薬剤保持体の形態等にあわせて適宜選択して用いられるものであるが、具体的には例えば、紙、織布、不織布、パルプ、リンター、木材等の薬液吸収性担体からなる例えばマット状物またはシート状物等の繊維質基材が挙げられる。また、後記する繊維製品そのものを基材として用いることもできる。
本薬剤を基材に保持させる方法としては、例えば本薬剤又は本薬剤を含有する組成物を散布、含浸、塗布等により基材に保持させる方法が挙げられ、また基材が熱可塑性樹脂等の合成高分子である場合には、基材と本薬剤とを溶融混練し、成型加工する方法が挙げられる。かかる薬剤保持体は薬剤透過性を有する形状または材質からなる容器等に収納された形態で用いられてもよく、また繊維製品収納容器内で懸吊して用いるために吊り部材を具備するものであってもよい。さらに薬剤保持体はファン等の気流発生手段と組合わせて、該気流発生手段によって生起する気流により薬剤が繊維製品収納容器内の全体に拡散するような形態で設置されていてもよい。 The agent capable of showing the control effect on the fiber pest used in the present invention (hereinafter sometimes referred to as the present drug) is particularly limited as long as the control effect on the fiber pest is confirmed by the present invention. Specifically, for example, 2,3,5,6-tetrafluoro-4-methylbenzyl 3- (1-propenyl) -2,2-dimethylcyclopropanecarboxylate, 2,3,5, 6-tetrafluoro-4-methoxymethylbenzyl 3- (1-propenyl) -2,2-dimethylcyclopropanecarboxylate, 2,3,5,6-tetrafluoro-4-methoxybenzyl 3- (1-propenyl) -2,2-dimethylcyclopropanecarboxylate, 2,3,5,6-tetrafluorobenzyl 3- (2,2-dichlorovinyl) -2,2- Examples include drugs containing pyrethroid compounds such as dimethylcyclopropanecarboxylate and empentrin as active ingredients.
The base material used for the drug carrier of the present invention is not particularly limited as long as it can hold the drug, and is appropriately selected and used according to the form of the drug carrier to be evaluated. Specifically, for example, a fibrous base material such as a mat-like material or a sheet-like material made of a chemical solution-absorbing carrier such as paper, woven fabric, non-woven fabric, pulp, linter, and wood can be used. Moreover, the fiber product itself mentioned later can also be used as a base material.
Examples of the method of holding the drug on the base material include a method of holding the drug or a composition containing the drug on the base material by spraying, impregnation, coating, etc., and the base material is a thermoplastic resin or the like. In the case of a synthetic polymer, a method of melt-kneading the base material and the present drug and molding it can be mentioned. Such a drug holding body may be used in a form stored in a container or the like made of a drug-permeable shape or material, and is provided with a suspension member for hanging in a textile product storage container. There may be. Further, the medicine holder may be installed in combination with airflow generating means such as a fan so that the medicine is diffused throughout the fiber product storage container by the airflow generated by the airflow generating means.

本発明において、繊維製品収納区（Ａ）及び（Ｂ）に用いられる繊維製品収納容器としては、いずれも繊維製品が収納可能なものであって、繊維製品を収納するために通常用いられるものであれば特に限定されるものではなく、通常は繊維製品収納区（Ａ）及び（Ｂ）には同一の繊維製品収納容器が用いられる。その具体例としては例えば、箪笥（洋タンス、和タンス）、衣装箱（紙製、プラスチック製など）が挙げられる。その形状や大きさは特に限定されるものではないが、本発明に用いられる試験空間の大きさに対して、繊維製品収納容器（Ａ）及び（Ｂ）各々の空間占有率が容積比で通常０．１〜１０％、好ましくは０．３％〜５％程度の大きさのものが用いられる。
本発明に用いられる繊維製品としては、防虫剤が通常用いられる場所に収納される繊維製品であればよく、詳しくは、例えば衣服、下着類，織物、靴下、手袋、マフラー等の衣料、タオル、布地が挙げられる。 In the present invention, the fiber product storage containers used in the fiber product storage zones (A) and (B) are both those that can store fiber products and are usually used for storing fiber products. If there is no particular limitation, the same textile product storage container is usually used in the textile product storage areas (A) and (B). Specific examples thereof include a bag (Western chiffon, Japanese chiffon) and a costume box (made of paper, plastic, etc.). Although the shape and size are not particularly limited, the space occupancy of each of the textile storage containers (A) and (B) is usually in volume ratio with respect to the size of the test space used in the present invention. Those having a size of about 0.1 to 10%, preferably about 0.3% to 5% are used.
The fiber product used in the present invention may be a fiber product stored in a place where insect repellents are usually used. For example, clothes, underwear, fabrics, socks, gloves, scarves and other clothing, towels, Examples include fabrics.

繊維製品収納区（Ａ）と繊維製品収納区（Ｂ）とは、いずれも繊維製品収納容器に繊維製品が収納されている。また繊維製品収納区（Ａ）には前記した薬剤保持体が収納され、一方で繊維製品収納区（Ｂ）には薬剤保持体が収納されていない点で相異なるが、代わりに薬剤保持体に用いられる基材が本薬剤を保持しないまま収納されていてもよい。   In both the textile product storage area (A) and the textile product storage area (B), the textile product is stored in the textile product storage container. The textile storage area (A) stores the above-described drug holder, while the textile storage area (B) is different in that no medicine holder is stored. The base material used may be stored without holding the drug.

本発明の評価方法は繊維害虫が逃亡しないように閉鎖された試験空間において行われるものであるが、かかる試験空間の形状は、通常は、例えば正方体及び直方体等の角柱構造のような、面対称な構造体もしくはそれに類する構造体であり、また、供試した繊維害虫が逃亡しない程度の大きさの通気口などの開口部を有していてもよい。かかる試験空間において、繊維製品収納区（Ａ）と繊維製品収納区（Ｂ）とは前記面対称の対称面により対称となる位置に設置されることが好ましい。そしてその設置形態としては、通常の繊維製品収納容器が設置される形態、即ち底面部に接した状態での設置が挙げられる。   The evaluation method of the present invention is performed in a test space closed so that fiber pests do not escape, but the shape of such a test space is usually plane-symmetric, such as a prismatic structure such as a rectangular parallelepiped and a rectangular parallelepiped. Or a structure similar to the above structure, and may have an opening such as a vent of a size that does not allow the tested fiber pests to escape. In such a test space, it is preferable that the textile storage zone (A) and the textile storage zone (B) are installed at positions that are symmetric with respect to the plane of symmetry. And as the installation form, the installation in the state in which the normal textiles container is installed, ie, the state which contacted the bottom face part, is mentioned.

本発明により、薬剤保持体の防除効力を評価するために供試される繊維害虫としては、例えばイガ、コイガ、ヒメマルカツオブシムシ及びヒメカツオブシムシが挙げられる。
本発明の評価方法においては、繊維害虫を試験空間の内部のうち、繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の外部の空間に供試されるが、その供試場所として前記した試験空間内の対称面上であることが好ましい。
本発明においては、試験空間内に前記した繊維製品収納区（Ａ）と繊維製品収納区（Ｂ）とを設置した後、直ちに繊維害虫を供試してもよく、また設置後に一定期間経過してから供試してもよい。 Examples of the fiber pests used for evaluating the control effect of the drug carrier according to the present invention include iga, koiga, himemarukatsushimushi and himemekatsushimushi.
In the evaluation method of the present invention, fiber pests are tested in the space outside the fiber product storage area (A) and the fiber product storage area (B) within the test space. Preferably on a plane of symmetry in the test space.
In the present invention, after installing the fiber product storage area (A) and the fiber product storage area (B) in the test space, the fiber pest may be used immediately, or after a certain period of time has elapsed after installation. You may also try it.

・工程（II）
前記工程（Ｉ）における繊維害虫の供試から一定時間経過後に、該繊維製品収納区（Ａ）と該繊維製品収納区（Ｂ）との各々の繊維製品収納容器内部に存在する繊維害虫の虫数及び卵数のうち少なくとも一方の数値を求める工程。 ・ Process (II)
Insects of fiber pests present in the fiber product storage containers of the fiber product storage area (A) and the fiber product storage area (B) after a lapse of a certain time from the test of the fiber pest in the step (I) A step of determining at least one of the number and the number of eggs.

本発明においては、前記の工程（Ｉ）における繊維害虫の供試した状態を維持し、所定の期間経過した段階時点での薬剤保持体の効力を評価するものである。従って、即効性や残効性など薬剤保持体の評価しようとする特性等により、供試した状態を維持する期間は適宜選択され得るものであるが、通常は１日間〜１週間程度となる。
かかる期間経過後に、繊維製品収納区（Ａ）と繊維製品収納区（Ｂ）との各々の繊維製品収納容器内部に存在する繊維害虫の数をカウントするものであるが、かかる繊維害虫の数とは各々の繊維製品収納区の内部に侵入した供試虫の数であってもよく、また、各々の繊維製品収納区の内部に産卵された卵の数であってもよい。 In the present invention, the test state of the fiber pest in the step (I) is maintained, and the efficacy of the drug carrier at the stage when a predetermined period has elapsed is evaluated. Therefore, the period for maintaining the tested state can be appropriately selected depending on the characteristics of the drug carrier to be evaluated, such as immediate effect and residual effect, but it is usually about 1 day to 1 week.
After such a period has elapsed, the number of fiber pests present in the respective fiber product storage containers in the fiber product storage area (A) and the fiber product storage area (B) is counted. May be the number of test insects that have entered the interior of each textile product storage area, or the number of eggs laid in each textile product storage area.

・工程（III）
前記工程（II）で求められる該繊維製品収納区（Ａ）における数値と該繊維製品収納区（Ｂ）における数値とを対比する工程。 ・ Process (III)
A step of comparing the numerical value in the textile product storage area (A) determined in the step (II) with the numerical value in the textile product storage area (B).

前記工程（II）によって求められた繊維製品収納区（Ａ）と繊維製品収納区（Ｂ）との各々における繊維害虫（供試虫又は卵）の数とを対比することにより、当該試験に供試した薬剤保持体の効力を評価することができる。
より詳しくは、次式（ｉ）により、防除効力を算出することができる。

Figure 2008266284
By comparing the number of fiber pests (test insects or eggs) in each of the fiber product storage area (A) and the fiber product storage area (B) obtained in the step (II), the test was performed. The efficacy of the tested drug carrier can be evaluated.
More specifically, the control efficacy can be calculated by the following formula (i).

Figure 2008266284

前記式（ｉ）により算出される防除効力の数値が１００に近づくほど当該試験においては供試した薬剤保持体の効力が優れることとなり、防除効力の数値が０に近づくほど当該試験においては供試した薬剤保持体の効力が劣ることとなる。   The closer the control efficacy value calculated by the formula (i) is to 100, the better the efficacy of the drug carrier tested in the test, and the closer the control efficacy value is to 0, the test in the test. The effectiveness of the drug carrier thus obtained is inferior.

以下、本発明を試験例等の実施例により詳しく説明するが、本発明は当該実施例のみに限定されるものではない。   EXAMPLES Hereinafter, although this invention is demonstrated in detail by Examples, such as a test example, this invention is not limited only to the said Example.

参考例１
２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート ２ｇをエアゾール缶に入れ、該エアゾール缶にエアゾールバルブを装着した後、ジメチルエーテル ９８ｇを充填し、振とうを加え、アクチュエーターを装着することによりエアゾール製剤を得た。 Reference example 1
2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate 2 g as an aerosol An aerosol formulation was obtained by placing it in a can and attaching an aerosol valve to the aerosol can, filling 98 g of dimethyl ether, adding shake, and attaching an actuator.

参考例２
２，３，５，６−テトラフルオロ−４−メトキシメチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート ２ｇをエアゾール缶に入れ、該エアゾール缶にエアゾールバルブを装着した後、ジメチルエーテル ９８ｇを充填し、振とうを加え、アクチュエーターを装着することによりエアゾール製剤を得た。 Reference example 2
2,3,5,6-tetrafluoro-4-methoxymethylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate 2 g After putting in an aerosol can and mounting an aerosol valve on the aerosol can, 98 g of dimethyl ether was charged, shaken, and an actuator was obtained by mounting an actuator.

参考例３
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を直径 ８ｃｍの円盤型に切り取り、２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート ８０ｍｇのアセトン溶液を該濾紙に均一に塗布した後、アセトンを風乾させて薬剤保持体を得る。該薬剤保持体を図１に示されるファン１、軸２及び回転手段３と組み立てて、図２で示される電動モーター式の薬剤拡散装置を得る。 Reference example 3
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) is cut into a disk shape having a diameter of 8 cm, and 2,3,5,6-tetrafluoro-4-methyl Benzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate After 80 mg of an acetone solution was uniformly applied to the filter paper, the acetone was air-dried. To obtain a drug carrier. The drug holder is assembled with the fan 1, the shaft 2 and the rotating means 3 shown in FIG. 1 to obtain the electric motor type drug diffusion device shown in FIG.

参考例４
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を直径 ８ｃｍの円盤型に切り取り、２，３，５，６−テトラフルオロ−４−メトキシメチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート ８０ｍｇのアセトン溶液を該濾紙に均一に塗布した後、アセトンを風乾させて薬剤保持体を得る。該薬剤保持体を図１に示されるファン１、軸２及び回転手段３と組み立てて、図２で示される電動モーター式の薬剤拡散装置を得る。 Reference example 4
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) is cut into a disk shape having a diameter of 8 cm, and 2,3,5,6-tetrafluoro-4-methoxy Methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate After 80 mg of an acetone solution was uniformly applied to the filter paper, acetone was added. Air dry to obtain a drug carrier. The drug holder is assembled with the fan 1, the shaft 2 and the rotating means 3 shown in FIG. 1 to obtain the electric motor type drug diffusion device shown in FIG.

試験例１
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を１０ｃｍ×１５ｃｍに裁断し、２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート１００ｍｇのアセトン溶液を該濾紙に均一に塗布した後、アセトンを風乾させて薬剤保持体（以下、本保持体１と記す。）を得た。
内部に、本保持体１を服５着と１０ｃｍ×１０ｃｍのウール布とともに収納したビニ−ルロッカ−（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、本保持体１の代わりに２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラートを含有しない濾紙を用いた以外は繊維製品収納区（Ａ）と同様の操作を行ったビニ−ルロッカ−を繊維製品収納区（Ｂ）とした。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に無処理区をその長辺が沿うように配置した。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存した。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆った。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求めた。
その結果、当該試験における防除効力は１００％であった。 Test example 1
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) is cut into 10 cm × 15 cm, and 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate 100 mg of acetone solution was uniformly applied to the filter paper, and then acetone was air-dried. Thus, a drug holder (hereinafter referred to as the present holder 1) was obtained.
Inside, a vinyl rocker (84 cm × 50 cm × 163 cm) in which the holder 1 is housed together with five clothes and a 10 cm × 10 cm wool cloth is used as a textile product storage area (A). Contains 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate A vinyl rocker that was operated in the same manner as the textile product storage area (A) except that a non-filter paper was used was designated as the textile product storage area (B).
The textile product storage section (A) is arranged along one side of the bottom surface in the chamber (28 m 3 ) so that its long side is along, and the non-treatment section is arranged along one side opposite to one side of the bottom surface. did. About 200 adult moths were released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. The two small windows at the top of the chamber were opened and covered with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) was counted, and the control effect was determined by formula (i).
As a result, the control effect in the test was 100%.

試験例２
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を１０ｃｍ×１５ｃｍに裁断し、２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート１００ｍｇのアセトン溶液を該濾紙に均一に塗布した後、アセトンを風乾させて薬剤保持体（以下、本保持体１と記す。）を得た。
内部に、本保持体１を服５着と１０ｃｍ×１０ｃｍのウール布とともに収納したビニ−ルロッカ−（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、本保持体１の代わりに２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラートを含有しない濾紙を用いた以外は繊維製品収納区（Ａ）と同様の操作を行ったビニ−ルロッカ−を繊維製品収納区（Ｂ）とした。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に無処理区をその長辺が沿うように配置した。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にイガ成虫約２００頭を放ち、温度２５±２℃下にて保存した。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆った。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求めた。
その結果、当該試験における防除効力は１００％であった。 Test example 2
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) is cut into 10 cm × 15 cm, and 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate 100 mg of acetone solution was uniformly applied to the filter paper, and then acetone was air-dried. Thus, a drug holder (hereinafter referred to as the present holder 1) was obtained.
Inside, a vinyl rocker (84 cm × 50 cm × 163 cm) in which the holder 1 is housed together with five clothes and a 10 cm × 10 cm wool cloth is used as a textile product storage area (A). Contains 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate A vinyl rocker that was operated in the same manner as the textile product storage area (A) except that a non-filter paper was used was designated as the textile product storage area (B).
The textile product storage section (A) is arranged along one side of the bottom surface in the chamber (28 m 3 ) so that its long side is along, and the non-treatment section is arranged along one side opposite to one side of the bottom surface. did. About 200 moths were released in a space other than the textile product storage area (A) and the textile product storage area (B) in the chamber, and stored at a temperature of 25 ± 2 ° C. The two small windows at the top of the chamber were opened and covered with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) was counted, and the control effect was determined by formula (i).
As a result, the control effect in the test was 100%.

試験例３
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を１０ｃｍ×１５ｃｍに裁断し、２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート１００ｍｇのアセトン溶液を該濾紙に均一に塗布した後、アセトンを風乾させて薬剤保持体（以下、本保持体１と記す。）を得た。
内部に、本保持体１を服５着と１０ｃｍ×１０ｃｍのウール布とともに収納したビニ−ルロッカ−（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、本保持体１の代わりに２，３，５，６−テトラフルオロ−４−メチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラートを含有しない濾紙を用いた以外は繊維製品収納区（Ａ）と同様の操作を行ったビニ−ルロッカ−を繊維製品収納区（Ｂ）とした。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に無処理区をその長辺が沿うように配置した。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にヒメカツオブシムシ成虫約１００頭を放ち、温度２５±２℃下にて保存した。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆った。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求めた。
その結果、当該試験における防除効力は１００％であった。 Test example 3
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) is cut into 10 cm × 15 cm, and 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate 100 mg of acetone solution was uniformly applied to the filter paper, and then acetone was air-dried. Thus, a drug holder (hereinafter referred to as the present holder 1) was obtained.
Inside, a vinyl rocker (84 cm × 50 cm × 163 cm) in which the holder 1 is housed together with five clothes and a 10 cm × 10 cm wool cloth is used as a textile product storage area (A). Contains 2,3,5,6-tetrafluoro-4-methylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate A vinyl rocker that was operated in the same manner as the textile product storage area (A) except that a non-filter paper was used was designated as the textile product storage area (B).
The textile product storage section (A) is arranged along one side of the bottom surface in the chamber (28 m 3 ) so that its long side is along, and the non-treatment section is arranged along one side opposite to one side of the bottom surface. did. About 100 adult worms were released in a space other than the textile product storage area (A) and the textile product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. The two small windows at the top of the chamber were opened and covered with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) was counted, and the control effect was determined by formula (i).
As a result, the control effect in the test was 100%.

試験例４
濾紙（標準用濾紙 Ｎｏ．２、東洋濾紙株式会社製、質量 １２５ｇ／ｍ2、厚さ ０，２６ｍｍ）を１０ｃｍ×１５ｃｍに裁断し、２，３，５，６−テトラフルオロ−４−メトキシメチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラート１００ｍｇのアセトン溶液を該濾紙に均一に塗布し、アセトンを風乾させて薬剤保持体（以下、本保持体２と記す。）を得る。
内部に、本保持体２を服５着と１０ｃｍ×１０ｃｍのウール布とともに設置したビニ−ルロッカ−（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、２，３，５，６−テトラフルオロ−４−メトキシメチルベンジル （１Ｒ）−トランス−３−（１−プロペニル（Ｚ／Ｅ＝８／１））−２，２−ジメチルシクロプロパンカルボキシラートを含有しない濾紙を用いる以外は繊維製品収納区（Ａ）と同様の操作を行ったビニ−ルロッカ−を繊維製品収納区（Ｂ）とする。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に無処理区をその長辺が沿うように配置する。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存する。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆う。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求める。
その結果、当該試験における防除効力が確認できる。 Test example 4
Filter paper (standard filter paper No. 2, manufactured by Toyo Roshi Kaisha, Ltd., mass 125 g / m 2 , thickness 0,26 mm) was cut into 10 cm × 15 cm, and 2,3,5,6-tetrafluoro-4-methoxymethyl Acetone solution of 100 mg of benzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2,2-dimethylcyclopropanecarboxylate is uniformly applied to the filter paper, and the acetone is air-dried. As a result, a drug holder (hereinafter referred to as the main holder 2) is obtained.
A vinyl rocker (84 cm × 50 cm × 163 cm) in which the holder 2 is installed with five clothes and a 10 cm × 10 cm wool cloth is used as the textile product storage area (A), while 2, 3, 5, 6-tetrafluoro-4-methoxymethylbenzyl (1R) -trans-3- (1-propenyl (Z / E = 8/1))-2, except that filter paper containing no 2-dimethylcyclopropanecarboxylate is used A vinyl rocker that has been operated in the same manner as the textile product storage area (A) is defined as a textile product storage area (B).
The textile product storage section (A) is arranged along one side of the bottom surface in the chamber (28 m 3 ) so that its long side is along, and the non-treated section is arranged along one side opposite to the one side of the bottom surface. To do. About 200 adult moths are released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. Open the two small windows at the top of the chamber and cover with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) is counted, and the control effect is obtained by formula (i).
As a result, the control effect in the test can be confirmed.

試験例５
内部に、服５着を１０ｃｍ×１０ｃｍのウール布とともに設置し、参考例１で得られるエアゾール製剤を１秒間噴霧したビニールロッカー（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、参考例１で得られるエアゾール製剤を噴霧しない以外は繊維製品収納区（Ａ）と同様の操作を行ったビニールロッカーを繊維製品収納区（B）とする。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に繊維製品収納区（Ｂ）をその長辺が沿うように配置する。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存する。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆う。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求める。
その結果、当該試験における防除効力が確認できる。 Test Example 5
Inside, a clothes locker (84 cm x 50 cm x 163 cm) sprayed with the aerosol formulation obtained in Reference Example 1 for 1 second was set as a textile product storage area (A) with 5 clothes of 10 cm x 10 cm and a wool cloth. The vinyl locker, which was operated in the same manner as the textile product storage area (A) except that the aerosol formulation obtained in Reference Example 1 was not sprayed, was defined as the textile product storage area (B).
The textile product storage section (A) is arranged on one side of the bottom surface in the chamber (28 m 3 ) so that the long side thereof is along, and the textile product storage section (B) is arranged on one side opposite to the one side of the bottom surface. Arrange along. About 200 adult moths are released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. Open the two small windows at the top of the chamber and cover with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) is counted, and the control effect is obtained by formula (i).
As a result, the control effect in the test can be confirmed.

試験例６
内部に、服５着を１０ｃｍ×１０ｃｍのウール布とともに設置し、参考例２で得られるエアゾール製剤を１秒間噴霧したビニールロッカー（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、参考例２で得られるエアゾール製剤を噴霧しない以外は繊維製品収納区（Ａ）と同様の操作を行ったビニールロッカーを繊維製品収納区（B）とする。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に繊維製品収納区（Ｂ）をその長辺が沿うように配置する。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存する。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆う。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求める。
その結果、当該試験における防除効力が確認できる。 Test Example 6
Inside, a clothes locker (84 cm x 50 cm x 163 cm) sprayed with the aerosol formulation obtained in Reference Example 1 for 1 second was installed as a textile product storage area (A) with 5 clothes of 10 cm x 10 cm wool cloth. The vinyl locker that was operated in the same manner as the textile product storage area (A) except that the aerosol preparation obtained in Reference Example 2 was not sprayed was designated as the textile product storage area (B).
The textile product storage section (A) is arranged on one side of the bottom surface in the chamber (28 m 3 ) so that the long side thereof is along, and the textile product storage section (B) is arranged on one side opposite to the one side of the bottom surface. Arrange along. About 200 adult moths are released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. Open the two small windows at the top of the chamber and cover with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) is counted, and the control effect is obtained by formula (i).
As a result, the control effect in the test can be confirmed.

試験例７
内部に、参考例３で得られる電動モーター式の薬剤拡散装置を服５着と１０ｃｍ×１０ｃｍのウール布とともに懸吊させ、該ファン製剤１を作動（４６０ｒｐｍ常時回転）させたビニールロッカー（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、参考例３で得られる電動モーター式の薬剤拡散装置を懸吊及び作動させない以外は繊維製品収納区（Ａ）と同様の操作を行ったビニールロッカーを繊維製品収納区（Ｂ）とする。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に繊維製品収納区（Ｂ）をその長辺が沿うように配置する。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存する。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆う。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求める。
その結果、当該試験における防除効力が確認できる。 Test Example 7
Inside, an electric motor type drug diffusion device obtained in Reference Example 3 was suspended together with five clothes and a 10 cm × 10 cm wool cloth, and the vinyl preparation (84 cm × 84 cm) in which the fan preparation 1 was operated (always rotating at 460 rpm). 50cm × 163cm) is designated as the textile product storage area (A), while the electric motor type drug diffusion device obtained in Reference Example 3 is suspended and operated in the same manner as the textile product storage area (A). Let the vinyl locker be the textile product storage area (B).
The textile product storage section (A) is arranged on one side of the bottom surface in the chamber (28 m 3 ) so that the long side thereof is along, and the textile product storage section (B) is arranged on one side opposite to the one side of the bottom surface. Arrange along. About 200 adult moths are released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. Open the two small windows at the top of the chamber and cover with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) is counted, and the control effect is obtained by formula (i).
As a result, the control effect in the test can be confirmed.

試験例８
内部に、参考例４で得られる電動モーター式の薬剤拡散装置を服５着と１０ｃｍ×１０ｃｍのウール布とともに懸吊させ、該ファン製剤１を作動（４６０ｒｐｍ常時回転）させたビニールロッカー（８４ｃｍ×５０ｃｍ×１６３ｃｍ）を繊維製品収納区（Ａ）とし、一方、参考例４で得られる電動モーター式の薬剤拡散装置を懸吊及び作動させない以外は繊維製品収納区（Ａ）と同様の操作を行ったビニールロッカーを繊維製品収納区（Ｂ）とする。
チャンバー（２８ｍ3）内の底面の一辺に繊維製品収納区（Ａ）をその長辺が沿うように配置し、該底面の一辺と対向する一辺に繊維製品収納区（Ｂ）をその長辺が沿うように配置する。該チャンバー内の繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）以外の空間にコイガ成虫約２００頭を放ち、温度２５±２℃下にて保存する。チャンバーの上部２箇所の小窓を開放し、供試虫の逃亡防止用にネットで覆う。３日後に繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の内部に産卵された卵数を数え、式（ｉ）により防除効力を求める。
その結果、当該試験における防除効力が確認できる。 Test Example 8
Inside, a plastic locker (84 cm × 84 cm) in which the electric motor type drug diffusion device obtained in Reference Example 4 was suspended with 5 clothes and a 10 cm × 10 cm wool cloth and the fan preparation 1 was operated (always rotating at 460 rpm). 50cm × 163cm) is designated as the textile product storage area (A), while the electric motor type drug diffusion device obtained in Reference Example 4 is suspended and operated in the same manner as the textile product storage area (A). Let the vinyl locker be the textile product storage area (B).
The textile product storage section (A) is arranged on one side of the bottom surface in the chamber (28 m 3 ) so that the long side thereof is along, and the textile product storage section (B) is arranged on one side opposite to the one side of the bottom surface. Arrange along. About 200 adult moths are released in a space other than the fiber product storage area (A) and the fiber product storage area (B) in the chamber and stored at a temperature of 25 ± 2 ° C. Open the two small windows at the top of the chamber and cover with a net to prevent the test insects from escaping. Three days later, the number of eggs laid in the textile product storage area (A) and the textile product storage area (B) is counted, and the control effect is obtained by formula (i).
As a result, the control effect in the test can be confirmed.

試験例７及び８で用いられる薬剤揮散装置の一形態の分解図である。It is an exploded view of one form of the chemical volatilization device used in Test Examples 7 and 8. 試験例７及び８で用いられる電動モーター式の薬剤揮散装置を用いた器具の一態様を示す斜視図。The perspective view which shows the one aspect | mode of the instrument using the electric motor type chemical volatilization apparatus used by the test examples 7 and 8. FIG.

符号の説明Explanation of symbols

１・・・ファン
２・・・軸
３・・・回転手段
４・・・薬剤保持体 DESCRIPTION OF SYMBOLS 1 ... Fan 2 ... Shaft 3 ... Rotating means 4 ... Drug holding body

Claims (6)

基材に繊維害虫に対する防除効力を示し得る薬剤が保持されてなる薬剤保持体、及び、繊維製品が繊維製品収納容器に収納されてなる繊維製品収納区（Ａ）
と、
少なくとも繊維製品が繊維製品収納容器に収納されてなり、かつ前記薬剤保持体が収納されていない繊維製品収納区（Ｂ）
とを収容し、繊維害虫が逃亡しないように閉鎖された試験空間において、該試験空間内部のうち、該繊維製品収納区（Ａ）及び該繊維製品収納区（Ｂ）の外部に繊維害虫を供試する工程（Ｉ）、
前記工程（Ｉ）における繊維害虫の供試から一定時間経過後に、該繊維製品収納区（Ａ）と該繊維製品収納区（Ｂ）との各々の繊維製品収納容器内部に存在する繊維害虫の虫数及び卵数のうち少なくとも一方の数値を求める工程（II）、
及び、
前記工程（II）で求められる該繊維製品収納区（Ａ）における数値と該繊維製品収納区（Ｂ）における数値とを対比する工程（III）、
を有してなる薬剤保持体の繊維害虫に対する防除効力の評価方法。 A medicine holder in which a medicine capable of exhibiting a pest control effect on fiber pests is held on a base material, and a textile product storage area (A) in which textile products are stored in a textile product storage container
When,
Textile product storage area (B) in which at least the textile product is stored in a textile product storage container and the medicine holder is not stored
In the test space closed so that the fiber pests do not escape, the fiber pests are provided outside the fiber product storage area (A) and the fiber product storage area (B) in the test space. Step (I) to try,
Insects of fiber pests present in the fiber product storage containers of the fiber product storage area (A) and the fiber product storage area (B) after a lapse of a certain time from the test of the fiber pest in the step (I) The step of obtaining at least one of the number and the number of eggs (II),
as well as,
Step (III) for comparing the numerical value in the textile product storage area (A) and the numerical value in the textile product storage area (B) determined in the step (II),
The evaluation method of the control effect with respect to the fiber pest of the chemical | medical agent holding body which has this. 試験空間全体に対する繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）の容積占有率が、それぞれ０．３〜５％である請求項１記載の評価方法。   The evaluation method according to claim 1, wherein the volume occupancy ratios of the fiber product storage area (A) and the fiber product storage area (B) with respect to the entire test space are each 0.3 to 5%. 繊維製品収納区（Ａ）及び繊維製品収納区（Ｂ）各々の配置が、試験空間の底面部に接した状態での配置である請求項１又は２記載の評価方法。   The evaluation method according to claim 1 or 2, wherein the arrangement of each of the textile product storage area (A) and the textile product storage area (B) is an arrangement in a state of being in contact with the bottom surface of the test space. 繊維製品収納容器（Ａ）と繊維製品収納容器（Ｂ）との各々の繊維製品収納容器内部に存在する繊維害虫の虫数及び卵数のうち少なくとも一方の数値が、繊維製品収納容器（Ａ）と繊維製品収納容器（Ｂ）との各々の繊維製品収納容器の内部に存在する繊維害虫の卵数である請求項１〜３いずれか一項記載の評価方法。   At least one of the number of fiber pests and the number of eggs in the fiber product storage container (A) and the fiber product storage container (B) is the fiber product storage container (A). The evaluation method according to any one of claims 1 to 3, which is the number of eggs of fiber pests existing in each of the fiber product storage containers of the container and the fiber product storage container (B). 基材が繊維質基材である請求項１〜４いずれか一項記載の評価方法。   The evaluation method according to any one of claims 1 to 4, wherein the substrate is a fibrous substrate. 繊維害虫が、イガ、コイガ、ヒメカツオブシムシ又はヒメマルカツオブシムシである請求項１〜５いずれか一項記載の評価方法。   The evaluation method according to any one of claims 1 to 5, wherein the fiber pest is a moth, a common moth, a long-horned beetle, or a long-horned beetle.
JP2007264154A 2007-03-22 2007-10-10 Method for evaluating controlling effect of agent support material on insect harmful to fiber Pending JP2008266284A (en)

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