JP2008231319A - Method and apparatus for extracting mushroom component - Google Patents

Method and apparatus for extracting mushroom component Download PDF

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JP2008231319A
JP2008231319A JP2007075180A JP2007075180A JP2008231319A JP 2008231319 A JP2008231319 A JP 2008231319A JP 2007075180 A JP2007075180 A JP 2007075180A JP 2007075180 A JP2007075180 A JP 2007075180A JP 2008231319 A JP2008231319 A JP 2008231319A
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mushroom
pressure kettle
hot water
bag
pressurized hot
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JP5272142B2 (en
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Shinnosuke Miyauchi
信之助 宮内
Kazunori Seki
一徳 関
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TOOTEKKU KK
Nagaoka University of Technology NUC
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TOOTEKKU KK
Nagaoka University of Technology NUC
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method and apparatus for extracting a mushroom component in which a waste mushroom cultivation bed and water are enclosed in a pressure vessel, which is then heated with a heating mechanism; and the pressure in the pressure vessel is increased by the heating and the water is heated to form pressurized hot water, which contacts the waste mushroom cultivation bed in the pressure vessel to dissolve the waste mushroom cultivation bed to extract a mushroom component, thus capable of improving extraction efficiency. <P>SOLUTION: Disclosed is a method for extracting a mushroom component in which a waste mushroom cultivation bed W and water are enclosed in a pressure vessel 1; the pressure vessel is heated to allow pressurized hot water N to contact the waste mushroom cultivation bed in the pressure vessel to thereby extract a mushroom component; and an extract solution T containing the extracted mushroom component is taken out. The method is characterized in that a separation column 4 which can encapsulate the waste mushroom cultivation bed is arranged in the pressure vessel; and the pressurized hot water in the pressure vessel is stirred by the circulation of the pressurized hot water which flows out of an outlet portion 3a provided in the pressure vessel and returns to the pressurized vessel through an inlet portion 3c to thereby extract the mushroom component from the waste mushroom cultivation bed. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明はキノコ栽培廃菌床からキノコ成分を抽出する際に用いられるキノコ成分抽出方法及びその装置に関するものである。   The present invention relates to a mushroom component extraction method and apparatus for use in extracting mushroom components from a mushroom cultivation waste fungus bed.

従来、この種のキノコ成分抽出方法及びその装置として、キノコ栽培廃菌床に加圧熱水を接触させることによりキノコ成分を抽出する方法及びその装置が知られている。このキノコ栽培廃菌床とは、例えば、シイタケ、マイタケ、ブナシメジ等のキノコの栽培においては、木粉に栄養分を入れて作ったキッドに菌糸を植えてキノコを栽培する方法が近年盛んであるが、キノコを採取した後に菌糸で固められた塊状物が残り、これをキノコ栽培廃菌床と呼んでいる。このキノコ栽培廃菌床にはバイオエネルギーになる木粉の他に有用な菌糸塊が含まれているにも拘わらず、廃棄処理されていることが多く、したがって、このキノコ栽培廃菌床に含まれている有用な主に多糖であるキノコ成分を抽出して再利用しようとするものである。
特開2006−176765
Conventionally, as a method and apparatus for extracting this kind of mushroom component, a method and apparatus for extracting a mushroom component by bringing pressurized hot water into contact with a mushroom cultivation waste fungus bed are known. This mushroom cultivation waste bed is, for example, in the cultivation of mushrooms such as shiitake mushrooms, maitake mushrooms, beech shimeji mushrooms, etc. Recently, methods for cultivating mushrooms by planting mycelia in a kid made by adding nutrients to wood flour are popular. After collecting the mushrooms, a lump solidified with mycelium remains, which is called mushroom cultivation waste fungus bed. Although this mushroom cultivation waste bed contains useful mycelium in addition to wood flour that becomes bioenergy, it is often disposed of, and therefore is included in this mushroom cultivation waste bed. It is intended to extract and reuse mushroom components, which are useful mainly polysaccharides.
JP 2006-176765 A

しかしながら、これらキノコ栽培廃菌床には塊状菌糸体を含むと共に粒子状であるからきわめて吸水性が大きく、抽出時において、キノコ栽培廃菌床の5倍から10倍の大量の水を必要とすることになり、抽出作業性が著しく低下し、しかも、抽出効率を高める観点からキノコ栽培廃菌床を撹拌する必要があり、キノコ栽培廃菌床は種類によっても異なるが、例えばエリンギは廃菌床を多量の菌塊が覆い、キノコ成分の割合が多く、菌糸塊泥状になり易く、一方、マイタケは木粉が多く、木粉が多量の水を吸い込み、おから状になり、加えて、木粉の分解成分も出て、多成分が溶液中に出たような外観となり、このような多成分のものを機械的に撹拌することは不向きであるという不都合も有している。   However, these mushroom cultivation waste fungus beds contain massive mycelium and are particulate so that they have extremely high water absorption and require 5 to 10 times as much water during extraction as the mushroom cultivation waste fungus beds. Therefore, it is necessary to stir the mushroom cultivation waste bed from the viewpoint of increasing the extraction efficiency, and the mushroom cultivation waste bed varies depending on the type. A large amount of fungus mass is covered, the ratio of mushroom components is large, and it tends to become a mycelium lump, while maitake is a lot of wood powder, the wood powder sucks a lot of water, becomes okara-like, in addition, The decomposition component of the wood flour also appears, giving the appearance that the multicomponent is in solution, and has the disadvantage that it is unsuitable to mechanically stir the multicomponent.

本発明はこれらの不都合を解決することを目的とするもので、本発明のうちで、請求項1記載の方法の発明は、キノコ栽培廃菌床及び水を圧力釜体内に封止して該圧力釜体を加熱し、該圧力釜体内のキノコ栽培廃菌床に加圧熱水を接触させることによりキノコ成分を抽出し、該キノコ成分を抽出した抽出液を取り出すに際し、上記圧力釜体内に上記キノコ栽培廃菌床を封入可能な分離カラムを配置すると共に上記圧力釜体内の加圧熱水が圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻る加圧熱水の循環により圧力釜体内の加圧熱水を水流撹拌させてキノコ栽培廃菌床からキノコ成分を抽出することを特徴とするキノコ成分抽出方法にある。   The present invention aims to solve these disadvantages. Among the present inventions, the invention of the method according to claim 1 is to seal the mushroom cultivation waste fungus bed and water in the pressure cooker. When the pressure kettle body is heated, the mushroom component is extracted by bringing pressurized hot water into contact with the mushroom cultivation waste fungus bed in the pressure kettle body, and the extract from which the mushroom component is extracted is taken into the pressure kettle body. Pressurized hot water in which a separation column capable of enclosing the mushroom cultivation waste fungus bed is disposed and the pressurized hot water in the pressure kettle body returns from the outlet portion provided in the pressure kettle body to the pressure kettle body again through the inlet portion In the method for extracting mushroom components, the hot water in the pressure kettle body is agitated with water circulation to extract mushroom components from the mushroom cultivation waste fungus bed.

又、請求項2記載の装置の発明にあっては、キノコ栽培廃菌床及び水を圧力釜体内に封止して該圧力釜体を加熱し、該圧力釜体内のキノコ栽培廃菌床に加圧熱水を接触させることによりキノコ成分を抽出し、該キノコ成分を抽出した抽出液を取り出す装置において、上記圧力釜体内に上記キノコ栽培廃菌床を封入可能な分離カラムを配置し、上記圧力釜体内の加圧熱水が圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻る加圧熱水の循環流により圧力釜体内の加圧熱水を水流撹拌させる循環管路を設けてなることを特徴とするキノコ成分抽出装置にある。   In the invention of the device according to claim 2, the mushroom cultivation waste fungus bed and water are sealed in the pressure cooker body, the pressure cooker body is heated, and the mushroom cultivation waste fungus bed in the pressure cooker body is formed. In the apparatus for extracting the mushroom component by contacting with pressurized hot water and taking out the extract from which the mushroom component has been extracted, a separation column capable of enclosing the mushroom cultivation waste fungus bed is disposed in the pressure kettle, Circulation in which pressurized hot water in the pressure kettle body is flow-stirred by a circulating flow of pressurized hot water that returns from the outlet portion provided in the pressure kettle body to the pressure kettle body through the inlet portion again. A mushroom component extracting apparatus is provided with a pipe line.

又、請求項3記載の装置の発明は、上記循環管路の途中に上記圧力釜体内の加圧熱水を圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻すための循環ポンプを設けてなることを特徴とするものであり、又、請求項4記載の装置の発明は、上記循環管路の途中に上記圧力釜体内の抽出液を取出可能な取出管路を設けてなることを特徴とするものである。   According to a third aspect of the present invention, the pressurized hot water in the pressure vessel is returned from the outlet provided in the pressure vessel through the inlet to the pressure vessel in the middle of the circulation pipe. Further, the invention of the device according to claim 4 is characterized in that an extraction pipe capable of taking out the extract in the pressure vessel is provided in the middle of the circulation pipe. It is characterized by being provided.

又、請求項5記載の装置の発明は、上記分離カラムは、上記キノコ栽培廃菌床が封入され、上記加圧熱水及び抽出液の通過が可能な袋状分離体からなることを特徴とするものであり、又、請求項6記載の装置の発明は、上記袋状分離体は、アラミド繊維、ガラス繊維、炭素繊維、ステンレス鋼からなる繊維などの金属繊維等の耐熱性繊維又はこれらの複合繊維により製作される網状体からなることを特徴とするものであり、又、請求項7記載の装置の発明は、上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成されていることを特徴とするものであり、又、請求項8記載の発明は、上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成され、該外袋状分離体と内袋状分離体との間の空間に濾過材を配置してなることを特徴とするものであり、又、請求項9記載の装置の発明は、上記圧力釜体内に上記袋状分離体を収納可能な枠状体を配置してなることを特徴とするものである。   Further, the invention of the apparatus according to claim 5 is characterized in that the separation column is formed of a bag-like separator in which the mushroom cultivation waste fungus bed is enclosed and the pressurized hot water and the extract can pass therethrough. Further, the invention of the device according to claim 6 is characterized in that the bag-like separator is made of heat-resistant fibers such as metal fibers such as aramid fibers, glass fibers, carbon fibers, fibers made of stainless steel, or the like. The invention according to claim 7 is characterized in that the bag-like separator is an inner bag in which the mushroom cultivation waste fungus bed is enclosed. The outer bag-shaped separator and the outer bag-shaped separator that covers the inner bag-shaped separator are formed into a double bag shape, and the invention according to claim 8 is characterized in that the bag-shaped separator is provided. The body is an inner bag-shaped separated body and an inner bag shape in which the mushroom cultivation waste fungus bed is enclosed It is formed in a double bag shape composed of an outer bag-shaped separator that covers a separation body, and a filter medium is disposed in a space between the outer bag-shaped separator and the inner bag-shaped separator. The invention of the device according to claim 9 is characterized in that a frame-like body capable of accommodating the bag-like separator is arranged in the pressure vessel.

本発明は上述の如く、請求項1又は2記載の発明にあっては、キノコ栽培廃菌床及び水を圧力釜体内に封止し、加熱機構により圧力釜体を加熱し、この加熱により圧力釜体内は昇圧すると共に水は加熱されて加圧熱水となり、この加圧熱水は圧力釜体内のキノコ栽培廃菌床に接触し、加圧熱水の接触によりキノコ栽培廃菌床は溶解してキノコ成分が抽出し、このキノコ成分が抽出された抽出液を取り出すことになり、この際、上記圧力釜体内の加圧熱水は循環管路により圧力釜体の出口部から再び入口部を介して圧力釜体内に戻る循環が繰り返され、この循環流により圧力釜体内の加圧熱水の水流現象が生じ、この水流現象によりキノコ栽培廃菌床は水流撹拌され、この水流撹拌によりキノコ栽培廃菌床からのキノコ成分の抽出効率を向上することができ、かつ、上記圧力釜体内に上記キノコ栽培廃菌床を封入可能な分離カラムを配置しているので、分離カラムによりキノコ栽培廃菌床の残渣とキノコ成分が抽出された抽出液とが分離され、循環管路内の抽出液の循環が良好になされ、それだけ、水流撹拌が良好になされ、抽出効率を向上することができると共にキノコ栽培廃菌床の残渣による循環管路内の詰まり現象や汚れ現象を抑制することができる。   As described above, in the present invention according to claim 1 or 2, the mushroom cultivation waste fungus bed and water are sealed in the pressure kettle body, the pressure kettle body is heated by a heating mechanism, and the pressure is increased by this heating. The pressure inside the kettle is increased and the water is heated to become pressurized hot water. This pressurized hot water comes into contact with the mushroom cultivation waste bed in the pressure kettle, and the contact with the pressurized hot water dissolves the mushroom cultivation waste bed. Then, the mushroom component is extracted, and the extract from which the mushroom component is extracted is taken out. At this time, the pressurized hot water in the pressure vessel body is recirculated from the outlet portion of the pressure vessel body to the inlet portion. The circulation returning to the pressure kettle body is repeated through this, and the flow of pressurized hot water in the pressure kettle body is caused by this circulation flow, and this water flow phenomenon stirs the mushroom cultivation waste fungus bed, and this water agitation Improve the extraction efficiency of mushroom components from the cultivation waste bed And a separation column capable of enclosing the mushroom cultivation waste fungus bed in the pressure kettle body, so that an extraction liquid from which the mushroom cultivation waste fungus bed residue and mushroom components are extracted by the separation column And the extraction liquid in the circulation pipe is circulated well, so that the water flow is well stirred, the extraction efficiency can be improved, and the clogging in the circulation pipe by the residue of mushroom cultivation waste fungus bed Phenomenon and dirt phenomenon can be suppressed.

又、請求項3記載の発明にあっては、上記循環管路の途中に上記圧力釜体内の加圧熱水を圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻すための循環ポンプを設けているから、加圧熱水の循環による水流撹拌構造を簡素化することができ、又、請求項4記載の発明にあっては、上記循環管路の途中に上記圧力釜体内の抽出液を取出可能な取出管路を設けてなるから、抽出液の取出構造を簡素化することができる。   According to a third aspect of the present invention, in the middle of the circulation pipe, the pressurized hot water in the pressure vessel is returned from the outlet provided in the pressure vessel to the pressure vessel again through the inlet. Since the circulation pump is provided, the water stirring structure by circulation of the pressurized hot water can be simplified. In the invention according to claim 4, the pressure is provided in the middle of the circulation line. Since the extraction conduit that can extract the extract in the pot is provided, the structure for extracting the extract can be simplified.

又、請求項5記載の発明にあっては、上記分離カラムは、上記キノコ栽培廃菌床が封入され、上記加圧熱水及び抽出液の通過が可能な袋状分離体からなるので、加圧熱水接触によるキノコ栽培廃菌床の膨潤による絞り出し効果を得ることができ、キノコ成分の抽出効率を向上することができ、又、請求項6記載の発明にあっては、上記袋状分離体は、アラミド繊維、ガラス繊維、炭素繊維、ステンレス鋼からなる繊維などの金属繊維等の耐熱性繊維により製作される網状体からなるので、耐久的に使用することができ、又、請求項7記載の発明にあっては、上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成されているので、キノコ栽培廃菌床の残渣による循環管路内の詰まり現象や汚れ現象を確実に抑制することができ、又、請求項8記載の発明にあっては、上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成され、かつ、外袋状分離体と内袋状分離体との間の空間に濾過材が配置されているので、濾過材により循環する抽出液は濾過され、キノコ栽培廃菌床の残渣による循環管路内の詰まり現象や汚れ現象を確実に抑制することができ、又、請求項9記載の発明にあっては、上記圧力釜体内に上記袋状分離体を収納可能な枠状体を配置してなるから、袋状分離体の圧力釜体に対する出し入れを良好に行うことができる。   In the invention according to claim 5, the separation column is formed of a bag-like separator in which the mushroom cultivation waste fungus bed is enclosed and the pressurized hot water and the extract can pass therethrough. The squeezing effect by swelling of the mushroom cultivation waste fungus bed by contact with pressurized water can be obtained, the extraction efficiency of mushroom components can be improved, and in the invention of claim 6, the bag-like separation The body is made of a net-like body made of a heat-resistant fiber such as metal fiber such as aramid fiber, glass fiber, carbon fiber, fiber made of stainless steel, etc., and can be used in a durable manner. In the described invention, the bag-like separated body is formed into a double bag shape comprising an inner bag-like separated body enclosing the mushroom cultivation waste fungus bed and an outer bag-like separated body covering the inner bag-like separated body. Since it is formed, circulation due to residues of mushroom cultivation waste fungus bed The clogging phenomenon and dirt phenomenon in the road can be surely suppressed, and in the invention according to claim 8, the bag-like separator is an inner bag shape in which the mushroom cultivation waste fungus bed is enclosed. A double bag comprising an outer bag-like separator covering the separator and the inner bag-like separator is formed, and a filter medium is disposed in a space between the outer bag-like separator and the inner bag-like separator. Therefore, the extract circulated by the filter medium is filtered, and the clogging phenomenon and dirt phenomenon in the circulation pipe line due to the residue of the mushroom cultivation waste fungus bed can be reliably suppressed, and the invention according to claim 9 In this case, since the frame-like body that can store the bag-like separator is disposed in the pressure vessel, the bag-like separator can be put in and out of the pressure vessel well.

図1乃至図8は本発明の実施の形態例を示し、図1乃至図6は第一形態例、図7は第二形態例、図8は第三形態例である。   1 to 8 show an embodiment of the present invention, FIGS. 1 to 6 show a first embodiment, FIG. 7 shows a second embodiment, and FIG. 8 shows a third embodiment.

図1乃至図6の第一形態例において、1は圧力釜体であって、ステンレス製等の耐熱容器が用いられ、上部開口部は蓋体1aにより密閉状態に閉止可能に設けられ、これにより圧力釜体1内は封止可能に設けられている。   In the first embodiment shown in FIGS. 1 to 6, reference numeral 1 denotes a pressure cooker body, a heat-resistant container made of stainless steel or the like is used, and the upper opening is provided so as to be closed in a sealed state by the lid body 1a. The inside of the pressure hook body 1 is provided so as to be able to be sealed.

2は加熱手段であって、上記圧力釜体1の側周面及底面に密閉状の加熱空間Rを存して一体に形成された隔壁体2aと、蒸気Gを所定圧力及び所定温度に制御して作製可能な蒸気ボイラー2bと、この蒸気ボイラー2bで発生した蒸気Gを蒸気口部2gより加熱空間R内に送入可能な送入管路2cと、圧力釜体1の底部に設けられ、加熱空間R内のドレン水Dを開閉弁2eを介して排出可能なドレン排出部2dからなり、この加熱空間R内に蒸気Gを送入して圧力釜体1の外壁部が加熱され、この加熱により蓋体2により封止された圧力釜体1の内部の温度が上昇して加圧雰囲気下に作製され、圧力釜体1内に収容された水は加圧下における熱水、即ち、加圧熱水となってキノコ栽培廃菌床Wに接触し、この加圧熱水Nの接触によりキノコ栽培廃菌床Wは溶解し、キノコ成分が抽出されることになる。   Reference numeral 2 denotes a heating means, which controls the steam G to a predetermined pressure and a predetermined temperature, and a partition wall 2a integrally formed with a sealed heating space R on the side peripheral surface and the bottom surface of the pressure pot body 1. The steam boiler 2b that can be manufactured in this manner, the feed pipe 2c that can feed the steam G generated in the steam boiler 2b into the heating space R from the steam port 2g, and the bottom of the pressure pot 1 are provided. The drain water D in the heating space R is composed of a drain discharge portion 2d capable of discharging through the on-off valve 2e. The steam G is fed into the heating space R to heat the outer wall portion of the pressure pot 1. Due to this heating, the temperature inside the pressure vessel body 1 sealed by the lid body 2 is increased and produced in a pressurized atmosphere, and the water stored in the pressure vessel body 1 is hot water under pressure, that is, Pressurized hot water comes into contact with the mushroom cultivation waste fungus bed W, and mushroom planting by the contact with the pressurized hot water N Haikin'yuka W is dissolved, so that the mushroom component is extracted.

3は循環管路であって、この場合、上記圧力釜体1の側部に出口部3aを形成し、出口部3aの内側に圧力釜体1内の底部に至る排出管3bを接続し、圧力釜体1の上部側部に入口部3cを設け、この出口部3aと入口部3cとの間に循環管路3を設け、循環管路3の途中に循環ポンプ3dを設けてなり、この循環ポンプ3dにより、圧力釜体1内の加圧熱水Nは出口部3aから循環管路3を経て再び入口部3cを介して圧力釜体1内に戻る循環を繰り返すことになり、この循環流により圧力釜体1内の加圧熱水の水流現象が生じ、この水流現象によりキノコ栽培廃菌床Wは水流撹拌されることになる。   3 is a circulation pipe, in this case, the outlet portion 3a is formed in the side portion of the pressure hook body 1, and the discharge pipe 3b reaching the bottom in the pressure hook body 1 is connected to the inside of the outlet portion 3a, An inlet 3c is provided on the upper side of the pressure hook body 1, a circulation line 3 is provided between the outlet 3a and the inlet 3c, and a circulation pump 3d is provided in the middle of the circulation line 3. By the circulation pump 3d, the pressurized hot water N in the pressure vessel body 1 is repeatedly circulated from the outlet portion 3a through the circulation line 3 and again into the pressure vessel body 1 through the inlet portion 3c. Due to the flow, a flow phenomenon of pressurized hot water in the pressure pot 1 occurs, and the mushroom cultivation waste fungus bed W is flow-stirred by this flow phenomenon.

この加圧熱水として、例えば、亜臨界水が用いられ、亜臨界水とは、水がその臨界点より温度、圧力が低い所定の範囲にある場合をいい、有機物を高速で水に溶ける低分子に分解することができるという特徴を有し、効率よくキノコの有効成分を抽出するために、加圧熱水(亜臨界水)の温度は、110℃から250℃の範囲とすることが好ましく、圧力については、0.1MPaから5MPaの範囲とすることが好ましい。また、加圧熱水(亜臨界水)となる原水は、通常の水道水でも使用できるが、イオン交換水や蒸留水、フィルター濾過した濾過水(たとえば、限外濾過水)等のように十分に精製した水を用いることが好ましい。   As this pressurized hot water, for example, subcritical water is used. Subcritical water refers to a case where water is in a predetermined range where the temperature and pressure are lower than the critical point. The temperature of pressurized hot water (subcritical water) is preferably in the range of 110 ° C. to 250 ° C. in order to efficiently extract the active ingredient of mushrooms, having the feature that it can be decomposed into molecules. The pressure is preferably in the range of 0.1 MPa to 5 MPa. In addition, the raw water used as pressurized hot water (subcritical water) can be used as normal tap water, but it is sufficient as ion-exchanged water, distilled water, filtered filtered water (for example, ultrafiltered water), etc. It is preferable to use purified water.

4は分離カラムであって、この場合、キノコ栽培廃菌床Wが封入され、蒸気加圧熱水N及び抽出液Tの通過が可能な袋状分離体4a及び上記圧力釜体1内に配置され袋状分離体4aを収納可能な枠状体4bからなり、この袋状分離体4aはアラミド繊維、ガラス繊維、炭素繊維、ステンレス鋼からなる繊維などの金属繊維等の耐熱性繊維を適宜大きさのメッシュの網目をもつ織成、網成等により製作される網状体からなり、内部にキノコ栽培廃菌床Wを詰入した後、紐体Fにより縛着可能に設けられている。   4 is a separation column. In this case, a mushroom cultivation waste fungus bed W is enclosed, and is disposed in a bag-like separation body 4a through which steam-pressurized hot water N and an extract T can pass and the pressure kettle body 1 The bag-shaped separator 4a is made of a heat-resistant fiber such as aramid fiber, glass fiber, carbon fiber, fiber made of stainless steel, or the like. It is made of a net-like body produced by weaving or meshing with a mesh mesh of the same size, and is provided so that it can be bound by a string body F after the inside of the mushroom cultivation waste fungus bed W is packed.

5は取出管路であって、上記循環管路3の途中を分岐して接続され、循環管路3に開閉弁3eを設けると共に取出管路5に開閉弁5aを設け、取出管路5の開放端部に抽出液受容器6を配置して構成している。   Reference numeral 5 denotes an extraction pipe, which is branched and connected in the middle of the circulation pipe 3. An opening / closing valve 3 e is provided in the circulation pipe 3 and an opening / closing valve 5 a is provided in the extraction pipe 5. An extraction liquid receiver 6 is arranged at the open end.

7は冷却管路であって、上記隔壁体2aの下部に送水口部7aを形成すると共に上部に排水口部7bを形成し、送水口部7aに冷却水Hを送水可能な図外の送水部を開閉弁7cを介して接続すると共に排水口部7bを図外の排水部に開閉弁7dを介して接続し、冷却水Hを上記加熱空間R内に送水することにより圧力釜体1を冷却したり、又は、圧力釜体1の加熱温度を制御することができるように構成している。   Reference numeral 7 denotes a cooling pipe, which forms a water supply port 7a at the lower part of the partition wall 2a and forms a drainage port part 7b at the upper part, and supplies water outside the figure that can supply cooling water H to the water supply port 7a. Are connected to each other via an on-off valve 7c, and the drain port 7b is connected to a drainage portion (not shown) through an on-off valve 7d, and the cooling water H is fed into the heating space R, thereby It cools or it is comprised so that the heating temperature of the pressure cooker body 1 can be controlled.

8は補助加熱管路であって、上記圧力釜体1の上部に圧送口部8aを形成し、この圧送口部8aと送入管路2cの途中との間を補助加熱管路8で接続し、送入管路2cに開閉弁2fを設けると共に補助加熱管路8の途中に開閉弁8bを設けて構成している。   Reference numeral 8 denotes an auxiliary heating pipe line. A pressure feed port 8a is formed in the upper part of the pressure pot body 1, and the auxiliary heating pipe line 8 connects between the pressure feed port 8a and the middle of the feed pipe line 2c. In addition, an opening / closing valve 2f is provided in the delivery pipe line 2c, and an opening / closing valve 8b is provided in the middle of the auxiliary heating pipe line 8.

この実施の第一形態例は上記構成であるから、キノコ栽培廃菌床W及び水を圧力釜体1内に封止し、加熱機構2の蒸気ボイラー2bを加熱空間R内に送入して圧力釜体1を加熱し、この加熱により圧力釜体1内は昇圧すると共に水は加熱されて水は加圧熱水となり、この加圧熱水は圧力釜体1内のキノコ栽培廃菌床Wに接触し、加圧熱水の接触によりキノコ栽培廃菌床Wは溶解してキノコ成分が抽出し、このキノコ成分が抽出された抽出液Tを取り出すことになり、この際、上記圧力釜体1内の加圧熱水Nは循環管路3により圧力釜体1の出口部3aから再び入口部3cを介して圧力釜体1内に戻る循環が繰り返され、この循環流により圧力釜体1内の加圧熱水Nの水流現象が生じ、この水流現象によりキノコ栽培廃菌床Wは水流撹拌され、この水流撹拌によりキノコ栽培廃菌床Wからのキノコ成分の抽出効率を向上することができ、かつ、上記圧力釜体1内に上記キノコ栽培廃菌床Wを封入可能な分離カラム4を配置しているので、分離カラム4によりキノコ栽培廃菌床Wの残渣とキノコ成分が抽出された抽出液とが分離され、循環管路3内の抽出液Tの循環が良好になされ、それだけ、水流撹拌が良好になされ、抽出効率を向上することができると共にキノコ栽培廃菌床Wの残渣による循環管路3内の詰まり現象や汚れ現象を抑制することができる。   Since the first embodiment of this embodiment has the above-described configuration, the mushroom cultivation waste fungus bed W and water are sealed in the pressure pot 1 and the steam boiler 2b of the heating mechanism 2 is fed into the heating space R. The pressure kettle body 1 is heated, and the pressure in the pressure kettle body 1 is increased by this heating, and the water is heated, and the water becomes pressurized hot water. The pressurized hot water is mushroom cultivation waste fungus bed in the pressure kettle body 1. The mushroom cultivation waste fungus bed W is dissolved by the contact with the pressurized hot water and the mushroom component is extracted, and the extract T from which the mushroom component is extracted is taken out. The pressurized hot water N in the body 1 is repeatedly circulated from the outlet 3a of the pressure vessel body 1 to the pressure vessel body 1 through the inlet portion 3c again by the circulation line 3, and this circulation flow causes the pressure vessel body to repeat. The flow phenomenon of pressurized hot water N in 1 occurs, and the mushroom cultivation waste fungus bed W is flow-stirred by this flow phenomenon, The separation column 4 that can improve the extraction efficiency of mushroom components from the mushroom cultivation waste fungus bed W and can enclose the mushroom cultivation waste fungus bed W in the pressure kettle 1 is arranged by stirring the water flow. Therefore, the separation column 4 separates the residue of the mushroom cultivation waste fungus bed W and the extract from which the mushroom components have been extracted, and the extraction liquid T in the circulation line 3 is circulated well, so that the water is stirred. The extraction efficiency can be improved, and the clogging phenomenon and dirt phenomenon in the circulation pipe line 3 due to the residue of the mushroom cultivation waste fungus bed W can be suppressed.

そして、この加圧熱水による抽出を所定時間行った後、開閉弁3eを閉じると共に開閉弁5aを開けて循環ポンプ3dにより圧力釜体1内の抽出液Tを取出管路5を介して抽出液受容器6に送って取り出すことになる。   Then, after performing the extraction with the pressurized hot water for a predetermined time, the on-off valve 3e is closed and the on-off valve 5a is opened, and the extraction liquid T in the pressure vessel body 1 is extracted through the extraction line 5 by the circulation pump 3d. It is sent to the liquid receiver 6 and taken out.

この場合、上記循環管路3の途中に上記圧力釜体1内の加圧熱水Nを圧力釜体1に設けた出口部3aから再び入口部3cを介して圧力釜体1内に戻すための循環ポンプ3dを設けているから、加圧熱水Nの循環による水流撹拌構造を簡素化することができ、又、この場合、上記循環管路3の途中に上記圧力釜体1内の抽出液Tを取出可能な取出管路5を設けてなるから、抽出液Tの取出構造を簡素化することができる。   In this case, the pressurized hot water N in the pressure vessel body 1 is returned to the pressure vessel body 1 through the inlet portion 3c again from the outlet portion 3a provided in the pressure vessel body 1 in the middle of the circulation pipe 3. Since the circulation pump 3d is provided, it is possible to simplify the structure of stirring the water flow by circulating the pressurized hot water N. In this case, the extraction in the pressure vessel body 1 is in the middle of the circulation line 3. Since the extraction conduit 5 capable of extracting the liquid T is provided, the extraction structure of the extraction liquid T can be simplified.

又、この場合、上記分離カラム4は、上記キノコ栽培廃菌床Wが封入され、上記加圧熱水N及び抽出液Tの通過が可能な布袋状の袋状分離体4aからなるので、加圧熱水N接触によるキノコ栽培廃菌床Wの膨潤による絞り出し効果を得ることができ、キノコ成分の抽出効率を向上することができ、又、この場合、上記袋状分離体4aは、アラミド繊維、ガラス繊維、炭素繊維、ステンレス鋼からなる繊維などの金属繊維等の耐熱性繊維により製作される網状体からなるので、耐久的に使用することができ、又、この場合、上記圧力釜体1内に上記袋状分離体4aを収納可能な枠状体4bを配置してなるから、袋状分離体4aの圧力釜体1に対する出し入れを良好に行うことができる。   In this case, the separation column 4 is made of a cloth-like bag-like separator 4a in which the mushroom cultivation waste fungus bed W is enclosed and the pressurized hot water N and the extract T can pass therethrough. The squeezing effect due to swelling of the mushroom cultivation waste fungus bed W by contact with the pressurized water N can be obtained, and the extraction efficiency of the mushroom component can be improved. In this case, the bag-like separated body 4a is composed of an aramid fiber. Since it is made of a net-like body made of heat-resistant fibers such as glass fibers, carbon fibers, and stainless steel fibers, it can be used in a durable manner. Since the frame-like body 4b capable of accommodating the bag-like separator 4a is disposed therein, the bag-like separator 4a can be taken in and out of the pressure hook body 1 in a good manner.

又、上記冷却管路7は抽出作業完了後等において、加熱空間R内に冷却水Hを供給し、圧力釜体1を冷却したり、又は、圧力容器内の圧力及び温度の制御に用いられ、又、補助加熱管路8は、必要に応じて、直接、圧力釜体1内に蒸気Gを直接送入する場合に用いられるものである。   The cooling pipe 7 is used for supplying cooling water H into the heating space R to cool the pressure vessel 1 or controlling the pressure and temperature in the pressure vessel after the extraction operation is completed. Further, the auxiliary heating pipe line 8 is used when the steam G is directly fed into the pressure vessel 1 as required.

図7の第二形態例は上記袋状分離体4aの別例構造を示し、この場合、上記キノコ栽培廃菌床Wが封入される内袋状分離体4c及び内袋状分離体4cを覆う外袋状分離体4dからなる二重袋状に形成されている。この場合、内袋状分離体4cは粗いメッシュ、一方、外袋状分離体4dは濾過用としての細かいメッシュのものを用いている。   The 2nd form example of FIG. 7 shows the other example structure of the said bag-shaped isolation | separation body 4a, and covers the inner bag-shaped isolation | separation body 4c and the inner bag-shaped isolation | separation body 4c by which the said mushroom cultivation waste bacteria bed W is enclosed in this case. It is formed in a double bag shape composed of the outer bag-shaped separator 4d. In this case, the inner bag-shaped separator 4c is a coarse mesh, while the outer bag-shaped separator 4d is a fine mesh for filtration.

この実施の第二形態例は上記構成であるから、上記第一形態例の作用効果に加えて、上記キノコ栽培廃菌床Wが封入される内袋状分離体4c及び内袋状分離体4cを覆う外袋状分離体4dからなる二重袋状に形成されているので、キノコ栽培廃菌床の残渣による循環管路内の詰まり現象や汚れ現象を確実に抑制することができる。   Since the second embodiment of this embodiment has the above-described configuration, in addition to the effects of the first embodiment, the inner bag-shaped separator 4c and the inner bag-shaped separator 4c in which the mushroom cultivation waste fungus bed W is enclosed. Since the outer bag-shaped separated body 4d is formed in a double bag shape, the clogging phenomenon and dirt phenomenon in the circulation pipe line due to the residue of the mushroom cultivation waste fungus bed can be reliably suppressed.

図8の第三形態例は上記袋状分離体4aの別例構造を示し、この場合、上記キノコ栽培廃菌床Wが封入される内袋状分離体4c及び内袋状分離体4cを覆う外袋状分離体4dからなる二重袋状に形成され、かつ、外袋状分離体4dと内袋状分離体4cとの間の空間にシリカ、炭などの濾過材4eを配置して構成している。そして、内袋状分離体4cは粗いメッシュ、一方、外袋状分離体4dは細かいメッシュのものを用いている。   The third embodiment in FIG. 8 shows another structure of the bag-like separator 4a. In this case, the inner bag-like separator 4c and the inner bag-like separator 4c in which the mushroom cultivation waste fungus bed W is enclosed are covered. It is formed in a double bag shape composed of an outer bag-shaped separator 4d, and a filter medium 4e such as silica or charcoal is arranged in a space between the outer bag-shaped separator 4d and the inner bag-shaped separator 4c. is doing. The inner bag-shaped separator 4c is a coarse mesh, while the outer bag-shaped separator 4d is a fine mesh.

この実施の第三形態例は上記構成であるから、上記第一形態例の作用効果に加えて、上記キノコ栽培廃菌床Wが封入される内袋状分離体4c及び内袋状分離体4cを覆う外袋状分離体4dからなる二重袋状に形成されているので、キノコ栽培廃菌床の残渣による循環管路内の詰まり現象や汚れ現象を確実に抑制することができ、かつ、外袋状分離体4dと内袋状分離体4cとの間の空間に例えば、シリカ、炭などの濾過材4eが配置されているので、この濾過材4eにより循環する抽出液は濾過され、キノコ栽培廃菌床Wの残渣による循環管路3内の詰まり現象や汚れ現象を確実に抑制することができる。   Since the third embodiment of this embodiment is configured as described above, in addition to the effects of the first embodiment, the inner bag-shaped separator 4c and the inner bag-shaped separator 4c in which the mushroom cultivation waste fungus bed W is enclosed. Since it is formed in a double bag shape consisting of the outer bag-like separator 4d covering the clogging, it is possible to reliably suppress clogging phenomenon and dirt phenomenon in the circulation pipe line due to residues of mushroom cultivation waste fungus bed, and In the space between the outer bag-shaped separator 4d and the inner bag-shaped separator 4c, for example, a filter medium 4e such as silica or charcoal is disposed. The clogging phenomenon and dirt phenomenon in the circulation pipe line 3 due to the residue of the cultivation waste bacteria bed W can be reliably suppressed.

尚、本発明は上記実施の形態例に限られるものではなく、圧力釜体1、加熱機構2、循環管路3の配置位置、構造や形態等は適宜設計して変更される。   In addition, this invention is not restricted to the said embodiment, The arrangement | positioning position, structure, form, etc. of the pressure vessel body 1, the heating mechanism 2, and the circulation conduit 3 are designed and changed suitably.

[実施例1]
乾燥したキノコ栽培廃菌床たるエリンギ廃菌床2kgを、分離カラム5たるアラミドの5メッシュのニット性筒状袋に封入した。次いで、これを水に1日浸せきした。浸せきによってエリンギ廃菌床は吸水して袋の中で膨潤した。全体が膨らんだ状態でさらに75メッシュの平織りのアラミドの袋で包んだ。この状態で上記の加圧熱水抽出処理を行った。処理は5℃/分で昇温し、140℃の飽和蒸気圧で1時間処理した。処理後空冷して室温に戻した。空冷した菌床を、中側の袋はそのままで、75メッシュのアラミドの袋から取り出し、そのまま流水をかけ水洗いを行い、この流水中にキノコ成分が抽出された抽出液(1)を得た。一方中側の袋を新たに、75メッシュのアラミド製の袋に入れ、再び加圧熱水装置にセットした。セット後同じ昇温速度で160℃まで加温し、160℃で10分間処理し100℃まで冷却した。100℃で1時間抽出処理し、室温に下げた。ここで処理を抽出液を取り出し抽出液(2)を得た。次に160℃の処理と同様なことを、180℃で繰り返し抽出液(3)を得た。抽出液(2)と(3)は濃縮し、βグルカンを主成分とする多糖を得た。多糖はあわせて100gであった。この抽出液(1)からもきのこに由来する物質を得た。
[Example 1]
2 kg of dried ringi cultivated bed, which is a dried mushroom cultivated microbial bed, was enclosed in a 5-mesh knitted cylindrical bag of aramid as a separation column 5. This was then immersed in water for 1 day. By soaking, the waste bed of eringi water absorbed and swollen in the bag. The whole was inflated and wrapped in a 75 mesh plain weave aramid bag. In this state, the pressurized hot water extraction treatment was performed. The treatment was performed at a temperature of 5 ° C./min and treated with a saturated vapor pressure of 140 ° C. for 1 hour. After the treatment, it was air-cooled and returned to room temperature. The air-cooled fungus bed was taken out from the 75-mesh aramid bag without changing the inner bag, and washed with running water as it was to obtain an extract (1) from which mushroom components were extracted. On the other hand, the inner bag was newly put in a 75 mesh aramid bag and set again in the pressurized hot water apparatus. After setting, the sample was heated to 160 ° C. at the same temperature increase rate, treated at 160 ° C. for 10 minutes, and cooled to 100 ° C. Extraction treatment was performed at 100 ° C. for 1 hour, and the temperature was lowered to room temperature. Here, the extract was extracted to obtain an extract (2). Next, the same process as that at 160 ° C. was repeated at 180 ° C. to obtain an extract (3). Extracts (2) and (3) were concentrated to obtain a polysaccharide mainly composed of β-glucan. The total amount of polysaccharide was 100 g. A substance derived from mushrooms was also obtained from this extract (1).

[実施例2]
乾燥したマイタケ廃菌床5kgを、アラミドの10メッシュのニット製筒状袋に封入した。これを水に1日浸せきした。浸せきによって吸水させた後、袋ごとさらに75メッシュ平織りのアラミドの袋で包んだ。この状態で上記の加圧熱水処理を行った。処理は5℃/分で昇温し、140℃の飽和蒸気圧で1時間処理した。処理後空冷して室温に戻した。空冷した菌床を、中側の袋はそのままで75メッシュのアラミド製の袋から取り出し、そのまま流水をかけ水洗いを行った。中側の袋を新たに、75メッシュのアラミド製の袋に入れ、再び加圧熱水処理を行い、同じ昇温速度で160℃まで加温し、160℃で10分間処理し100℃まで冷却した。100℃で1時間抽出処理し、室温に下げた。この処理後の抽出液を取り出し抽出液(1)を得た。次に160℃の処理を行い、さらに、同様なことを、180℃、200℃で繰り返し抽出液(2)、(3)を得た。抽出液(1)と(2)は濃縮、乾燥し、マイタケ成分に由来する(βグルカンを主成分)する多糖を得た。多糖はあわせて100gであった。一方抽出液成分(2)を濃縮、乾燥し、菌床に由来する多糖0.5kg(主としてキリロールオリゴマー)を得た。
[Example 2]
5 kg of dried maitake mushroom beds were enclosed in an aramid 10-mesh knitted cylindrical bag. This was immersed in water for one day. After water absorption by dipping, the entire bag was wrapped in a 75 mesh plain weave aramid bag. In this state, the pressurized hot water treatment was performed. The treatment was performed at a temperature of 5 ° C./min and treated with a saturated vapor pressure of 140 ° C. for 1 hour. After the treatment, it was air-cooled and returned to room temperature. The air-cooled fungus bed was taken out of the 75 mesh aramid bag while leaving the inner bag as it was, and washed with running water as it was. The inside bag is newly put into a 75 mesh aramid bag, is subjected to pressurized hot water treatment again, heated to 160 ° C. at the same temperature rise rate, treated at 160 ° C. for 10 minutes, and cooled to 100 ° C. did. Extraction treatment was performed at 100 ° C. for 1 hour, and the temperature was lowered to room temperature. The extract after this treatment was taken out to obtain an extract (1). Next, the process of 160 degreeC was performed, and also the same thing was repeated at 180 degreeC and 200 degreeC, and the extract liquids (2) and (3) were obtained. Extracts (1) and (2) were concentrated and dried to obtain polysaccharides derived from maitake components (β-glucan as a main component). The total amount of polysaccharide was 100 g. On the other hand, the extract component (2) was concentrated and dried to obtain 0.5 kg of polysaccharides (mainly Kirirol oligomer) derived from the fungus bed.

以上、所期の目的を充分達成することができる。   As described above, the intended purpose can be sufficiently achieved.

本発明の実施の第一形態例の全体系統説明図である。BRIEF DESCRIPTION OF THE DRAWINGS It is whole system explanatory drawing of the example of 1st Embodiment of this invention. 本発明の実施の第一形態例の部分断面図である。It is a fragmentary sectional view of the example of the 1st embodiment of the present invention. 本発明の実施の第一形態例の部分斜視図である。It is a fragmentary perspective view of the first embodiment of the present invention. 本発明の実施の第一形態例の部分平面図である。It is a fragmentary top view of the 1st example of an embodiment of the invention. 本発明の実施の第一形態例の部分斜視図である。It is a fragmentary perspective view of the first embodiment of the present invention. 本発明の実施の第一形態例の部分側断面図である。It is a fragmentary sectional side view of the first embodiment of the present invention. 本発明の実施の第二形態例の部分側断面図である。It is a fragmentary sectional side view of the 2nd example of an embodiment of the invention. 本発明の実施の第三形態例の部分側断面図である。It is a fragmentary sectional side view of the 3rd embodiment of this invention.

符号の説明Explanation of symbols

R 加熱空間
W キノコ栽培廃菌床
N 加圧熱水
T 抽出液
1 圧力釜体
3 循環管路
3a 出口部
3c 入口部
4 分離カラム
4a 袋状分離体
4b 枠状体
4c 内袋状分離体
4d 外袋状分離体
4e 濾過材
R Heating space W Mushroom cultivation waste fungus bed N Pressurized hot water T Extraction liquid 1 Pressure kettle body 3 Circulation line 3a Outlet part 3c Inlet part 4 Separation column 4a Bag-like separation body 4b Frame-like body 4c Inner bag-like separation body 4d Outer bag-shaped separator 4e Filter material

Claims (9)

キノコ栽培廃菌床及び水を圧力釜体内に封止して該圧力釜体を加熱し、該圧力釜体内のキノコ栽培廃菌床に加圧熱水を接触させることによりキノコ成分を抽出し、該キノコ成分を抽出した抽出液を取り出すに際し、上記圧力釜体内に上記キノコ栽培廃菌床を封入可能な分離カラムを配置すると共に上記圧力釜体内の加圧熱水が圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻る加圧熱水の循環により圧力釜体内の加圧熱水を水流撹拌させてキノコ栽培廃菌床からキノコ成分を抽出することを特徴とするキノコ成分抽出方法。   The mushroom cultivation waste fungus bed and water are sealed in a pressure kettle body, the pressure kettle body is heated, and mushroom components are extracted by bringing pressurized hot water into contact with the mushroom cultivation waste fungus bed in the pressure kettle body, When taking out the extract from which the mushroom component has been extracted, an outlet is provided in which the separation column capable of enclosing the mushroom cultivation waste fungus bed is disposed in the pressure kettle and pressurized hot water in the pressure kettle is provided in the pressure kettle The mushrooms are extracted from the mushroom cultivation waste fungus bed by agitating the pressurized hot water in the pressure kettle through the circulation of the pressurized hot water returning to the pressure kettle through the inlet again Component extraction method. キノコ栽培廃菌床及び水を圧力釜体内に封止して該圧力釜体を加熱し、該圧力釜体内のキノコ栽培廃菌床に加圧熱水を接触させることによりキノコ成分を抽出し、該キノコ成分を抽出した抽出液を取り出す装置において、上記圧力釜体内に上記キノコ栽培廃菌床を封入可能な分離カラムを配置し、上記圧力釜体内の加圧熱水が圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻る加圧熱水の循環流により圧力釜体内の加圧熱水を水流撹拌させる循環管路を設けてなることを特徴とするキノコ成分抽出装置。   The mushroom cultivation waste fungus bed and water are sealed in a pressure kettle body, the pressure kettle body is heated, and mushroom components are extracted by bringing pressurized hot water into contact with the mushroom cultivation waste fungus bed in the pressure kettle body, In the apparatus for extracting the extract from which the mushroom component has been extracted, a separation column capable of enclosing the mushroom cultivation waste fungus bed is disposed in the pressure kettle body, and pressurized hot water in the pressure kettle body is provided in the pressure kettle body. A mushroom component extraction device comprising a circulation pipe for agitating the pressurized hot water in the pressure kettle by a circulating flow of the pressurized hot water returning from the outlet to the pressure kettle again through the inlet. . 上記循環管路の途中に上記圧力釜体内の加圧熱水を圧力釜体に設けた出口部から再び入口部を介して圧力釜体内に戻すための循環ポンプを設けてなることを特徴とする請求項2記載のキノコ成分抽出装置。   A circulation pump is provided in the middle of the circulation line to return the pressurized hot water in the pressure kettle from the outlet provided in the pressure kettle to the pressure kettle again through the inlet. The mushroom component extraction device according to claim 2. 上記循環管路の途中に上記圧力釜体内の抽出液を取出可能な取出管路を設けてなることを特徴とする請求項2又は3記載のキノコ成分抽出装置。   4. The mushroom component extracting device according to claim 2, wherein an extraction pipe capable of taking out the extract from the pressure vessel is provided in the middle of the circulation pipe. 上記分離カラムは、上記キノコ栽培廃菌床が封入され、上記加圧熱水及び抽出液の通過が可能な袋状分離体からなることを特徴とする請求項2〜4のいずれか1項に記載のキノコ成分抽出装置。   5. The separation column according to claim 2, wherein the mushroom cultivation waste fungus bed is enclosed, and the separation column is formed of a bag-like separated body through which the pressurized hot water and the extract can pass. The mushroom component extraction apparatus described. 上記袋状分離体は、アラミド繊維、ガラス繊維、炭素繊維、ステンレス鋼からなる繊維などの金属繊維等の耐熱性繊維又はこれらの複合繊維により製作される網状体からなることを特徴とする請求項5記載のキノコ成分抽出装置。   The bag-like separator is formed of a heat-resistant fiber such as a metal fiber such as aramid fiber, glass fiber, carbon fiber, or stainless steel fiber, or a net-like body made of these composite fibers. 5. A mushroom component extraction apparatus according to 5. 上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成されていることを特徴とする請求項5記載のキノコ成分抽出装置。   The bag-like separator is formed in a double bag shape composed of an inner bag-like separator that encloses the mushroom cultivation waste fungus bed and an outer bag-like separator that covers the inner bag-like separator. The mushroom component extraction device according to claim 5. 上記袋状分離体は、上記キノコ栽培廃菌床が封入される内袋状分離体及び内袋状分離体を覆う外袋状分離体からなる二重袋状に形成され、該外袋状分離体と内袋状分離体との間の空間に濾過材を配置してなることを特徴とする請求項5記載のキノコ成分抽出装置。   The bag-like separated body is formed into a double bag shape comprising an inner bag-like separated body enclosing the mushroom cultivation waste fungus bed and an outer bag-like separated body covering the inner bag-like separated body, and the outer bag-like separated body. 6. The mushroom component extracting device according to claim 5, wherein a filtering material is disposed in a space between the body and the inner bag-shaped separator. 上記圧力釜体内に上記袋状分離体を収納可能な枠状体を配置してなることを特徴とする請求項5〜8のいずれか1項に記載のキノコ成分抽出装置。
The mushroom component extraction device according to any one of claims 5 to 8, wherein a frame-like body capable of accommodating the bag-like separator is disposed in the pressure cooker.
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010095579A (en) * 2008-10-15 2010-04-30 Kumamoto Univ Method for clarifying organic porous material
WO2023068103A1 (en) * 2021-10-18 2023-04-27 環境エネルギー株式会社 Production method for water-soluble extract of spent mushroom bed used for mushroom cultivation , biofilm inhibitor, production method for biofilm inhibitor, and biofilm inhibition method
WO2023095568A1 (en) * 2021-11-25 2023-06-01 大倉工業株式会社 Method for producing hydroxytyrosol from olive leaves, and hydroxytyrosol-containing composition
JP7482538B2 (en) 2022-01-19 2024-05-14 環境エネルギー株式会社 Method for producing compressed hot water extract from waste mushroom cultivation bed, and radical scavenger

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04325484A (en) * 1991-04-26 1992-11-13 Shigenobu Watari Treatment of waste mushroom bed
JPH0625A (en) * 1992-06-19 1994-01-11 Toyo Seikan Kaisha Ltd Cultivation of edible mushroom and medium therefor
JPH06219874A (en) * 1993-01-22 1994-08-09 Nippon Seibutsu Sangyo Kk Method for reforming mushroom-grown bed and soil activator
JPH08181A (en) * 1994-06-17 1996-01-09 Noboru Yamamoto Production of feed, fertilizer, etc., using waste mushroom cultivation medium
JPH0951939A (en) * 1995-08-11 1997-02-25 Rion Netsugaku Kk Processing method of waste culture medium
JPH11171677A (en) * 1997-12-11 1999-06-29 Nagano Prefecture Nokyo Hiryo Kk Compost and its production
JPH11196818A (en) * 1998-01-08 1999-07-27 Shingo Kikuchi Production of essence product from plants and mushrooms on factory scale
JPH11302672A (en) * 1998-04-23 1999-11-02 Toshihide Kondo Production of carbonization product, and carbonization product

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04325484A (en) * 1991-04-26 1992-11-13 Shigenobu Watari Treatment of waste mushroom bed
JPH0625A (en) * 1992-06-19 1994-01-11 Toyo Seikan Kaisha Ltd Cultivation of edible mushroom and medium therefor
JPH06219874A (en) * 1993-01-22 1994-08-09 Nippon Seibutsu Sangyo Kk Method for reforming mushroom-grown bed and soil activator
JPH08181A (en) * 1994-06-17 1996-01-09 Noboru Yamamoto Production of feed, fertilizer, etc., using waste mushroom cultivation medium
JPH0951939A (en) * 1995-08-11 1997-02-25 Rion Netsugaku Kk Processing method of waste culture medium
JPH11171677A (en) * 1997-12-11 1999-06-29 Nagano Prefecture Nokyo Hiryo Kk Compost and its production
JPH11196818A (en) * 1998-01-08 1999-07-27 Shingo Kikuchi Production of essence product from plants and mushrooms on factory scale
JPH11302672A (en) * 1998-04-23 1999-11-02 Toshihide Kondo Production of carbonization product, and carbonization product

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010095579A (en) * 2008-10-15 2010-04-30 Kumamoto Univ Method for clarifying organic porous material
WO2023068103A1 (en) * 2021-10-18 2023-04-27 環境エネルギー株式会社 Production method for water-soluble extract of spent mushroom bed used for mushroom cultivation , biofilm inhibitor, production method for biofilm inhibitor, and biofilm inhibition method
JP7525212B2 (en) 2021-10-18 2024-07-30 環境エネルギー株式会社 Method for producing water-soluble extract of waste mushroom cultivation bed, biofilm inhibitor, and method for producing biofilm inhibitor
WO2023095568A1 (en) * 2021-11-25 2023-06-01 大倉工業株式会社 Method for producing hydroxytyrosol from olive leaves, and hydroxytyrosol-containing composition
JP7482538B2 (en) 2022-01-19 2024-05-14 環境エネルギー株式会社 Method for producing compressed hot water extract from waste mushroom cultivation bed, and radical scavenger

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