JP2008031558A - Gas shower head, treatment device, treatment method and maintenance method for treatment device - Google Patents

Gas shower head, treatment device, treatment method and maintenance method for treatment device Download PDF

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JP2008031558A
JP2008031558A JP2007268190A JP2007268190A JP2008031558A JP 2008031558 A JP2008031558 A JP 2008031558A JP 2007268190 A JP2007268190 A JP 2007268190A JP 2007268190 A JP2007268190 A JP 2007268190A JP 2008031558 A JP2008031558 A JP 2008031558A
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shower head
gas
substrate
gas shower
metal
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JP2008031558A5 (en
JP4816616B2 (en
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Masashi Murakami
誠志 村上
Yoshiyuki Hanada
良幸 花田
Takashi Kakegawa
崇 掛川
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Tokyo Electron Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a shower head composed in such a manner that a plurality of metallic members are superimposed, and capable of feeding, e.g., a film deposition gas to a substrate, in which the cleaning of each gas flow passage can be easily performed, and the generation of reaction products is suppressed. <P>SOLUTION: A shower head composed in such a manner that metallic sheets made of nickel are superimposed in three steps is prepared, and is tacked with bolts, and is installed in a chamber. Next, heating is performed with both heaters provided on a mounting stand and at the upper face of the shower head in the chamber, thus fine ruggedness in the respective contact faces of the metallic sheets each other starts to be melted, and the contact faces start to be metallically diffused and coupled each other from the melted parts. Then, even if the bolts are removed, by continuing the heating to a degree at which the metallic sheets are not separated, the gaps present at the contact faces till then are vanished, and the whole contact face is air-tightly joined. <P>COPYRIGHT: (C)2008,JPO&INPIT

Description

本発明は、半導体ウエハ等の基板に対してガスの供給を行うガスシャワーヘッド、このガスシャワーヘッドを用いて前記基板の表面に処理を行う処理装置及び処理方法並びに処理装置のメンテナンス方法に関する。   The present invention relates to a gas shower head for supplying a gas to a substrate such as a semiconductor wafer, a processing apparatus and a processing method for processing the surface of the substrate using the gas shower head, and a maintenance method for the processing apparatus.

半導体装置の製造プロセスの一つにCVD(Chemical vapor deposition)処理により被処理体上に成膜を行うものがあり、この処理を行う装置の一つに枚葉式の成膜装置がある。この成膜装置は例えば内部に半導体ウエハ(以下ウエハと略す)を載置するための載置台を備える処理容器と、この載置台と対向して設けられ、ウエハ表面に向けて成膜ガスの供給を行うガスシャワーヘッドとを備えている。このシャワーヘッドは、複数種の成膜ガスが互いに混じらないように且つ横方向に拡散されてウエハ表面に均一に供給されるようにガス流路が形成されており、そのため金属板(金属製の拡散板)を例えば三段に積み重ねて構成される。これら金属板は例えばボルトにて互いに固定され且つ処理容器に取り付けられており、上面側から供給される成膜ガスが三段の金属板内を貫通する流路を下方に流れ、下端面に形成される多数の孔部からウエハの表面全体に均一に供給されることとなる。このようなガスシャワーヘッドは、複数種の成膜ガスを同時に供給できるようになっており、例えばチタンナイトライド(TiN)を成膜するために、TiCl4ガスとNH3ガスとが互いに混じらないように通過して処理容器内に供給される。   One of the semiconductor device manufacturing processes is to form a film on a target object by CVD (Chemical Vapor Deposition), and one of apparatuses for performing this process is a single-wafer type film forming apparatus. For example, this film forming apparatus is provided with a processing container having a mounting table for mounting a semiconductor wafer (hereinafter abbreviated as “wafer”) inside, and facing the mounting table, and supplying a film forming gas toward the wafer surface. A gas shower head. This shower head has a gas flow path formed so that a plurality of types of film forming gases are not mixed with each other and are diffused in the lateral direction and supplied uniformly to the wafer surface. Diffusion plates) are stacked, for example, in three stages. These metal plates are fixed to each other by, for example, bolts and attached to the processing container, and a film forming gas supplied from the upper surface flows downward through a flow path penetrating the inside of the three-stage metal plate, and is formed on the lower end surface. Thus, the wafer is uniformly supplied to the entire surface of the wafer from the many holes. Such a gas shower head can supply a plurality of types of film forming gases simultaneously. For example, in order to form titanium nitride (TiN), TiCl 4 gas and NH 3 gas are not mixed with each other. It passes and is supplied in a processing container.

図2はこのような二種類のガスを別々に供給可能なガスシャワーヘッドを示す縦断面図であり、図3はこれを三段に分解して示した縦断面図である。図示するようにTiCl4ガスについてはガス供給管21から上段部3aと中段部3bとの間に形成される空間31及び第1のガス流路32を介して第1の孔部33に、NH3については第2のガス流路42及び空間41を介して第2の孔部43に夫々向かうように構成されている。また第1の孔部33及び第2の孔部43の配置は互い違いとされており、両方の成膜ガスが共にウエハの表面全体に均等に行き渡るようになっている。   FIG. 2 is a longitudinal sectional view showing such a gas shower head capable of separately supplying two kinds of gases, and FIG. 3 is a longitudinal sectional view showing the gas shower head exploded in three stages. As shown in the figure, the TiCl4 gas is transferred from the gas supply pipe 21 to the first hole 33 via the space 31 and the first gas flow path 32 formed between the upper step portion 3a and the middle step portion 3b. Is configured to be directed to the second hole 43 through the second gas flow path 42 and the space 41, respectively. The arrangement of the first hole portion 33 and the second hole portion 43 is staggered so that both deposition gases are spread evenly over the entire surface of the wafer.

しかしながら、上述したような複数種の成膜ガスを供給するためのガスシャワーヘッドには以下のような問題がある。即ち、ネジ止めにより固定される各段の金属板間の接触面(接合面)P2には図7に示すように機械的研磨では解消し得ない微小な凹凸があるため、ネジ止めをしても完全に密着することはなく、図8に示すような数μmのごく微小な隙間が生じてしまう。従ってこの隙間を介してTiCl4ガスとNH3ガスとが混じり合ってしまうことがあり、この場合にガスシャワーヘッド内で生成物が生じることがある。   However, the gas shower head for supplying a plurality of types of film forming gases as described above has the following problems. That is, the contact surface (joint surface) P2 between the metal plates at each stage fixed by screwing has minute irregularities that cannot be eliminated by mechanical polishing as shown in FIG. However, it does not adhere completely, and a very small gap of several μm as shown in FIG. 8 is generated. Therefore, TiCl4 gas and NH3 gas may be mixed through this gap, and in this case, a product may be generated in the gas shower head.

即ち、両成膜ガスは熱エネルギーにより反応を起こすため、通常はその裏面側を加熱されるウエハの表面近傍で反応が起こるのであるが、ガスシャワーヘッドとウエハとは接近しているため、ウエハから放射される熱によりガスシャワーヘッドも加熱され、その一部がガスシャワーヘッド内で反応してしまうのである。こうして生じた反応生成物はパーティクルの原因となるおそれがある。   That is, since both film forming gases react with each other by heat energy, the reaction usually takes place near the surface of the wafer heated on the back side, but the gas shower head and the wafer are close to each other. The gas shower head is also heated by the heat radiated from the gas, and a part thereof reacts in the gas shower head. The reaction product generated in this way may cause particles.

一方、前記隙間への対策としては、拡散板の接合時に当該拡散板の接合面にろう材を塗布しておくことで前記隙間を塞ぐという手法もある。しかしながら、この手法を採ると拡散板内の流路近傍部位でろう材と成膜ガスとが反応し、その反応生成物がパーティクルとなるおそれがある。具体的には、上述構成の装置において、例えばAg、Cu、Zn等のガスシャワーヘッドの構成母材以外のろう材を用いた場合に、成膜ガス中のClやF等がろう材と反応し、反応生成物が発生してしまう。またろう材を用いると各拡散板を分解することが困難となるため、洗浄作業を行う場合に不便であるという問題もある。   On the other hand, as a countermeasure against the gap, there is a method of closing the gap by applying a brazing material to the joining surface of the diffusion plate when the diffusion plate is joined. However, when this method is adopted, the brazing material and the film forming gas react at a site near the flow path in the diffusion plate, and the reaction product may become particles. Specifically, in the apparatus having the above-described configuration, for example, when a brazing material other than the constituent base material of the gas shower head such as Ag, Cu, Zn or the like is used, Cl or F in the film forming gas reacts with the brazing material. Then, a reaction product is generated. In addition, when brazing material is used, it is difficult to disassemble each diffusion plate, and there is a problem that it is inconvenient when performing a cleaning operation.

本発明はこのような事情に基づいてなされたものであり、その目的は、複数の金属部材を重ね合わせて構成され、基板に対して複数種の成膜ガスを供給可能なガスシャワーヘッドにおいて、各金属部材の接触面同士に生じる隙間から異なる種類の成膜ガスが混じり合うことを防ぐ技術を提供することにある。他の発明の目的は、前記ガスシャワーヘッドを処理装置に適用し、パーティクルの発生を抑えることにある。   The present invention has been made based on such circumstances, and the object thereof is a gas shower head configured by stacking a plurality of metal members and capable of supplying a plurality of types of film forming gases to a substrate. An object of the present invention is to provide a technique for preventing different kinds of film forming gases from being mixed from a gap generated between contact surfaces of metal members. Another object of the present invention is to apply the gas shower head to a processing apparatus to suppress the generation of particles.

本発明に係るガスシャワーヘッドは、基板の表面と対向して設けられると共に前記基板と対向する面部に多数の孔部を備え、ガス供給路から送られるガスを、これら孔部を介して前記基板に同時に供給するガスシャワーヘッドにおいて、
複数の金属部材を上下に重ね合わせた状態で加熱することにより、各金属部材の接触面同士を金属拡散接合したシャワーヘッド本体と、
このシャワーヘッド本体内の前記接触面を横切るように貫通し、独立して形成される複数のガス流路と、を備えることを特徴とする。
The gas shower head according to the present invention is provided so as to face the surface of the substrate and includes a large number of holes in the surface facing the substrate, and gas sent from a gas supply path is passed through the holes to the substrate In the gas shower head that supplies to the
By heating in a state where a plurality of metal members are stacked one above the other, a shower head body in which the contact surfaces of each metal member are metal diffusion bonded,
And a plurality of gas flow paths that are formed so as to cross the contact surface in the shower head body and are formed independently.

このような構成によれば、ガスシャワーヘッドをなす金属部材の接触面同士を加熱により化学的に結合させているので、当該接合面にある機械的な結合では解消し得なかった微小な凹凸により形成される微小な隙間を解消することができる。従って、各ガス流路におけるガス漏れを抑えると共に、ガスシャワーヘッド内で異なる成膜ガス同士が混じり合い、反応生成物が生じることを防ぐことができる。   According to such a configuration, the contact surfaces of the metal members forming the gas shower head are chemically bonded to each other by heating, and therefore, due to minute unevenness that could not be eliminated by mechanical bonding on the bonding surface. The minute gaps that are formed can be eliminated. Accordingly, it is possible to prevent gas leakage in each gas flow path and prevent the formation of reaction products by mixing different film forming gases in the gas shower head.

また本発明に係るガスシャワーヘッドは以上のような効果を有することから、例えば処理装置に適用することが好ましく、処理装置には例えば基板を載置するための載置台が設けられた処理容器と、前記処理容器内を排気する真空ポンプと、を備えたものが用いられる。なお、上記金属部材としては例えばニッケルまたはニッケル合金を用いることが好ましい。   Further, since the gas shower head according to the present invention has the above effects, it is preferably applied to, for example, a processing apparatus. The processing apparatus includes, for example, a processing container provided with a mounting table for mounting a substrate. And a vacuum pump for exhausting the inside of the processing container. For example, nickel or a nickel alloy is preferably used as the metal member.

また本発明に係る処理方法は、処理容器内の載置台に載置された基板に対して、当該基板に対向するガスシャワーヘッドからガスを供給し、処理を行う処理方法において、
前記ガスシャワーヘッドは、複数の金属部材を重ね合わせた状態で、これを加熱して各金属部材の接触面同士の金属拡散接合をして構成され、
このガスシャワーヘッドからガスを基板に供給し、当該基板の表面に処理を行うことを特徴とする。
また本発明は、処理容器内の載置台に載置された基板に対して、当該基板に対向するガスシャワーヘッドからガスを基板に供給し、当該基板の表面に処理を行う処理装置をメンテナンスする方法において、
ガスシャワーヘッドを構成する複数の金属部材を重ね合わせた状態で、これを加熱して各金属部材の接触面同士を金属拡散接合してガスシャワーヘッドを組み立てる工程を含むことを特徴とする。
また上述の処理装置のメンテナンス方法において、ガスシャワーヘッドを組み立てる工程は、前記各金属部材の接触面同士を金属拡散接合する工程に加えて更に複数の金属部材を重ね合わせてネジ止めを行う工程を設けるようにしてもよい。さらに成膜処理を行った後、金属拡散接合による結合力が弱まったときに、前記ネジ止めされている下段側の金属部材が自重で上段側の金属部材から離脱するように当該ネジ止めに用いられているネジを緩めた状態でガスシャワーヘッドを保持し、この状態でガスシャワーヘッドを加熱して、複数の金属部材を互いに分離する工程を設けるようにしてもよい。
Further, the processing method according to the present invention is a processing method in which a gas is supplied from a gas shower head facing the substrate to the substrate placed on the mounting table in the processing container, and the processing is performed.
The gas shower head is configured by metal diffusion bonding between the contact surfaces of each metal member by heating the metal member in a state where a plurality of metal members are overlapped,
A gas is supplied from the gas shower head to the substrate, and the surface of the substrate is processed.
In addition, the present invention maintains a processing apparatus that supplies a gas to a substrate from a gas shower head facing the substrate and processes the surface of the substrate placed on a mounting table in a processing container. In the method
In a state in which a plurality of metal members constituting the gas shower head are overlapped, the process includes heating the metal members and bonding the contact surfaces of the metal members to each other by metal diffusion bonding to assemble the gas shower head.
Moreover, in the maintenance method of the processing apparatus described above, the step of assembling the gas shower head includes a step of screwing by overlapping a plurality of metal members in addition to the step of metal diffusion bonding of the contact surfaces of the metal members. You may make it provide. Further, after the film forming process is performed, when the bonding force by metal diffusion bonding is weakened, the lower metal member that is screwed is used for screwing so that the lower metal member is detached from the upper metal member by its own weight. A step of holding the gas shower head in a loosened state and heating the gas shower head in this state to separate the plurality of metal members from each other may be provided.

このような方法において、ガスシャワーヘッドをなす各金属部材の加熱は、ガスシャワーヘッドを処理容器に装着して、基板を加熱するための加熱部及びガスシャワーヘッドに設けられた加熱部の少なくとも一方を用いて行うことが好ましい。   In such a method, each metal member constituting the gas shower head is heated by attaching at least one of a heating unit for heating the substrate by mounting the gas shower head on the processing container and a heating unit provided in the gas shower head. It is preferable to carry out using.

本発明によれば、複数の金属部材を重ね合わせて構成され、基板に対して複数種の成膜ガスを供給可能なガスシャワーヘッドにおいて、各金属部材の接触面同士に生じる隙間から異なる種類の成膜ガスが混じり合うことを防ぐことができる。他の発明によれば、前記ガスシャワーヘッドを処理装置に適用することで、パーティクルの発生を抑えることができる。   According to the present invention, in a gas shower head that is configured by overlapping a plurality of metal members and can supply a plurality of types of film forming gases to the substrate, different types of gaps are generated from the contact surfaces of the metal members. It is possible to prevent the deposition gas from being mixed. According to another invention, generation of particles can be suppressed by applying the gas showerhead to a processing apparatus.

以下に本発明に係るガスシャワーヘッドを適用した成膜装置の実施の形態を、図1〜図3を参照しながら説明する。11は例えばアルミニウムよりなる処理容器をなすチャンバであり、このチャンバ11内には基板であるウエハWを載置するためのウエハWより僅かに大きな円板状をなす載置台12と、この載置台12を下方側で支持する支持体13とが設けられている。載置台12内には、例えば抵抗加熱体を用いてなる加熱部をなす第1のヒータ14が埋設されており、成膜処理時において例えばウエハWを全面に亘って均等に昇温させ、或いは後述するガスシャワーヘッドの組み立て及び分解の各作業時にガスシャワーヘッドを所定温度に加熱するように、例えば装置外に設けられる電力供給部15から各用途に応じて温度制御を行う構成とされている。   Embodiments of a film forming apparatus to which a gas shower head according to the present invention is applied will be described below with reference to FIGS. Reference numeral 11 denotes a chamber which forms a processing container made of, for example, aluminum. In this chamber 11, a mounting table 12 having a disk shape slightly larger than the wafer W for mounting a wafer W as a substrate, and the mounting table The support body 13 which supports 12 on the lower side is provided. A first heater 14 that forms a heating unit using, for example, a resistance heater is embedded in the mounting table 12, and for example, the temperature of the wafer W is uniformly increased over the entire surface during the film formation process, or In order to heat the gas shower head to a predetermined temperature during each operation of assembling and disassembling the gas shower head, which will be described later, for example, the temperature is controlled according to each application from the power supply unit 15 provided outside the apparatus. .

チャンバ11の天井部にはガスシャワーヘッド本体30及びその側方を支持するシールド部30aにて構成されるガスシャワーヘッド3が設けられている。このガスシャワーヘッド3は、ガス供給路をなすガス供給管21,22と接続され、その下端面に形成される多数の孔部(ここでは図示を省略)を介して前記載置台12に載置されるウエハWの表面に成膜ガスの供給を行うものである。またガスシャワーヘッド3の上面部には第2のヒータ23が設けられており、上述した第1のヒータ14と同様に電力供給部15にて温度制御を行うように構成されている。更にまた、ガスシャワーヘッド3には整合器20aを介して高周波電源部20bが接続されており、成膜処理時においてウエハWに供給される成膜ガスをプラズマ化し、成膜反応を促進できるようになっている。   A gas shower head 3 constituted by a gas shower head main body 30 and a shield part 30 a that supports the side thereof is provided on the ceiling of the chamber 11. The gas shower head 3 is connected to gas supply pipes 21 and 22 forming a gas supply path, and is mounted on the mounting table 12 through a large number of holes (not shown here) formed in the lower end surface thereof. A film forming gas is supplied to the surface of the wafer W to be formed. In addition, a second heater 23 is provided on the upper surface of the gas shower head 3, and the temperature is controlled by the power supply unit 15 in the same manner as the first heater 14 described above. Furthermore, the gas shower head 3 is connected to a high frequency power supply unit 20b through a matching unit 20a, so that the film forming gas supplied to the wafer W during the film forming process can be converted into plasma to promote the film forming reaction. It has become.

チャンバ11の側方にはウエハWの搬入出のためのゲートバルブ16が設けられている。載置台12には、ゲートバルブ16を介して進入してきた図示しない搬送アームとの間でウエハWの受け渡しを行えるようにリフトピン17(実際には例えば3本ある)が突没自在に設けられている。リフトピン17の昇降は、その下端部を支持する支持部材17aを介し昇降機構17bの働きにより行われる。また支持体13の周囲には図示するように排気口11aが形成されており、この排気口11aには排気管18及びバルブV1を介して真空ポンプ19が接続されている。   A gate valve 16 for loading and unloading the wafer W is provided on the side of the chamber 11. The mounting table 12 is provided with lift pins 17 (actually, for example, three) that can project and retract so that the wafer W can be transferred to and from a transfer arm (not shown) that has entered through the gate valve 16. Yes. The lift pins 17 are lifted and lowered by the lifting mechanism 17b through a support member 17a that supports the lower end portion thereof. An exhaust port 11a is formed around the support 13 as shown in the figure, and a vacuum pump 19 is connected to the exhaust port 11a via an exhaust pipe 18 and a valve V1.

次に本実施の形態の要部をなすシャワーヘッド本体30について図2及び図3を参照して説明する。図2はこのシャワーヘッド本体30の全体構造を示す縦断面図であり、例えばニッケルよりなる3つの金属部材である金属板を上下に積み重ねた構成とされている。各金属板の接触面(接合面)は例えば機械加工、機械研磨、化学研磨または電解研磨等によって加工がなされており、その粗さは例えばRa3.2〜0.2程度である。   Next, the shower head main body 30 which is a main part of the present embodiment will be described with reference to FIGS. FIG. 2 is a longitudinal sectional view showing the entire structure of the shower head main body 30. The shower head main body 30 has a structure in which, for example, three metal members made of nickel are stacked vertically. The contact surface (joint surface) of each metal plate is processed by, for example, machining, mechanical polishing, chemical polishing, or electrolytic polishing, and the roughness is, for example, about Ra 3.2 to 0.2.

図3はこれら三段の金属板を分解して示したものであり、各金属板を便宜的に上段部3a、中段部3b、下段部3cと呼ぶものとすると、接合手順等の詳細は後述するが上段部3aと中段部3bとの接合面P1、及び中段部3bと下段部3cとの接合面P2は共に拡散接合により隙間なく接合されており、上段部3aと中段部3bとの間には空間31が、中段部3bと下段部3cとの間には空間41が夫々形成されている。中段部3bには空間31から下段部3cへと貫通する多数の第1のガス流路32と、空間31へは連通せず空間41へと連通する第2のガス流路42とが形成されている。下段部3cには第1のガス流路32に連通する多数の第1の孔部33と、空間41に連通する多数の第2の孔部43とが形成されている。また、上段部3aと中段部3bとの間についてはボルト34aによっても固定(ネジ止め)可能とされており、同様に中段部3bと下段部3cとの間についてもボルト34bにより固定が可能とされている。   FIG. 3 is an exploded view of these three metal plates. For convenience, each metal plate will be referred to as an upper step portion 3a, a middle step portion 3b, and a lower step portion 3c. However, the joint surface P1 between the upper step portion 3a and the middle step portion 3b and the joint surface P2 between the middle step portion 3b and the lower step portion 3c are joined together by diffusion bonding so that there is no gap between the upper step portion 3a and the middle step portion 3b. A space 31 is formed, and a space 41 is formed between the middle step portion 3b and the lower step portion 3c. A large number of first gas passages 32 penetrating from the space 31 to the lower step portion 3c and a second gas passage 42 communicating with the space 41 without being communicated with the space 31 are formed in the middle portion 3b. ing. A large number of first holes 33 that communicate with the first gas flow path 32 and a large number of second holes 43 that communicate with the space 41 are formed in the lower stage portion 3 c. Further, the upper step portion 3a and the middle step portion 3b can be fixed (screwed) by the bolt 34a, and similarly, the middle step portion 3b and the lower step portion 3c can be fixed by the bolt 34b. Has been.

上段部3aの上面には、既述のようにガス供給管21及びガス供給管22が夫々接続されているが、ガス供給管21は空間31に連通し、ガス供給管22は第2のガス流路を介して空間41へと連通している。ここで空間31及び空間41の形状について図3を参照しながら説明すると、空間31は中段部3bの上面に形成される例えば円柱状の凹部35aと、上段部3aの下面35bとで囲まれる円柱状の空間であり、横方向に連通する一体的空間として構成されている。空間41については中段部3bの下面に形成される例えば円柱状の多数の凹部36aと下段部3cの上面36bとで囲まれ、且つ各凹部36aが図示しない流路を介して各々が横方向に連通する一体的空間として構成されている。   As described above, the gas supply pipe 21 and the gas supply pipe 22 are connected to the upper surface of the upper stage portion 3a. The gas supply pipe 21 communicates with the space 31, and the gas supply pipe 22 is connected to the second gas. The space 41 communicates with the space 41. Here, the shape of the space 31 and the space 41 will be described with reference to FIG. 3. The space 31 is a circle surrounded by, for example, a cylindrical recess 35a formed on the upper surface of the middle step 3b and a lower surface 35b of the upper step 3a. It is a columnar space and is configured as an integral space communicating in the lateral direction. The space 41 is surrounded by a large number of, for example, columnar concave portions 36a formed on the lower surface of the middle step portion 3b and the upper surface 36b of the lower step portion 3c, and each of the concave portions 36a is laterally arranged through a flow path (not shown). It is configured as an integral space that communicates.

このため、ガス供給管21から送られてくる成膜ガスは空間31にて横方向に分散し、第1のガス流路32を介して第1の孔部33へと向かい、ガス供給管22から送られてくる成膜ガスは、第2のガス流路を介して空間41へと流入し、この空間41内で横方向に分散して第2の孔部43へと向かう。即ち、ガスシャワーヘッド3は、ガス供給管21及び22を流れる2種類の成膜ガスがシャワーヘッド本体30内で混じりあうことなしに独立してウエハWに向かうマトリックスタイプとなっている。   For this reason, the film forming gas sent from the gas supply pipe 21 is dispersed in the lateral direction in the space 31, travels toward the first hole portion 33 through the first gas flow path 32, and reaches the gas supply pipe 22. The film-forming gas sent from the air flows into the space 41 through the second gas flow path, and is dispersed in the lateral direction in the space 41 toward the second hole 43. That is, the gas shower head 3 is a matrix type in which two kinds of film forming gases flowing through the gas supply pipes 21 and 22 are directed to the wafer W independently without being mixed in the shower head main body 30.

次いでガス供給管21、22の上流側について説明する。ガス供給管21の上流側にはバルブV2を介して第1の成膜ガス(TiCl4)供給源21aが、またガス供給管22の上流側にはバルブV3を介して第2の成膜ガス(NH3)供給源22aが夫々接続されている。第1及び第2の成膜ガス供給源21a,22aには夫々の成膜成分である液体ソースが貯留されており、例えば成膜処理時にはキャリアガスを用いてこの液体ソースを気化させて蒸気とし、この蒸気をガス供給管21,22を介してガスシャワーヘッド3に送る構成とされている。   Next, the upstream side of the gas supply pipes 21 and 22 will be described. A first film-forming gas (TiCl 4) supply source 21 a is provided upstream of the gas supply pipe 21 via a valve V 2, and a second film-forming gas (TiCl 4) is provided upstream of the gas supply pipe 22 via a valve V 3. NH3) supply sources 22a are connected to each other. The first and second film forming gas supply sources 21a and 22a store liquid sources that are respective film forming components. For example, during the film forming process, the liquid source is vaporized using a carrier gas to form a vapor. The vapor is sent to the gas shower head 3 through the gas supply pipes 21 and 22.

次に上述実施の形態における作用について図4に示す工程図に沿って説明していく。先ずウエハWへの成膜処理に先立ち、ガスシャワーヘッド3の組み立てを行う。これは例えば洗浄などを行うために分解されたシャワーヘッド本体30をなす3つの金属板を接合するものであり、例えばチャンバ11の外部にて上段部3a、中段部3b、下段部3cを所定の向き及び位置で密着させ、上段部3aと中段部3bとの間はボルト34aにて、中段部3bと下段部3cとの間はボルト35bにて、各箇所を例えば30kg/cmのトルクで仮止めする(ステップS1)。そして仮止めされたガスシャワーヘッド3をチャンバ11内の所定位置に装着し、チャンバ11内に例えば図示しない窒素ガス供給手段から3600cc/分で窒素ガスを供給すると共に、圧力が1.33322×10Pa(1Torr)となるように排気流量の調節を行い、係る状態で第1のヒータ14及び第2のヒータ23を用いてチャンバ11内の加熱を開始する。するとシャワーヘッド本体30内の上段部3aの下面と中段部3bの上面との接合面P1及び中段部3bの下面と下段部3cの上面との接合面P2をなすニッケル同士が融解し、当該接合面P1,P2における微小な隙間を埋めながら、極表層で金属拡散接合が進行する。そして例えばボルト34a,34bを外しても接合面P1または接合面P2が分離しない程度の結合力を得られるまでそのまま加熱を継続することで、ガスシャワーヘッド3の組み立てが終了する。具体的には接合面P1,P2が所定の結合力を得ることが必要であり、例えば接合面P1の面積が50cm以上好ましくは100cm以上であるときには、500℃以上で12時間の加熱を行うことが好ましい。 Next, the operation of the above embodiment will be described with reference to the process chart shown in FIG. First, prior to the film forming process on the wafer W, the gas shower head 3 is assembled. For example, three metal plates constituting the shower head main body 30 disassembled to perform cleaning or the like are joined. For example, the upper stage portion 3a, the middle step portion 3b, and the lower step portion 3c are connected to a predetermined portion outside the chamber 11, for example. It is closely attached in the direction and position, and a bolt 34a is provided between the upper step portion 3a and the middle step portion 3b, and a bolt 35b is provided between the middle step portion 3b and the lower step portion 3c, for example, at a torque of 30 kg / cm 2 . Temporarily fix (step S1). The temporarily stopped gas shower head 3 is mounted at a predetermined position in the chamber 11, nitrogen gas is supplied into the chamber 11 from a nitrogen gas supply means (not shown), for example, at 3600 cc / min, and the pressure is 1.33322 × 10. The exhaust gas flow rate is adjusted to 2 Pa (1 Torr), and heating in the chamber 11 is started using the first heater 14 and the second heater 23 in this state. Then, nickel forming the bonding surface P1 between the lower surface of the upper step portion 3a and the upper surface of the middle step portion 3b in the shower head body 30 and the bonding surface P2 between the lower surface of the middle step portion 3b and the upper surface of the lower step portion 3c is melted. Metal diffusion bonding proceeds at the extreme surface layer while filling minute gaps on the surfaces P1 and P2. For example, the assembly of the gas shower head 3 is completed by continuing the heating as it is until the bonding surface P1 or the bonding surface P2 is separated even if the bolts 34a and 34b are removed. Specifically, it is necessary for the bonding surfaces P1 and P2 to obtain a predetermined bonding force. For example, when the area of the bonding surface P1 is 50 cm 2 or more, preferably 100 cm 2 or more, heating is performed at 500 ° C. or more for 12 hours. Preferably it is done.

続いてウエハWに対して成膜処理を行う。先ずゲートバルブ16を開くと図示しない搬送アームがチャンバ11内へと進入し、ウエハWは搬送アームからリフトピン17へと受け渡される。しかる後リフトピンを下降させてウエハWを載置台12の中央に載置し、ステップS3に示す成膜処理工程を開始する。この工程は先ず第1のヒータ14及び第2のヒータ23によりウエハWの表面温度が所定のプロセス温度例えば450℃〜700℃となるまで昇温させ、バルブV1を開いてチャンバ11内が所定の真空度に維持されるように排気口11aを介して真空ポンプ19から排気を行って、しかる後バルブV2及びV3を開いてガスシャワーヘッド3への成膜ガスの供給を開始する。このとき図示しない制御部ではTiCl4ガス及びNH3ガスが所定の流量でガスシャワーヘッド3に向かうように、例えば図示しない流量調節手段を介して各成膜ガスの流量調節を行う。   Subsequently, a film forming process is performed on the wafer W. First, when the gate valve 16 is opened, a transfer arm (not shown) enters the chamber 11, and the wafer W is transferred from the transfer arm to the lift pins 17. Thereafter, the lift pins are lowered to place the wafer W on the center of the mounting table 12, and the film forming process shown in step S3 is started. In this process, first, the surface temperature of the wafer W is raised by the first heater 14 and the second heater 23 until the surface temperature reaches a predetermined process temperature, for example, 450 ° C. to 700 ° C., the valve V1 is opened, and the inside of the chamber 11 is predetermined. Exhaust is performed from the vacuum pump 19 through the exhaust port 11a so that the degree of vacuum is maintained, and then the valves V2 and V3 are opened to start supplying the film forming gas to the gas shower head 3. At this time, a control unit (not shown) adjusts the flow rate of each film forming gas via, for example, a flow rate adjusting unit (not shown) so that the TiCl 4 gas and the NH 3 gas are directed to the gas shower head 3 at a predetermined flow rate.

ガスシャワーヘッド3内において、TiCl4ガス及びNH3ガスは、各流路内において下方側に向かいながら夫々混じり合うことなく分散していき、互い違いに配置される第1の孔部33及び第2の孔部43を介してウエハWの表面全体に均等に供給される。そして、成膜ガスはウエハWの表面近傍にて当該ウエハWから放射される熱エネルギーを受けて分解し、ウエハWの表面には熱エネルギーによる化学的気相反応によりTiNの薄膜が形成される。所定時間経過後バルブV2及びV3を閉じて成膜ガスの供給を停止し、更に第1のヒータ14による加熱を停止して、このチャンバ11内における所定の後工程を行った後、搬入時とは逆の順序でウエハWの搬出を行う。   In the gas shower head 3, the TiCl 4 gas and the NH 3 gas are dispersed without being mixed with each other while being directed downward in each flow path, and the first hole portion 33 and the second hole that are alternately arranged. It is evenly supplied to the entire surface of the wafer W via the portion 43. The film forming gas is decomposed by receiving thermal energy radiated from the wafer W in the vicinity of the surface of the wafer W, and a TiN thin film is formed on the surface of the wafer W by a chemical vapor reaction by the thermal energy. . After a predetermined time elapses, the valves V2 and V3 are closed to stop the supply of the film forming gas, the heating by the first heater 14 is stopped, and a predetermined post-process in the chamber 11 is performed. The wafers W are unloaded in the reverse order.

ガスシャワーヘッド3は例えば所定枚数の成膜処理を行うと、図示しないガス供給源から送られるクリーニングガス例えばClF3ガスをチャンバ11内に供給し、チャンバ11内に成膜された不要な膜の除去(クリーニング)を行う(ステップS4)。しかる後、内部の洗浄を行うためにガスシャワーヘッド3は再び解体(分解)される(ステップS5)。このガスシャワーヘッド3の解体工程は、基本的にステップS1及びS2にて説明した組み立て工程と逆の順序で行うものであるが、最初にガスシャワーヘッド3をチャンバ11から取り出してステップS1にて行った仮止めのときよりもボルト34a,34bを例えば1mm程度ゆるませる。そして再びガスシャワーヘッド3をチャンバ11内に戻して加熱を行うと、接合面P1及びP2における結合力が弱まり、シャワーヘッド本体30を構成する各金属板同士が脱離する。   When the gas shower head 3 performs a predetermined number of film formation processes, for example, a cleaning gas such as ClF3 gas sent from a gas supply source (not shown) is supplied into the chamber 11 to remove unnecessary films formed in the chamber 11. (Cleaning) is performed (step S4). Thereafter, the gas shower head 3 is disassembled (disassembled) again to clean the inside (step S5). The disassembling process of the gas shower head 3 is basically performed in the reverse order of the assembly process described in steps S1 and S2. First, the gas shower head 3 is removed from the chamber 11 and then the process is performed in step S1. The bolts 34a and 34b are loosened by about 1 mm, for example, compared to the temporary fixing performed. When the gas showerhead 3 is returned to the chamber 11 and heated again, the bonding force at the joint surfaces P1 and P2 is weakened, and the metal plates constituting the showerhead body 30 are detached.

このときの加熱条件はステップS2と概ね同じであるが、加熱温度については組み立て時よりも同じか僅かに高いことが好ましく、上述した例と同様のシャワーヘッド本体30について言えば、組み立て時の接合加熱温度が500℃であったものを分解時には500℃以上、好ましくは550℃以上とすることが好ましい。そして加熱を停止し、冷却後、上段部3a、中段部3b及び下段部3cが夫々分離して、チャンバー11から取り出してボルト34a及びボルト34bを夫々外すことで解体工程が完了する。   The heating conditions at this time are substantially the same as in step S2, but the heating temperature is preferably the same or slightly higher than that during assembly. For the shower head body 30 similar to the example described above, When the heating temperature is 500 ° C., it is preferably 500 ° C. or higher, preferably 550 ° C. or higher when decomposing. Then, heating is stopped, and after cooling, the upper step portion 3a, the middle step portion 3b, and the lower step portion 3c are separated from each other, removed from the chamber 11, and the bolt 34a and the bolt 34b are removed, thereby completing the disassembly process.

このように本実施の形態によれば、ガスシャワーヘッド3(シャワーヘッド本体30)を構成する複数の金属面間を加熱により化学的に結合させているため、例えばネジ止め等の前記金属板の機械的な結合では解消できなかった隙間、即ち当該接合面にある機械的研磨では解消し得ない微小な凹凸による隙間を解消することができる。従って各金属板間の接合面を横断して形成される成膜ガスの流路において、前記接合面でのガス漏れを完全に抑えることができるため、ガスシャワーヘッド3内で異なる種類の成膜ガス同士が混じり合うことを抑えられると共に、この混じり合いに伴う反応生成物の発生をも完全に抑えることができる。   As described above, according to the present embodiment, since the plurality of metal surfaces constituting the gas shower head 3 (shower head body 30) are chemically bonded by heating, for example, the metal plate such as screwing is used. A gap that cannot be eliminated by mechanical bonding, that is, a gap due to minute unevenness that cannot be eliminated by mechanical polishing on the joint surface can be eliminated. Accordingly, in the film forming gas flow path formed across the bonding surfaces between the metal plates, gas leakage at the bonding surfaces can be completely suppressed. Mixing of gases can be suppressed, and generation of reaction products associated with the mixing can be completely suppressed.

即ち、本実施の形態では上記混じり合いを完全に防ぐことで、各成膜ガスをガスシャワーヘッド3の孔部32(32a、32b)の配列に沿って、ウエハW表面上の全体に高い精度で均一に供給できるため、薄膜の面内均一性が向上する。更にガスシャワーヘッド3内における反応生成物の発生を抑えることで、パーティクルの原因が消滅するため、ウエハW上のパーティクル等の汚染のおそれが完全になくなり製品の歩留まりが向上するという効果もある。   That is, in the present embodiment, the above-mentioned mixing is completely prevented, so that each film-forming gas is highly accurate on the entire surface of the wafer W along the arrangement of the holes 32 (32a, 32b) of the gas shower head 3. In-plane uniformity of the thin film is improved. Further, by suppressing the generation of reaction products in the gas shower head 3, the cause of the particles disappears, so that there is an effect that the possibility of contamination of particles on the wafer W is completely eliminated and the yield of products is improved.

更に本実施の形態では、金属面の接合にろう材を用いることもないため、ガスシャワーヘッド3の組み立てと同様の手順で簡易に接合面を分離することができ、例えばガスシャワーヘッド3内に形成されている各ガス流路の洗浄を容易に行うことができる。   Furthermore, in this embodiment, since a brazing material is not used for joining the metal surfaces, the joining surfaces can be easily separated by the same procedure as the assembly of the gas shower head 3, for example, in the gas shower head 3. Each formed gas flow path can be easily cleaned.

なお、本実施の形態ではガスシャワーヘッド3の組み立て及び解体のいずれについても成膜処理を行うチャンバ11内で行うようにしたが、これらの作業は例えばチャンバ11とは別個に設けた加熱炉等にて行うようにしてもよい。またガスシャワーヘッド3を構成する金属は成膜ガスと反応することがなく、且つ加熱による金属拡散接合及び分離が可能な金属であれば、ニッケル以外のものであってもよく、例えばアルミニウム及びその合金、或いはニッケル、クロム系の合金等であっても同様の効果を得ることができる。更にまた、同様の効果を奏するものである限り、複数の金属板は全て同じ種類の金属である必要はない。具体的には例えばニッケル製の金属板とアルミニウム製の金属板との組み合わせ等が可能である。また、ガスシャワーヘッド3の組み立て及び解体における加熱に際し、使用するヒータは第1のヒータ14,第2のヒータ23のいずれか一方であってもよい。   In the present embodiment, both the assembly and disassembly of the gas shower head 3 are performed in the chamber 11 where the film forming process is performed. These operations are performed, for example, in a heating furnace provided separately from the chamber 11 or the like. You may make it perform in. The metal constituting the gas shower head 3 may be other than nickel as long as it does not react with the film forming gas and can be metal diffusion bonded and separated by heating. Similar effects can be obtained even with an alloy, or a nickel or chromium alloy. Furthermore, as long as the same effect is obtained, the plurality of metal plates need not be the same type of metal. Specifically, for example, a combination of a nickel metal plate and an aluminum metal plate is possible. In addition, when heating the gas shower head 3 during assembly and disassembly, the heater used may be either the first heater 14 or the second heater 23.

また、シャワーヘッド本体30の構成は上記実施の形態のものに限定されるものではなく、例えばTi膜或いはTiN膜等の成膜に用いられる図6に示すシャワーヘッド本体5によっても上述実施の形態と同様の効果を得ることが可能である。以下シャワーヘッド本体5の構成について簡単に説明する。シャワーヘッド本体5についても複数例えば三段の金属板からなり、これら金属板を上側から順に上段部5a,中段部5b及び下段部5cと呼ぶものとすると、夫々の接合面Q1,Q2は金属拡散接合にて密着されており、これに加えて下段部3cの下面側から上段部3aまで貫通するボルト50によっても固定が可能とされている。上段部5aと中段部5bとの間には、中段部5bの上面に凹部を形成してなる空間51が形成されており、中段部5bと下段部5cとの間には中段部5bの下面に凹部を形成してなる空間61が夫々形成されている。   Further, the configuration of the shower head main body 30 is not limited to that of the above-described embodiment, and the above-described embodiment is also provided by the shower head main body 5 shown in FIG. 6 used for forming a Ti film or a TiN film, for example. The same effect can be obtained. The configuration of the shower head body 5 will be briefly described below. The shower head main body 5 is also composed of a plurality of, for example, three-stage metal plates. If these metal plates are referred to as an upper step portion 5a, a middle step portion 5b, and a lower step portion 5c in this order from the upper side, the respective joint surfaces Q1 and Q2 are metal diffusion. In addition to this, it can be fixed by a bolt 50 penetrating from the lower surface side of the lower step portion 3c to the upper step portion 3a. Between the upper step portion 5a and the middle step portion 5b, a space 51 is formed by forming a recess on the upper surface of the middle step portion 5b, and the lower surface of the middle step portion 5b is formed between the middle step portion 5b and the lower step portion 5c. Spaces 61 each formed with a recess are formed in each.

中段部5bには、空間51から下段部5cへと連通する多数の第1のガス流路52と、空間51には連通せず空間61から上段部5aへと連通する第2のガス流路62とが夫々形成されている。下段部5cには第1のガス流路52と連通する多数の第1の孔部53と、空間61と連通する多数の第2の孔部63とが夫々形成されており、第1の孔部53と第2の孔部63とは例えば互い違いとなるように配列される。上段部5aについては、上面に第1の成膜ガスを供給するガス供給管54と第2の成膜ガスを供給するガス供給管64とが接続されている。また上段部5a内にはガス供給管54と空間51とを連通させる第3のガス流路55と、ガス供給管64と第2の流路62とを連通させる第4のガス流路65とが形成されている。従って第1の成膜ガスは、ガス供給管54→第3のガス流路55→空間51→第1のガス流路52→第1の孔部53という経路でウエハWへと供給される、第2の成膜ガスは、ガス供給管64→第4のガス流路65→第2のガス流路62→空間61→第2の孔部63という経路でウエハWへと供給され、各々はシャワーヘッド本体5内で混じり合うことがない。なお本実施の形態においても、シャワーヘッド本体5に用いられる金属は上述実施の形態と同様であるため、加熱による接合、離脱についても同様の条件下で行うことが可能である。   A number of first gas passages 52 that communicate from the space 51 to the lower step portion 5c and a second gas passage that does not communicate with the space 51 and communicates from the space 61 to the upper step portion 5a are provided in the middle portion 5b. 62 are formed. A large number of first holes 53 communicating with the first gas flow path 52 and a large number of second holes 63 communicating with the space 61 are formed in the lower stage portion 5c, respectively. For example, the portions 53 and the second hole portions 63 are arranged to be staggered. Regarding the upper stage portion 5a, a gas supply pipe 54 for supplying a first film-forming gas and a gas supply pipe 64 for supplying a second film-forming gas are connected to the upper surface. Further, in the upper stage portion 5a, a third gas flow path 55 for communicating the gas supply pipe 54 and the space 51, and a fourth gas flow path 65 for communicating the gas supply pipe 64 and the second flow path 62, Is formed. Therefore, the first film forming gas is supplied to the wafer W through the path of the gas supply pipe 54 → the third gas flow path 55 → the space 51 → the first gas flow path 52 → the first hole 53. The second film forming gas is supplied to the wafer W through a path of the gas supply pipe 64 → the fourth gas flow path 65 → the second gas flow path 62 → the space 61 → the second hole 63, and There is no mixing in the shower head body 5. In the present embodiment, the metal used for the shower head body 5 is the same as that in the above-described embodiment, so that joining and detachment by heating can be performed under the same conditions.

上述実施の形態における加熱条件とニッケル同士の結合力を確認するため、一組のニッケル製の試験片を用意して両者の結合力と加熱温度との関係を調べる試験を行った。この試験において用いた試験片同士の接触面積は25cmであり、加熱装置としては本実施の形態にて用いた成膜装置と同様のものを使用した。また当該成膜装置におけるチャンバ内の圧力は1.33322×10Pa(1Torr)に維持し、更に窒素ガスを3600cc/分の流量で供給すると共に加熱時間を12時間として試験を行った。 In order to confirm the heating conditions and the bonding strength between nickels in the above-described embodiment, a set of nickel test pieces was prepared, and a test was conducted to examine the relationship between the bonding strength between them and the heating temperature. The contact area between the test pieces used in this test was 25 cm 2 , and a heating apparatus similar to the film forming apparatus used in this embodiment was used. The pressure in the chamber of the film forming apparatus was maintained at 1.33322 × 10 2 Pa (1 Torr), nitrogen gas was supplied at a flow rate of 3600 cc / min, and the heating time was set to 12 hours.

図5はこの試験の結果を示す特性図であり、図示するようにニッケルの結合力は試験片の温度が500℃以上において急激に上昇することが分かる。なお図中一点鎖線で示す結合力αは、本実施の形態で用いたガスシャワーヘッド3において接合面P1の面積が50cm以上好ましくは100cm以上であるときに、接合面P1が分離しない結合力を示すものである。このように拡散接合された金属面同士は高い結合力で結ばれ、接合面の微小な隙間が解消されることが確認できた。 FIG. 5 is a characteristic diagram showing the results of this test. As shown in the figure, it can be seen that the bonding strength of nickel increases rapidly when the temperature of the test piece is 500 ° C. or higher. Note that the bonding force α indicated by the alternate long and short dash line in the figure indicates that the bonding surface P1 does not separate when the area of the bonding surface P1 is 50 cm 2 or more, preferably 100 cm 2 or more in the gas shower head 3 used in the present embodiment. Power. It was confirmed that the metal surfaces diffusion-bonded in this way are connected with a high bonding force, and a minute gap between the bonded surfaces is eliminated.

本発明に係る成膜装置の実施の形態を示す縦断面図である。1 is a longitudinal sectional view showing an embodiment of a film forming apparatus according to the present invention. 前記成膜装置に設けられるシャワーヘッド本体の構成を示す縦断面図である。It is a longitudinal cross-sectional view which shows the structure of the shower head main body provided in the said film-forming apparatus. 前記シャワーヘッド本体を分解して示した縦断面図である。It is the longitudinal cross-sectional view which decomposed | disassembled and showed the said shower head main body. 本実施の形態における作用を示す工程図である。It is process drawing which shows the effect | action in this Embodiment. 本実施の形態の効果を確認するために行った試験の結果を示す特性図である。It is a characteristic view which shows the result of the test done in order to confirm the effect of this Embodiment. 本発明に係る成膜装置の他の実施の形態におけるシャワーヘッド本体の構成を示す縦断面図である。It is a longitudinal cross-sectional view which shows the structure of the shower head main body in other embodiment of the film-forming apparatus which concerns on this invention. 従来の技術に係るガスシャワーヘッドの課題について示す概略説明図である。It is a schematic explanatory drawing shown about the subject of the gas shower head which concerns on a prior art. 従来の技術に係るガスシャワーヘッドの課題について示す概略説明図である。It is a schematic explanatory drawing shown about the subject of the gas shower head which concerns on a prior art.

符号の説明Explanation of symbols

W 半導体ウエハ
P1,P2 接合面
V1,V2,V3 バルブ
11 チャンバ
12 載置台
14 第1のヒータ
15 電力供給部
21,22 ガス供給管
23 第2のヒータ
3 ガスシャワーヘッド
3a 上段部
3b 中段部
3c 下段部
30 シャワーヘッド本体
30a シールド部
31,41 空間
32 第1のガス流路
33 第1の孔部
42 第2のガス流路
43 第2の孔部
W Semiconductor wafers P1, P2 Bonding surfaces V1, V2, V3 Valve 11 Chamber 12 Mounting table 14 First heater 15 Power supply unit 21, 22 Gas supply pipe 23 Second heater 3 Gas shower head 3a Upper stage part 3b Middle stage part 3c Lower stage portion 30 Shower head main body 30a Shield portions 31, 41 Space 32 First gas flow path 33 First hole 42 Second gas flow path 43 Second hole

Claims (9)

基板の表面と対向して設けられると共に前記基板と対向する面部に多数の孔部を備え、ガス供給路から送られるガスを、これら孔部を介して前記基板に同時に供給するガスシャワーヘッドにおいて、
複数の金属部材を上下に重ね合わせた状態で加熱することにより、各金属部材の接触面同士を金属拡散接合したシャワーヘッド本体と、
このシャワーヘッド本体内の前記接触面を横切るように貫通し、独立して形成される複数のガス流路と、を備えることを特徴とするガスシャワーヘッド。
In the gas shower head that is provided facing the surface of the substrate and has a large number of holes in the surface facing the substrate, and simultaneously supplies the gas sent from the gas supply path to the substrate through these holes,
By heating in a state where a plurality of metal members are stacked one above the other, a shower head body in which the contact surfaces of each metal member are metal diffusion bonded,
A gas shower head, comprising: a plurality of gas flow paths that are formed so as to penetrate the contact surface in the shower head body and are independently formed.
金属部材はニッケル、ニッケル合金、アルミニウム及びアルミニウム合金から選ばれるものであることを特徴とする請求項1記載のガスシャワーヘッド。 2. The gas shower head according to claim 1, wherein the metal member is selected from nickel, nickel alloy, aluminum and aluminum alloy. 基板を載置するための載置台が設けられた処理容器と、
前記処理容器内を排気する真空ポンプと、
前記処理容器に設けられる請求項1または2記載のガスシャワーヘッドと、を備えたことを特徴とする処理装置。
A processing vessel provided with a mounting table for mounting the substrate;
A vacuum pump for evacuating the processing vessel;
A processing apparatus comprising: the gas showerhead according to claim 1 or 2 provided in the processing container.
処理容器内の載置台に載置された基板に対して、当該基板に対向するガスシャワーヘッドからガスを供給し、処理を行う処理方法において、
前記ガスシャワーヘッドは、複数の金属部材を重ね合わせた状態で、これを加熱して各金属部材の接触面同士を金属拡散接合して構成され、このガスシャワーヘッドからガスを基板に供給し、当該基板の表面に処理を行うことを特徴とする処理方法。
In the processing method of supplying a gas from a gas shower head facing the substrate and processing the substrate placed on the mounting table in the processing container,
The gas shower head is formed by metal diffusion bonding between the contact surfaces of each metal member by heating the metal member in a state where a plurality of metal members are overlapped, and supplying gas from the gas shower head to the substrate, A processing method characterized by performing processing on the surface of the substrate.
金属部材はニッケル、ニッケル合金、アルミニウム及びアルミニウム合金から選ばれるものであることを特徴とする請求項4記載の処理方法。 5. The processing method according to claim 4, wherein the metal member is selected from nickel, a nickel alloy, aluminum, and an aluminum alloy. 処理容器内の載置台に載置された基板に対して、当該基板に対向するガスシャワーヘッドからガスを基板に供給し、当該基板の表面に処理を行う処理装置をメンテナンスする方法において、
ガスシャワーヘッドを構成する複数の金属部材を重ね合わせた状態で、これを加熱して各金属部材の接触面同士を金属拡散接合してガスシャワーヘッドを組み立てる工程を含むことを特徴とする処理装置のメンテナンス方法。
In a method for maintaining a processing apparatus for supplying a gas to a substrate from a gas shower head facing the substrate and processing the surface of the substrate with respect to the substrate placed on a mounting table in a processing container,
A processing apparatus comprising a step of assembling a gas shower head by metal diffusion bonding the contact surfaces of each metal member by heating the plurality of metal members constituting the gas shower head in a stacked state. Maintenance method.
ガスシャワーヘッドを組み立てる工程は、前記各金属部材の接触面同士を金属拡散接合する工程に加えて更に複数の金属部材を重ね合わせてネジ止めを行う工程を含むことを特徴とする請求項6記載の処理装置のメンテナンス方法。 7. The step of assembling a gas shower head includes a step of screwing together a plurality of metal members in addition to the step of metal diffusion bonding the contact surfaces of the metal members. Maintenance method of the processing apparatus. 成膜処理を行った後、金属拡散接合による結合力が弱まったときに、前記ネジ止めされている下段側の金属部材が自重で上段側の金属部材から離脱するように当該ネジ止めに用いられているネジを緩めた状態でガスシャワーヘッドを保持し、この状態でガスシャワーヘッドを加熱して、複数の金属部材を互いに分離する工程を含むことを特徴とする請求項7記載の処理装置のメンテナンス方法。 After the film forming process, when the bonding force by metal diffusion bonding is weakened, the screw is used for screwing so that the screwed lower metal member is detached from the upper metal member by its own weight. 8. The processing apparatus according to claim 7, further comprising a step of holding the gas shower head in a loosened state and heating the gas shower head in this state to separate a plurality of metal members from each other. Maintenance method. ガスシャワーヘッドの加熱は、ガスシャワーヘッドを処理容器に装着して、基板を加熱するための加熱部及びガスシャワーヘッドに設けられた加熱部の少なくとも一方を用いて行うことを特徴とする請求項6、7または8記載の処理装置のメンテナンス方法。 The gas shower head is heated using at least one of a heating unit for heating the substrate by mounting the gas shower head on the processing vessel and a heating unit provided in the gas shower head. The maintenance method of the processing apparatus of 6, 7 or 8.
JP2007268190A 2007-10-15 2007-10-15 Gas shower head, processing apparatus, processing method, and maintenance method of processing apparatus Expired - Fee Related JP4816616B2 (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010062382A (en) * 2008-09-04 2010-03-18 Sharp Corp Vapor phase deposition device and vapor phase deposition method
JP6146840B1 (en) * 2016-08-04 2017-06-14 日本新工芯技株式会社 Electrode plate
JP2019208016A (en) * 2018-05-29 2019-12-05 東京エレクトロン株式会社 Vacuum processing apparatus, shower head, and method of assembling vacuum processing apparatus
US11746419B2 (en) * 2018-10-25 2023-09-05 Aixtron Se Shield plate for a CVD reactor
WO2024029379A1 (en) * 2022-08-03 2024-02-08 日本発條株式会社 Head for injecting reactive gas for film formation and method for manufacturing same

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09256153A (en) * 1996-03-15 1997-09-30 Anelva Corp Substrate processor
JPH10226885A (en) * 1997-02-17 1998-08-25 Ebara Corp Gas injection head
JP2001064777A (en) * 1999-08-30 2001-03-13 Ebara Corp Gas jet head
JP2001323377A (en) * 2000-03-16 2001-11-22 Applied Materials Inc Upper and lower connected gas face plates for shower head of semiconductor wafer treatment system
WO2001099171A1 (en) * 2000-06-21 2001-12-27 Tokyo Electron Limited Gas supply device and treating device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09256153A (en) * 1996-03-15 1997-09-30 Anelva Corp Substrate processor
JPH10226885A (en) * 1997-02-17 1998-08-25 Ebara Corp Gas injection head
JP2001064777A (en) * 1999-08-30 2001-03-13 Ebara Corp Gas jet head
JP2001323377A (en) * 2000-03-16 2001-11-22 Applied Materials Inc Upper and lower connected gas face plates for shower head of semiconductor wafer treatment system
WO2001099171A1 (en) * 2000-06-21 2001-12-27 Tokyo Electron Limited Gas supply device and treating device

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010062382A (en) * 2008-09-04 2010-03-18 Sharp Corp Vapor phase deposition device and vapor phase deposition method
JP6146840B1 (en) * 2016-08-04 2017-06-14 日本新工芯技株式会社 Electrode plate
WO2018025781A1 (en) * 2016-08-04 2018-02-08 日本新工芯技株式会社 Electrode plate
JP2018022802A (en) * 2016-08-04 2018-02-08 日本新工芯技株式会社 Electrode plate
US10580621B2 (en) 2016-08-04 2020-03-03 Thinkon New Technology Japan Corporation Electrode Plate
JP2019208016A (en) * 2018-05-29 2019-12-05 東京エレクトロン株式会社 Vacuum processing apparatus, shower head, and method of assembling vacuum processing apparatus
JP7308637B2 (en) 2018-05-29 2023-07-14 東京エレクトロン株式会社 Vacuum processing apparatus, shower head, and method for assembling vacuum processing apparatus
US11746419B2 (en) * 2018-10-25 2023-09-05 Aixtron Se Shield plate for a CVD reactor
WO2024029379A1 (en) * 2022-08-03 2024-02-08 日本発條株式会社 Head for injecting reactive gas for film formation and method for manufacturing same

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