JP2007332108A5 - - Google Patents
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- Publication number
- JP2007332108A5 JP2007332108A5 JP2006168251A JP2006168251A JP2007332108A5 JP 2007332108 A5 JP2007332108 A5 JP 2007332108A5 JP 2006168251 A JP2006168251 A JP 2006168251A JP 2006168251 A JP2006168251 A JP 2006168251A JP 2007332108 A5 JP2007332108 A5 JP 2007332108A5
- Authority
- JP
- Japan
- Prior art keywords
- mol
- reaction
- methoxycyclohexanol
- trans
- reaction solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006243 chemical reaction Methods 0.000 description 26
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 18
- 239000000243 solution Substances 0.000 description 17
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- DCQQZLGQRIVCNH-RNFRBKRXSA-N (1r,2r)-2-methoxycyclohexan-1-ol Chemical compound CO[C@@H]1CCCC[C@H]1O DCQQZLGQRIVCNH-RNFRBKRXSA-N 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000011780 sodium chloride Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- JYJURPHZXCLFDX-UHFFFAOYSA-N 2-methoxycyclohexan-1-one Chemical compound COC1CCCCC1=O JYJURPHZXCLFDX-UHFFFAOYSA-N 0.000 description 4
- 239000005708 Sodium hypochlorite Substances 0.000 description 4
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- QRUYAODUCVMGQQ-UHFFFAOYSA-N 2-(2-oxocyclohexyl)acetic acid Chemical compound OC(=O)CC1CCCCC1=O QRUYAODUCVMGQQ-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- HFCSXCKLARAMIQ-UHFFFAOYSA-L disodium;sulfate;hydrate Chemical compound O.[Na+].[Na+].[O-]S([O-])(=O)=O HFCSXCKLARAMIQ-UHFFFAOYSA-L 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006168251A JP2007332108A (ja) | 2006-06-19 | 2006-06-19 | ２−メトキシシクロヘキサノンの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006168251A JP2007332108A (ja) | 2006-06-19 | 2006-06-19 | ２−メトキシシクロヘキサノンの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2007332108A JP2007332108A (ja) | 2007-12-27 |
| JP2007332108A5 true JP2007332108A5 (enExample) | 2009-07-02 |
Family
ID=38931910
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006168251A Pending JP2007332108A (ja) | 2006-06-19 | 2006-06-19 | ２−メトキシシクロヘキサノンの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2007332108A (enExample) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62155225A (ja) * | 1985-12-27 | 1987-07-10 | Nippon Shirika Kogyo Kk | 亜臭素酸またはその塩を用いる酸化方法 |
| JPH10204018A (ja) * | 1996-11-22 | 1998-08-04 | Toray Ind Inc | 光学活性脂環式ケトンの製造法 |
-
2006
- 2006-06-19 JP JP2006168251A patent/JP2007332108A/ja active Pending
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