JP2007124958A - Method for producing alcoholic beverage by using brown sugar - Google Patents
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- JP2007124958A JP2007124958A JP2005321165A JP2005321165A JP2007124958A JP 2007124958 A JP2007124958 A JP 2007124958A JP 2005321165 A JP2005321165 A JP 2005321165A JP 2005321165 A JP2005321165 A JP 2005321165A JP 2007124958 A JP2007124958 A JP 2007124958A
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本発明は、蒸米と米麹と水を原料とし、固形状又は粉状の黒砂糖を仕込み時又は醪に添加し発酵させ、琥珀色で黒砂糖の風味を有したアルコール7%〜18%のアルコール飲料の製造方法に関する。さらに、本アルコール飲料は、カルシウム、カリウム、マグネシウム等のミネラルが通常の清酒に比べて7〜24倍多く含んでいるアルコール飲料の製造方法に関する。 The present invention uses steamed rice, rice bran and water as raw materials, and solid or powdered brown sugar is added or fermented to the koji and fermented. The present invention relates to a method for producing an alcoholic beverage. Furthermore, this alcoholic beverage is related with the manufacturing method of the alcoholic beverage which contains minerals, such as calcium, potassium, and magnesium, 7-24 times more compared with normal sake.
さとうきびを原料としてそのまま煮詰めた黒砂糖の形態は、レンガ状のもの、砕いたもの、粉状のものがあり、一般の白砂糖に比べ、ミネラル(カルシウム、リン、鉄、ナトリウム、カリウムなど)や、ビタミンを多く含んだ天然の総合栄養剤ともいわれる。
黒砂糖を用いたアルコール飲料としては黒糖焼酎が知られており、酒税法上、鹿児島県の奄美群島(奄美大島、喜界島、徳之島、沖伊良部島、与論島)だけに認められた乙類焼酎である。
Brown sugar, which is boiled as raw material from sugarcane, comes in brick, crushed, and powdered forms. Compared to ordinary white sugar, minerals (calcium, phosphorus, iron, sodium, potassium, etc.) It is also said to be a natural nutritional supplement that contains a lot of vitamins.
Brown sugar shochu is known as an alcoholic beverage that uses brown sugar, and it is recognized by the liquor tax law only on the Amami Islands (Amami Oshima, Kikaijima, Tokunoshima, Okinoirabujima, Yoronjima) in Kagoshima Prefecture. It is.
近年の開発例として、「梅干しの製造方法」や「黒糖酢及びその製造方法」、「黒糖を原料とした食酢の製造方法」、「酢」に黒砂糖を利用してミネラルやビタミン等の栄養素を多く含有し、付加価値を高くした発明がある。また、アルコール飲料としては、麦芽及び廃糖蜜又は黒糖を含む原料から製造した発泡酒「発酵アルコール飲料」の開発例や、アルコール濃度30%の焼酎に黒砂糖を添加して作る「果実酒用アルコール飲料」の開発例等があるが、米と麹と黒砂糖を原料として、平衡復発酵により発酵させて製造したアルコール飲料の発明例はない。このような背景の基に研究を進め本発明が行われた。
「米と米麹と水を原料に発酵させてこしたもの」が清酒の定義であり、黒砂糖を用いた場合は清酒以外のアルコール飲料となる。黒砂糖を利用して発酵させる場合、仕込配合や発酵温度、さらに、黒砂糖の使用量や添加時期によって発酵の状態が異なり、やもすれば、発酵阻害や、できたアルコール飲料にオフフレーバーが出たり、黒糖の風味が強すぎて甘すぎたり、苦みが出る等の問題を解決することを目的とした。 “Sake made by fermenting rice, rice bran, and water as raw materials” is the definition of sake, and when brown sugar is used, it becomes an alcoholic beverage other than sake. When fermenting using brown sugar, the state of fermentation varies depending on the preparation blending and fermentation temperature, and the amount of brown sugar used and the time of addition. The purpose was to solve problems such as brewing, brown sugar flavor that was too strong and bitter.
本発明は、米、米麹、黒砂糖を原料として、平衡復発酵により発酵させたアルコール飲料の開発を目的とした。清酒の仕込みを基本として黒砂糖を用いて、仕込配合と発酵温度、黒砂糖の使用量と添加時期を検討し、ミネラル含有量が高く、黒砂糖由来の濃い琥珀色で黒砂糖の風味を有したアルコール飲料の製造方法の確立を目的とした。 The object of the present invention is to develop an alcoholic beverage fermented by equilibrium re-fermentation using rice, rice bran, and brown sugar as raw materials. Based on the preparation of sake, brown sugar is used, and the blending and fermentation temperature, the amount of brown sugar used and the timing of addition are examined, the mineral content is high, and dark brown color derived from brown sugar has a brown sugar flavor. The purpose was to establish a production method for alcoholic beverages.
重量%として、蒸米(白米として80%)と米麹(白米として20%)と紛状の黒砂糖を40%を基本仕込配合として、汲み水歩合(白米当たりの水の量)と黒砂糖添加時期を変えて仕込み、各成分値と官能試験から最適な酒質で上槽することにより前記の問題点を解決した。また、本発明の黒砂糖を用いてアルコール飲料を製造する場合は、(財)日本醸造協会の清酒用「きょうかい酵母」を使用すればよい。特に酒質とコスト面を考慮すると、精米歩合は70%から60%が望ましく、最高温度は12〜15℃以下の3段仕込みが適当である。 As a weight percent, steamed rice (80% as white rice), rice bran (20% as white rice) and 40% powdered brown sugar as basic ingredients, pumped water ratio (water per white rice) and brown sugar added The above-mentioned problems were solved by charging at different times and placing the tank with the optimal quality of liquor from each component value and sensory test. Moreover, when manufacturing an alcoholic beverage using the brown sugar of this invention, what is necessary is just to use "Kyokai yeast" for sake of Japan Brewing Association. Considering the quality of the liquor and the cost, the rice polishing rate is preferably 70% to 60%, and the maximum temperature is 3 to 15 ° C. or less.
すなわち、請求項1記載の本発明は、蒸米と米麹と水を原料とし、黒砂糖を仕込み時又は醪に添加し平衡復発酵させ、黒砂糖由来の琥珀色で黒砂糖の風味を有したアルコール7%〜18%のアルコール飲料の製造方法である。
請求項2記載の本発明は、前記黒砂糖が固形状又は紛状であることを特徴とする請求項1記載のアルコール飲料の製造方法である。
請求項3記載の本発明は、前記アルコール飲料のミネラルが清酒の7〜24倍であることを特徴とする請求項1又は2記載のアルコール飲料の製造方法である。
That is, the present invention according to claim 1 uses steamed rice, rice bran and water as raw materials, and brown sugar is added to the koji at the time of charging or equilibrated and fermented, and has a brown sugar flavor with a brown color derived from brown sugar. This is a method for producing an alcoholic beverage containing 7% to 18% alcohol.
The present invention according to claim 2 is the method for producing an alcoholic beverage according to claim 1, wherein the brown sugar is solid or powdery.
The present invention according to claim 3 is the method for producing an alcoholic beverage according to claim 1 or 2, characterized in that the mineral of the alcoholic beverage is 7 to 24 times that of sake.
本発明により、カルシウム、カリウム、マグネシウム等のミネラルが通常の清酒に比べて7〜24倍多く含んでいて、琥珀色で黒砂糖由来の風味を有したアルコール7%〜18%の香味のバランスが優れているアルコール飲料を提供することができる。 According to the present invention, minerals such as calcium, potassium and magnesium are contained 7 to 24 times more than ordinary sake, and the flavor balance of the alcohol 7% to 18% having the flavor derived from dark sugar and brown sugar is obtained. An excellent alcoholic beverage can be provided.
本発明に用いる黒砂糖は、奄美大島産のさとうきびを原料とした粉状のものであり、レンガ状のもの、砕いたものでも可能である。 The brown sugar used in the present invention is a powdery material made from sugarcane from Amami Oshima, and can be a brick or crushed one.
黒砂糖を用いるアルコール飲料の製造は、基本的に清酒に類似した方法に従って行えば良い。酵母は、秋田流・花酵母(AK−1)を用いて、麹エキス液体培地(Be6.5)で30℃で3日間培養した培養液を使用する。原料米の精米歩合は70%から60%が望ましく、3段仕込みで醪最高温度を12〜15℃の平衡復発酵させるのが適当である。
成分値と官能から香味のバランスの良い酒質になる15〜20日に上槽すると、黒砂糖由来の琥珀色と黒砂糖由来の風味を有したアルコール7%〜18%のアルコール飲料を製造することができる。上槽後のアルコール飲料についてミネラルを定量した結果、通常の清酒に比べて7〜24倍多くなった。
The production of an alcoholic beverage using brown sugar may basically be performed according to a method similar to sake. As the yeast, a culture solution obtained by culturing at 30 ° C. for 3 days in an agate extract liquid medium (Be6.5) using Akita-style / flower yeast (AK-1) is used. The milling rate of the raw rice is preferably 70% to 60%, and it is appropriate to equilibrate and re-ferment at a maximum temperature of 12 to 15 ° C. with three stages.
When the tank is placed on the 15th to 20th days, the alcoholic beverage has a good balance of flavor from the component values and sensuality, and produces an alcoholic beverage of 7% to 18% alcohol having a dark brown color derived from brown sugar and a flavor derived from brown sugar. be able to. As a result of quantifying minerals in the alcoholic beverage after the upper tank, it was 7 to 24 times more than ordinary sake.
以下に、本発明を実施例により詳しく説明するが、本発明はこれらに限定されるものではない。 Hereinafter, the present invention will be described in more detail with reference to examples, but the present invention is not limited thereto.
原料米は、精米歩合60%の白米を用いて総米1000gで、イ〜ヌの10種類の小仕込試験を行った。基本仕込配合を、白米換算にして蒸米800g、麹米200gと紛状黒砂糖400gとし、3段仕込とした。黒砂糖の添加時期は、イ、ロ、ハ、ニ、ホの5仕込は、醪7日目に200gと醪15日目に200g添加した。ヘ、ホ、チ、リ、ヌの5仕込は3段仕込みの留時に200gと醪10日目に200g添加した。また、汲水は、イとヘは1600ml、ロとトは1700ml、ハとチは1800ml、ニとリは1900ml、ホとヌは2000mlとした。酵母は、すべて秋田流・花酵母(AK−1)を用いて、酵母仕込で行った。
仕込配合を表1に示す。
The raw rice was a white rice with a polishing rate of 60% and a total rice of 1000 g. The basic charge composition was 800 g of steamed rice, 200 g of glutinous rice and 400 g of powdered brown sugar in terms of white rice. As for the timing of adding brown sugar, 200 g on the 7th day and 200g on the 15th day were added to the 5 preparations of (i), (b), (c), (c), (d), (d) and (d). 5 charges of f, ho, chi, li, and nu were added at the time of the third stage charge, and 200 g was added on the 10th day. In addition, the water to be pumped was 1600 ml for Lee and F, 1700 ml for Ro and To, 1800 ml for Ha and Chi, 1900 ml for Ni and Li, and 2000 ml for Ho and Nu. All yeasts were prepared using yeast using Akita-ryu and flower yeast (AK-1).
The charging composition is shown in Table 1.
発酵温度は、3段仕込みの1段目(添え仕込み)は12℃、次の日(踊り)は13℃、2段目(仲添え)は10℃、3段目(留添え)は8℃とし、1日1℃づつ品温を上げ、最高15℃で発酵させた。 Fermentation temperature is 12 ° C for the first stage (additional charge) of the third stage, 13 ° C for the next day (dance), 10 ° C for the second stage (medium), and 8 ° C for the third stage (end). The product temperature was raised by 1 ° C. per day and fermented at a maximum of 15 ° C.
5日毎に醪を遠心分離し、そのろ液について分析した。発酵能は、日本酒度とアルコール生成量を指標とした。日本酒度は、振動式密度計により、アルコール生成量はアルコメイトによりそれぞれ測定した。また、有機酸は、総酸度、つまり国税庁所定分析法注解に従い、遊離している有機酸の総量を中和滴定によって測定した。アミノ酸度は、国税庁所定分析法注解に従い、ホルモール法により測定した。香気成分は、国税庁所定分析法注解に従い、ガスクロマトグラフィーを用いてヘッドスペース法で測定した。また、カルシウム、カリウム、マグネシウム等のミネラルは、プラズマ発光分光分析器で測定した。官能的に香味のバランスの良い時期に醪を遠心分離し、製成酒とした。
上槽時の日本酒度とアルコール度数と酸度とアミノ酸度の分析値を表2に示す。上槽後の香気成分の測定値を表3に示す。
The sputum was centrifuged every 5 days and the filtrate was analyzed. Fermentation ability was based on the degree of sake and the amount of alcohol produced. The degree of sake was measured with a vibrating densimeter, and the amount of alcohol produced was measured with an alcoholate. The organic acid was measured by neutralization titration according to the total acidity, that is, the total amount of the free organic acid according to the National Tax Agency prescribed analytical method. The amino acid content was measured by the Formol method according to the analytical method prescribed by the National Tax Agency. The aroma component was measured by the headspace method using gas chromatography in accordance with the analytical method prescribed by the National Tax Agency. In addition, minerals such as calcium, potassium and magnesium were measured with a plasma emission spectrometer. The koji was centrifuged at a time when the balance of the flavor was sensuously good, and the sake was made.
Table 2 shows the analytical values of sake degree, alcohol degree, acidity and amino acid degree in the upper tank. Table 3 shows the measured values of the aroma components after the upper tank.
黒砂糖の添加時期が各成分に与える影響を見ると、醪の遅い時期(イ〜ホ:醪7日目と醪14日目)に添加したのに比べ、早い時期(ヘ〜ヌ:留添え時と醪10日目)に添加すると、アルコールが生成する傾向があり、酸度とアミノ酸度が高くなる傾向があった。
また、汲み水の量が各成分に与える影響を見た。つまり、イ〜ホ、またはヘ〜ヌを比べると、汲み水が多くなると日本酒度が+になる傾向があり、アルコール生成量と酸度とアミノ酸度が低くなる傾向があった。
Looking at the effect of brown sugar addition on each ingredient, it was earlier (Hu-nu: garnished) than when it was added later (i-ho: 醪 7th day and 醪 14th day) When added on the 10th day), there was a tendency for alcohol to be formed, and there was a tendency for the acidity and amino acidity to increase.
We also looked at the effect of the amount of pumped water on each component. In other words, when comparing i-ho or han-nu, when the amount of pumped water increases, the degree of sake tends to become +, and the amount of alcohol produced, the acidity, and the degree of amino acid tend to decrease.
黒砂糖の添加時期が香気成分に与える影響を見ると、醪の遅い時期(イ〜ホ:醪7日目と醪14日目)に添加したのに比べ、早い時期(ヘ〜ヌ:留添え時と醪10日目)に添加すると、EtOAc(酢酸エチル)とi―BuOH(イソブタノール)とi−AmOAc(酢酸イソアミル)とi−AmOH(イソアミルアルコール)がやや増加する傾向があった。
また、汲み水の量が香気成分に与える影響を見た。つまり、イ〜ホ、またはヘ〜ヌを比べると、汲み水が多くなるとEtOAc(酢酸エチル)とn−PuOH(ノルマルプロパノール)とi―BuOH(イソブタノール)とi−AmOAc(酢酸イソアミル)とi−AmOH(イソアミルアルコール)とEtOCap(カプロン酸エチル)の6成分すべてが減少する傾向があった。
Looking at the effect of brown sugar on the fragrance component, it was earlier (Hae-nu: garnished) than when it was added late in the cocoon (I-ho: 醪 7th day and 醪 14th day) When added on the 10th day), EtOAc (ethyl acetate), i-BuOH (isobutanol), i-AmOAc (isoamyl acetate) and i-AmOH (isoamyl alcohol) tended to increase slightly.
We also looked at the effect of the amount of pumped water on aroma components. In other words, comparing i-ho or ha-nu, when the amount of pumped water increases, EtOAc (ethyl acetate), n-PuOH (normal propanol), i-BuOH (isobutanol), i-AmOAc (isoamyl acetate) and i There was a tendency for all six components -AmOH (isoamyl alcohol) and EtOCap (ethyl caproate) to decrease.
市販清酒と本発明である黒砂糖を用いたアルコール飲料のミネラルの定量値を表4に示す。 Table 4 shows the quantitative values of minerals of alcoholic beverages using commercially available sake and brown sugar according to the present invention.
市販清酒に比べ、黒砂糖を用いたアルコール飲料のミネラル含有量は8成分のいずれも高含有であり、ナトリウムが約4倍、マグネシウムが約20倍、カリウムが約2倍、カルシュウムが約8倍、マンガンが約40倍、リンが約4倍、鉄が約150倍、亜鉛が約70倍となった。
ミネラル総量は、普通酒に比べて黒砂糖を用いたアルコール飲料は7倍〜27倍となった。
Compared to commercial sake, the mineral content of alcoholic beverages using brown sugar is high in any of the 8 components, sodium is about 4 times, magnesium is about 20 times, potassium is about 2 times, and calcium is about 8 times. Manganese was about 40 times, phosphorus was about 4 times, iron was about 150 times, and zinc was about 70 times.
The total amount of minerals was 7 to 27 times that of alcoholic beverages using brown sugar compared to ordinary sake.
製成酒をパネラー6名で官能試験を行った結果を表5に示す。 Table 5 shows the results of a sensory test of the sake made by 6 panelists.
醪の遅い時期(イ〜ホ:醪7日目と醪14日目)に添加したものは、黒砂糖の風味が強く濃醇タイプとなり、早い時期(ヘ〜ヌ:留添時と醪10日目)に添加したものは、酸に特徴がある軽快タイプの酒質となった。
アルコールと黒砂糖の甘味と酸のバランスからみると、汲み水が少ないものは黒糖の風味が強すぎて甘味が強く、黒砂糖に由来する苦味が感じられた。一方、汲み水が多いものは黒砂糖の風味が少なく、甘味に比べてアルコールが高く、アルコールに由来する苦味や渋みが感じられた。
最終的に、濃醇タイプとしてハまたは二、軽快タイプとしてチの仕込みが黒砂糖由来の琥珀色を有し、黒砂糖の風味とアルコールと酸のバランスが良く、官能的に最も良い評価を得ることができた。
What was added in the late season of rice cake (i-ho: 7th day and 14th day of rice cake) has a strong brown sugar flavor and becomes a dark blue type. What was added to the eye) became a light type of liquor characterized by acid.
From the balance between the sweetness and acidity of alcohol and brown sugar, those with less pumped water had a strong brown sugar flavor and a strong sweetness, and a bitter taste derived from brown sugar was felt. On the other hand, those with a lot of pumped water had less brown sugar flavor, higher alcohol than sweet, and felt bitterness and astringency derived from alcohol.
Eventually, the dark blue type has two or two, and the light type has a brown color derived from brown sugar, has a good balance of brown sugar flavor and alcohol and acid, and has the best sensory evaluation. I was able to.
上記実施例の黒砂糖添加量と上槽時期を変えることにより、アルコール7%〜18%のアルコール飲料を製造することも可能である。 By changing the amount of brown sugar added and the upper tank time in the above embodiment, it is also possible to produce an alcoholic beverage of 7% to 18% alcohol.
Claims (4)
The method for producing an alcoholic beverage according to claim 1 or 2, wherein the mineral content of the alcoholic beverage is 7 to 24 times that of sake.
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JP2012110323A (en) * | 2010-11-22 | 2012-06-14 | Jung Jun Pae | Method for producing black makgoli |
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