JP2007009353A - Method and apparatus for continuous dyeing and finishing - Google Patents
Method and apparatus for continuous dyeing and finishing Download PDFInfo
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本発明は織物など繊維構造物の連続染色加工法ならびに装置に係り、詳しくは上記連続加工において過熱水蒸気と、遠赤外線放射エネルギーを併用し、染色における乾燥効率の向上をはかり、短時間染着を可能ならしめる上記連続染色加工法ならびにその装置に関するものである。 The present invention relates to a continuous dyeing method and apparatus for textile structures such as textiles, and more specifically, in the above continuous processing, superheated steam and far-infrared radiation energy are used in combination to improve drying efficiency in dyeing and to perform dyeing in a short time. The present invention relates to the continuous dyeing processing method and apparatus which can be realized.
織物などの連続染色においては、近年、反応染料でも染液をパッドした後、乾燥し、次いでアルカリ発色剤,ソーダ灰,芒硝などからなるケミカル液で再びパッドし、スチーミングして染着する2工程法のパッド・ドライ・ケミカルパッド・スチーミング法が主流として実施されており、一部、コールド・パッド・バッチ法も行なわれているが、更に合理的な効率のよい短時間連続染色開発が進められ、過熱水蒸気や遠赤外線放射エネルギーを利用する方法が試みられている。 In continuous dyeing of textiles and the like, in recent years, a dyeing solution is padded with a reactive dye, and then dried, and then padded again with a chemical solution composed of an alkali color former, soda ash, sodium sulfate, etc., and then dyed by steaming. The process method pad, dry, chemical pad, and steaming are mainly used, and some cold pad batch methods are also used. Advances have been made in methods that utilize superheated steam or far-infrared radiation energy.
勿論、過熱水蒸気や、遠赤外線放射エネルギーを個々に利用することは従来より知られており、例えば特許文献1では染液をパッドした後、マイクロ波誘電加熱による蒸熱処理を施し、染料の発色,固定を行なうに際し、蒸熱処理部に連続搬送する途上、遠赤外線放射領域を通過熱水蒸気せしめることによって予備加熱を施し、昇温時間を短縮して加熱効率を向上させる方法が提案されており、また、例えば特許文献2では繊維製品に染液を付与した後、過熱水蒸気を用いて染料を固着することが提案されている。
しかし、上記従来の過熱水蒸気や遠赤外線の個々の利用は染料の固定,乾燥効率の向上に夫々、効果的であるとしても、各々単独に利用されているだけで短時間染着効果には未だ充分とは云えず、染液パッド後の予備乾燥のための設備も必要であった。 However, each use of the above conventional superheated steam and far infrared rays is effective for fixing dyes and improving drying efficiency, but it is still used for short-time dyeing effects only by using them individually. It was not sufficient, and equipment for preliminary drying after the dyeing pad was also required.
本発明は上述の如き実状に対処し、過熱水蒸気と遠赤外線放射の有効な併用を見出すことにより、一工程で染液パッド,染着を完了し、かつ染着進行に必要な水分の供給保持と、高染着に必要な温度保持を正確とし、均一な温度分布を得て安定した連続染色加工を達成することを目的とするものである。 The present invention addresses the above situation and finds an effective combination of superheated steam and far-infrared radiation to complete the dyeing pad and dyeing in one step and to supply and maintain moisture necessary for the dyeing process. In addition, the purpose is to accurately maintain the temperature necessary for high dyeing and to obtain a uniform temperature distribution and achieve stable continuous dyeing.
即ち、上記目的を達成する本発明は、その1つは連続染色加工法に係り、繊維構造物の連続染色加工において、染液をパッドした後、常圧における過熱水蒸気100%の空気のない状態で遠赤外線放射エネルギーと併用して高温スチーミング処理を行なうことを基本的特徴とする。 That is, the present invention that achieves the above object relates to a continuous dyeing process, and in the continuous dyeing process of a fiber structure, after the dyeing liquid is padded, 100% of superheated water vapor at normal pressure is free of air. The basic feature is that high-temperature steaming is performed in combination with far-infrared radiation energy.
請求項2〜4は上記基本的特徴における過熱水蒸気と遠赤外線放射エネルギーの併用の具体的な態様であり、請求項2は遠赤外線を放射する、アルミナ,チタニア及び酸化ニッケルよりなるセラミックを溶射したアルミニウムパイプをヒーターとしてスチーマー内に配備し、過熱水蒸気を上記ヒーター内へ通し、遠赤外線輻射エネルギーを放出しながらスチーマー内の温度上昇を図ると共に、ヒーターを出た過熱水蒸気をスチーマー内へ放出し、常圧における過熱水蒸気100%の空気のない状態で高温スチーミング処理を行なう態様、請求項3は、遠赤外線を放射するアルミナ,チタニア及び酸化ニッケルよりなるセラミックを溶射し、フッ素樹脂により表面を被覆した複数のシリンダーを閉鎖領域である高熱処理部内に配備し、過熱水蒸気を前記シリンダー内に通すと共に、高熱処理部に過熱水蒸気を放出して常圧における過熱水蒸気100%の空気のない状態で高温スチーミング処理を行なう態様である。 Claims 2 to 4 are specific embodiments of the combined use of superheated steam and far-infrared radiant energy in the above basic features, and claim 2 is a thermal spraying of a ceramic made of alumina, titania and nickel oxide that emits far-infrared rays. An aluminum pipe is installed in the steamer as a heater, superheated steam is passed into the heater, the temperature inside the steamer is increased while releasing far-infrared radiation energy, and the superheated steam exiting the heater is released into the steamer. An embodiment in which high-temperature steaming is performed in the absence of air of 100% superheated steam at normal pressure. Claim 3 is a method in which a ceramic made of alumina, titania and nickel oxide that emits far infrared rays is sprayed and the surface is coated with a fluororesin. Multiple cylinders in the high heat treatment section, which is a closed area, Together with passing into the cylinder, an aspect of performing high-temperature steaming process in the absence of superheated steam of 100% of the air in the release to normal pressure superheated steam at a high thermal processing.
また、請求項4は染液をパッドした後、上記請求項2記載のヒーターを配備したスチーマーと、上記請求項3記載の複数のシリンダーを配備した高熱処理部とを順次、配置して通過させ、夫々遠赤外線放射エネルギーと過熱水蒸気100%の併用で空気のない状態で高温スチーミング処理を行なう態様を特徴とする。 According to a fourth aspect of the present invention, after the dyeing liquid is padded, the steamer provided with the heater according to the second aspect and the high heat treatment portion provided with the plurality of cylinders according to the third aspect are sequentially arranged and passed. Each is characterized in that the high-temperature steaming treatment is performed in the absence of air with the combination of far-infrared radiation energy and superheated steam 100%.
請求項5は上記連続染色加工におけるヒーター又はシリンダー内に通す過熱水蒸気の好ましい温度であり、400〜500℃であることを特徴とする。なお、請求項6は上記連続染色加工が施される繊維構造物の具体例であり、糸,織物,編物形態の何れに対しても連続染色加工が施される。 A fifth aspect of the present invention is a preferable temperature of the superheated steam that is passed through the heater or cylinder in the continuous dyeing process, and is 400 to 500 ° C. Note that claim 6 is a specific example of the fiber structure subjected to the continuous dyeing process, and the continuous dyeing process is applied to any of yarn, woven fabric and knitted fabric.
請求項7は、上記の連続染色加工が施される装置の構成であり、染液をパッドするパッダーと、該パッダーで染液が付与された繊維構造物に対し高温スチーミング処理を行なう第1又は/及び第2の高温スチーミング部からなり、第1のスチーミング部は遠赤外線を放射する、アルミナ,チタニア及び酸化ニッケルよりなるセラミックを溶射したアルミニウムパイプをヒーターとしてスチーマー内に配備し、ヒーター内に400〜500℃の過熱水蒸気を通すと共にヒーターを出た過熱水蒸気をスチーマー内へ放出し、スチーマー内を過熱水蒸気100%の空気のない状態とするスチーマーであり、第2のスチーミング部は遠赤外線を放射するアルミナ,チタニア及び酸化ニッケルよりなるセラミックを溶射し、フッ素樹脂により表面を被覆したシリンダーを処理部内部に配備し、シリンダー内に400〜500℃の過熱水蒸気を通すと共に処理部内を過熱水蒸気100%の空気のない状態とする高熱処理部であることを特徴とする。 A seventh aspect of the present invention is a configuration of an apparatus that performs the above-described continuous dyeing process, and includes a padder for padding a dye solution and a first high-temperature steaming process for a fiber structure to which the dye solution is applied by the padder. Or / and comprising a second high-temperature steaming section, the first steaming section radiating far-infrared rays, and an aluminum pipe sprayed with a ceramic made of alumina, titania and nickel oxide is disposed in the steamer as a heater, and the heater It is a steamer that passes superheated steam at 400 to 500 ° C. inside and releases superheated steam that has exited the heater into the steamer, and makes the steamer 100% superheated steam free of air, and the second steaming part is A ceramic made of alumina, titania and nickel oxide that emits far infrared rays is sprayed and the surface is covered with a fluororesin. Cylinders deployed on internal processing unit, characterized in that it is a high thermal processor to the absence of treatment portion of superheated steam of 100% air with passing superheated steam 400 to 500 ° C. in the cylinder.
上記本発明はアルミナ,チタニア及び酸化ニッケルからなるセラミックを溶射したアルミニウムパイプをヒーターとしてスチーマー内に、あるいはシリンダーとして高熱処理部内に配備して、これに400〜500℃の過熱水蒸気を通し、より高い遠赤外線放射エネルギーを急速染着に利用し、更に過熱水蒸気をスチーマー内に放出し、空気を含まない100%過熱水蒸気による染着ドライを進行させる。 In the present invention, an aluminum pipe sprayed with a ceramic composed of alumina, titania and nickel oxide is provided in a steamer as a heater or in a high heat treatment part as a cylinder, and superheated steam at 400 to 500 ° C. is passed through it, and the higher Far-infrared radiant energy is used for rapid dyeing, and superheated steam is discharged into the steamer, and dyeing and drying with 100% superheated steam that does not contain air proceeds.
この場合、例えば染布に60〜65%の絞り率の染液を付けてスチーマー内に入ると、130〜140℃の蒸気を瞬時に400〜500℃に昇温させる能力をもつ過熱水蒸気発生器で発生した過熱水蒸気により1秒内外で100℃に達し、同時に布に凝結水が生じ、布が水分を持っている間は布温度は100℃を保っていることで染着に必要な水分の供給保持と、高染着に必要な温度保持が正確になされることになる。 In this case, for example, a superheated steam generator capable of instantaneously raising the steam at 130 to 140 ° C. to 400 to 500 ° C. when a dyeing solution having a drawing ratio of 60 to 65% is attached to the dyed cloth and enters the steamer. The superheated steam generated in step 1 reaches 100 ° C within 1 second, and at the same time, condensed water is generated in the fabric. While the fabric has moisture, the fabric temperature is kept at 100 ° C so that the moisture necessary for dyeing can be maintained. The supply and the temperature required for high dyeing can be accurately maintained.
上記本発明によれば遠赤外線を放射するセラミックを溶射したアルミニウムパイプをヒーターとして高熱処理部内に配備し、あるいは前記セラミックスを溶射したシリンダーを高熱処理部内に配備して400〜500℃の高温過熱水蒸気を通し、しかもスチーマー又は高熱処理部に該過熱水蒸気を放出して空気を含まない100%過熱水蒸気による雰囲気内でスチーミング処理を行なうため、スチーマーあるいは処理部内の温度上昇と維持が図られ、従来の2工程法における染着前の工程の染色乾燥部門を不要として染液パッド,高温スチーミングの1工程で染着完了が得られ、染色加工時間の短縮化と共に省エネルギーで高効率が達成され、現下の小ロット,多様化,短サイクルの連続染色に顕著な効果が期待される。 According to the present invention, a high-temperature superheated steam at 400 to 500 ° C. is provided by using an aluminum pipe sprayed with ceramics radiating far-infrared rays as a heater in a high heat treatment section, or a cylinder sprayed with the ceramic in a high heat treatment section. In addition, the steaming process is performed in an atmosphere of 100% superheated steam that does not contain air by discharging the superheated steam to the steamer or the high heat treatment part, so that the temperature rise and maintenance in the steamer or the treatment part can be achieved. The dyeing and drying department of the process before dyeing in the two-step method is unnecessary, and dyeing is completed in one step of the dyeing pad and high-temperature steaming. The dyeing process time is shortened and energy saving and high efficiency are achieved. Significant effects are expected for current small lots, diversification, and short cycle continuous dyeing.
以下、更に添付図面にもとづいて本発明の具体的実施態様を説明する。 Hereinafter, specific embodiments of the present invention will be described with reference to the accompanying drawings.
図1は本発明に係る連続染色加工を実施する装置の1例を示す概要図であり、供給部1より引き出された綿織物などの繊維構造物Fがガイドロールを介して送出され、パッダーPにおいて染液槽2内に含浸すると共に絞りロール3で絞って染液をパッドした後、スチーマーA及び高温熱処理部Bに順次送り、図示していないが、併設されている130〜140℃の蒸気を瞬時に400〜500℃に昇温させる能力のある過熱水蒸気発生器を用いてこの高温過熱水蒸気を前記スチーマーA及び高熱処理部Bへ通しこれらスチーマーA及び高熱処理部Bにおいて遠赤外線輻射エネルギーを放射しながら室内の温度上昇と維持を図ると共に、該過熱水蒸気をスチーマー及び処理部内に放出して夫々、常圧における過熱水蒸気100%の空気のない状態で高温スチーミングを行ない、順次後方へ送出して本願発明の一連の連続染色加工が行なわれる。 FIG. 1 is a schematic view showing an example of an apparatus for performing continuous dyeing processing according to the present invention. A fiber structure F such as cotton fabric drawn out from a supply unit 1 is sent out through a guide roll, After impregnating the dye liquor 2 and squeezing the dye liquor with the squeeze roll 3, the dye liquor is sequentially sent to the steamer A and the high temperature heat treatment part B. Using a superheated steam generator capable of instantaneously raising the temperature to 400 to 500 ° C., this high temperature superheated steam is passed through the steamer A and the high heat treatment part B, and far infrared radiation energy is radiated in the steamer A and the high heat treatment part B. While maintaining and raising the temperature in the room, the superheated steam is discharged into the steamer and the processing section, and 100% of the superheated steam at normal pressure is free from air. Then, high-temperature steaming is performed, and the products are sequentially sent backward to perform a series of continuous dyeing processes of the present invention.
前記スチーマーAは図示のように5〜10ミクロンの波長の遠赤外線を放出するアルミナ,チタニア,酸化ニッケルよりなるセラミックを溶射したアルミニウムパイプをヒーター4として、該ヒーターをスチーマー内に多数併設配置して構成されており、織物等を上下に蛇行させてヒーターを通過させ、遠赤外線輻射エネルギーを放射しながらスチーマー内の温度上昇と維持を図ると共にヒーターを出た高温過熱水蒸気をスチーマー内へ放出し、スチーマー内で常圧における過熱水蒸気100%の空気のない状態での高温スチーミング処理を行なうようになっている。
As shown in the figure, the steamer A has an aluminum pipe sprayed with ceramic made of alumina, titania and nickel oxide that emits far-infrared rays having a wavelength of 5 to 10 microns as a
一方、高熱処理部Bは前記スチーマーと同じく赤外線を放射するアルミナ,チタニア,酸化ニッケルよりなるセラミックを溶射し、その表面をフッ素樹脂により被覆した遠赤外線放射力をもつシリンダー5を閉鎖された処理部内に併設配置することによって同様にシリンダー5内に過熱水蒸気を送り、遠赤外線輻射エネルギーを放射しながら高温処理室内の温度を上昇と維持を図り、更に同処理部B内へ過熱水蒸気を放出して常圧における過熱水蒸気100%の空気のない状態で高温スチーミング乾燥を通じて加工を達成させる。 On the other hand, the high heat treatment part B, like the steamer, sprays ceramics made of alumina, titania and nickel oxide that emits infrared rays, and the cylinder 5 having far infrared radiation force whose surface is coated with fluororesin is closed. In the same manner, superheated steam is sent into the cylinder 5 to raise and maintain the temperature in the high-temperature processing chamber while emitting far-infrared radiation energy, and further, superheated steam is discharged into the processing section B. Processing is achieved through high temperature steam drying in the absence of 100% superheated steam air at normal pressure.
なお、図示例においては、アルミニウムパイプのヒーターによるスチーマーAと、シリンダーによる高熱処理部Bの両室を順次配置して繊維構造物Fに連続染色加工を施しているが、必らずしも両者を併用することなく、何れか一方のみで常圧における空気のない過熱水蒸気100%の高温スチーミングを遠赤外線放射エネルギーと併用して行なってもよく、これによってスチーミング乾燥,ベーキング等の機能を行なうケミラクターとして加工を一工程で達成することが出来る。 In the illustrated example, both the steamer A by the heater of the aluminum pipe and the high heat treatment part B by the cylinder are arranged in order, and the fiber structure F is subjected to continuous dyeing processing. In combination with far-infrared radiation energy, high-temperature steaming of 100% superheated steam without air at normal pressure can be performed in combination with far-infrared radiant energy. Processing can be accomplished in one step as a chemiractor to perform.
かくして前述のように織物等の繊維構造物に60〜65%の絞り率の染液を付けて上記スチーマーや高温熱処理部に入ると、1秒内外に100℃に達し、同時に織物等に凝結水が生じ、織物が水分を持っている間は織物温度は100℃を保っていることで、このことが染着進行に必要な水分の供給保持と、高染着に必要な温度保持を正確になし、短時間染着完了の効果を発揮する。 Thus, as described above, when a dyeing solution having a drawing ratio of 60 to 65% is applied to a textile structure such as a woven fabric and enters the steamer or high-temperature heat treatment section, the temperature reaches 100 ° C. in one second or outside, and at the same time, condensed water is applied to the woven fabric or the like. While the fabric has moisture, the fabric temperature is kept at 100 ° C., which accurately maintains the moisture supply necessary for the dyeing process and the temperature required for the high dyeing. None, the effect of completion of short-time dyeing is demonstrated.
実施例1
綿織物に対し下記配合例による染液を付与し、染液パッドを行なった。
Example 1
The dyeing liquid by the following compounding example was provided with respect to the cotton fabric, and the dyeing liquid pad was performed.
染液配合例
反応染料 X g/L
ソーダ灰 20 g/L
還元防止剤 3 g/L
染液パッド後、直ちに遠赤外線放射力をもつアルミニウムパイプをヒーターとして配備したスチーマーAと、続いて遠赤外線放射力をもつシリンダーで構成した高熱処理部へ通し常圧における空気のない過熱水蒸気100%の180℃スチーミングを遠赤外線放射エネルギーと併用して行なったところ、30秒で染着が完了した。
Dyeing liquid formulation example Reactive dye X g / L
Soda ash 20 g / L
Anti-reducing agent 3 g / L
Immediately after the dyeing pad, 100% of superheated steam without air at normal pressure is passed through a high heat treatment section consisting of an aluminum pipe with far-infrared radiant power as a heater, followed by a cylinder with far-infrared radiant power. When 180 ° C. steaming was performed in combination with far-infrared radiation energy, dyeing was completed in 30 seconds.
同様にして数回、繰り返して実施したところ、最大限でも60秒で染着完了が確認された。
実施例2
次に上記実施例1に準じ一工程法でバット染料,硫化染料等についても必要還元剤,薬剤等を加えた染液を配合し、これら各染液についてもパッドし、過熱水蒸気100%の180℃スチーミングを遠赤外線放射エネルギーと併用して行なったところ、何れも20秒から30秒で染着完了が確認された。
When repeated several times in the same manner, the completion of dyeing was confirmed in 60 seconds at the maximum.
Example 2
Next, in accordance with the above-mentioned Example 1, a dye solution containing a necessary reducing agent, a chemical agent, etc. is blended with a vat dye, sulfur dye, etc. in a one-step method, and each dye solution is also padded and 180% of superheated steam 100%. When steaming at 0 ° C. was used in combination with far-infrared radiation energy, it was confirmed that dyeing was completed in 20 to 30 seconds.
以上の実施例に対し従来の2工程法により先ず第1工程で、染料 Xg/L,マイグレーション防止剤10g/L,還元防止剤10g/Lよりなる染液をパッドし、プレ乾燥を行なった後、第2工程としてアルカリ発色剤40g/L,ソーダ灰20g/L,芒硝200g/Lよりなるケミカル液をパッドし、発色スチーマーで染着を行なったところ、プレ乾燥完了に100℃で2分要し、スチーマー処理による染着までに100℃で1分間要し、合計で染着に3分を要した。 In the first step according to the conventional two-step method, the dyeing solution consisting of the dye Xg / L, the migration inhibitor 10 g / L, and the reduction inhibitor 10 g / L is padded and pre-dried. In the second step, a chemical solution consisting of 40 g / L alkali color former, 20 g / L soda ash, and 200 g / L sodium sulfate was padded and dyed with a color developing steamer. However, it took 1 minute at 100 ° C. until dyeing by the steamer treatment, and 3 minutes in total.
以上の実施例,比較例の対比より、本発明はマイグレーション防止剤10g/L,アルカリ発色剤40g/L,芒硝200g/Lが不要であり、省資源効果を有するのみならず、1工程簡略化することにより染着完了までの時間も短縮され、現在求められる小ロッド,多様化に充分対応できることが実証された。 From the comparison of the above examples and comparative examples, the present invention does not require a migration inhibitor 10 g / L, an alkali color former 40 g / L, and a sodium sulfate 200 g / L, which not only has a resource saving effect but also simplifies one process. By doing so, the time to complete the dyeing was shortened, and it was proved that it can sufficiently cope with the small rods and diversification currently required.
A:スチーマー
B:高熱処理部
F:繊維構造物
P:パッダー
1:繊維構造物供給部
2:染液槽
3:絞りロール
4:ヒーター(アルミニウムパイプ)
5:シリンダー
A: Steamer B: High heat treatment part F: Fiber structure P: Padder 1: Fiber structure supply part 2: Dyeing tank 3: Drawing roll 4: Heater (aluminum pipe)
5: Cylinder
Claims (7)
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JP2007009353A true JP2007009353A (en) | 2007-01-18 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100885551B1 (en) * | 2008-02-28 | 2009-02-26 | 주식회사 나노텍스 | Method for dyeing nanofiber cloth |
WO2010120129A2 (en) * | 2009-04-16 | 2010-10-21 | 한국생산기술연구원 | Method for dyeing nano-fabrics |
KR101083463B1 (en) | 2010-11-02 | 2011-11-16 | 김병길 | Dyeing system for radiating far infrared ray |
CN104911848A (en) * | 2015-05-19 | 2015-09-16 | 江苏工程职业技术学院 | Viscose loose fiber continuous dyeing process and adopted viscose loose fiber continuous dyeing machine |
-
2005
- 2005-06-29 JP JP2005189322A patent/JP2007009353A/en active Pending
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100885551B1 (en) * | 2008-02-28 | 2009-02-26 | 주식회사 나노텍스 | Method for dyeing nanofiber cloth |
WO2010120129A2 (en) * | 2009-04-16 | 2010-10-21 | 한국생산기술연구원 | Method for dyeing nano-fabrics |
WO2010120129A3 (en) * | 2009-04-16 | 2011-03-31 | 한국생산기술연구원 | Method for dyeing nano-fabrics |
KR101033471B1 (en) | 2009-04-16 | 2011-05-09 | 주식회사 나노시스 | Dyeing methods for nano-fabrics |
KR101083463B1 (en) | 2010-11-02 | 2011-11-16 | 김병길 | Dyeing system for radiating far infrared ray |
CN104911848A (en) * | 2015-05-19 | 2015-09-16 | 江苏工程职业技术学院 | Viscose loose fiber continuous dyeing process and adopted viscose loose fiber continuous dyeing machine |
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