JP2006161133A - Method for producing blank for wear resistance excellent in cold-forging - Google Patents

Method for producing blank for wear resistance excellent in cold-forging Download PDF

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JP2006161133A
JP2006161133A JP2004357510A JP2004357510A JP2006161133A JP 2006161133 A JP2006161133 A JP 2006161133A JP 2004357510 A JP2004357510 A JP 2004357510A JP 2004357510 A JP2004357510 A JP 2004357510A JP 2006161133 A JP2006161133 A JP 2006161133A
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wear resistance
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annealing
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Hiroaki Onouchi
浩明 尾内
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Sanyo Special Steel Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for producing a blank for wear resistance excellent in a cold-forging which is suitable to sliding parts for internal combustion engine requiring the high wear resistance, such as a valve lifter (tappet), a pump lifter or a plunger of a diesel fuel injecting device, etc. <P>SOLUTION: The method for producing the blank for wear resistance excellent in the cold-forging comprises the steps of: cold-rolling a high carbon alloy tool steel and performing continuous annealing thereto; and drawing the steel at 10-20% reduction of area and successively performing one or two times of annealing at 850-900°C to the steel. In the method, the steel blank contains 1.40-1.60% C, 11-13% Cr, 0.5-1.5% Mo+1/2W, 0.2-1.0% V+1/2Nb and the balance Fe with inevitable impurities. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

本発明は、エンジンのバルブリフター(タペット)やディーゼル燃料噴射装置のポンプリフターやプランジャーなどの、高耐摩耗性を要求される内燃機関用の摺動部品に適した冷間鍛造性に優れた耐摩耗用素材の製造方法に関するものである。   The present invention has excellent cold forgeability suitable for sliding parts for internal combustion engines that require high wear resistance, such as engine valve lifters (tuppets) and diesel fuel injection pump lifters and plungers. The present invention relates to a method for manufacturing a wear-resistant material.

従来、耐摩耗性が要求される部品に、高C、高V系の冷間用工具鋼が使用される場合が多くある。これらの部品の製造には、切削加工が多く用いられていたが、しかし、近年の塑性加工技術の進歩とコスト低減要求に伴い、部品の製造方法も切削加工から冷間鍛造へと移行しつつある。これらの鋼種は硬度が高く、硬質な炭化物が多数含んでいるため、冷間での加工性が劣り製造工程中に割れ等の不良が発生し問題となっている。これらを改善する方法として、例えば特開平8−193246号公報(特許文献1)に開示されているように、CとCrの含有量の範囲制限により一次炭化物を起点とする割れは回避され、二次炭化物の性状を制御することが冷間鍛造性を向上させるとしている。また、特開2000−63944号公報(特許文献2)に開示されているように、冷間、温間塑性加工を行なった後に、最適な熱処理により炭化物の割れを修復し、機械的特性を改善するものが提案されている。   Conventionally, high-C, high-V cold tool steel is often used for parts that require wear resistance. Cutting is often used in the manufacture of these parts. However, with the recent progress in plastic processing technology and cost reduction requirements, the part manufacturing method is also shifting from cutting to cold forging. is there. Since these steel types have high hardness and contain a large number of hard carbides, they are inferior in workability in the cold, causing defects such as cracks during the manufacturing process. As a method for improving these, for example, as disclosed in JP-A-8-193246 (Patent Document 1), cracks originating from primary carbides are avoided by limiting the range of C and Cr contents. Controlling the properties of the next carbide improves the cold forgeability. Also, as disclosed in Japanese Patent Application Laid-Open No. 2000-63944 (Patent Document 2), after performing cold and warm plastic working, the cracking of carbide is repaired by an optimum heat treatment, and mechanical properties are improved. What to do has been proposed.

特開平8−193246号公報JP-A-8-193246 特開2000−63944号公報JP 2000-63944 A

しかしながら、上述した特許文献1は、CとCrの含有量が最適範囲でないため一次炭化物が粗大であり、かつ冷間鍛造時の主な割れ起点となる一次炭化物凝集部の凝集サイズと割れ発生率の相関について検証されておらず、割れ対策が不十分である。また、特許文献2は、引抜加工時のダイス欠け、焼付き等のトラブル防止の対策がなく、また、引抜き焼鈍を行う際の硬度の低下についての対策については取り込まれていないという問題がある。 However, in Patent Document 1 described above, the primary carbide is coarse because the C and Cr contents are not in the optimum range, and the aggregate size and crack generation rate of the primary carbide aggregate part that is the main crack starting point during cold forging. No correlation has been verified and crack countermeasures are insufficient. Further, Patent Document 2 has a problem that there is no measure for preventing troubles such as die chipping and seizure at the time of drawing, and there is a problem that measures for reducing the hardness at the time of drawing annealing are not incorporated.

一方、近年の内燃機関に対する要求として高出力化と製造コスト低減が掲げられ、前者については、高回転を目的とした動弁系部品の軽量化および耐摩耗性の向上など、後者については、従来の切削加工から冷間鍛造への移行などが検討されている。現在、耐摩耗性を要求される摺動部品にはJIS SKD11等の材料を用いて、一体製部品にすることで軽量化を図っているが、冷間鍛造性が悪いために、複数の加工プロセスを必要として高コストとなるだけでなく冷間鍛造後の一次炭化物の凝集部での割れ残存により、摺動部品としての性能のバラツキが懸念されているのが現状である。   On the other hand, demands for internal combustion engines in recent years include higher output and lower manufacturing costs. For the former, the latter has conventionally been reduced in weight and improved wear resistance for the purpose of high rotation. The transition from cutting to cold forging has been studied. Currently, JIS SKD11 and other materials are used for sliding parts that require wear resistance, and the weight is reduced by making them into one-piece parts. The present situation is that there is a concern about variation in performance as a sliding part due to cracks remaining in the agglomerated portion of the primary carbide after cold forging as well as high cost due to the process.

さらに、近年の環境問題への高まりを受け、燃料向上が必達の課題とされる中で、内燃機関におけるフリクションロスの低減への取組が盛んになってきている。現在、摺動部品への表面処理適用による摩擦抵抗低減などが取組まれているが、高コストであるだけでなく表面処理膜の剥離など信頼性が不十分なため、量産部品への適用に向けて、さらなる検討が進めれているのが実状である。   Furthermore, in response to the recent increase in environmental problems, improvement of fuel is an indispensable issue, and efforts to reduce friction loss in internal combustion engines have become active. Currently, efforts are being made to reduce frictional resistance by applying surface treatment to sliding parts, but it is not only costly but also has insufficient reliability such as peeling of the surface treatment film. The actual situation is that further studies are underway.

上述したような問題を解消するために、本発明は、内燃機関用の摺動部品として要求される、冷間鍛造性、耐摩耗性、耐焼付き性について、鋭意、実験検討を重ねた結果、冷間での加工性が劣るために製造工程中に割れ等の不良が発生するのを防止するための製造方法を提供するものである。その本発明の要旨とするところは、
(1)高炭素合金工具鋼をコイル圧延後、連続焼鈍し、その後、10〜20%の減面率で引抜き、引続き850〜900℃で1回または2回焼鈍を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法。
In order to solve the problems as described above, the present invention is a result of intensive and experimental studies on cold forgeability, wear resistance, and seizure resistance, which are required as sliding parts for internal combustion engines. The present invention provides a manufacturing method for preventing defects such as cracks during the manufacturing process due to inferior cold workability. The gist of the present invention is that
(1) Cold rolling characterized in that high carbon alloy tool steel is continuously annealed after coil rolling, then drawn at a reduction in area of 10 to 20%, and subsequently annealed once or twice at 850 to 900 ° C. A method for manufacturing wear-resistant materials with excellent forgeability.

(2)前記(1)に記載の方法において、C:1.40〜1.60%、Cr:11〜13%、Mo+1/2W:0.5〜1.5%、V+1/2Nb:0.2〜1.0%を含有し、残部をFeと不可避的不純物からなる鋼素材の処理を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法。
(3)前記(1)に記載の方法において、C:0.70〜1.10%、Cr:7.0〜9.0%、Mo+1/2W:1.5〜3.0%、V+1/2Nb:0.2〜2.0%を含有し、残部をFeと不可避的不純物からなる鋼素材の処理を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法にある。
(2) In the method according to (1), C: 1.40 to 1.60%, Cr: 11 to 13%, Mo + 1 / 2W: 0.5 to 1.5%, V + 1 / 2Nb: 0. A method for producing a wear-resistant material excellent in cold forgeability, characterized in that a steel material comprising 2 to 1.0% and the balance comprising Fe and inevitable impurities is processed.
(3) In the method described in (1) above, C: 0.70 to 1.10%, Cr: 7.0 to 9.0%, Mo + 1 / 2W: 1.5 to 3.0%, V + 1 / 2Nb: 0.2 to 2.0% in the manufacturing method of a wear-resistant material excellent in cold forgeability, characterized in that a steel material consisting of Fe and inevitable impurities is processed in the balance. .

以上述べたように、本発明によりコイル材からの製造によるコストダウンと冷間鍛造用途への拡販することが出来る極めて優れた効果を奏するものである。   As described above, according to the present invention, it is possible to reduce the cost by manufacturing from a coil material and to achieve an extremely excellent effect capable of expanding sales to cold forging applications.

以下、本発明について詳細に説明する。
本発明に係る方法として、引抜加工時のダイス欠け、焼付き等のトラブルを防止するために、引抜前に軟化目的で1回または2回熱処理を行なう。その後、引抜き、焼鈍を行ない硬度を低下させるが、これは鋼材内部に適度な歪みを発生させ、炭化物の球状化が促進されるためである。また、焼鈍を複数回実施することで、さらに効果が得られ安定した軟化硬さが得られる。
Hereinafter, the present invention will be described in detail.
As a method according to the present invention, heat treatment is performed once or twice for the purpose of softening before drawing in order to prevent troubles such as die chipping and seizure during drawing. Thereafter, drawing and annealing are performed to reduce the hardness. This is because moderate distortion is generated inside the steel material and spheroidization of the carbide is promoted. Further, by performing annealing a plurality of times, further effects are obtained and stable softening hardness is obtained.

以下、本発明に係る成分組成の限定理由について説明する。
C:0.70〜1.60%
Cは、焼入焼戻し後の硬度を確保するために、0.70%以上必要である。しかし、1.60%を超える添加は一次炭化物を粗大化し、一次炭化物の凝集部のサイズが大きくなり、冷間鍛造性が著しく悪化する。従って、その範囲を0.70〜1.60%とした。
Hereinafter, the reasons for limiting the component composition according to the present invention will be described.
C: 0.70 to 1.60%
C needs to be 0.70% or more in order to ensure the hardness after quenching and tempering. However, addition exceeding 1.60% coarsens the primary carbide, increases the size of the agglomerated portion of the primary carbide, and remarkably deteriorates the cold forgeability. Therefore, the range was made 0.70 to 1.60%.

Cr:7〜13%
Crは、焼入性と耐摩耗性を確保するために、7%以上必要である。しかし、13%を超える添加は一次炭化物が粗大化し、一次炭化物の凝集部のサイズが大きくなり、冷間鍛造性が著しく悪化する。従って、その範囲を7〜13%とした。
Cr: 7-13%
Cr needs to be 7% or more to ensure hardenability and wear resistance. However, addition exceeding 13% coarsens the primary carbide, increases the size of the agglomerated portion of the primary carbide, and remarkably deteriorates the cold forgeability. Therefore, the range was 7 to 13%.

Mo+1/2W:0.5〜3.0%
MoおよびWは、焼入性の確保と高温焼戻の析出炭化物による耐摩耗性と耐焼付き性を改善するために、0.5%以上必要である。しかし、3.0%を超える添加をすると析出炭化物の凝集が顕著になり、耐焼付き性や靱性が低下する。従って、その範囲を0.5〜3.0%とした。
Mo + 1 / 2W: 0.5-3.0%
Mo and W are required to be 0.5% or more in order to ensure hardenability and improve wear resistance and seizure resistance due to precipitated carbides during high temperature tempering. However, if it exceeds 3.0%, the agglomeration of precipitated carbides becomes remarkable, and seizure resistance and toughness are reduced. Therefore, the range was made 0.5 to 3.0%.

V+1/2Nb:0.2〜2.0%
VおよびNbは、高温焼戻しによる二次硬化時に、鋼中に微細炭化物を分散析出させることで、耐摩耗性と耐焼付き性を改善する。この効果を得るため、0.2%以上必要である。しかし、2.0%を超える添加をすると析出炭化物の凝集が顕著になり、耐焼付き性や靱性が低下する。従って、その範囲を0.2〜2.0%とした。
V + 1 / 2Nb: 0.2-2.0%
V and Nb improve wear resistance and seizure resistance by dispersing and precipitating fine carbides in steel during secondary hardening by high temperature tempering. In order to obtain this effect, 0.2% or more is necessary. However, if the addition exceeds 2.0%, the agglomeration of the precipitated carbides becomes remarkable, and seizure resistance and toughness deteriorate. Therefore, the range was made 0.2 to 2.0%.

連続焼鈍した後、10〜20%の減面率で引き抜く。しかし、減面率10%未満では、鋼材内部に残留する歪みが不十分であり、軟化の程度が小さい。20%を超えると、引抜き時ダイスが欠け、焼付き等が発生する危険が高くなる。引続き850〜900℃で1回または2回焼鈍する。その理由は、炭化物の球状化促進であり、850℃未満では、軟化が不十分であり、900℃お超えると逆に硬度が高くなる。従って、その温度範囲を850〜900℃とした。   After continuous annealing, it is pulled out with a reduction in area of 10 to 20%. However, if the area reduction rate is less than 10%, the strain remaining in the steel material is insufficient and the degree of softening is small. If it exceeds 20%, the risk of chipping and seizure at the time of drawing increases. Subsequently, annealing is performed once or twice at 850 to 900 ° C. The reason is to promote the spheroidization of the carbide. When the temperature is lower than 850 ° C., the softening is insufficient, and when the temperature exceeds 900 ° C., the hardness increases. Therefore, the temperature range was set to 850 to 900 ° C.

以下、本発明について実施例によって具体的に説明する。
表1に示す本発明鋼A〜Dと比較鋼E、F、Gを、それぞれ1t真空溶解炉にて出鋼し、造塊、ビレット鍛伸後、圧延して、φ18のコイル材を得た後、表2に示す焼鈍条件および減面率にて冷間加工した後、引続き焼なまし処理したときの焼なまし硬さ、および冷間加工性、その後、焼入焼戻しを行い60HRCに調質した材料についての耐摩耗性についての結果を表2に示す。また、耐摩耗性試験は摩擦距離200m、最終荷重61.7N、摩擦速度2.44m/sで摩耗量を測定した。その結果、○印は耐摩耗性に優れ、×印は耐摩耗性が劣る。また、冷間加工性については、○印は優れ、△印は劣り、×印は悪い、ことを示す。
Hereinafter, the present invention will be specifically described with reference to examples.
Invention steels A to D and comparative steels E, F, and G shown in Table 1 were each produced in a 1-t vacuum melting furnace, and after ingot forming and billet forging and rolling, a φ18 coil material was obtained. Then, after cold working under the annealing conditions and area reduction ratio shown in Table 2, the annealing hardness and cold workability after annealing were subsequently adjusted to 60 HRC by quenching and tempering. Table 2 shows the results of the wear resistance of the quality materials. In the wear resistance test, the amount of wear was measured at a friction distance of 200 m, a final load of 61.7 N, and a friction speed of 2.44 m / s. As a result, ◯ marks are excellent in wear resistance, and X marks are inferior in wear resistance. Further, regarding the cold workability, ◯ indicates that it is excellent, Δ indicates that it is poor, and X indicates that it is bad.

Figure 2006161133
Figure 2006161133

Figure 2006161133
Figure 2006161133

表2に示すように、No.1〜11は本発明鋼であり、No.12〜16は比較鋼であり、No.17〜18は従来品である。比較例No.12は減面率が低く、従来材と変わらず、焼なまし硬さが硬く、冷間加工性が悪い。比較鋼No.13は焼なまし温度が低いために、焼なまし硬さが硬く、冷間加工性が悪い。比較鋼No.14は逆に焼なまし温度が高いために、焼なまし硬さが硬く、冷間加工性が悪い。比較鋼No.15、16はいずれも減面率が高いために、ダイス焼付が起こり、工程がストップした。従来品No.17、18は減面率0の場合であり、焼なまし硬さが硬く、かつ冷間加工性が劣る。これに対し、本発明鋼であるNo.1〜11は、いずれの特性についても優れていることが分かる。   As shown in Table 2, no. Nos. 1 to 11 are steels of the present invention. Nos. 12 to 16 are comparative steels. 17 to 18 are conventional products. Comparative Example No. No. 12 has a low area reduction rate, is not different from the conventional material, has a high annealing hardness, and has poor cold workability. Comparative steel No. Since No. 13 has a low annealing temperature, the annealing hardness is hard and the cold workability is poor. Comparative steel No. In contrast, since No. 14 has a high annealing temperature, the annealing hardness is high and the cold workability is poor. Comparative steel No. Since both 15 and 16 had a high area reduction rate, die baking occurred and the process was stopped. Conventional product No. 17 and 18 are cases where the area reduction rate is 0, the annealing hardness is hard, and the cold workability is inferior. On the other hand, No. which is steel of the present invention. It can be seen that 1 to 11 are excellent in any of the characteristics.

上述したように、高C、高Cr鋼材をコイル圧延後に焼鈍を行ない、その後、最適減面率で引抜き、焼鈍を行なうことにより、鋼材内部に適度な歪みを発生させ、炭化物の球状化を促進し、また、焼鈍を数回行うことで、さらに安定した軟化硬さが得られ、加工性の良い耐摩耗性の優れた冷間鍛造用鋼が低コストにて得られ、その結果、特にエンジン部品など生産材への開発鋼の拡販を優位に進めることが出来る優れた効果が得られるものである。


特許出願人 山陽特殊製鋼株式会社
代理人 弁理士 椎 名 彊
As described above, high C and high Cr steels are annealed after coil rolling, and then are pulled and annealed at the optimum area reduction rate, thereby generating moderate strain inside the steel and promoting carbide spheroidization. In addition, by performing annealing several times, more stable softening hardness can be obtained, and steel for cold forging with good workability and wear resistance can be obtained at low cost. It is possible to obtain an excellent effect that can promote the sales of the developed steel to production materials such as parts.


Patent Applicant Sanyo Special Steel Co., Ltd.
Attorney: Attorney Shiina

Claims (3)

高炭素合金工具鋼をコイル圧延後、連続焼鈍し、その後、10〜20%の減面率で引抜き、引続き850〜900℃で1回または2回焼鈍を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法。 Cold forging, characterized in that high-carbon alloy tool steel is continuously annealed after coil rolling, then drawn at a reduction in area of 10 to 20%, and subsequently annealed once or twice at 850 to 900 ° C. Manufacturing method for wear-resistant materials. 請求項1に記載の方法において、
C:1.40〜1.60%、
Cr:11〜13%、
Mo+1/2W:0.5〜1.5%、
V+1/2Nb:0.2〜1.0%を含有し、残部をFeと不可避的不純物からなる鋼素材の処理を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法。
The method of claim 1, wherein
C: 1.40 to 1.60%
Cr: 11-13%,
Mo + 1 / 2W: 0.5-1.5%
V + 1 / 2Nb: A method for producing a wear-resistant material excellent in cold forgeability, characterized in that a steel material containing 0.2 to 1.0% and the balance being Fe and inevitable impurities is processed. .
請求項1に記載の方法において、
C:0.70〜1.10%、
Cr:7.0〜9.0%、
Mo+1/2W:1.5〜3.0%、
V+1/2Nb:0.2〜2.0%を含有し、残部をFeと不可避的不純物からなる鋼素材の処理を行なうことを特徴とする冷間鍛造性に優れた耐摩耗用素材の製造方法。
The method of claim 1, wherein
C: 0.70 to 1.10%,
Cr: 7.0 to 9.0%,
Mo + 1 / 2W: 1.5-3.0%,
V + 1 / 2Nb: A method for producing a wear-resistant material excellent in cold forgeability, characterized in that a steel material comprising 0.2 to 2.0% and the balance being Fe and inevitable impurities is processed. .
JP2004357510A 2004-12-10 2004-12-10 Method for producing blank for wear resistance excellent in cold-forging Withdrawn JP2006161133A (en)

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