JP2006003235A - Electron beam system and datum sample therefor - Google Patents

Abstract

<P>PROBLEM TO BE SOLVED: To provide an electron beam system and a datum sample therefor, capable of carrying out a precise image measurement of a sample, without depending on the tilt angle nor the height of the sample. <P>SOLUTION: The electron beam system, which is shown in Figure for example, is equipped with: an electron beam source 1 emitting an electron beam; an electronic optical system 2 which converges the electron beam 7 emitted from the electron beam source 1 and irradiates a sample 9 with it; a detecting section 4 which receives an electron 7d from the sample 9 irradiated with the electron beam 7; a sample support section 3 which supports the sample 9; a sample tilting section 5(5a, 5b) which tilts the sample 9 relatively to the electron beam 7 impinging on the sample 9 being supported by the sample support section 3; and a data processing section 20 which receives detection signals from the detecting section 4 that receives electrons from the datum sample 9a being supported by the sample support section 3 so as to be relatively tiltable and having at least two tilt surfaces, at each state of the tilt surfaces, and which obtains a tilt angle of the datum sample 9a from images of the two tilt surfaces and the datum dimension of the datum sample 9a. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

  The present invention relates to an electron beam system that accurately performs three-dimensional measurement of a sample using a sample image captured by an electron microscope, and a reference sample for an electron beam system, and more particularly to a scanning charged particle beam apparatus for 3D measurement. The present invention relates to an electron beam system capable of adjusting correction of an angle and magnification at the time of tilting a beam or a sample, or correction in an electron optical system so as to be suitable for image measurement, and a reference sample for the electron beam system.

  In a scanning charged particle beam apparatus such as a conventional scanning electron microscope (SEM), an off-axis aberration of an electron lens is corrected in order to increase the resolution of a scanning electron microscope image or the like. The off-axis aberration of the electron lens is performed, for example, by compensating for spherical aberration, coma aberration, field aberration, astigmatism, and field distortion. Also, with regard to spherical aberration, Zelzer's theorem is known, and it is known that an axially symmetric electron lens used in an electron microscope or the like cannot eliminate spherical aberration regardless of electrostatic type or magnetic type. It has been. Therefore, in order to compensate for spherical aberration, an aspherical mesh or an aspherical form is used as the electrostatic electrode shape or the magnetic pole shape.

  On the other hand, in the case of a transmission electron microscope (TEM), a sample is tilted, transmission images with different tilt angles are obtained, and stereo observation of the sample is performed using this as a left and right image. For example, as shown in Non-Patent Document 1, in the case of a scanning electron microscope (SEM), a sample is tilted or an electron beam is tilted to obtain reflected images having different tilt angles. Stereo observation is performed as left and right images. And, for example, as shown in Patent Documents 1 and 2, in the field of semiconductor manufacturing equipment, the stereo detection data obtained from the electron microscope is appropriately processed so that the sample image can be stereoscopically observed accurately and accurately, and Based on this, an electron beam apparatus and a data processing apparatus for an electron beam apparatus that can perform three-dimensional shape measurement have been proposed.

JP, 2002-270126, A [0005], FIG. 3, FIG. JP-A-2002-270127 [0005], FIG. 3, FIG. "Medical / biological electron microscopy" pp. 278-299, published in 1982

  However, in particular, when a sample such as a semiconductor chip or a silicon wafer is to be measured in 3D, it is necessary to accurately obtain the tilt angle and magnification of the beam and sample during measurement imaging. There are electron beam distortion and magnification distortion depending on the tilt direction and height direction of the sample. If the tilt angle or magnification is not accurate, or if electron beam distortion or magnification distortion is included in the measurement direction of the sample image, the value when measuring the sample by image measurement cannot be obtained correctly, and the accuracy further varies. There was a problem. In recent semiconductor microfabrication, for example, the pattern width formed on a chip is miniaturized to the submicron order, and the dimensional error allowed for three-dimensional shape measurement is more severe than in the past. Therefore, the conventional methods of compensating for the tilt angle value and magnification, and the off-axis aberration of the electronic lens such as spherical aberration, have a problem that the accuracy required for stereo image measurement cannot be obtained.

  The present invention solves the above-described problems, and provides an electron beam apparatus and a reference sample for an electron beam apparatus that can perform accurate sample image measurement without depending on the inclination angle or height of the sample. Objective.

  An electron beam system according to the present invention that achieves the above-described object includes an electron beam source 1 that emits an electron beam, as shown in FIG. 1, for example, and converges an electron beam 7 emitted from the electron beam source 1 to a sample 9. Electron optical system 2 for irradiating; detecting unit 4 for receiving electrons 7d from sample 9 irradiated with electron beam 7; sample supporting unit 3 for supporting sample 9; sample 9 supported by sample supporting unit 3 A sample tilting portion 5 (5a, 5b) for relatively tilting the irradiated electron beam 7 and the sample 3; and at least tilted 2 supported by the sample support portion 3 so that the relative tilting is possible. The detection signal from the detection unit 4 that has received electrons from the reference sample 9a having a surface is received for each inclination, and the inclination angle of the reference sample 9a is determined from the two inclined images and the reference dimensions of the reference sample 9a. A data processing unit 20 and the like.

  The data processing unit may be further configured to obtain a magnification of the sample image in the electron beam system.

  The data processing unit may be configured to obtain a correction coefficient for the sample inclination amount based on the obtained inclination angle, and to correct the inclination angle based on the correction coefficient for the sample inclination amount. The sample here is typically a sample to be measured.

  The data processing unit obtains a correction coefficient for the sample inclination amount with respect to the inclination between the measured inclination angles based on the obtained plurality of inclination angles, and the sample inclination amount with respect to an inclination angle other than the measured inclination angle. You may be comprised so that correction | amendment may be performed.

An electron beam system according to the present invention that achieves the above object includes, as shown in FIG. 1, for example, an electron beam source 1 that emits an electron beam; and an electron beam 7 emitted from the electron beam source 1 is converged and irradiated onto a sample. An electron optical system 2; a detection unit 4 that receives electrons from a sample 9 irradiated with an electron beam 7; a sample support unit 3 that supports the sample 9; and a sample 9 supported by the sample support unit 3 A sample inclination part 5 (5a, 5b) for relatively inclining the electron beam 7 and the sample 9; and at least two inclined surfaces supported by the sample support part 3 so that the relative inclination can be freely performed. A detection signal from the detection unit 4 that has received electrons from the reference sample 9a is received for each tilt, and based on an image of the sample 9 at a position where the displacement of the electron beam optical system is small due to the tilt of the sample 9, Two inclined images in the image and the reference Data processing for performing processing for obtaining the tilt angle of the reference sample 9a from the reference dimensions of the material 9a, processing for obtaining a correction coefficient based on the difference between the magnification at the tilt angle in the peripheral image and the magnification of the image based on the detection signal A part.
The electron beam system typically performs image correction such as angle measurement, electron lens distortion, and scan distortion, and typically performs parallel projection.

  In the electron beam system, the sample tilting unit 5 is configured to tilt the sample 9 with respect to the electron beam 7 by tilt control 5b (for example, FIG. 1) of the sample holder 3 or the electron beam 7 with respect to the sample 9 at different angles. It may be configured to perform any one of deflection control 5a (for example, FIG. 17) of the electron beam 7 to be irradiated.

  The data processing unit may include an image forming unit 24 that forms a sample image in which electron lens distortion, scan distortion, and the like are corrected based on a signal from the electron beam detection unit 4 using a correction coefficient. The sample here is typically a sample to be measured. The electrons detected by the electron beam detector 4 correspond to secondary electrons and reflected electrons.

  In the electron beam system, the data processing unit may be configured to obtain, by interpolation, a correction coefficient for an inclination for which measurement has not been performed, in addition to a correction coefficient for the inclination for which measurement has been performed.

  The reference sample 9a of the present invention that achieves the above object is a pattern comprising a bottom portion, a top portion, and a side surface portion connecting the top portion with a predetermined taper angle, and the dimensions, angle and height of each portion are known. A reference sample used in the electron beam system.

  In the reference sample 9a, the pattern may be a line and space pattern.

  In the reference sample 9a, the line and space pattern may be formed in a direction orthogonal to the tilt direction of the sample.

  According to the electron beam apparatus and the reference sample for the electron beam apparatus of the present invention, for example, the tilt angle, magnification, and distortion associated with the electron optical system are calculated and corrected to correct the photographed image. Measurement can be performed.

[Height measurement]
Prior to the description of the present invention, the basic principle of height measurement will be described.
2 and 3 are a coordinate diagram and a perspective view for explaining the tilt of the holder at the time of tilt image acquisition and the coordinate system of the sample holder 3 (see FIG. 1). In the coordinate system of the sample holder 3, the Y axis is the rotation axis, and the angle θ is the clockwise direction in the + direction.

FIG. 4 is a front view showing the relationship between the image and the sample when the measurement object 9 is irradiated with an electron beam. From geometric relationship,
Left image Lx = (X × cosθ + Z × sinθ) × s (1)
Ly = Y
Right image Rx = (X × cosθ−Z × sinθ) × s (2)
Ry = Y
s: Resolution (1 pixel)
Thus, when the three-dimensional coordinates are obtained from the orientation matrix in consideration of the rotation angle of the image and the sample, the following is obtained.
X = Lx + Rx (3)
Z = Lx−Rx
Y = Ly = Ry
As shown in FIG. 5, the expression (3) is effective only when the left and right images have an angle across the Z axis as the shooting direction of the stereo image. Next, we will derive a formula that can be used without depending on the angle. FIG. 6 shows a case where the left and right images are inclined by θ1 and θ2 with respect to the Z axis as the shooting direction of the stereo image, respectively.

The angle of the left image is θ1, and the angle of the right image is θ2, and a Z ′ axis obtained by inclining the Z axis by θ ′ is assumed. Here, it is assumed that the left and right shooting directions of the stereo image in FIG. 5 are symmetrical with respect to the Z ′ axis. Then, by applying the pseudo coordinates (X ′, Y ′, Z ′), the angle of the image becomes θ ′ ± θ, and the equation (2) is used to further change to the coordinates XYZ later by θ 'Rotate.
Z ′ = ((Lx−Rx) / (2 × sin θ)) × s (4)
X ′ = ((Lx + Rx) / (2 × cos θ)) × s
Y '= Ly = Ry
Therefore, the following equation is established.
X = X ′ × cos θ′−Z ′ × sin θ ′ (5)
Z = X ′ × sin θ ′ + Z ′ × cos θ ′
Y = Y

[principle]
The basic principle of the present invention is that the reference template is obtained from the known shape data of the reference template as the reference sample and the reference template data obtained by inclining the electron beam measuring device, the tilt angle θ, the magnification, and the electron optics. Calculate strains caused by the system, store these values, and use the tilt angle, magnification, and electron optical system strain calculated in advance in the reference template when measuring the sample at the corrected tilt angle. Then, the image is corrected and 3D measurement is performed.
As the reference template, a template having a known shape is used, or when a template having an unknown shape is used, it is measured and used as a reference template. The reference template may be uneven, such as a line and space as shown in FIG. 7, but the known data required as the reference template is as shown in FIGS. The shape of the unevenness, that is, the interval L between the unevenness (pitch interval L in the case of a line & space pattern), the height h of the unevenness, the taper angle φ, and the like.
Then, the pitch interval L ′ and the side surface interval d ′ (x ′) are obtained from the image of the reference template obtained by photographing with the electron beam system of the present invention.
When these are obtained, the tilt angle θ and the magnification s of the electron beam measuring apparatus when the image is taken can be calculated from the following equations.

☆ Calculation formula: Inclination angle, magnification calculation
S and θ when an L / S sample with a known pitch interval L [nm], taper angle φ [degrees], and height h [nm] is photographed at a magnification S [times] and an inclination angle θ [degrees] Ask for.

The pitch interval L '[pixel] when tilted by θ is defined as 1 pixel size s [nm].
L '= L x cosθ / s ...... E1

The side width d '[pixel] when tilted by θ is
d ′ = l × cos (φ−θ) / s
= (H / sinφ) × cos (φ−θ) / s …… E2

Solving E1 and E2 for s,
L × cosθ / L ′ = (h / sinφ) × cos (φ−θ) / d ′
= (H / sinφ) x (cosφcosθ + sinφsinθ) / d '

∴θ = tan ^-1 (Ld '/ h L'- (1 / tanφ)) ...... E3

☆ Distortion correction Furthermore, calculation of distortion correction parameters for the electron optical system will be described.
The distortion of the electron optical system can be corrected by providing correction coefficients for the distortion aberration of the lens system, the scanning distortion of the electron beam, and other distortions of the entire electron optical system.
For example, when the reference template is a line and space as shown in FIG. 7, the boundary between the side surface and the top surface and the side surface and the bottom surface of the reference template is a straight line, and correction can be performed by approximating this part as a straight line. .
That is, the straight line can be approximated by the following equation (see FIG. 19).
xsinα + ycosα = q
When considering the distortion of the electron optical system, the above equation is
(x + Δx) sinα + (y + Δy) cosα = q
Here, Δx and Δy are strain amounts.
The above equation shows the condition that several points (bent due to strain) on the side and bottom surfaces and the side and top surfaces of the reference template are “points on a straight line”.
The distortion model is adjusted so that it becomes a straight line when these points are corrected.

[Lens distortion correction]
When the distortion aberration of the electron lens constituting the electron optical system 2 is obtained, it can be corrected by the equation (6). That is, if the x and y coordinates obtained by correcting the lens distortion in equations (11) and (12) are x ′ and y ′, the following equation is established.
x ′ = x + Δx (6)
y ′ = y + Δy
Here, when k1 and k2 are radial lens distortion coefficients, the following equation is used.

The distortion of the electron lens is calculated by the successive approximation method by applying the above equation by measuring the image coordinates and the target coordinates. In the calculation of the distortion aberration of the electron lens, the lens distortion coefficient increases as an unknown variable. Therefore, it is preferable to measure the image coordinates and the target coordinates using a large number of points on the straight line as reference points, and calculate by the fitting successive approximation method. In addition, the lens distortion coefficient is the radial lens distortion in equation (7), but in addition to tangential lens distortion, spiral lens distortion, and other elements necessary for correcting the distortion aberration of the electronic lens, expression (7) is added. If a lens distortion coefficient is calculated | required, those calibration (calibration) will be attained.
For example, if the beam is scanned so as to correct the lens distortion using the obtained lens distortion coefficient, a corrected image can be acquired as a result. Alternatively, lens distortion in an image can be corrected by storing lens distortion in a memory and performing beam scanning so as to correct the lens distortion.
As described above, if the reference template is tilted in the direction in which it is desired to be tilted, and the actual tilt angle, magnification, and distortion of the electron optical system are calculated in advance and stored in advance, the sample is measured when the sample is measured. Alternatively, an accurate three-dimensional shape can be obtained by using these values when the beam is tilted. It may be configured such that an inclination angle at the time of measurement is obtained, each correction coefficient corresponding to the inclination angle is obtained by calculation, and correction is performed.

The procedure will be described below with reference to the flowchart of FIG.
FIG. 7 shows, for example, a line & space pattern as the reference template 9a. FIG. 8 is a diagram illustrating the pitch interval and inclination of the line & space pattern, and FIG. .
For example, the reference template 9a is a line and space pattern as shown in FIG.
This reference template may be a commercially available pitch standard sold as a reference template, or if not, a line & space pattern as shown in FIG. 7 may be measured by a measuring device such as a CD-AFM. .
From this reference template, values of the pitch interval L, taper angle φ, and height h of the sample are used if they are commercially available products, otherwise these data are measured in advance.
S1000: Set the tilt angle of the sample or beam of the electron beam measuring device and tilt it.
This tilt angle is performed for all or representative tilt angles to be measured in advance.
S1010: Shooting the reference template with an electron beam measuring device
S1020: The pitch interval L ′ and side width d ′ (x ′) of the photographed reference template are calculated by image processing.

[Line edge detection processing]
In order to accurately calculate the pitch interval on the image and correct the magnification and angle, the edges of the line and space are obtained with sub-pixel accuracy. In the method, a straight line detection operator is applied to the acquired image of the reference template (generator) to detect an edge point.
The straight line detection operator may be anything such as a 3 × 3 filter type often used in image processing.
Based on the obtained all edge points, the edge group connected from the threshold is recognized as a line (straight line) of the reference template by using the edge connectivity. FIG. 21 shows an example of actual edge detection.

S1030: Calculate the tilt angle and magnification at the time of shooting, and distortion caused by the electron optical system. This is calculated using the formula explained in the principle above.
S1040: The calculated tilt angle, magnification, and distortion parameters are stored in the correction coefficient storage unit.
S1050: If all the set tilt angles have been performed, the process ends. If not, the process returns to S1000 to repeatedly change the tilt angle to calculate each parameter.

In the apparatus configured as described above, the electron beam measuring apparatus acquires the shape on the reference template image at each inclination angle, and the inclination necessary for the three-dimensional measurement from the reference template measured in advance. The correction coefficient for removing the image distortion caused by the angle, the magnification, and the electron optical system is acquired. Next, a sample 9 instead of the reference template is placed on the sample holder 3 and an image of the sample 9 is acquired by an electron beam measuring apparatus using the sample 9 as an object at an arbitrary inclination angle.

  Hereinafter, embodiments of the present invention will be described with reference to the drawings. FIG. 1 is a block diagram illustrating a first embodiment of the present invention, and shows a case where a stereo image is obtained by adjusting a tilt angle of an object by adjusting a rotation angle of a holder that holds the object. . In the figure, an electron beam apparatus 10 (scanning microscope) as an image forming optical system in an electron beam system includes an electron beam source 1 that emits an electron beam 7 and an electron optical that irradiates an object 9 with an electron beam (beam) 7. System 2, sample holder 3 that holds the object 9 in a tiltable manner, a magnification changing unit 6 that changes the magnification of the electron optical system 2, a scanning power source 6 a that supplies power to the magnification changing unit 6, and an object irradiated with an electron beam 7 A detector 4 for detecting secondary electrons or reflected electrons from an object, a holder tilt control unit 5b as a tilt control unit 5 for controlling the tilt of the sample holder 3, and attenuating energy of secondary electrons emitted from the object 9. And a secondary electron conversion target 8 to be reflected by the detector 4. The beam tilt control unit 5a as the tilt control unit 5 that controls the tilt of the electron beam 7 is not used in the first embodiment, but is used in a third embodiment to be described later.

  The electron optical system 2 includes a condenser lens 2a that changes the electron flow density, opening angle, irradiation area, etc. of the electron beam 7 emitted from the electron beam source 1, and a deflection lens 2b that controls the incident angle of the electron beam 7 on the sample surface. A scanning lens 2c that deflects the finely focused electron beam 7 to scan the sample surface two-dimensionally, and an objective lens 2d that focuses the incident probe on the sample surface along with the function of the final stage reduction lens. ing. In accordance with the magnification change command of the magnification changing unit 6, the region on the sample surface where the electron beam 7 is scanned by the scanning lens 2c is determined. The beam tilt control unit 5b sends a tilt control signal to the sample holder 3, and the sample holder 3L in the first posture in which the sample holder 3 and the irradiation electron beam 7 form the first relative tilt angle, and the second relative Switching is made between the sample holder 3R in the second posture having an inclination angle.

Three-dimensional coordinate system _{C L} of the object 9 to be placed on the sample holder 3L in the first posture, when an electron beam device 10 as a fixed coordinate _system, the _{(X L, Y L, Z} L) . Also, three-dimensional coordinate system _{C R} of the object 9 to be placed on the sample holder 3R second posture, when an electron beam device 10 as a fixed coordinate _{system, (X R, Y R,} Z R) It becomes. In addition, although the relative inclination angle of the sample holder 3 and the irradiation electron beam 7 by the holder inclination control unit 5b is set to be switched between two ways of rising to the right and rising to the left, here, two steps are illustrated. However, in order to obtain stereo detection data, a minimum of two stages is required. For example, when a yaw axis, a pitch axis, and a roll axis are set as the three-dimensional coordinate system of the object 9, the yaw axis corresponds to the Z axis, the pitch axis corresponds to the X axis, and the roll axis corresponds to the Y axis.

  The object 9 is, for example, a semiconductor chip such as a silicon semiconductor or a gallium / arsenic semiconductor, but may be an electronic component such as a power transistor, a diode, or a thyristor, or a glass such as a liquid crystal panel or an organic EL panel. The display device parts used may be used. Under typical scanning microscope observation conditions, the electron beam source 1 is applied to −3 kV, and the object 9 is applied to −2.4 kV. The secondary electrons emitted from the object 9 collide with the secondary electron conversion target 8 and the energy is weakened and detected by the detector 4.

  1, the electron beam system includes a measurement unit 20 as a first measurement unit, a calibration data creation unit 30, a known reference data storage unit 32, a calibration unit 40, an electron lens aberration compensation unit 42, and a form / coordinate measurement unit 50. An image correction unit 60, a correction coefficient calculation unit 62, and a correction coefficient storage unit 64.

  The measuring unit 20 relatively tilts the reference template 9 a held by the sample holder 3 and the irradiation electron beam 7 by the sample tilting unit 5, and displays the captured image of the reference template 9 a captured by the electron beam detecting unit 4. Based on this, the form or coordinate values (pitch interval L, taper angle φ, height h, etc.) of the reference template 9a are obtained. The measuring unit 20 includes an incident angle adjusting unit 22, an image forming unit 24, a reference template measuring unit 26, and a display device 28.

  The incident angle adjustment unit 22 adjusts the posture of the object 9 (including the reference template 9 a), and the relative incident angle between the electron beam 7 projected on the object 9 by the electron beam apparatus 10 and the object 9. Are adjusted so that a stereo image can be formed for the object 9. That is, the incident angle adjustment unit 22 adjusts the posture of the object 9 by sending a control signal to the holder inclination control unit 5b. Further, the incident angle adjusting unit 22 sends a control signal to the holder tilt control unit 5b to adjust the reference plane scanned by the electron beam 7 emitted from the electron beam source 1 and form a stereo image. Left and right images can be formed. The image forming unit 24 creates an image on the sample surface using the secondary electron beam detected by the detector 4 when the scanning lens 2c scans the region on the sample surface. The reference template measurement unit 26 obtains the form or coordinate value of the reference template 9a based on the image of the reference template 9a photographed by the electron beam detection unit 4. The display device 28 displays left and right images of the stereo image of the object 9 (including the reference template 9a) photographed by the electron beam detector 4, and for example, a CRT or a liquid crystal display is used.

The calibration data creation unit 30 creates correction coefficients and calibration data for a stereo image photographed by the electron beam system using the measurement result of the reference template in the measurement unit 20 and the known reference data regarding the reference template 9a. The reference template known reference data storage unit 32 stores the form of the reference template 9a (pitch interval, taper angle, height, etc.). The calibration data of the electron beam system created by the calibration data creation unit 30 includes the following.
(1) Calibration data of the tilt amount of the sample tilt portion 5.
(2) Calibration data of the irradiation direction with respect to the irradiation electron beam 7 of the electron optical system 2.
(3) Calibration data relating to the magnification of the electron optical system 2.
(4) Calibration data relating to distortion correction of the electron optical system 2.

The calibration unit 40 performs calibration based on the calibration data so as to reduce the aberration of the sample image detected by the electron beam detection unit 4. The calibration unit 40 has the following modes according to the calibration data of the electron beam system created by the calibration data creation unit 30 described above.
(1) The calibration unit 40 is configured so that the tilt amount of the sample tilting unit 5 is calibrated.
(2) The calibration unit 40 is configured so that the irradiation direction of the irradiation electron beam 7 of the electron optical system 2 is calibrated.
(3) The calibration unit 40 is configured so that the scanning range of the electron optical system 2 is calibrated.
(4) The calibration unit 40 is configured so that the scanning direction of the scanning coil of the electron optical system 2 is calibrated.

  The electron lens aberration compensation unit 42 compensates the distribution state of the magnetic field potential and electrostatic potential of the electron lens constituting the electron optical system 2 in accordance with the calibration signal output from the calibration unit 40, thereby reducing the aberration of the sample image. Thus, the electron optical system 2 suitable for image measurement is adjusted. When the electron beam apparatus 10 has an electromagnetic prism called ExB that separates the secondary electrons emitted from the sample 9 from the electron beam 7 emitted from the electron beam source 1 and sends them to the electron beam detector 4, the calibration is performed. The electron optical system 2 to be calibrated by the unit 40 includes an electromagnetic prism called ExB.

  The form / coordinate measuring unit 50 is a sample 9 placed on the sample holder 3 that has been calibrated by the calibrating unit 40, and is photographed by the electron beam detecting unit 4 in a tilted state formed by the sample tilting unit 5. On the basis of the stereo image of the sample 9, the form or coordinate value of the sample 9 is obtained. The form / coordinate measuring unit 50 uses the incident angle adjusting unit 22, the image forming unit 24, and the display device 28 of the measuring unit 20 in common with the reference template measuring unit 26.

  Next, with reference to FIG. 12, a calibration procedure of the electron beam apparatus necessary for stereo image measurement by the apparatus configured as described above will be described. FIG. 12 is a flowchart of electron beam measurement including a calibration procedure for the electron beam apparatus according to the first embodiment of the present invention. FIG. 12 shows a processing flow in which the electron beam apparatus is calibrated using the reference template 9a and then the sample image measurement is performed (S100). First, the reference template 9a is placed on the sample holder 3, and the sample holder 3 or the electron beam 7 is shifted to an inclined state (S102). For example, a tilt control signal is sent to the sample holder 3 by the beam tilt control unit 5b, and the relative incident angle between the electron beam 7 and the object 9 is adjusted by the incident angle adjusting unit 22. This inclination angle is set with respect to the inclination angle of the reference template 9a to be measured. For example, the inclination angle is set to the inclination state shown in FIG. 2A or the inclination state shown in FIG. When there are a plurality of inclination angles, it is preferable to set the inclination angles to angles that can be measured in advance and acquire images.

  The measurement unit 20 acquires an inclined image of the reference template 9a obtained from the electron beam detection unit 4 (S104). Then, the measurement unit 20 obtains the form of the reference template 9a based on the image of the reference template 9a photographed by the electron beam detection unit 4 (S106). Regarding the processing of S106, the edge extraction processing described in the principle may be used.

  The calibration data creation unit 30 calculates a correction coefficient using the measurement result of the reference template 9a in S106 and the known reference data related to the reference template 9a (described in the principle section), and is photographed by the electron beam apparatus 10. Stereo image calibration data is created (S108). Based on the calibration data, the calibration unit 40 calibrates the electron beam apparatus 10 so as to reduce the aberration of the sample image detected by the electron beam detection unit 4 (S110).

  Next, the sample (measurement object) 9 is placed on the sample holder 3 (S112). Then, the electron beam 7 or the sample holder 3 is placed in a desired inclination state, and the sample 9 is photographed by the electron beam detector 4 (S114). For example, when a three-dimensional image measurement of the sample 9 is performed, a desired tilt state is selected such that an angle with a small blind spot or an angle at which a target to be measured is particularly well photographed. Then, based on the stereo image of the sample 9 in a desired tilt state, the form or coordinate value of the sample 9 is obtained (S116). This processing can be obtained by stereo matching processing from two stereo images.

[Stereo matching processing]
Next, as an example of stereo matching processing, a matching method using an area-based normalized correlation coefficient will be described with reference to FIG. FIG. 13 is an explanatory diagram of the matching method using the normalized correlation coefficient. In the figure, the right image is a reference image and the left image is a search image. Here, M is a reference data block in a reference image composed of N pieces of data, and I is a search data block in a search image starting from coordinates (U, V).

  In the matching method using the normalized correlation coefficient, the similarity between the reference data block M and the search data block I at each position is obtained from the correlation coefficient while performing a raster scan of the reference data block M in the search data block I. Is the method. Here, the raster scanning means that the reference data block M is moved from the left to the right in the search data block I, goes down to the right end of the search data block I, returns to the left end, and the search data block I is moved from the left to the right. The scanning state moved to. If the maximum position of the correlation coefficient value R is searched, the same location as the reference data block M in the search data block I can be searched.

M = M (Xi, Yi) 1 ≦ i ≦ N (8)
I = I (U + Xi, V + Yi) (9)
Then, the normalized correlation coefficient R (U, V) is
R (U, V) = (NΣIiMi−ΣIiΣMi)
/ SQRT [{NΣIi ² − (ΣIi) ² } × {NΣMi ² − (ΣMi) ² }] (10)
It becomes. The correlation coefficient value R always takes a value from −1 to +1. When the correlation coefficient value R is +1, the template and the search image are completely matched.

Then, the correction coefficient calculation unit 62 (see FIG. 1) uses the selected reference image and uses the correspondence relationship of the stereo pair image with respect to the non-reference image of the inclined image that is a stereo pair. A first correction coefficient for determining the reference image as an image distortion state of the reference image is obtained. The obtained first correction coefficient is stored in, for example, the correction coefficient storage unit 64 in a state where it can be used by the measurement unit 20, the form / coordinate measurement unit 50, and the image correction unit 60, for example. The first correction coefficient is modeled using points detected by the parallel projection calibration method, approximated by a curve approximation method using the least square method, affine transformation, etc., and the coefficient used for the approximation is calculated. The coefficient for performing the image conversion process while correcting the image distortion by various arithmetic processes such as a calculation method is obtained.
In order to observe the sample, a stereo image of the sample 9 is displayed on the display device 28 based on the electron beam detected by the electron beam detector 4 (S118). If the form or coordinate value of the sample 9 can be acquired, a return is returned (S120).

The image correction unit 60 uses the correction coefficient calculated by the correction coefficient calculation unit 62 without using the calibration data creation unit 30, the calibration unit 40, and the electron lens aberration compensation unit 42 described so far. If correct correction is possible by correcting the image and obtaining a three-dimensional measurement value in the form / coordinate measurement unit 50, they may be omitted.
In that case, it is not necessary to calibrate the electron beam system based on the calibration data creation in S108 and the calibration data in S110 in the flowchart of FIG.

[Parallel projection]
Here, parallel projection, which is a precondition for the calibration procedure of the electron beam apparatus, will be described. Since the electron microscope has a wide range of magnifications from low magnification to high magnification (ex. 2 to several million times), the electron optical system 2 can be regarded as center projection at low magnification and parallel projection at high magnification. The magnification that can be regarded as parallel projection is preferably determined based on the calculation accuracy of the deviation correction parameter. For example, 1000 or 10000 times is used as the reference magnification. The displacement correction parameter is a parameter for correcting the displacement of the left and right images of the sample so that the stereoscopic image can be stereoscopically viewed.

FIG. 14 is an explanatory diagram of parallel projection. In the case of parallel projection, if the coordinate system (X _R , Y _R , Z _R ) taking rotation into consideration is used as the target coordinate system 74 and K1 and K2 are selected as the scale factors, the following equation is established.
Then, using the origin (Xo, Yo, Zo) selected in the target coordinate system 74 and the orientation matrix A, it can be expressed as follows.
Here, for the elements a i, j of the orientation matrix A, the inclinations ω, φ, κ of the rotation matrix elements a i, j with respect to the three axes X, Y, Z constituting the target coordinate system 74 of the image coordinate system 72 are used. And can be expressed as:

In the calculation of the displacement correction parameter, six external orientation elements ω, φ, κ, Xo, Yo, and Zo included in the expressions (11) and (12) are obtained. In other words, these six external orientation elements are calculated from the above equations by forming an observation equation by using at least three reference marks and sequentially resolving them. Specifically, an approximate value of an unknown variable is given, Taylor expansion around the approximate value is linearized, a correction amount is obtained by the least square method, the approximate value is corrected, and the same operation is repeated to obtain a convergence solution These six external orientation elements can be obtained by an approximate solution method. Further, in place of the equations (11) and (12), the calculation may be performed by appropriately adopting from various arithmetic expressions used as external orientation in single photo orientation, relative orientation, and other aerial triangulation.

  FIG. 15 is a block diagram illustrating a second embodiment of the present invention. In the figure, the electron beam system includes the measurement unit 20, the calibration data creation unit 30, the known reference data storage unit 32, the calibration unit 40, the electron lens aberration compensation unit 42, the form / coordinate measurement unit 50, the image correction unit 60, A correction coefficient calculation unit 62, a correction coefficient storage unit 64, and a correction coefficient inference unit 54 are provided. Here, the calibration data creation unit 30, the known reference data storage unit 32, the calibration unit 40, the correction coefficient calculation unit 62, the correction coefficient storage unit 64, the correction coefficient inference unit 54, and the like constitute a data processing unit.

Although the correction coefficient storage unit 64 stores correction coefficients such as the tilt angle, magnification, and electron optical system for each tilt angle, the correction coefficient inference unit 54 stores the tilt angles that are not stored. These correction coefficients are obtained by inferring (interpolating) from the correction coefficients.
Inference (interpolation) can be performed by creating a correction function for each coefficient by curve fitting or other methods. By adding this function, it is possible to perform accurate three-dimensional measurement in which an image is captured and corrected at any tilt angle.

  Next, a procedure for calibrating the electron beam apparatus necessary for stereo image measurement by the apparatus configured as described above will be described with reference to FIG. FIG. 16 is a flowchart of electron beam measurement including a calibration procedure for the electron beam apparatus according to the third embodiment of the present invention. FIG. 16 shows a processing flow in which the electron beam apparatus is calibrated using the reference template 9a and then the sample image measurement is performed (S200). First, S202 to S210 are the same as those described in S102 to S110. That is, the reference template 9a is placed on the sample holder 3, and the sample holder 3 or the electron beam 7 is shifted to an inclined state (S202). The measurement unit 20 acquires an inclined image of the reference template 9a obtained from the electron beam detection unit 4 (S204). Then, the measurement unit 20 obtains the form or coordinate value of the reference template 9a based on the image of the reference template 9a photographed by the electron beam detection unit 4 (S206). The calibration data creation unit 30 calculates a correction coefficient using the measurement result of the reference template 9a in S206 and the known reference data related to the reference template 9a, and obtains calibration data of an image photographed by the electron beam apparatus 10. Create (S208). The calibration unit 40 calibrates the electron beam apparatus 10 based on the calibration data so as to reduce the aberration of the sample image detected by the electron beam detection unit 4 (S210). The correction coefficient calculation unit 62 calculates a correction coefficient for an image photographed by the electron beam detection unit 4 for a plurality of tilt states formed by the sample tilting unit 5, stores the correction coefficient in the correction coefficient storage unit 64, and corrects the correction coefficient. The inference unit 54 creates correction functions based on the inclination angles of various correction coefficients (S212).

  Next, the sample (measurement object) 9 is placed on the sample holder 3 (S214). Then, the electron beam 7 or the sample holder 3 is set in a desired inclination state, and the sample 9 is photographed by the electron beam detector 4 (S216). For example, when a three-dimensional image measurement of the sample 9 is performed, a desired tilt state is selected such that an angle with a small blind spot or an angle at which a target to be measured is particularly well photographed. Then, based on the stereo image of the sample 9 in a desired tilt state, the rough measurement unit 52 obtains the form or coordinate value of the sample 9 (S218).

If the form or the coordinate value of the sample 9 can be acquired precisely, a return is returned (S226). Preferably, a stereo image corrected by the image correction unit 60 is displayed on the display device 28 in order to observe the sample.
In the case where a plurality of inclinations are used, not only stereo matching but also multi-matching (corresponding points are obtained from images from two or more images and coordinates are measured) may be performed. Of course, these correction coefficients are also used in this case.
Further, the tilt direction may be tilted not only in the uniaxial direction but also in a perpendicular direction and an oblique direction as shown in FIG. 20, and the correction coefficients may be calculated to correspond to tilts in all directions.
Further, as a correspondence to the plurality of directions, the reference template may be corrected with the reference template mixedly mounted in a plurality of directions as shown in FIG. Since these processes are the same only when the direction is increased to a plurality of directions, the description is omitted.

FIG. 17 is an overall configuration block diagram for explaining the third embodiment of the present invention. In the first and second embodiments, the holder is tilted when a stereo image is obtained. However, the third embodiment shows a case where a stereo image is obtained by deflecting an electron beam of a scanning microscope. Here, in FIG. 17, the same components as those in FIG. Here, a beam tilt control unit 5 a is provided as the tilt control unit 5 that controls the tilt of the electron beam 7. The beam tilt control unit 5a sends a tilt control signal to the deflecting lens 2b, and the electron beam 7R having the first relative tilt angle between the sample holder 3 and the irradiation electron beam 7 and the electron having the second relative tilt angle. Switching with line 7L. Note that the relative tilt angle between the sample holder 3 and the irradiation electron beam 7 by the beam tilt control unit 5a is not limited to two but may be set in multiple stages, but at least two are necessary to obtain stereo detection data. is there.

  FIG. 18 is an overall configuration block diagram for explaining the fourth embodiment of the present invention. In addition to the measurement unit 20 described in the first embodiment, the electron beam system includes a form / coordinate measurement unit 50, an image correction unit 60, a correction coefficient calculation unit 62, a correction coefficient storage unit 64, a third measurement unit, It has. Further, a correction coefficient inference unit 54 is added. Others are the same as those in FIG. 15 except that the sample tilt is changed to the beam tilt. In FIG.

  Since the operation of the apparatus of the fourth embodiment configured in this way is the same as the flowchart of FIG. 16 except that the beam is tilted instead of tilting the sample, the description thereof is omitted.

In the above embodiment, as the calibration data of the electron beam system created by the calibration data creation unit, the calibration data of the tilt amount of the sample tilting unit 5 and the irradiation direction of the irradiation electron beam 7 of the electron optical system 2 Although the calibration data, the calibration data regarding the magnification of the electron optical system 2 and the calibration data regarding the distortion correction of the electron optical system 2 are shown, the present invention is not limited to this, and in short, the calibration created by the calibration data creation unit The data may be any data that can be calibrated by the calibration unit so as to reduce the aberration of the sample image detected by the electron beam detection unit 4.
In these embodiments as well, the image correction unit 60 uses the correction coefficient calculated by the correction coefficient calculation unit 62 without performing calibration using the calibration data creation unit 30, the calibration unit 40, and the electron lens aberration compensation unit 42. If correct correction is possible by correcting the image and obtaining a three-dimensional measurement value in the form / coordinate measurement unit 50, they may be omitted.

BRIEF DESCRIPTION OF THE DRAWINGS It is a whole block diagram explaining Example 1 of this invention. It is explanatory drawing of the inclination state in the sample holder of an electron beam system. 3 is a perspective view for explaining a coordinate system of a sample holder 3. FIG. It is a front view which shows the relationship between an image and a sample when the measurement object 9 is irradiated with an electron beam. As a stereo image shooting direction, a case where the left and right images have an angle with the Z axis interposed therebetween is shown. As a stereo image capturing direction, the left and right images are inclined by θ1 and θ2 with respect to the Z axis, respectively. It is a top view of the reference | standard template which comprised the line & space. It is a figure explaining the pitch space | interval and inclination of the reference | standard template of FIG. The shape of the unevenness, that is, the interval L between the unevenness (pitch interval L in the case of a line & space pattern), the height h of the unevenness, the taper angle φ, etc. It is a figure which extracts and shows the side surface of the reference | standard template of FIG. It is a figure which shows the example of the reference | standard template which mixedly mounted the reference | standard template as shown in FIG. 7 in several directions. It is a pre-process flowchart explaining the example of the procedure which calculates | requires an exact three-dimensional shape. It is a flowchart of the electron beam measurement including the calibration procedure of the electron beam apparatus in Example 1 of this invention. It is explanatory drawing of the matching method by a normalized correlation coefficient. It is explanatory drawing of parallel projection. It is a block diagram explaining a second embodiment of the present invention. It is a flowchart of the electron beam measurement including the calibration procedure of the electron beam apparatus in Example 2 of this invention. It is a whole block diagram explaining Example 3 of the present invention. It is a whole block diagram explaining Example 4 of the present invention. It is a figure explaining the type | formula which carries out the linear approximation of the boundary part of the side surface and upper surface of a reference | standard template like FIG. 7, and a side surface and a bottom face. It is a figure which shows that an inclination direction may be made to incline not only in a uniaxial direction but in a right angle direction and an oblique direction. It is a top view which shows the example which actually detected the edge.

Explanation of symbols

9 Sample (object to be measured)
9a Reference template 10 Electron beam device 20 Measurement unit 30 Calibration data creation unit 40 Calibration unit 50 Form / coordinate measurement unit 52 Approximate measurement unit 54 Precision measurement unit 60 Image correction unit 64 Correction coefficient storage unit

Claims (11)

An electron beam source for emitting an electron beam;
An electron optical system that converges the electron beam emitted from the electron beam source and irradiates the sample;
A detector for receiving electrons from the sample irradiated with the electron beam;
A sample support for supporting the sample;
A sample tilting section for relatively tilting the electron beam irradiated to the sample supported by the sample support section and the sample;
A detection signal from the detection unit that receives electrons from a reference sample having at least two inclined surfaces supported by the sample support unit so as to allow the relative inclination is received for each inclination, and the inclination is performed. A data processing unit for obtaining an inclination angle of the reference sample from two-plane images and a reference dimension of the reference sample;
Electron beam system. The electron beam system according to claim 1, wherein the data processing unit is further configured to obtain a magnification of the sample image. The data processing unit is configured to obtain a correction coefficient for the sample inclination amount based on the obtained inclination angle, and to correct the inclination angle based on the correction coefficient for the sample inclination amount. The electron beam system described in 1. The data processing unit obtains a correction coefficient for the sample inclination amount with respect to the inclination between the measured inclination angles based on the obtained plurality of inclination angles, and the sample inclination amount with respect to an inclination angle other than the measured inclination angle. The electron beam system according to claim 3, wherein the electron beam system is configured to perform correction. An electron beam source for emitting an electron beam;
An electron optical system that converges the electron beam emitted from the electron beam source and irradiates the sample;
A detector for receiving electrons from the sample irradiated with the electron beam;
A sample support for supporting the sample;
A sample tilting section for relatively tilting the electron beam irradiated to the sample supported by the sample support section and the sample;
A detection signal from the detection unit that receives electrons from a reference sample having at least two inclined surfaces supported by the sample support unit so as to allow the relative inclination is received for each inclination, Based on the image of the image where the displacement in the electron beam optical system is small due to the tilt of the sample, the tilt of the reference sample is determined from the two tilted images in the image and the reference dimension of the reference sample. A data processing unit that performs processing for obtaining an angle, processing for obtaining a correction coefficient based on a difference between the magnification at the inclination angle of the peripheral image and the magnification of the image based on the detection signal;
Electron beam system. The sample tilting part performs either tilt control of a sample holder that tilts the sample with respect to the electron beam or deflection control of the electron beam that causes the electron beam to be irradiated to the sample at different angles. The electron beam system according to claim 1 or 5, which is configured as described above. The electron according to claim 5, wherein the data processing unit includes an image forming unit that forms a sample image in which electronic lens distortion, scan distortion, and the like are corrected based on a signal from the electron beam detection unit using a correction coefficient. Line system. The electron beam system according to claim 5, wherein the data processing unit is configured to obtain, by interpolation, a correction coefficient for an inclination for which measurement has not been performed, in addition to a correction coefficient for the inclination for which measurement has been performed. The said reference sample is a pattern which consists of a bottom part with a predetermined taper angle, a top part, and the side part which connects this, The dimension of each part, the angle of a side part, and height are known. Reference sample used in the electron beam system. The reference sample used for the electron beam system according to claim 9, wherein the pattern is composed of a line and space pattern. The reference sample used for the electron beam system according to claim 9, wherein the line and space pattern is formed in a direction orthogonal to the inclination direction of the sample.