JP2005333885A - Paste material composition - Google Patents

Paste material composition Download PDF

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JP2005333885A
JP2005333885A JP2004157638A JP2004157638A JP2005333885A JP 2005333885 A JP2005333885 A JP 2005333885A JP 2004157638 A JP2004157638 A JP 2004157638A JP 2004157638 A JP2004157638 A JP 2004157638A JP 2005333885 A JP2005333885 A JP 2005333885A
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paste
viscosity
composition
gum
dispersed
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JP4535779B2 (en
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Yoshinori Seko
義則 瀬古
Hideji Nishikawa
秀二 西川
Tomohiro Kimura
友宏 木村
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Taiyo Kagaku KK
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Taiyo Kagaku KK
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Abstract

<P>PROBLEM TO BE SOLVED: To obtain a paste material composition capable of rapidly developing viscosity or gelation by adding it to an object containing water. <P>SOLUTION: The above problem is solved by containing glycerol and propylene glycol or/and ethanol into the composition. The composition containing the paste material in a high ratio can disperse the paste material having high viscosity in liquid state in a high concentration and develops viscosity by adding a small amount of the composition to the object and does not form undissolved lump when the composition is dissolved in the object. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

本発明は、水を含む目的物に添加して簡便に粘性やゲル化を発現させる糊料組成物に関わり、特に清涼飲料、たれ、ソース、ドレッシング、汁物、ムース、ゼリー等を簡便に増粘させる食品用途や、摂食障害により咀嚼・嚥下困難となった患者の食事等に少量添加して粘性やゲル化を発現させる用途に適した糊料組成物に関する。   The present invention relates to a paste composition that can be easily added to an object containing water to develop viscosity and gelation, and in particular, can easily thicken soft drinks, sauces, sauces, dressings, soups, mousses, jelly, etc. The present invention relates to a paste composition suitable for food applications to be used, and for applications in which a small amount is added to a meal or the like of a patient who has difficulty chewing or swallowing due to eating disorders to develop viscosity or gelation.

従来より多くの糊料が増粘安定目的で様々な食品用途に使用されている。糊料は一般的に水に分散・溶解させることにより、その機能を発揮する。しかしながら、一般消費者が糊料を食品等に添加・溶解する際には糊料が粉末の場合ダマになりやすく、ダマになった糊料はその機能を発揮できない状態になりやすい。また、液状に調製された添加液では、糊料の分散割合が少なく10〜20%程度の添加が必要であった。   Many pasting agents have been used for various food applications for the purpose of thickening and stabilizing. In general, the paste exhibits its function by being dispersed and dissolved in water. However, when a general consumer adds or dissolves a paste to foods or the like, the paste tends to be lumped if the paste is a powder, and the lumped glue tends to fail to perform its function. In addition, the additive solution prepared in a liquid form has a small dispersion ratio of the paste and needs to be added in an amount of about 10 to 20%.

糊料を水に分散・溶解する技術として、エタノールに分散し、水等の目的物に分散・溶解する技術が知られている。この方法で、エタノールに糊料を高濃度分散させた場合には、分散状態を保つ為に撹拌が必要となり、撹拌しない状態では糊料は沈殿し、沈殿した糊料の分散性・粘度発現性は著しく低下する。また、粘度をつけたい目的物にも撹拌が必要で、静置した状態で添加した場合には粉末の状態と同様にダマになってしまう。また、工業的にはグリセリンに分散する方法も知られているが、グリセリンに糊料を高濃度分散させた場合には糊料は20%以下の濃度でしか分散できず、経時的に粘性が発現し流動性はなくなってしまう。   As a technique for dispersing and dissolving the paste in water, a technique is known in which it is dispersed in ethanol and then dispersed and dissolved in a target product such as water. In this method, when a high concentration of paste is dispersed in ethanol, stirring is necessary to maintain the dispersed state, and in the state without stirring, the paste is precipitated, and the dispersibility / viscosity of the precipitated paste Is significantly reduced. Moreover, stirring is required also for the target object to which viscosity is to be added, and when it is added in a stationary state, it becomes lumpy like the powder state. In addition, industrially, a method of dispersing in glycerin is also known, but when a high concentration of paste is dispersed in glycerin, the paste can be dispersed only at a concentration of 20% or less, and the viscosity of the paste increases with time. Appears and loses fluidity.

液状に調製された増粘用添加液では、水とエタノール等を分散剤に使用し、高粘性糊料を10%程度溶解するか、又は低粘性糊料を10%程度溶解し、その後高粘性糊料を5%程度併用することで粘性発現を抑制し流動性のある液体として調製されている(例えば特許文献1参照。)。その為、増粘させる目的物への添加割合が10〜20%程度の添加割合が必要であった。また、目的物に10〜20%増粘用添加液を添加した場合、最終食品の味を阻害することとなった。
特開2000−41594号公報(第3−4頁)
In the additive solution for thickening prepared in a liquid state, water and ethanol are used as the dispersant, and about 10% of the high-viscosity paste is dissolved, or about 10% of the low-viscosity paste is dissolved, and then the high viscosity is obtained. It is prepared as a fluid liquid that suppresses the expression of viscosity by using about 5% of a paste (see, for example, Patent Document 1). Therefore, an addition ratio of about 10 to 20% is necessary for the target to be thickened. Moreover, when the 10-20% thickening additive solution was added to the target product, the taste of the final food was inhibited.
JP 2000-41594 A (page 3-4)

従って、粉体の場合のようにダマになることなく、目的物の味を阻害しないよう少量の添加で粘性又はゲル化を発現する組成物が求められている。特に咀嚼・嚥下困難者の介護食や訓練食に粘性や凝固を与える糊料として、そのような特性が強く求められる。本発明は、水を含む目的物に添加し、速やかに粘性又はゲル化を発現する事が可能な糊料組成物を提供する事を目的とする。   Therefore, there is a demand for a composition that can be viscous or gelled with a small amount of addition so as not to disturb the taste of the target product without becoming lumpy as in the case of powder. In particular, such characteristics are strongly demanded as a paste that gives viscosity and coagulation to nursing food and training food for those who have difficulty chewing or swallowing. An object of this invention is to provide the paste composition which can be added to the target object containing water and can express viscosity or gelatinization rapidly.

本発明者らは、高粘性糊料の高濃度分散液と水分を含む目的物に添加した際の速やかな粘性又はゲル化の発現について鋭意研究した結果、グリセリン、プロピレングリコール、エタノールの組み合わせによるバランスで解決できることを見出した。   As a result of intensive research on the rapid expression of viscosity or gelation when added to a high-concentration dispersion of high-viscosity paste and moisture, the present inventors have found that the balance by a combination of glycerin, propylene glycol and ethanol I found out that it can be solved.

糊料組成物を作るにあたって問題になるのは、水分を含む目的物に添加し速やかに粘性又はゲル化を発現できるように1.高粘性糊料が高濃度で均一に分散していること2.組成物の粘性が一定で流動性をたもっていることがあげられる。さらに3.分散した高粘性糊料が膨潤している状態であることが好ましい。
糊料を高濃度分散させるためには、貧溶媒を用いて分散させる方法が知られている。従来より糊料の製造方法として、水溶液として抽出された糊料をエチルアルコール等を用いて沈殿させる方法が用いられている。貧溶媒を用いれば糊料の粘性発現を抑制することができ、高濃度で分散させることは可能であるが分散した状態は維持できない。糊料を均一に分散し、また水を含む目的物に添加して速やかに粘性又はゲル化を発現させるためには組成物が適度な粘性を有する必要がある。その粘性は低ければ組成物自体が分離し、高ければ水等の目的物に分散できない。
加えて水等の目的物を速やかに粘性発現するためには組成物中の糊料が膨潤していることが望ましい。グリセリンに糊料を分散させ、目的物に溶解し粘性を発現させる方法は工業的に行われている。グリセリンに糊料を分散させる際には糊料20%程度は分散し膨潤させることができる。しかし、分散後経時的に組成物の粘度は上昇し、最終的には凝固してしまう。水等の目的物に速やかに粘性またはゲル化を発現させるためには、グリセリン中で糊料を膨潤状態とし、組成物の粘度上昇を抑える必要がある。本発明では、溶媒としてグリセリンとプロピレングリコール及び/またはエタノールをバランスよく配合することで上記1〜3を解決した。
The problem in making a paste composition is that it can be quickly added to a target object containing water so that viscosity or gelation can be developed. 1. Highly viscous paste is uniformly dispersed at a high concentration. It is mentioned that the viscosity of the composition is constant and fluid. Furthermore, 3. The dispersed high-viscosity paste is preferably in a swollen state.
In order to disperse the paste at a high concentration, a method of dispersing using a poor solvent is known. Conventionally, as a method for producing a paste, a method of precipitating a paste extracted as an aqueous solution using ethyl alcohol or the like has been used. If a poor solvent is used, the viscosity of the paste can be suppressed and can be dispersed at a high concentration, but the dispersed state cannot be maintained. In order to disperse the paste uniformly and to quickly add viscosity or gelation by adding it to the object containing water, the composition needs to have an appropriate viscosity. If the viscosity is low, the composition itself is separated. If the viscosity is high, the composition cannot be dispersed in a target such as water.
In addition, it is desirable that the paste in the composition is swollen in order to rapidly develop a target such as water. A method in which a paste is dispersed in glycerin and dissolved in a target product to develop viscosity is industrially performed. When the paste is dispersed in glycerin, about 20% of the paste can be dispersed and swollen. However, the viscosity of the composition increases over time after dispersion, and eventually solidifies. In order to quickly develop viscosity or gelation in a target product such as water, it is necessary to make the paste swell in glycerin to suppress an increase in the viscosity of the composition. In this invention, said 1-3 were solved by mix | blending glycerol and propylene glycol and / or ethanol as a solvent with sufficient balance.

本発明には、実質的に水分を含まない成分Aと成分Bが用いられる。
成分A:糊料または糊料及び塩類。
成分B:グリセリンと、プロピレングリコール及び/またはエタノール。
本発明における糊料は、粉末状に化工された通常食品に使用されている糊料であれば特に限定するものではないがキサンタンガム、グアーガム、ローカストビーンガム、タラガム、タマリンドガム、カラヤガム、ペクチン、カラギナン、アルギン酸ナトリウム、サイリウムシードガム、CMC、CMCナトリウム、コンニャク粉、澱粉、ゼラチンがあげられ、目的物に少量添加し粘性を発現させる点からキサンタン、タラガム、グアーガム、カラギナンが好ましい。特に限定するものではないが、20℃のイオン交換水に0.5%分散溶解した溶液のB形粘度計(東京計器製)で測定した粘度が100mPa・s以上のものが目的物への粘度調製の点で好ましい。
本発明における塩類とは、粉末状に加工され一般的に食品に使用されるものであれば特に限定するものではないが、塩化ナトリウム、塩化カリウム、クエン酸一カリウム、クエン酸三カリウム、クエン酸カルシウム、クエン酸三ナトリウム、酢酸ナトリウム、DL−酒石酸水素カリウム、L−酒石酸水素カリウム、焼成カルシウム、未焼成カルシウム、水酸化カルシウム、炭酸カリウム、炭酸カルシウム、炭酸水素ナトリウム、乳酸カルシウム、ピロリン酸四カリウム、ピロリン酸四ナトリウム、ピロリン酸二水素二ナトリウム、ポリリン酸カリウム、ポリリン酸ナトリウム、メタリン酸カリウム、メタリン酸ナトリウム、リン酸三カリウム、リン酸三カルシウム、リン酸三ナトリウム、リン酸水素二アンモニウム、リン酸二水素アンモニウム、リン酸水素二カリウム、リン酸二水素カリウム、リン酸一水素カルシウム、リン酸二水素カルシウム、リン酸水素二ナトリウム、硫酸カルシウムがあげられる。糊料と塩類の配合比については特に限定されるものではないが通常100:0〜100:50、好ましくは100:0〜100:20である。
In the present invention, component A and component B substantially free of moisture are used.
Component A: Paste or paste and salts.
Component B: Glycerin and propylene glycol and / or ethanol.
The paste in the present invention is not particularly limited as long as it is a paste used in ordinary foods processed into a powder form, but xanthan gum, guar gum, locust bean gum, tara gum, tamarind gum, caraya gum, pectin, carrageenan , Sodium alginate, psyllium seed gum, CMC, CMC sodium, konjac flour, starch and gelatin. Xanthan, tara gum, guar gum and carrageenan are preferred from the viewpoint of adding a small amount to the target substance to develop viscosity. Although not particularly limited, a solution obtained by dispersing and dissolving 0.5% in 20 ° C. ion-exchanged water with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd.) having a viscosity of 100 mPa · s or more is a viscosity to the target product. Preferred in terms of preparation.
Salts in the present invention are not particularly limited as long as they are processed into powder and generally used in foods, but sodium chloride, potassium chloride, monopotassium citrate, tripotassium citrate, citric acid Calcium, trisodium citrate, sodium acetate, DL-potassium hydrogen tartrate, potassium potassium L-tartrate, calcined calcium, uncalcined calcium, calcium hydroxide, potassium carbonate, calcium carbonate, sodium bicarbonate, calcium lactate, tetrapotassium pyrophosphate , Tetrasodium pyrophosphate, disodium dihydrogen pyrophosphate, potassium polyphosphate, sodium polyphosphate, potassium metaphosphate, sodium metaphosphate, tripotassium phosphate, tricalcium phosphate, trisodium phosphate, diammonium hydrogen phosphate, Ammonium dihydrogen phosphate , Dipotassium hydrogen phosphate, potassium dihydrogen phosphate, calcium hydrogen phosphate, calcium dihydrogen phosphate, disodium hydrogen phosphate, calcium sulfate and the like. The blending ratio of the paste and the salt is not particularly limited, but is usually 100: 0 to 100: 50, preferably 100: 0 to 100: 20.

本発明における流動性のある状態とは、保存時に液体状糊料を注入した透明容器を横に倒した際に、液体状糊料がゆっくりと流れることが可能な程度をいう。好ましくは、B形粘度計(東京計器製)で測定した粘度が300〜5,000mPa・s程度のものをいう。流動性を保つためのグリセリン、プロピレングリコール及び/またはエタノールの割合は特に限定するものではないが、グリセリン100に対し60〜140の範囲でプロピレングリコール及び/またはエタノールを配合する事が好ましい。   The fluid state in the present invention refers to the extent to which the liquid paste can flow slowly when the transparent container into which the liquid paste has been poured is stored. Preferably, the viscosity measured with a B-type viscometer (manufactured by Tokyo Keiki) is about 300 to 5,000 mPa · s. The ratio of glycerin, propylene glycol and / or ethanol for maintaining fluidity is not particularly limited, but it is preferable to blend propylene glycol and / or ethanol in the range of 60 to 140 with respect to glycerin 100.

本発明における少量の添加で速やかに粘度を発現できる状態とは、水を含む目的物に対して通常液体状糊料5%以下、好ましくは液体状糊料2%以下の添加量で粘度を発現させる事を可能にしたことをいい、B形粘度計(東京計器製:回転速度30rpm、30秒後、No.3ローター)で測定した粘度が1,000mPa・s以上発現する状態をいう。   In the present invention, the state where the viscosity can be quickly expressed with a small amount of addition means that the viscosity is expressed with an addition amount of usually 5% or less of liquid paste, preferably 2% or less of liquid paste with respect to the object containing water. It means that the viscosity measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 3 rotor) is manifested at 1,000 mPa · s or more.

以下、実施例及を示して本発明を具体的に説明するが、本発明は下記実施例に制限されるものではない。   EXAMPLES Hereinafter, the present invention will be specifically described with reference to examples, but the present invention is not limited to the following examples.

第一に、目的物に加えて簡単に粘性を発現できる方法について述べる。
実施例1
グリセリン30g、プロピレングリコール30gを混合した分散剤に、キサンタンガム35gと塩化カリウム5gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ2,240mPa・sであり、室温にて1ヶ月保存し再度粘度を測定したところ1,960mPa・sであった。この液体状糊料6gをイオン交換水294gに投入し、低回転ディスパー(特殊機化工業製)で600rpm、1分間分散し5分間静置後の粘度を測定したところ3,920mPa・sであった。また、1ヶ月室温保存した液体状糊料を同様にイオン交換水に分散溶解したところ3,880mPa・sであった。
First, a method that can easily develop viscosity in addition to the object will be described.
Example 1
In a dispersant in which 30 g of glycerin and 30 g of propylene glycol were mixed, 35 g of xanthan gum and 5 g of potassium chloride were dispersed to prepare 100 g of a liquid paste. When the viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor), it was 2,240 mPa · s. When the viscosity was measured, it was 1,960 mPa · s. When 6 g of this liquid paste was put into 294 g of ion-exchanged water, dispersed at 600 rpm for 1 minute with a low rotation disper (manufactured by Tokushu Kika Kogyo Co., Ltd.), and the viscosity after standing for 5 minutes was measured, it was 3,920 mPa · s. It was. Further, when the liquid paste stored at room temperature for 1 month was similarly dispersed and dissolved in ion-exchanged water, it was 3,880 mPa · s.

実施例2
実施例1と同様にプロピレングリコールに一部をエタノールで置き換えた試験を実施した。
グリセリン30g、プロピレングリコール20g、エタノール10gを混合した分散剤に、キサンタンガム35gと塩化カリウム5gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ1,680mPa・sであり、室温にて1ヶ月保存し再度粘度を測定したところ1,540mPa・sであった。この液体状糊料6gをイオン交換水294gに投入し、低回転ディスパー(特殊機化工業製)で600rpm、1分間分散し5分間静置後の粘度を測定したところ3,440mPa・sであった。また、1ヶ月室温保存した液体状糊料を同様にイオン交換水に分散溶解したところ3,260mPa・sであった。
Example 2
In the same manner as in Example 1, a test was conducted in which part of propylene glycol was replaced with ethanol.
100 g of a liquid paste was prepared by dispersing 35 g of xanthan gum and 5 g of potassium chloride in a dispersant in which 30 g of glycerin, 20 g of propylene glycol and 10 g of ethanol were mixed. When the viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor), it was 1,680 mPa · s. When the viscosity was measured, it was 1,540 mPa · s. 6 g of this liquid paste was put into 294 g of ion-exchanged water, dispersed at 600 rpm for 1 minute with a low rotation disper (manufactured by Tokushu Kika Kogyo), and the viscosity after standing for 5 minutes was measured to be 3,440 mPa · s. It was. Moreover, when the liquid paste preserve | saved at room temperature for 1 month was similarly disperse-dissolved in ion-exchange water, it was 3,260 mPa * s.

実施例3
実施例1のキサンタンガムをグアーガムに置換え同様の試験を実施した。
グリセリン30g、プロピレングリコール30gを混合した分散剤に、グアーガム40gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ2,380mPa・sであり、室温にて1ヶ月保存し再度粘度を測定したところ2,320mPa・sであった。この液体状糊料6gをイオン交換水294gに投入し、低回転ディスパー(特殊機化工業製)で600rpm、1分間分散し5分後の粘度を測定したところ2,100mPa・sであった。また、1ヶ月室温保存した液体状糊料を同様にイオン交換水に分散溶解したところ2,050mPa・sであった。
Example 3
A similar test was conducted by replacing the xanthan gum of Example 1 with guar gum.
40 g of guar gum was dispersed in a dispersant in which 30 g of glycerin and 30 g of propylene glycol were mixed to prepare 100 g of a liquid paste. When the viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotation speed 30 rpm, 30 seconds later, No. 4 rotor), it was 2,380 mPa · s. It was 2,320 mPa * s when the viscosity was measured. 6 g of this liquid paste was put into 294 g of ion-exchanged water, dispersed at 600 rpm for 1 minute with a low rotation disper (manufactured by Tokushu Kika Kogyo Co., Ltd.), and the viscosity measured after 5 minutes was 2,100 mPa · s. Further, when the liquid paste stored at room temperature for 1 month was similarly dispersed and dissolved in ion-exchanged water, it was 2,050 mPa · s.

比較例1
比較例としてグリセリン、プロピレングリコール、エタノールを各々単独で分散剤とした試験例を示した。
グリセリン60gを溶媒としキサンタンガム35g、塩化カリウム5gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ20,000mPa・s以上となり測定限界を超える高い粘度となった。また、1ヶ月室温保存した液体状糊料は固化し流動性はなかった。
Comparative Example 1
As a comparative example, a test example using glycerin, propylene glycol, and ethanol alone as a dispersant was shown.
Using 60 g of glycerin as a solvent, 35 g of xanthan gum and 5 g of potassium chloride were dispersed to prepare 100 g of a liquid paste. When the viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor), the viscosity was 20,000 mPa · s or higher, which was a high viscosity exceeding the measurement limit. . Moreover, the liquid paste which was stored at room temperature for 1 month was solidified and was not fluid.

比較例2
プロピレングリコール60gを溶媒としキサンタンガム35g、塩化カリウム5gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ260mPa・sであった。1ヶ月室温保存した液体状糊料はキサンタンガムと塩化カリウムの沈殿が生じプロピレングリコールとの分離が発生し、同様にイオン交換水に分散溶解したところ820mPa・sであり、分散性も悪くダマが出現した。
Comparative Example 2
100 g of liquid paste was prepared by dispersing 35 g of xanthan gum and 5 g of potassium chloride using 60 g of propylene glycol as a solvent. The viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor) and found to be 260 mPa · s. Liquid paste that was stored at room temperature for 1 month caused precipitation of xanthan gum and potassium chloride, resulting in separation from propylene glycol. Similarly, when dispersed and dissolved in ion-exchanged water, it was 820 mPa · s, dispersibility was poor, and lumps appeared. did.

比較例3
エタノール60gを溶媒としキサンタンガム35g、塩化カリウム5gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ220mPa・sであった。1ヶ月室温保存した液体状糊料はキサンタンガムと塩化カリウムの沈殿が生じエタノールとの分離が発生し、同様にイオン交換水に分散溶解したところ690mPa・sであり、分散性も悪くダマが出現した。
Comparative Example 3
Using 60 g of ethanol as a solvent, 35 g of xanthan gum and 5 g of potassium chloride were dispersed to prepare 100 g of a liquid paste. The viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor) and found to be 220 mPa · s. The liquid paste stored at room temperature for 1 month caused precipitation of xanthan gum and potassium chloride, resulting in separation from ethanol. Similarly, when it was dispersed and dissolved in ion-exchanged water, it was 690 mPa · s. .

実施例1〜3、比較例1〜3の結果からグリセリンを単独で分散剤とした系では経時的に粘性が発現し1ヶ月後には固化していた。プロピレングリコールまたはエタノール単独では液状糊料に分離が発生し、イオン交換水への分散性も悪くなった。実施例ではグリセリン、プロピレングリコール、エタノールをバランスよく配合することにより液体状態を維持でき、イオン交換水への分散性も良好で、目的物に加えてすぐに粘性を発現できる状態にあることがわかった。   From the results of Examples 1 to 3 and Comparative Examples 1 to 3, in the system using glycerin alone as a dispersant, viscosity developed over time and solidified after one month. Propylene glycol or ethanol alone caused separation in the liquid paste, and the dispersibility in ion-exchanged water also deteriorated. In Examples, it was found that a liquid state can be maintained by blending glycerin, propylene glycol, and ethanol in a well-balanced manner, the dispersibility in ion-exchanged water is good, and a viscosity can be immediately developed in addition to the target product. It was.

第2に目的物に加えて簡単にゲル化を発現する方法について述べる
実施例4
グリセリン30g、プロピレングリコール30gを混合した分散剤に、キサンタンガム20gとタラガム20gを分散し液体状糊料100gを調製した。この液体状糊料の粘度をB形粘度計(東京計器製:回転速度30rpm、30秒後、No.4ローター)で測定したところ1,620mPa・sであり、室温にて1ヶ月保存し再度粘度を測定したところ1,540mPa・sであった。この液体状糊料2gをイオン交換水98gに投入し、撹拌・溶解した後10℃に冷却したところゲルを形成した。
Second, a method for easily expressing gelation in addition to the target product will be described. Example 4
100 g of liquid paste was prepared by dispersing 20 g of xanthan gum and 20 g of cod gum in a dispersant in which 30 g of glycerin and 30 g of propylene glycol were mixed. When the viscosity of this liquid paste was measured with a B-type viscometer (manufactured by Tokyo Keiki Co., Ltd .: rotational speed 30 rpm, 30 seconds later, No. 4 rotor), it was 1,620 mPa · s. When the viscosity was measured, it was 1,540 mPa · s. 2 g of this liquid paste was added to 98 g of ion-exchanged water, stirred and dissolved, and then cooled to 10 ° C. to form a gel.

飲食品への実施例
実施例5
実施例1で調製した液体状糊料を用い、表1に示した配合でフレンチドレッシングを調製した。各種の原料を簡単に混ぜ合わせることで粘性が発現し、簡単に粘性を発現させることが可能であった。
Example to food and drink Example 5
Using the liquid paste prepared in Example 1, a French dressing was prepared with the composition shown in Table 1. Viscosity was expressed by simply mixing various raw materials, and it was possible to easily develop viscosity.

Figure 2005333885
Figure 2005333885

以上述べたようにこの発明による糊料高含有製剤は、高粘性糊料を高濃度で液状に分散でき、目的物に少量の添加で粘度を発現させ、また溶解時にダマを生じさせないことを可能にした発明品である。   As described above, the high-paste-containing preparation according to the present invention can disperse a high-viscosity paste in a liquid form at a high concentration, can develop a viscosity with a small amount of addition to the target product, and does not cause lumps when dissolved This is an invention.

Claims (4)

次の成分A及びBを含有することを特徴とする糊料組成物。
成分A:糊料または糊料及び塩類。
成分B:グリセリンと、プロピレングリコール及び/またはエタノール。
A paste composition comprising the following components A and B:
Component A: Paste or paste and salts.
Component B: Glycerin and propylene glycol and / or ethanol.
請求項1記載の糊料が、キサンタンガム、グアーガム、ローカストビーンガム、タラガム、タマリンドガム、カラヤガム、ペクチン、カラギナン、アルギン酸ナトリウム、サイリウムシードガム、CMC、CMCナトリウム、コンニャク粉、澱粉、ゼラチンからなる群より選ばれる少なくとも一種以上であることを特徴とする請求項1記載の糊料組成物。 The paste according to claim 1 is selected from the group consisting of xanthan gum, guar gum, locust bean gum, tara gum, tamarind gum, karaya gum, pectin, carrageenan, sodium alginate, psyllium seed gum, CMC, CMC sodium, konjac powder, starch, gelatin. The paste composition according to claim 1, wherein the paste composition is at least one or more selected. 請求項1または2記載の糊料組成物を含有する増粘またはゲル化用組成物。 A composition for thickening or gelling containing the paste composition according to claim 1 or 2. 請求項3記載の増粘またはゲル化用組成物を含有する飲食品。 A food or drink containing the thickening or gelling composition according to claim 3.
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008020497A1 (en) * 2006-08-16 2008-02-21 Taiyo Kagaku Co., Ltd. Thickening composition improved in viscosity development
JP2009060794A (en) * 2007-09-04 2009-03-26 Taiyo Kagaku Co Ltd Starch adhesive composition
US7744942B2 (en) 2005-03-11 2010-06-29 Taiyo Kagaku Co., Ltd. Thickening composition having improved viscosity-emerging property
WO2011140598A1 (en) * 2010-05-11 2011-11-17 Trisco Investments Pty Ltd As Trustee For The Trisco Investment Trust Flowable liquid composition
WO2012067174A1 (en) * 2010-11-18 2012-05-24 グリーンフェノール・高機能フェノール樹脂製造技術研究組合 Coryneform bacterium transformant and method for producing phenol using same
JP2018102274A (en) * 2016-12-28 2018-07-05 日清オイリオグループ株式会社 Tablet type thickening composition

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52130933A (en) * 1976-04-20 1977-11-02 Sanei Kagaku Kogyo Kk Glycerine food
JPS5743649A (en) * 1981-07-21 1982-03-11 San Ei Chem Ind Ltd Glycerol food product
JPH02145158A (en) * 1988-11-29 1990-06-04 Japan Organo Co Ltd Glue solution
JP2000041594A (en) * 1998-07-31 2000-02-15 Ina Food Ind Co Ltd Liquid additive for thickening
JP2004059881A (en) * 2002-07-31 2004-02-26 Ina Food Ind Co Ltd Gel material solution, and food, medicine, quasi-drug, medical supplies, cosmetic, sanitary goods, daily goods, feed, fish feed, pet food, fertilizer, eutrophic and agrichemical each containing the same

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52130933A (en) * 1976-04-20 1977-11-02 Sanei Kagaku Kogyo Kk Glycerine food
JPS5743649A (en) * 1981-07-21 1982-03-11 San Ei Chem Ind Ltd Glycerol food product
JPH02145158A (en) * 1988-11-29 1990-06-04 Japan Organo Co Ltd Glue solution
JP2000041594A (en) * 1998-07-31 2000-02-15 Ina Food Ind Co Ltd Liquid additive for thickening
JP2004059881A (en) * 2002-07-31 2004-02-26 Ina Food Ind Co Ltd Gel material solution, and food, medicine, quasi-drug, medical supplies, cosmetic, sanitary goods, daily goods, feed, fish feed, pet food, fertilizer, eutrophic and agrichemical each containing the same

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7744942B2 (en) 2005-03-11 2010-06-29 Taiyo Kagaku Co., Ltd. Thickening composition having improved viscosity-emerging property
WO2008020497A1 (en) * 2006-08-16 2008-02-21 Taiyo Kagaku Co., Ltd. Thickening composition improved in viscosity development
AU2007285310B2 (en) * 2006-08-16 2012-08-09 Taiyo Kagaku Co., Ltd. Thickening composition improved in viscosity development
US11578194B2 (en) 2006-08-16 2023-02-14 Taiyo Kagaku Co., Ltd. Thickening composition improved in viscosity development
JP2009060794A (en) * 2007-09-04 2009-03-26 Taiyo Kagaku Co Ltd Starch adhesive composition
WO2011140598A1 (en) * 2010-05-11 2011-11-17 Trisco Investments Pty Ltd As Trustee For The Trisco Investment Trust Flowable liquid composition
AU2011252754B2 (en) * 2010-05-11 2015-05-07 Trisco ICAP Pty Ltd Flowable liquid composition
WO2012067174A1 (en) * 2010-11-18 2012-05-24 グリーンフェノール・高機能フェノール樹脂製造技術研究組合 Coryneform bacterium transformant and method for producing phenol using same
US8846367B2 (en) 2010-11-18 2014-09-30 Green Phenol Development Co., Ltd. Coryneform bacterium transformant and process for producing phenol using the same
JP2018102274A (en) * 2016-12-28 2018-07-05 日清オイリオグループ株式会社 Tablet type thickening composition

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