JP2004261683A5 - - Google Patents

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Publication number
JP2004261683A5
JP2004261683A5 JP2003053338A JP2003053338A JP2004261683A5 JP 2004261683 A5 JP2004261683 A5 JP 2004261683A5 JP 2003053338 A JP2003053338 A JP 2003053338A JP 2003053338 A JP2003053338 A JP 2003053338A JP 2004261683 A5 JP2004261683 A5 JP 2004261683A5
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Japan
Prior art keywords
polymerizable substance
easily polymerizable
distilling
cylinder
gas phase
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JP2003053338A
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Japanese (ja)
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JP4095471B2 (en
JP2004261683A (en
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Priority to JP2003053338A priority Critical patent/JP4095471B2/en
Priority claimed from JP2003053338A external-priority patent/JP4095471B2/en
Publication of JP2004261683A publication Critical patent/JP2004261683A/en
Publication of JP2004261683A5 publication Critical patent/JP2004261683A5/ja
Application granted granted Critical
Publication of JP4095471B2 publication Critical patent/JP4095471B2/en
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Expired - Lifetime legal-status Critical Current

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Claims (7)

易重合性物質を含む気相が通過する経路の一部を構成する筒体を備えるとともに、前記筒体は、その外周を囲むジャケットを備え、前記ジャケット内には減圧水蒸気を通すようになっている、ことを特徴とする易重合性物質の通過装置。  The cylinder includes a cylinder that forms part of a path through which a gas phase containing an easily polymerizable substance passes, and the cylinder includes a jacket that surrounds an outer periphery of the cylinder. An easily polymerizable material passage device. 前記筒体は、前記経路における、気相の温度分布が2℃以内である部分に設置される筒体である、請求項1に記載の易重合性物質の通過装置。  2. The easily polymerizable substance passage device according to claim 1, wherein the cylindrical body is a cylindrical body installed in a portion of the path in which a gas phase temperature distribution is within 2 ° C. 3. 前記減圧水蒸気の温度が前記筒体内を通過する気相の温度よりも、0.1〜15℃だけ高くなるよう設定されている、請求項1または2に記載の易重合性物質の通過装置。  The easily polymerizable substance passage device according to claim 1 or 2, wherein the temperature of the reduced-pressure steam is set to be higher by 0.1 to 15 ° C than the temperature of the gas phase passing through the cylindrical body. 前記ジャケット内に生じる蒸気ドレンの排出パイプを有し、この排出パイプは、前記ジャケットの底部から鉛直下方向に伸長し、U字形に反転して立ち上がり、常時開放状態の排出口に繋がっている、請求項1から3までのいずれかに記載の易重合性物質の通過装置。  It has a discharge pipe for the steam drain generated in the jacket, this discharge pipe extends vertically downward from the bottom of the jacket, rises in a U-shape, and is connected to a discharge port that is always open. The easily polymerizable substance passage device according to any one of claims 1 to 3. 蒸留塔と蒸気送り出しラインとコンデンサを用いて易重合性物質を蒸留する方法であって、前記蒸留塔の空塔部分から前記蒸気送り出しラインに掛けての部分の少なくとも一部を構成する筒体を、請求項1から4までのいずれかに記載の易重合性物質の通過装置の筒体で構成してなる、ことを特徴とする易重合性物質の蒸留方法。  A method of distilling an easily polymerizable substance using a distillation column, a steam delivery line, and a condenser, comprising: a cylindrical body constituting at least a part of a portion of the distillation tower that extends from an empty portion to the steam delivery line A method for distilling an easily polymerizable substance, comprising: the easily polymerizable substance passing device cylinder according to any one of claims 1 to 4. ヒドロキシアルキル(メタ)アクリレートを生成する工程と蒸留する工程とを備え、かつ、前記蒸留する工程が蒸留塔と蒸気送り出しラインとコンデンサを備えて行われる、ヒドロキシアルキル(メタ)アクリレートの製造方法における、前記蒸留する工程である、請求項5に記載の易重合性物質の蒸留方法。  In the method for producing hydroxyalkyl (meth) acrylate, comprising a step of producing a hydroxyalkyl (meth) acrylate and a step of distillation, wherein the step of distillation is performed with a distillation column, a vapor feed line and a condenser. The method for distilling an easily polymerizable substance according to claim 5, which is the step of distilling. 蒸留塔と蒸気送り出しラインとコンデンサを用いて易重合性物質を蒸留する方法であって、前記蒸留塔の空塔部分から前記蒸気送り出しラインに掛けての部分の少なくとも一部を構成し、前記易重合性物質の蒸気を含む100℃未満の気相が通過する筒体を、前記気相の温度よりも0.1〜15℃高い温度で均一に加熱・保温することで、前記易重合性物質の凝縮・重合を起こさないようにして前記気相を前記筒体に通過させる、ことを特徴とする易重合性物質の蒸留方法。A method of distilling an easily polymerizable substance using a distillation column, a steam delivery line, and a condenser, comprising at least part of a portion of the distillation tower that extends from an empty portion to the steam delivery line, The easily polymerizable substance is obtained by uniformly heating and maintaining the cylinder through which a gas phase of less than 100 ° C. containing the vapor of the polymerizable substance passes at a temperature 0.1 to 15 ° C. higher than the temperature of the gas phase. A method for distilling an easily polymerizable substance, wherein the gas phase is allowed to pass through the cylinder without causing condensation or polymerization of the polymer.
JP2003053338A 2003-02-28 2003-02-28 Distillation method of easily polymerizable substances Expired - Lifetime JP4095471B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2003053338A JP4095471B2 (en) 2003-02-28 2003-02-28 Distillation method of easily polymerizable substances

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2003053338A JP4095471B2 (en) 2003-02-28 2003-02-28 Distillation method of easily polymerizable substances

Publications (3)

Publication Number Publication Date
JP2004261683A JP2004261683A (en) 2004-09-24
JP2004261683A5 true JP2004261683A5 (en) 2005-10-13
JP4095471B2 JP4095471B2 (en) 2008-06-04

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JP2003053338A Expired - Lifetime JP4095471B2 (en) 2003-02-28 2003-02-28 Distillation method of easily polymerizable substances

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105683145B (en) 2013-10-29 2017-11-14 三菱化学株式会社 The vacuum distillation method and method for producing acrylic acid of easily polymerizable compound
WO2017102297A1 (en) * 2015-12-15 2017-06-22 Basf Se Production of tert-butyl esters of ethylenically unsaturated carboxylic acids
WO2023153132A1 (en) * 2022-02-08 2023-08-17 株式会社日本触媒 Handling device for easily polymerizable substance

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0710794B2 (en) * 1986-08-07 1995-02-08 三井東圧化学株式会社 Method for distilling 2-hydroxyalkyl (meth) acrylate
JPH0641601Y2 (en) * 1988-10-12 1994-11-02 昭和鉄工株式会社 Vacuum concentrator
JPH0660417U (en) * 1993-02-02 1994-08-23 有限会社太陽機工 Drain removal device
JPH0771783A (en) * 1993-08-31 1995-03-17 Takenaka Komuten Co Ltd Suction type air conditioner
JP2002267094A (en) * 2001-03-08 2002-09-18 Mitsubishi Heavy Ind Ltd Water seal piping

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