JP2003080005A - Defoaming apparatus and defoaming method - Google Patents

Defoaming apparatus and defoaming method

Info

Publication number
JP2003080005A
JP2003080005A JP2001378638A JP2001378638A JP2003080005A JP 2003080005 A JP2003080005 A JP 2003080005A JP 2001378638 A JP2001378638 A JP 2001378638A JP 2001378638 A JP2001378638 A JP 2001378638A JP 2003080005 A JP2003080005 A JP 2003080005A
Authority
JP
Japan
Prior art keywords
liquid
defoaming
inner pipe
bubbles
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2001378638A
Other languages
Japanese (ja)
Other versions
JP3936579B2 (en
Inventor
Kunio Muto
邦夫 武藤
Yasunori Ichikawa
靖典 市川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujifilm Holdings Corp
Original Assignee
Fuji Photo Film Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd
Priority to JP2001378638A priority Critical patent/JP3936579B2/en
Publication of JP2003080005A publication Critical patent/JP2003080005A/en
Application granted granted Critical
Publication of JP3936579B2 publication Critical patent/JP3936579B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Abstract

PROBLEM TO BE SOLVED: To improve defoaming effect on liquid, particularly coating liquid. SOLUTION: A defoaming apparatus for removing bubbles in the liquid is provided with an outside pipe and an inside pipe each facing in the vertical direction. The inside pipe is provided with a means for producing an upward flow inside the inside pipe. The bubbles in the liquid are removed by rotating the inside pipe to pass the liquid spirally downward between the outside pipe and the inside pipe, moving the bubbles in the liquid downward while moving the bubbles to the inside by a centrifugal force and moving the bubbles reaching the lower end of the inside pipe upward through the inside pipe.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、液体中、特に塗布
液中に含まれる気泡を除去する脱泡方法および脱泡装置
に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a defoaming method and a defoaming apparatus for removing air bubbles contained in a liquid, particularly a coating liquid.

【0002】[0002]

【従来の技術】一般的に、液体からの気泡の除去が必要
とされることがある。例えば、塗布液では、気泡が混入
した状態で支持体に塗布されると、気泡の部分が塗布欠
陥となって一様な膜を形成することができず、得率ダウ
ンの大きな原因の一つとなるため、脱泡処理を行うこと
が必要とされている。例えば銀塩感光材料の塗布液に対
しては、特開平11−5001号、同11−90110
号、同4−143747号公報などに、超音波を利用し
た脱泡方法が記載されている。
BACKGROUND OF THE INVENTION Generally, it is sometimes necessary to remove bubbles from a liquid. For example, when the coating liquid is applied to the support in a state where bubbles are mixed, the bubble portion becomes a coating defect and a uniform film cannot be formed, which is one of the major causes of the decrease in the yield. Therefore, it is necessary to perform defoaming treatment. For example, Japanese Patent Application Laid-Open Nos. 11-5001 and 11-90110 disclose coating solutions for silver salt photosensitive materials.
No. 4,143,747 and the like describe a defoaming method using ultrasonic waves.

【0003】[0003]

【発明が解決しようとする課題】これまで、脱泡容器の
形態や、超音波照射の強度や方向等については、上記の
公報に記載されているように様々な発明がなされている
が、塗布液の完全な脱泡をするまでには至っておらず、
更なる脱泡効果の向上が求められている。特に銀塩感光
材料塗布においては、近年、ハロゲン化銀濃度増加に伴
い高粘度化し、また、塗布速度のアップに伴い送液流量
も増大していることから、従来の超音波照射による脱泡
では十分な脱泡効果が得られず、更なる脱泡効果の向上
が求められている。本発明は、以上のような状況を解決
するために考案されたものであり、脱泡効果を、より高
めることを課題とする。
Various inventions have been made so far regarding the form of the defoaming container, the intensity and direction of ultrasonic irradiation, etc., as described in the above publications. It has not reached the point where the liquid is completely defoamed,
Further improvement of the defoaming effect is required. Particularly in the coating of silver salt light-sensitive materials, in recent years, the viscosity has increased as the silver halide concentration has increased, and the liquid delivery flow rate has also increased with the increase in coating speed. Since a sufficient defoaming effect cannot be obtained, further improvement of the defoaming effect is required. The present invention has been devised to solve the above situation, and an object thereof is to further enhance the defoaming effect.

【0004】[0004]

【課題を解決するための手段】超音波照射による脱泡効
果として、微泡を塗布液中に溶解させ脱泡する効果と泡
を合一浮上させて除去する効果が確認されているが、塗
布液の粘度が上昇し、送液流量が増大すると、塗布液中
に溶解することもできず、しかも浮上することもできず
に超音波脱泡器を通過してしまう気泡が発生し、これが
塗布工程における泡欠陥の原因となっている。そこで、
本発明では、超音波脱泡器中、あるいは超音波脱泡器の
直前で、気泡の浮上を促進させる手段をもうけることを
特徴とする。
[Means for Solving the Problems] As a defoaming effect by ultrasonic irradiation, it has been confirmed that the effect of dissolving fine bubbles in a coating solution to remove bubbles and the effect of removing bubbles by floating them together. When the viscosity of the liquid rises and the flow rate of the liquid is increased, bubbles are generated that cannot be dissolved in the coating liquid and cannot float and pass through the ultrasonic defoamer. It is a cause of bubble defects in the process. Therefore,
The present invention is characterized in that a means for promoting floating of bubbles is provided in the ultrasonic defoamer or immediately before the ultrasonic defoamer.

【0005】即ち、前記課題は以下の技術的手段により
達成することができる。 (1) 液体中の気泡を除去する脱泡装置において、上
下方向に向いた外側配管と内側配管を備え、内側配管は
内側配管内部に上昇流を起こさせる手段を備え、内側配
管を回転させることにより外側配管と内側配管の間を螺
旋状下向きに液体を流し、液体中の気泡を遠心力により
内側に移動させつつ下降させ、内側配管の下端に到達す
る気泡を内側配管内部を通して上昇させることで液体中
の気泡を除去することを特徴とする脱泡装置。 (2) 液体の供給口が外側配管の中段に位置すること
を特徴とする上記(1)に記載の脱泡装置。 (3) 内側配管を、液体の流入力で回転させることを
特徴とする上記(1)または(2)に記載の脱泡装置。 (4) 内側配管内部に上昇流を起こさせる傾斜翼を内
側配管内部に備えることを特徴とする上記(1)〜
(3)のいずれかに記載の脱泡装置。 (5) 脱泡装置が超音波脱泡器の上流または内部に設
置されることを特徴とする上記(1)〜(4)のいずれ
かに記載の脱泡装置。
That is, the above-mentioned object can be achieved by the following technical means. (1) In a defoaming device for removing air bubbles in a liquid, it is provided with an outer pipe and an inner pipe which are oriented in a vertical direction, the inner pipe is provided with a means for causing an upward flow inside the inner pipe, and the inner pipe is rotated. The liquid is caused to flow spirally downward between the outer pipe and the inner pipe, and the bubbles in the liquid are moved downward by the centrifugal force while moving, and the bubbles reaching the lower end of the inner pipe are raised through the inside of the inner pipe. A defoaming device that removes bubbles in a liquid. (2) The defoaming device as described in (1) above, wherein the liquid supply port is located in the middle stage of the outer pipe. (3) The defoaming device as described in (1) or (2) above, wherein the inner pipe is rotated by a liquid flow input. (4) The above-mentioned (1) to (1), characterized in that an inclined blade for causing an ascending flow in the inner pipe is provided in the inner pipe.
The defoaming device according to any one of (3). (5) The defoaming device according to any one of (1) to (4) above, wherein the defoaming device is installed upstream or inside the ultrasonic defoamer.

【0006】(6) 液体中の気泡を除去する脱泡方法
において、上下方向に向いた外側配管と内側配管の間に
液体を供給し、液体を螺旋状下向きに流すことで液体中
の気泡を遠心力により内側に集め、該気泡を内側配管内
部を通して上昇させることで液体中の気泡を除去するこ
とを特徴とする脱泡方法。 (7) 液体の供給を連続的に行うことを特徴とする上
記(6)に記載の脱泡方法。 (8) 上記(6)または(7)に記載の脱泡方法によ
り脱泡された液体に、さらに超音波を照射することを特
徴とする脱泡方法。 (9) 上記(6)または(7)に記載の脱泡方法によ
り液体の脱泡を行うのと同時に、液体に超音波を照射す
ることを特徴とする脱泡方法。 (10) 上記(6)〜(9)のいずれかに記載の脱泡
方法により脱泡した感光材料用塗布液を用いて作製され
ることを特徴とする感光材料。
(6) In a defoaming method for removing bubbles in a liquid, the liquid is supplied between an outer pipe and an inner pipe which are vertically oriented, and the liquid is flowed in a spiral downward direction to remove the bubbles in the liquid. A defoaming method, characterized in that the bubbles in the liquid are removed by collecting the bubbles inside by a centrifugal force and raising the bubbles through the inside of the inner pipe. (7) The defoaming method according to (6), wherein the liquid is continuously supplied. (8) A defoaming method, wherein the liquid defoamed by the defoaming method according to (6) or (7) above is further irradiated with ultrasonic waves. (9) A defoaming method, wherein the liquid is defoamed by the defoaming method according to (6) or (7), and at the same time, the liquid is irradiated with ultrasonic waves. (10) A photosensitive material produced using the coating solution for a photosensitive material that has been defoamed by the defoaming method according to any one of (6) to (9).

【0007】[0007]

【発明の実施の形態】以下で、図面を参照にして本発明
を説明するが、本発明はそれらに限定されるわけではな
い。また、塗布液からの脱泡を例として本発明を説明す
るが、本発明は塗布液に限らず泡を嫌うような液体であ
れば、いずれの液に対しても利用可能である。
The present invention will be described below with reference to the drawings, but the present invention is not limited thereto. Further, although the present invention will be described by taking defoaming from the coating liquid as an example, the present invention is not limited to the coating liquid and can be applied to any liquid as long as it is a liquid that dislikes bubbles.

【0008】本発明に係る脱泡装置の実施形態の一例を
図1に示す。図1(b)が脱泡装置の概略図であり、脱
泡装置は、上下方向の向きで配置された外側配管1とそ
の内部に内側配管2を備える。さらに、内側配管2の下
端内側には、内側配管内に上昇流を起こさせる手段とし
て傾斜翼3が備えられている。外側配管1と内側配管2
の間に供給され、下向きに流れる塗布液は、回転モータ
ー7により内側配管2が回転することにより回転流が生
じ、螺旋状に流れる。螺旋状下向きに流れながら、遠心
力の作用により、塗布液中の気泡は内側に移動しながら
下降する。内側配管2の下端に到達した気泡は、傾斜翼
3が内側配管2内に起こす上昇流により内側配管2内を
上昇し、内側配管2の最上部の出口5に到達する。大き
な気泡はそのまま液面に浮上し除去され、小さな気泡は
再び外側配管1と内側配管2の間を回転しながら下向き
に流れるが、小さな気泡も内側配管2の内外を上下流す
るうちに他の気泡と合一して大きな気泡となり、最終的
には液面に浮上し除去される。
An example of an embodiment of the defoaming apparatus according to the present invention is shown in FIG. FIG. 1B is a schematic diagram of the defoaming device. The defoaming device includes an outer pipe 1 arranged in a vertical direction and an inner pipe 2 inside thereof. Further, inside the lower end of the inner pipe 2, inclined blades 3 are provided as means for causing an upward flow in the inner pipe. Outer pipe 1 and inner pipe 2
The coating liquid supplied in the downward direction and flowing downward generates a rotational flow when the inner pipe 2 is rotated by the rotation motor 7, and flows in a spiral shape. While flowing in a spiral downward direction, the bubbles in the coating solution move downward due to the action of centrifugal force. The bubbles that have reached the lower end of the inner pipe 2 ascend in the inner pipe 2 due to the upward flow generated by the inclined blades 3 in the inner pipe 2, and reach the uppermost outlet 5 of the inner pipe 2. The large bubbles float on the liquid surface as they are and are removed, and the small bubbles again flow downward while rotating between the outer pipe 1 and the inner pipe 2. The bubbles coalesce into large bubbles, which eventually float to the liquid surface and are removed.

【0009】塗布液供給口4は外側配管1の中段に設置
することが好ましく、このことにより、内側配管2の最
上部の出口5から塗布液が供給される外側配管1の中段
までの間の塗布液の下降流速は、塗布液が供給される外
側配管1の中段より下側の下降流速より小さくすること
ができ、気泡をより浮上させやすく、脱泡効果を向上さ
せることができる。また、塗布液供給口4は、図1
(a)に示すように塗布液の供給方向が内側配管2の回
転方向に沿うように設置することが好ましい。外側配管
1と内側配管2は、図1(b)に示すように垂直に配置
されていることが好ましいが、その向きは上下方向に向
いていればよく、垂直配置の状態(図1(b)の状態)
から45度程度まで傾斜した向きで配置することができ
る。
The coating liquid supply port 4 is preferably installed in the middle stage of the outer pipe 1, so that the uppermost outlet 5 of the inner pipe 2 to the middle stage of the outer pipe 1 to which the coating liquid is supplied. The downward flow velocity of the coating liquid can be made smaller than the downward flow velocity below the middle stage of the outer pipe 1 to which the coating liquid is supplied, so that the bubbles can be more easily floated and the defoaming effect can be improved. The coating liquid supply port 4 is shown in FIG.
As shown in (a), it is preferable to install the coating liquid so that the supply direction is along the rotation direction of the inner pipe 2. The outer pipe 1 and the inner pipe 2 are preferably arranged vertically as shown in FIG. 1 (b), but the orientation of the outer pipe 1 and the inner pipe 2 is only required to be in the vertical direction, and the vertically arranged state (see FIG. ) State)
Can be arranged in an inclined direction from about 45 degrees.

【0010】塗布液の供給は連続的に行うが、その場
合、塗布液の送液流量は、本発明では特に制限しない。
また、内側配管の回転速度は、塗布液の粘度や送液流量
に応じて、よりよい脱泡効果を得ることができるように
定めることができる。
The coating liquid is continuously supplied, but in this case, the flow rate of the coating liquid is not particularly limited in the present invention.
In addition, the rotation speed of the inner pipe can be determined depending on the viscosity of the coating liquid and the flow rate of the liquid to be delivered so that a better defoaming effect can be obtained.

【0011】以上の構成により脱泡処理された塗布液
を、さらに超音波脱法器に送り、超音波照射すること
で、より高い脱泡効果を得ることができる。本発明の脱
泡装置と超音波脱泡器との組み合わせ方としては、本発
明による脱泡装置を、超音波脱泡装置内に設置して、本
発明の方法で脱泡するのと同時に超音波により脱泡を行
ってもよいし、図1(b)に示すように本発明による脱
泡装置を超音波脱泡装置の上流側に設置して、本発明の
方法で脱泡した後に超音波により脱泡を行ってもよい。
A higher defoaming effect can be obtained by further sending the defoaming-treated coating liquid having the above-mentioned constitution to an ultrasonic degasser and irradiating it with ultrasonic waves. As a method of combining the defoaming apparatus of the present invention with an ultrasonic defoamer, the defoaming apparatus of the present invention is installed in an ultrasonic defoaming apparatus, and at the same time as defoaming by the method of the present invention Defoaming may be performed by sonic waves, or the defoaming device according to the present invention may be installed upstream of the ultrasonic defoaming device as shown in FIG. Defoaming may be performed by sound waves.

【0012】次に、本発明に係る脱泡装置の他の実施形
態を図2に示す。本実施形態において脱泡装置は、内側
配管内に上昇流を起こさせる手段として傾斜翼3を、内
側配管2の上端内部に備え、また、内側配管上端から液
面までの回転流を抑制するためにバッフル10を備え
る。本発明の脱泡装置では内側配管の回転により液面に
は渦が発生しやすい。渦が発生すると気体が液中に巻き
込まれるため、浮上してきた気泡の除去を妨げることに
なる。バッフル10により、内側配管上端から液面まで
の回転流を制御することで、この渦の発生を抑制し、ま
た、内側配管内の上昇流をより強くすることにもなるの
で、気泡の除去効果を高めることができる。内側配管内
に上昇流を起こさせる手段は、内側配管内に上昇流を起
こすことができれば、どの位置に備えてもよいが、本実
施形態のようにバッフルを備える場合は、内側配管内の
上昇流を強くする点から、内側配管上端に備えることが
好ましい。
Next, another embodiment of the defoaming apparatus according to the present invention is shown in FIG. In the present embodiment, the defoaming device is provided with the inclined blades 3 as means for causing an ascending flow in the inner pipe, inside the upper end of the inner pipe 2, and for suppressing the rotational flow from the upper end of the inner pipe to the liquid surface. The baffle 10 is provided. In the defoaming device of the present invention, a vortex is easily generated on the liquid surface due to the rotation of the inner pipe. When the vortex is generated, the gas is caught in the liquid, which hinders the removal of the floating bubbles. By controlling the rotational flow from the upper end of the inner pipe to the liquid surface by the baffle 10, the generation of this vortex is suppressed and the upward flow in the inner pipe is further strengthened. Can be increased. The means for causing an ascending flow in the inner pipe may be provided at any position as long as it can cause an ascending flow in the inner pipe. However, when a baffle is provided as in the present embodiment, the ascending flow in the inner pipe is increased. From the viewpoint of strengthening the flow, it is preferable to provide the inner pipe at the upper end.

【0013】本発明に係る脱法装置のさらに他の実施形
態を図3に示す。内側配管2は塗布液の流入力により回
転させることもでき、そのために、本実施形態の脱泡装
置は、塗布液供給口4からの塗布液の流れを受け、内側
配管を回転させる回転板12を備える。この構成には、
内側配管を回転させるための回転モーターなどの手段を
必要としない利点がある。
FIG. 3 shows still another embodiment of the decapsulation apparatus according to the present invention. The inner pipe 2 can be rotated by the flow input of the coating liquid, and therefore the defoaming device of the present embodiment receives the flow of the coating liquid from the coating liquid supply port 4 and rotates the inner pipe 12. Equipped with. This configuration includes
There is an advantage that no means such as a rotation motor for rotating the inner pipe is required.

【0014】[0014]

【実施例】(実施例1)外側配管は、内径50mm、長
さ500mmで、塗布液の供給口は上端より200mm
の位置より内側配管回転方向に接続した。外側配管上端
より回転モーターに繋がる回転軸(100mm)を設
け、それに外径30mm、内径28mm、長さ200m
mの内側配管を接続した。内側配管の上端内側には上昇
流用の傾斜翼を4枚取り付けた。また、内側配管上端か
ら液面までの回転流を制御するバッフルを取り付けた
(具体的な構成は図2を参照)。内側配管はインバータ
制御で最大600rpmまで回転させられるようにし、
塗布液の粘度と送液流量を変化させて超音波脱泡器のみ
の場合と、本発明と超音脱泡器を組み合わせた場合の脱
泡効果を比較した結果を表1に示す。脱泡度の評価は泡
検出器で行い、×印は脱泡が不十分、○印は十分に脱泡
されていることを示す。なお、本発明の内側配管は30
0rpmで回転させ、内側配管内上昇流速は約1L/m
inであった。
Example 1 The outer pipe has an inner diameter of 50 mm and a length of 500 mm, and the coating liquid supply port is 200 mm from the upper end.
The connection was made in the rotation direction of the inner pipe from the position of. A rotary shaft (100 mm) connected to the rotary motor is provided from the upper end of the outer pipe, and the outer diameter is 30 mm, the inner diameter is 28 mm, and the length is 200 m.
m inner piping was connected. Four inclined blades for upward flow were attached to the inside of the upper end of the inner pipe. In addition, a baffle for controlling the rotational flow from the upper end of the inner pipe to the liquid surface was attached (see FIG. 2 for the specific configuration). The inner pipe can be rotated up to 600 rpm by inverter control,
Table 1 shows the results of comparing the defoaming effects of the ultrasonic defoamer alone and the combined effect of the ultrasonic defoamer by changing the viscosity of the coating liquid and the flow rate of the liquid. The degree of defoaming was evaluated with a bubble detector. X indicates that defoaming was insufficient, and ○ indicates that defoaming was sufficient. The inner pipe of the present invention is 30
Rotated at 0 rpm, the rising velocity in the inner pipe is about 1 L / m
It was in.

【0015】[0015]

【表1】 [Table 1]

【0016】表1により、塗布液の粘度や送液流量が増
加しても、より高い脱泡効果が本発明により得られてい
ることが分かる。
It can be seen from Table 1 that a higher defoaming effect can be obtained by the present invention even if the viscosity of the coating liquid and the flow rate of the liquid are increased.

【0017】(実施例2)内径50mm、長さ800m
mの外側配管に、上端より300mmの位置に塗布液供
給口を内側配管回転方向に接続し、外径25mm、内径
23mm、長さ700mmの内側配管を外側配管の上端
から100mmの位置に設けた。内側配管の下端内部
に、上昇流用の傾斜翼を4枚取り付けた(装置の具体的
な構成は、図1参照)。内側配管をインバータ制御で最
大600rpmまで回転させられるようにし、塗布液の
粘度と送液流量を変え、超音波脱泡器の場合と、本発明
と超音波脱泡器と組み合わせた場合とで脱泡効果を比較
したところ、実施例1と同様な効果が得られた。
(Embodiment 2) Inner diameter 50 mm, length 800 m
A coating liquid supply port was connected to the outer pipe of m at a position 300 mm from the upper end in the rotation direction of the inner pipe, and an inner pipe having an outer diameter of 25 mm, an inner diameter of 23 mm and a length of 700 mm was provided at a position of 100 mm from the upper end of the outer pipe. . Four inclined blades for upward flow were attached inside the lower end of the inner pipe (see FIG. 1 for the specific configuration of the device). The inner pipe can be rotated up to 600 rpm by inverter control, the viscosity of the coating liquid and the flow rate of the liquid to be sent are changed, and defoaming is performed in the case of the ultrasonic defoamer and in the case of combining the present invention with the ultrasonic defoamer. When the foam effects were compared, the same effect as in Example 1 was obtained.

【0018】[0018]

【発明の効果】本発明により、塗布液中の気泡を効率良
く除去することができ、塗布液の粘度が上昇したり、送
液流量がアップしても、塗布液の脱泡効果を高め、気泡
除去を完全に行うことができる脱泡装置および脱泡方法
を提供することができる。また、本発明は、あらゆる種
類の液体に対して、その液体中からの気泡除去に適用で
きるものである。
EFFECTS OF THE INVENTION According to the present invention, it is possible to efficiently remove bubbles in the coating liquid, and enhance the defoaming effect of the coating liquid even if the viscosity of the coating liquid increases or the flow rate of the liquid is increased. It is possible to provide a defoaming device and a defoaming method capable of completely removing bubbles. Further, the present invention can be applied to all kinds of liquids to remove bubbles from the liquids.

【図面の簡単な説明】[Brief description of drawings]

【図1】(a)本発明に係る塗布液の脱泡装置の概略図
である。 (b)(a)の脱泡装置の断面図である。
FIG. 1 (a) is a schematic view of a defoaming device for a coating liquid according to the present invention. (B) It is sectional drawing of the defoaming apparatus of (a).

【図2】(a)本発明に係る塗布液の脱泡装置の他の実
施形態を示す概略図である。 (b)(a)の脱泡装置の断面図である。
FIG. 2 (a) is a schematic view showing another embodiment of a defoaming device for a coating liquid according to the present invention. (B) It is sectional drawing of the defoaming apparatus of (a).

【図3】(a)本発明に係る塗布液の脱泡装置のさらに
別の実施形態を示す概略図である。 (b)(a)の脱泡装置の断面図である。
FIG. 3 (a) is a schematic view showing still another embodiment of the defoaming device for coating liquid according to the present invention. (B) It is sectional drawing of the defoaming apparatus of (a).

【符号の説明】[Explanation of symbols]

1 外側配管 2 内側配管 3 傾斜翼 4 塗布液供給口 5 内側配管最上部出口 6 超音波脱泡器 7 回転モーター 8 洗浄水入口 9 ドレン、エアー抜き 10 バッフル 11 回転板 1 Outer piping 2 Inside piping 3 inclined wings 4 Coating liquid supply port 5 Inner piping top outlet 6 Ultrasonic defoamer 7 rotation motor 8 Wash water inlet 9 Drain and air vent 10 baffles 11 rotating plate

───────────────────────────────────────────────────── フロントページの続き Fターム(参考) 2H023 EA00 EA01 4D011 AA01 AA06 AA18 AC01 AC04 AD01    ─────────────────────────────────────────────────── ─── Continued front page    F term (reference) 2H023 EA00 EA01                 4D011 AA01 AA06 AA18 AC01 AC04                       AD01

Claims (10)

【特許請求の範囲】[Claims] 【請求項1】液体中の気泡を除去する脱泡装置におい
て、上下方向に向いた外側配管と内側配管を備え、内側
配管は内側配管内部に上昇流を起こさせる手段を備え、
内側配管を回転させることにより外側配管と内側配管の
間を螺旋状下向きに液体を流し、液体中の気泡を遠心力
により内側に移動させつつ下降させ、内側配管の下端に
到達する気泡を内側配管内部を通して上昇させることで
液体中の気泡を除去することを特徴とする脱泡装置。
1. A defoaming device for removing air bubbles in a liquid, comprising an outer pipe and an inner pipe which are oriented in a vertical direction, and the inner pipe is provided with means for causing an ascending flow inside the inner pipe.
By rotating the inner pipe, the liquid is made to flow in a spiral downward direction between the outer pipe and the inner pipe, and the bubbles in the liquid are moved inward by the centrifugal force and lowered, and the bubbles reaching the lower end of the inner pipe are conveyed to the inner pipe. A defoaming device characterized by removing air bubbles in a liquid by raising it through the inside.
【請求項2】液体の供給口が外側配管の中段に位置する
ことを特徴とする請求項1に記載の脱泡装置。
2. The defoaming device according to claim 1, wherein the liquid supply port is located in the middle stage of the outer pipe.
【請求項3】内側配管を、液体の流入力で回転させるこ
とを特徴とする請求項1または2に記載の脱泡装置。
3. The defoaming device according to claim 1, wherein the inner pipe is rotated by the flow input of the liquid.
【請求項4】内側配管内部に上昇流を起こさせる傾斜翼
を内側配管内部に備えることを特徴とする請求項1〜3
のいずれかに記載の脱泡装置。
4. A slanting blade for causing an ascending flow in the inner pipe is provided in the inner pipe.
The defoaming device according to any one of 1.
【請求項5】脱泡装置が超音波脱泡器の上流または内部
に設置されることを特徴とする請求項1〜4のいずれか
に記載の脱泡装置。
5. The defoaming device according to claim 1, wherein the defoaming device is installed upstream or inside the ultrasonic defoamer.
【請求項6】液体中の気泡を除去する脱泡方法におい
て、上下方向に向いた外側配管と内側配管の間に液体を
供給し、液体を螺旋状下向きに流すことで液体中の気泡
を遠心力により内側に集め、該気泡を内側配管内部を通
して上昇させることで液体中の気泡を除去することを特
徴とする脱泡方法。
6. In a defoaming method for removing bubbles in a liquid, the liquid is supplied between an outer pipe and an inner pipe which are oriented vertically, and the liquid is spirally flown downward to centrifuge the bubbles in the liquid. A defoaming method, characterized in that air bubbles in a liquid are removed by collecting the bubbles inside by force and raising the bubbles through the inside of the inner pipe.
【請求項7】液体の供給を連続的に行うことを特徴とす
る請求項6に記載の脱泡方法。
7. The defoaming method according to claim 6, wherein the liquid is continuously supplied.
【請求項8】請求項6または7に記載の脱泡方法により
脱泡された液体に、さらに超音波を照射することを特徴
とする脱泡方法。
8. A defoaming method, wherein the liquid defoamed by the defoaming method according to claim 6 or 7 is further irradiated with ultrasonic waves.
【請求項9】請求項6または7に記載の脱泡方法により
液体の脱泡を行うのと同時に、液体に超音波を照射する
ことを特徴とする脱泡方法。
9. A defoaming method, wherein the liquid is defoamed by the defoaming method according to claim 6 or 7, and at the same time, the liquid is irradiated with ultrasonic waves.
【請求項10】請求項6〜9のいずれかに記載の脱泡方
法により脱泡した感光材料用塗布液を用いて作製される
ことを特徴とする感光材料。
10. A photosensitive material prepared by using the coating solution for a photosensitive material which has been defoamed by the defoaming method according to any one of claims 6 to 9.
JP2001378638A 2001-06-28 2001-12-12 Defoaming apparatus and defoaming method Expired - Lifetime JP3936579B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2001378638A JP3936579B2 (en) 2001-06-28 2001-12-12 Defoaming apparatus and defoaming method

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2001-196816 2001-06-28
JP2001196816 2001-06-28
JP2001378638A JP3936579B2 (en) 2001-06-28 2001-12-12 Defoaming apparatus and defoaming method

Publications (2)

Publication Number Publication Date
JP2003080005A true JP2003080005A (en) 2003-03-18
JP3936579B2 JP3936579B2 (en) 2007-06-27

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Country Link
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20030010486A (en) * 2002-03-28 2003-02-05 주식회사 피엠시코리아 Dearating apparatus for coating colour
JP2008516763A (en) * 2004-10-19 2008-05-22 ポム テクノロジー オイ エービー Method and apparatus for improving gas removal

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55167454U (en) * 1979-05-18 1980-12-02
JPH01199607A (en) * 1988-02-02 1989-08-11 Fuji Photo Film Co Ltd Treatment of photosensitive coating solution
JPH08187403A (en) * 1995-01-09 1996-07-23 Oval Corp Gas/liquid separation device
JPH115001A (en) * 1997-06-17 1999-01-12 Konica Corp Ultrasonic deforming method and ultrasonic defoaming device
JPH1190110A (en) * 1997-09-16 1999-04-06 Konica Corp Ultrasonic deforming method, manufacture of photosensitive material and ultrasonic deforming device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55167454U (en) * 1979-05-18 1980-12-02
JPH01199607A (en) * 1988-02-02 1989-08-11 Fuji Photo Film Co Ltd Treatment of photosensitive coating solution
JPH08187403A (en) * 1995-01-09 1996-07-23 Oval Corp Gas/liquid separation device
JPH115001A (en) * 1997-06-17 1999-01-12 Konica Corp Ultrasonic deforming method and ultrasonic defoaming device
JPH1190110A (en) * 1997-09-16 1999-04-06 Konica Corp Ultrasonic deforming method, manufacture of photosensitive material and ultrasonic deforming device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20030010486A (en) * 2002-03-28 2003-02-05 주식회사 피엠시코리아 Dearating apparatus for coating colour
JP2008516763A (en) * 2004-10-19 2008-05-22 ポム テクノロジー オイ エービー Method and apparatus for improving gas removal
US7947122B2 (en) 2004-10-19 2011-05-24 Pom Technology Oy Ab Method and an arrangement for improving gas removal

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