JP2001002453A - Device for producing double-layered glass including gas - Google Patents

Device for producing double-layered glass including gas

Info

Publication number
JP2001002453A
JP2001002453A JP11167383A JP16738399A JP2001002453A JP 2001002453 A JP2001002453 A JP 2001002453A JP 11167383 A JP11167383 A JP 11167383A JP 16738399 A JP16738399 A JP 16738399A JP 2001002453 A JP2001002453 A JP 2001002453A
Authority
JP
Japan
Prior art keywords
gas
vacuum chamber
double
glass
replacing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11167383A
Other languages
Japanese (ja)
Inventor
Masato Tao
正人 田尾
Hiroaki Arai
宏明 荒井
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Central Glass Co Ltd
Original Assignee
Central Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Central Glass Co Ltd filed Critical Central Glass Co Ltd
Priority to JP11167383A priority Critical patent/JP2001002453A/en
Publication of JP2001002453A publication Critical patent/JP2001002453A/en
Pending legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00Adapting or protecting infrastructure or their operation
    • Y02A30/24Structural elements or technologies for improving thermal insulation
    • Y02A30/249Glazing, e.g. vacuum glazing
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02BCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
    • Y02B80/00Architectural or constructional elements improving the thermal performance of buildings
    • Y02B80/22Glazing, e.g. vaccum glazing

Abstract

PROBLEM TO BE SOLVED: To prevent fracture of glass during replacing gas by providing a drier and a heater between a tank for storing gas, which is used for filling a hollow layer of a double-layered and closed two glass sheets, and a vacuum chamber and supplying dried gas into the vacuum chamber while heating the gas. SOLUTION: A double-layered glass having a hole for replacing gas is introduced into a vacuum chamber 6, and an opening and shutting valve 2i is opened so as to exhaust the inside of the chamber 6 by a vacuum pump. Then, the opening and shutting valve 2i is closed and opening and shutting valves 2g, 2f are opened, thereby the inside of the vacuum chamber 6 and the hollow layer of the double-layered glass are filled with a prescribed gas. As the gas supplied from gas tanks 1, 1' for storing replacing gases is supplied through a drier 8 filled with a drying agent such as calcium chloride or silica gel, moisture contained in the replacing gas is removed. The lowering of the temp. caused by the adiabatic expansion in the vacuum chamber 6 and of the vacuum chamber 6 is inhibited by winding a heater 9 such as a tungsten wire on the tube through which the replacing gas passes, thereby the occurrence of dew condensation is inhibited.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、建物の開口部に用
いられる複層ガラスにおいて、中空層の空気の大部分を
空気以外のガスで置換し、中空層が空気の複層ガラスよ
り防音性能および断熱性能に優れている複層ガラスを製
造する装置に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a double glazing used for an opening of a building, in which most of the air in the hollow layer is replaced with a gas other than air, and the hollow layer has a more soundproof performance than the double glazing of air. The present invention also relates to an apparatus for producing a double glazing having excellent heat insulation performance.

【0002】[0002]

【従来の技術】夏期の冷房負荷や冬季の暖房負荷を軽減
させるために、2枚の板ガラスを対向配置させその周辺
をシールした、断熱性能の高い複層ガラスが建物の開口
部に使われている。この複層ガラスは、板ガラスの間に
空気層があるため、室外のガラス面の熱伝達と室内のガ
ラス面の熱伝達の間に、空気の熱伝達があり、板ガラス
1枚の窓に比べ、断熱性能は比較にならないほど向上す
る。
2. Description of the Related Art In order to reduce a cooling load in summer and a heating load in winter, a double-glazed glass having high heat insulation performance, in which two sheets of glass are disposed to face each other and the periphery thereof is sealed, is used for an opening of a building. I have. In this double glazing, since there is an air layer between the glass sheets, there is heat transfer of air between the heat transmission of the outdoor glass surface and the heat transmission of the indoor glass surface. The insulation performance is incomparably improved.

【0003】しかしながら、近年の環境破壊問題に伴
い、開口部に用いられる複層ガラスの断熱性能をより優
れたものにする必要が生じている。このような複層ガラ
スとして、複層ガラスの中空層の空気をArガスやKr
ガスに置換した、ガス入り複層ガラスが、知られてい
た。また、Heガスで空気を置換した複層ガラスは、分
子の比重が空気より軽く、防音性能も向上することが知
られている。
However, with the recent problem of environmental destruction, it has become necessary to improve the heat insulating performance of the double glazing used for the opening. As such a double-glazed glass, the air in the hollow layer of the double-glazed glass is mixed with Ar gas,
Gas-filled insulating glasses replaced with gas have been known. Further, it is known that a double-layer glass in which air is replaced with He gas has a specific gravity of molecules lower than that of air and also has improved soundproofing performance.

【0004】ガス入り複層ガラスは、中間層が空気の複
層ガラスを作り、該複層ガラスの周辺のシール部にガス
置換用の孔を2箇所設けて、図4に示すような、配管2
3から置換ガスを中空層に充填し、置換ガスで中空層の
空気を配管22から押し出すという方法が行われてき
た。
[0004] The gas-filled double-glazed glass is made by forming a double-glazed glass with an intermediate layer of air, and providing two holes for gas replacement in a seal portion around the double-glazed glass, as shown in FIG. 2
3, a method of filling the hollow layer with the replacement gas and pushing out the air of the hollow layer from the pipe 22 with the replacement gas has been performed.

【0005】[0005]

【発明が解決しようとする課題】図4に示すような、複
層ガラスの中間層の空気を、置換するガスの充填で排気
する方法は、圧力調整が難しく、ガスの置換中にガラス
を破損することが多かった。また破損を少なくしようと
すると、圧力を微妙に調整しなければならず、ガス置換
に長時間かかるため、生産性が悪く、置換するガスを多
量に必要とするという欠点があった。
In the method of exhausting the air in the intermediate layer of the double-glazed glass by filling with a replacement gas as shown in FIG. 4, it is difficult to adjust the pressure, and the glass is damaged during the replacement of the gas. I often did. Further, in order to reduce the damage, the pressure must be finely adjusted, and the gas replacement takes a long time, so that there is a disadvantage that productivity is poor and a large amount of gas to be replaced is required.

【0006】[0006]

【課題を解決するための手段】本発明は、2枚のガラス
板をガラス板のの周縁部に配置したスペーサーを介して
対向配置し、該2枚のガラス板の周縁を、空気を置換す
るための穴を設けて接着シール材で密封して2枚のガラ
ス板を複層化した後、密封された中空層の空気の一部ま
たは全部を空気以外のガスで置換するための、真空ポン
プと、空気と置換する1種類以上の所望のガスを入れて
ある容器と、該複層化した2枚のガラス板を入れる真空
チャンバーとが、開閉バルブを介して連結した装置にお
いて、真空チャンバーと充填するためのガスの容器の間
に乾燥機とヒータを設け、該真空チャンバーに乾燥した
ガスを加熱して供給することを特徴とするガス入り複層
ガラスの製造装置である。また、空気を2種類以上の置
換ガスの混合ガスで置換するために、真空チャンバーを
2個以上としたことを特徴とするガス入り複層ガラスの
製造装置である。
According to the present invention, two glass plates are arranged to face each other via a spacer disposed at the peripheral edge of the glass plate, and the peripheral edges of the two glass plates are replaced with air. Vacuum pump for replacing a part or all of the air in the sealed hollow layer with a gas other than air after forming two holes by providing a hole for sealing and sealing with an adhesive sealing material And a container in which one or more kinds of desired gas to be replaced with air are stored, and a vacuum chamber in which the two laminated glass plates are connected through an opening / closing valve. A drying apparatus and a heater are provided between containers of gas to be filled, and a dry gas is heated and supplied to the vacuum chamber. Further, there is provided an apparatus for producing a double-glazed glass containing gas, wherein two or more vacuum chambers are provided in order to replace air with a mixed gas of two or more kinds of replacement gases.

【0007】乾燥機により、置換ガスが含んでいる水分
を取り除く。ヒータは置換ガスが真空チャンバーに供給
されるときの断熱膨張による、真空チャンバー内と真空
チャンバーの温度低下を防ぎ、真空チャンバーを開放し
たときの真空チャンバー内の結露を避ける。
[0007] The dryer removes the moisture contained in the replacement gas. The heater prevents the temperature inside the vacuum chamber and the vacuum chamber from lowering due to adiabatic expansion when the replacement gas is supplied to the vacuum chamber, and prevents dew condensation inside the vacuum chamber when the vacuum chamber is opened.

【0008】[0008]

【発明の実施の形態】図1に本発明によって、複層ガラ
スの中空層の空気を所定のガスに置換する装置例を示
す。
DESCRIPTION OF THE PREFERRED EMBODIMENTS FIG. 1 shows an example of an apparatus for replacing air in a hollow layer of a double glazing with a predetermined gas according to the present invention.

【0009】ガス容器1,1’は空気と置換するための
所定のガスが入っている。所定のガスとは、例えばAr
ガス、KrガスあるいはHeガスである。ガス容器1,
1’は乾燥機8および真空チャンバー6とを結ぶ配管4
に弁2a、2bを介して繋がっている。またガス容器に
は圧力計を付けて、容器内のガス量がわかるようにして
おく。
The gas containers 1, 1 'contain a predetermined gas for replacing air. The predetermined gas is, for example, Ar
Gas, Kr gas or He gas. Gas container 1,
1 ′ is a pipe 4 connecting the dryer 8 and the vacuum chamber 6
Through valves 2a and 2b. A pressure gauge is attached to the gas container so that the amount of gas in the container can be determined.

【0010】ガス容器1,1’からのガスは乾燥機8を
通して、真空チャンバー6に供給される。置換するガス
がほとんど水分を含まず、低温時の結露が問題とならな
い場合は、バルブ2cと2eを閉じ、バルブ2dを開い
て、ガスの供給を行う。
The gas from the gas containers 1, 1 'is supplied to the vacuum chamber 6 through the dryer 8. If the gas to be replaced contains almost no moisture and dew condensation at low temperature is not a problem, the valves 2c and 2e are closed and the valve 2d is opened to supply the gas.

【0011】真空チャンバー6はバルブ2iを介して、
配管で真空ポンプと連結されている。
The vacuum chamber 6 is connected via a valve 2i to
It is connected to a vacuum pump by piping.

【0012】真空チャンバー6の中の空気を、開閉バル
ブ2g、2fを閉じて、開閉バルブ2iを開き、真空ポ
ンプで排気する。真空チャンバー6の中には、ガスを置
換するための複層ガラスを入れておき、複層ガラスの中
空層の空気も排気される。
The air in the vacuum chamber 6 is exhausted by a vacuum pump by closing the opening and closing valves 2g and 2f and opening the opening and closing valve 2i. In the vacuum chamber 6, a multi-layer glass for replacing gas is put, and air in a hollow layer of the multi-layer glass is also exhausted.

【0013】中空層の空気を所定のガスで置換する複層
ガラスは、2枚以上の板ガラスを金属製スペーサあるい
はプラスチック製スペーサを介して対向配置し、周辺の
端部をシール材で封止したものや、スペーサを使わずに
シール材のみでガラス板を対向配置したものなどで、板
ガラスの間は密封空間としたものである。さらに、中空
構造の金属製スペーサあるいはプラスチック製スペーサ
に、ゼオライトなどの乾燥剤で充填したり、乾燥剤を混
入したシーリング材を使用しても良い。
In the double glazing in which the air in the hollow layer is replaced with a predetermined gas, two or more plate glasses are arranged to face each other via a metal spacer or a plastic spacer, and the peripheral edge is sealed with a sealing material. The space between the glass plates is a sealed space, such as a glass plate or a glass plate facing only with a sealing material without using a spacer. Further, a sealing material in which a hollow metal spacer or a plastic spacer is filled with a desiccant such as zeolite or a desiccant is mixed may be used.

【0014】複層ガラスの周辺には、ガスを置換するた
めの孔を設けておく。該孔は、シーリング材が硬化した
後、ドリルを用いてあけてもよい。また、シール材が固
化する前にパイプを設けてもよい。スペーサを使用した
複層ガラスでは、前もってスペーサに孔をあけて、パイ
プなどを付けて、ガスの置換用の孔とする。また、パイ
プの付いたスペーサを用いても良い。
In the periphery of the double glazing, holes for replacing gas are provided. The holes may be drilled after the sealant has hardened. Further, a pipe may be provided before the sealing material is solidified. In the case of a double glazing using a spacer, a hole is formed in the spacer in advance and a pipe or the like is attached to form a hole for gas replacement. Alternatively, a spacer with a pipe may be used.

【0015】真空チャンバー6の中の圧力を所定の圧力
に減圧した後、開閉バルブ2iを閉じ、開閉バルブ2
g、2fを開いて、所定のガスで真空チャンバー6の中
を充填する。同時に複層ガラスの中空層も所定のガスで
充填される。
After the pressure in the vacuum chamber 6 is reduced to a predetermined pressure, the open / close valve 2i is closed and the open / close valve 2
g, 2f are opened, and the inside of the vacuum chamber 6 is filled with a predetermined gas. At the same time, the hollow layer of the double glazing is also filled with a predetermined gas.

【0016】乾燥機8は、塩化カルシウム、シリカゲル
あるいはゼオライトなどの乾燥剤を充填し、その中にガ
スを通して乾燥させるものである。
The drier 8 is for filling a desiccant such as calcium chloride, silica gel or zeolite, and drying it by passing a gas therethrough.

【0017】ヒータ9は、タングステン線ヒータあるい
はニクロム線ヒータを、充填するガスの通る管に巻き付
けたもの、あるいは赤外線ヒータで充填するガスが通る
管を加熱するもの、あるいはニクロム線ヒータを充填す
るガスの通る管の中に設置したものである。真空チャン
バー6をガスで充填するとき、ガスの断熱膨張で真空チ
ャンバー内の温度が低下する。温度が低下した状態で、
真空チャンバーを開けると、真空チャンバーの外の空気
が、真空チャンバーの内壁や複層ガラスの表面に触れ
て、結露する。ヒータ9は、該結露を防ぐ程度に、充填
するガスを加熱する。
The heater 9 is obtained by winding a tungsten wire heater or a nichrome wire heater around a pipe through which a gas to be filled is filled, or heating the pipe through which a gas to be filled with an infrared heater, or a gas to fill a nichrome wire heater. It was installed in a pipe through When the vacuum chamber 6 is filled with gas, the temperature in the vacuum chamber decreases due to adiabatic expansion of the gas. With the temperature lowered,
When the vacuum chamber is opened, the air outside the vacuum chamber comes into contact with the inner wall of the vacuum chamber and the surface of the double glazing to form dew. The heater 9 heats the gas to be charged to such an extent that the condensation is prevented.

【0018】真空チャンバー6に設けている圧力計7
は、排気を行っている時の真空チャンバー6の中の到達
圧力とガス充填時の真空チャンバー6の中の圧力を監視
するためのものである。
A pressure gauge 7 provided in a vacuum chamber 6
Is for monitoring the ultimate pressure in the vacuum chamber 6 during evacuation and the pressure in the vacuum chamber 6 during gas filling.

【0019】真空チャンバー6に設けている、開閉バル
ブ2hが付いた配管は、真空チャンバー6の外から空気
を入れて、真空チャンバー6が設置されている室内の圧
力と真空チャンバー6の中の圧力を同じにし、真空チャ
ンバー6の開閉が容易に出来るようにするためである。
The piping provided with the opening / closing valve 2h provided in the vacuum chamber 6 is provided with air from outside the vacuum chamber 6 so that the pressure inside the chamber in which the vacuum chamber 6 is installed and the pressure inside the vacuum chamber 6 are increased. In order to make the opening and closing of the vacuum chamber 6 easy.

【0020】図2に示す装置は、2個の真空チャンバー
6a,6bを用いて、所望の混合ガスで空気を置換する
ための装置例である。例えば、真空チャンバー6aに中
空層を混合ガスで置換する複層ガラスを起き、真空チャ
ンバー6bでガスAとガスBの混合ガスを作る場合、ま
ず、真空チャンバー6aと真空チャンバー6bを共に減
圧する。次に、バルブ12、13を閉じて、まずガスA
で目的の混合比になるように真空チャンバー6bを充填
し、次いで、ガスBで真空チャンバー6bを充填する。
バルブ14を閉じ、バルブ12を開いて真空チャンバー
6bで作った混合ガスで、真空チャンバー6aの中を充
填し、真空チャンバー6aの中に置いた複層ガラスの中
空層を充填する。
The apparatus shown in FIG. 2 is an example of an apparatus for replacing air with a desired mixed gas by using two vacuum chambers 6a and 6b. For example, when a double glazing in which the hollow layer is replaced with a mixed gas in the vacuum chamber 6a and a mixed gas of the gas A and the gas B is formed in the vacuum chamber 6b, first, both the vacuum chamber 6a and the vacuum chamber 6b are depressurized. Next, the valves 12 and 13 are closed, and the gas A
Then, the vacuum chamber 6b is filled so as to have a desired mixing ratio, and then the gas B is filled into the vacuum chamber 6b.
The valve 14 is closed and the valve 12 is opened to fill the vacuum chamber 6a with the mixed gas created in the vacuum chamber 6b, and to fill the hollow layer of the double glazing placed in the vacuum chamber 6a.

【0021】図3に示す装置は、ガス置換のプロセスを
効率よく行うための装置例である。該装置では、真空チ
ャンバー6cが開閉バルブ18を閉じ、開閉バルブ13
aを開いて排気を行って減圧しているときに、開閉バル
ブ13bを閉じ、開閉バルブ20を開いて圧力チャンバ
ー6dを所望の置換ガスで充填し、真空チャンバー6d
の中に置いた複層ガラスの中空層を所望のガスで置換す
る。逆に、真空チャンバー6cが排気を終了し、ガスを
充填している間に、真空チャンバー6dの中を排気す
る。このように、2つの真空チャンバーで、排気とガス
の充填を同時に行うため、真空ポンプは常に稼働状態と
なり、効率のよい製造が出来る。
The apparatus shown in FIG. 3 is an example of an apparatus for efficiently performing a gas replacement process. In this device, the vacuum chamber 6c closes the open / close valve 18 and the open / close valve 13
When the pressure is reduced by opening the valve a and opening the valve 13b, the valve 13b is closed and the valve 20 is opened to fill the pressure chamber 6d with a desired replacement gas.
The hollow layer of double glazing placed in is replaced with the desired gas. Conversely, the inside of the vacuum chamber 6d is evacuated while the evacuation of the vacuum chamber 6c is completed and the gas is being filled. As described above, since the evacuation and the gas filling are performed simultaneously in the two vacuum chambers, the vacuum pump is always in an operating state, and efficient production can be performed.

【0022】なお、バルブは、電気的に開閉できるもの
が好ましいが、手動で開閉するものでもよい。
The valve is preferably one that can be opened and closed electrically, but may be one that can be opened and closed manually.

【0023】[0023]

【実施例】実施例1 図1の装置において、圧力容器1はArガスの入ったガ
スボンベを用い、圧力容器1’にHeガスの入ったガス
ボンベを用いた。容器厚み3mmのフロート板ガラスを
もちいて作製した複層ガラスに、ガス置換用の孔を2箇
所設けた。該複層ガラスを図1の真空チャンバー6に設
置し、図1の、バルブ2a、2bおよび2fは閉じ、他
のバルブは全て開いて、真空ポンプにより、真空チャン
バー内の圧力が1Paになるまで減圧した。
EXAMPLE 1 In the apparatus shown in FIG. 1, a gas cylinder containing Ar gas was used for the pressure vessel 1 and a gas cylinder containing He gas was used for the pressure vessel 1 '. Two holes for gas replacement were provided in a double glazing made using a float plate glass having a container thickness of 3 mm. The double glazing is set in the vacuum chamber 6 of FIG. 1, and the valves 2a, 2b and 2f of FIG. 1 are closed and all other valves are opened, and the pressure in the vacuum chamber is reduced to 1 Pa by the vacuum pump. The pressure was reduced.

【0024】減圧を終了後、バルブ2iと2dを閉じ、
Arガスの入ったガスボンベにつけたバルブ2bを開い
て、圧力チャンバーをArガスで充填した。該Arガス
は、ゼオライトを充填した乾燥機8で水分をとり、さら
に、ニクロム線を巻いた配管でできたヒータ9で加熱し
た。
After the pressure reduction is completed, the valves 2i and 2d are closed,
The valve 2b attached to the gas cylinder containing Ar gas was opened, and the pressure chamber was filled with Ar gas. The Ar gas was dehydrated by a dryer 8 filled with zeolite, and further heated by a heater 9 made of a pipe around which a nichrome wire was wound.

【0025】Arガスで圧力チャンバーを充填し、圧力
チャンバー内の圧力が大気圧になった後、バルブ2hを
開いて圧力チャンバーから複層ガラスを取り出した。
The pressure chamber was filled with Ar gas, and after the pressure in the pressure chamber reached atmospheric pressure, the valve 2h was opened to take out the double-glazed glass from the pressure chamber.

【0026】複層ガラスの置換用の孔は、圧力チャンバ
ーから取り出した後直ちにシール材で封止した。
The replacement hole of the double-glazed glass was sealed with a sealing material immediately after being taken out of the pressure chamber.

【0027】なお、圧力チャンバー6の中に、置換用の
孔が上になるように複層ガラスを設置し、置換用の孔を
封止するまでに、該複層ガラスの中空層にArガスより
比重の小さい空気が進入しないようにした。
In the pressure chamber 6, a double glazing is placed so that the replacement hole is on the upper side, and Ar gas is inserted into the hollow layer of the double glazing until the replacement hole is sealed. Air with lower specific gravity was prevented from entering.

【0028】置換したガスの濃度をガスクロマトグラフ
ィーで測定したところ、100%の置換率であった。ま
た、露点温度はー70℃以下であった。
When the concentration of the replaced gas was measured by gas chromatography, the replacement ratio was 100%. Further, the dew point temperature was -70 ° C or less.

【0029】実施例2 置換ガスをHeガスとし、バルブ2bを閉じたままで、
真空チャンバー6をHeガスで充填するときにバルブ2
aを開き、さらに複層ガラスに設けた置換用の孔を下に
して、複層ガラスを圧力チャンバーに設置した他は、実
施例1と同様にして、複層ガラスの中空層の空気をHe
ガスでの置換した。
Example 2 He gas was used as the replacement gas, and the valve 2b was kept closed.
When filling the vacuum chamber 6 with He gas, the valve 2
a, and the air in the hollow layer of the double-glazed glass was discharged in the same manner as in Example 1 except that the double-glazed glass was placed in the pressure chamber with the replacement hole provided in the double-glazed glass facing down.
Replaced with gas.

【0030】置換したガスの濃度をガスクロマトグラフ
ィーで測定したところ、100%の置換率であった。ま
た、露点温度はー70℃以下であった。
When the concentration of the replaced gas was measured by gas chromatography, the replacement ratio was 100%. Further, the dew point temperature was -70 ° C or less.

【0031】実施例3 圧力容器1はArガスの入ったガスボンベを用い、圧力
容器1’にKrガスの入ったガスボンベを用いた。また
図2に示すように、真空チャンバー6a、6bの2台用
いた。
Example 3 A gas cylinder containing Ar gas was used for the pressure vessel 1, and a gas cylinder containing Kr gas was used for the pressure vessel 1 '. As shown in FIG. 2, two vacuum chambers 6a and 6b were used.

【0032】中空層をArガスとKrガスの混合ガスで
置換する複層ガラスは、置換用の孔を2箇所開け、該孔
を上にして真空チャンバー6a内に設置した。
The double-layer glass in which the hollow layer was replaced with a mixed gas of Ar gas and Kr gas was placed in a vacuum chamber 6a with two holes for replacement, with the holes facing up.

【0033】ガス容器に近いバルブ(図1バルブ2a、
2b)とバルブ16,17を閉じて、真空ポンプで真空
チャンバー6a、6bの圧力が1Pa以下になるまで減
圧し、バルブ12を閉じた。
A valve close to the gas container (FIG. 1, valve 2a,
2b) and the valves 16 and 17 were closed, the pressure in the vacuum chambers 6a and 6b was reduced by a vacuum pump until the pressure became 1 Pa or less, and the valve 12 was closed.

【0034】減圧を終了した後、真空チャンバー6b
を、ArガスとKrガスが所望の比率となるように、は
じめArガスのみで充填し次いでKrガスのみで真空チ
ャンバー6bを充填し、ArガスとKrガスの混合ガス
で真空チャンバー6b内が少なくとも大気圧の2倍以上
の圧力となるようにした。
After the pressure reduction is completed, the vacuum chamber 6b
Is first filled only with Ar gas, and then the vacuum chamber 6b is filled only with Kr gas so that the Ar gas and Kr gas have a desired ratio, and at least the inside of the vacuum chamber 6b is mixed with a mixed gas of Ar gas and Kr gas. The pressure was set to more than twice the atmospheric pressure.

【0035】次いで、バルブ13を閉じ、バルブ14,
15を開いて、真空チャンバー6aの中を真空チャンバ
ー6bの中の混合ガスで充填し、真空チャンバー6aの
中に設置した複層ガラスの中空層を所定の混合ガスで置
換した。
Next, the valve 13 is closed, and the valves 14,
15 was opened, the inside of the vacuum chamber 6a was filled with the mixed gas in the vacuum chamber 6b, and the hollow layer of the double glazing placed in the vacuum chamber 6a was replaced with a predetermined mixed gas.

【0036】この方法での混合ガスの置換にかかる時間
は、実施例1や実施例2とほとんど差がなかった。また
ガスクロマトグラフィーでガス濃度を調べた結果、所望
のガス混合比になっていた。
The time required for the replacement of the mixed gas by this method was almost the same as in Examples 1 and 2. Further, as a result of examining the gas concentration by gas chromatography, a desired gas mixture ratio was obtained.

【0037】比較例1 混合ガスで置換するための複層ガラスを、置換用の孔を
2箇所あけて真空チャンバー6bの中に設置した。バル
ブ14は閉じたままにした。はじめに、真空チャンバー
6bを、所望の混合ガスの比になるように、はじめはA
rガスのみで充填し、次いでKrガスのみで充填し、真
空チャンバー6bの中を大気圧にした。
Comparative Example 1 A double glazing to be replaced with a mixed gas was placed in a vacuum chamber 6b with two replacement holes. Valve 14 was kept closed. First, the vacuum chamber 6b is initially set at A so as to have a desired mixed gas ratio.
It was filled only with r gas, and then only with Kr gas, and the inside of the vacuum chamber 6b was brought to atmospheric pressure.

【0038】大気圧になった後、複層ガラスを取り出し
て置換用の孔を封止した。
After reaching the atmospheric pressure, the double-glazed glass was taken out and the replacement hole was sealed.

【0039】封止後、中空層のガス濃度を調べたが、A
rガスの濃度が大きく、中空層のガスの混合比を所望の
比にするには、真空チャンバー6bを、Krガスで大気
圧にした後、かなりの時間を要すると推定した。
After sealing, the gas concentration in the hollow layer was examined.
It has been estimated that considerable time is required after the vacuum chamber 6b is brought to atmospheric pressure with Kr gas in order for the concentration of r gas to be large and the mixture ratio of the gas in the hollow layer to a desired ratio.

【0040】実施例4 図3に示すように、圧力チャンバー6c,6dの2台用
いて、真空チャンバー6cが減圧の時は真空チャンバー
6dはガスの充填を行い、逆に、圧力チャンバー6cが
ガスを充填している時は真空チャンバー6dは減圧を行
うようにして、複層ガラスの中空層をArガスで置換し
た。
Embodiment 4 As shown in FIG. 3, two pressure chambers 6c and 6d are used, and when the vacuum chamber 6c is under reduced pressure, the vacuum chamber 6d is filled with gas. Is filled, the vacuum chamber 6d is depressurized, and the hollow layer of the double glass is replaced with Ar gas.

【0041】実施例1の場合に較べ、単位時間の製造量
はほぼ倍とすることができた。
As compared with Example 1, the production amount per unit time could be almost doubled.

【0042】[0042]

【発明の効果】本発明の製造装置は、多種類に渡るガス
入り複層ガラスを、効率よく生産せしめ、安価なガス入
り複層ガラスの提供を実現した。
According to the manufacturing apparatus of the present invention, it is possible to efficiently produce a wide variety of gas-containing double glazings and to provide an inexpensive gas double glazing.

【図面の簡単な説明】[Brief description of the drawings]

【図1】ガス入り複層ガラスを製造するための装置の概
略図。
FIG. 1 is a schematic view of an apparatus for producing a gas-filled double-glazed glass.

【図2】混合ガスで中空層を置換するための装置を示す
図。
FIG. 2 is a diagram showing an apparatus for replacing a hollow layer with a mixed gas.

【図3】真空チャンバー2台による製造装置の配管を示
す図。
FIG. 3 is a diagram showing piping of a manufacturing apparatus using two vacuum chambers.

【図4】従来のガス置換方法を示す概略図。FIG. 4 is a schematic diagram showing a conventional gas replacement method.

【符号の説明】[Explanation of symbols]

1、1’ 置換用ガス容器 6、6a、6b、6c、6d 真空チャンバー 8 乾燥機 9 ヒータ 24 複層ガラス 1, 1 'Replacement gas container 6, 6a, 6b, 6c, 6d Vacuum chamber 8 Dryer 9 Heater 24 Double glass

───────────────────────────────────────────────────── フロントページの続き Fターム(参考) 2E016 AA01 BA01 BA02 CA01 CB01 CC02 EA02 FA01 GA01 GA02 2E039 AB01 4G061 AA09 AA11 BA01 CB06 CD02 CD21 DA61  ──────────────────────────────────────────────────続 き Continued on the front page F term (reference) 2E016 AA01 BA01 BA02 CA01 CB01 CC02 EA02 FA01 GA01 GA02 2E039 AB01 4G061 AA09 AA11 BA01 CB06 CD02 CD21 DA61

Claims (5)

【特許請求の範囲】[Claims] 【請求項1】複層ガラスの密封された中空層の空気の一
部または全部を、空気以外のガスで置換するガス入り複
層ガラスの製造装置において、空気を置換する複層ガラ
スを入れる真空チャンバーと、該真空チャンバーの空気
を排気するための真空ポンプと、該真空チャンバーを充
填する1種類以上の所望のガスを入れてある容器とが、
開閉バルブを介して連結されていることを特徴とする製
造装置。
1. A gas-filled multilayer glass manufacturing apparatus for replacing a part or all of air in a sealed hollow layer of a multilayer glass with a gas other than air. A chamber, a vacuum pump for evacuating the air in the vacuum chamber, and a container containing one or more kinds of desired gas filling the vacuum chamber,
A manufacturing apparatus, wherein the manufacturing apparatus is connected via an opening / closing valve.
【請求項2】真空チャンバーと充填するためのガスの容
器の間に乾燥機とヒータを設け、該真空チャンバーに乾
燥したガスを加熱して供給することを特徴とする請求項
1記載の製造装置。
2. The manufacturing apparatus according to claim 1, wherein a dryer and a heater are provided between the vacuum chamber and a gas container for filling, and the dried gas is heated and supplied to the vacuum chamber. .
【請求項3】真空チャンバーに開放バルブと圧力計を設
けたことを特徴とする請求項1に記載の製造装置
3. The manufacturing apparatus according to claim 1, wherein an opening valve and a pressure gauge are provided in the vacuum chamber.
【請求項4】空気を混合ガスで置換するために、真空チ
ャンバーを2個以上としたことを特徴とする請求項1乃
至3に記載の製造装置。
4. The manufacturing apparatus according to claim 1, wherein two or more vacuum chambers are provided for replacing air with a mixed gas.
【請求項5】真空チャンバーを2個以上設け、真空チャ
ンバーを減圧する工程とガスを充填する工程が、同時に
行えるようにしたこと特徴とする請求項1乃至3に記載
の製造装置。
5. The manufacturing apparatus according to claim 1, wherein two or more vacuum chambers are provided, and the step of depressurizing the vacuum chamber and the step of filling with gas can be performed simultaneously.
JP11167383A 1999-06-14 1999-06-14 Device for producing double-layered glass including gas Pending JP2001002453A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11167383A JP2001002453A (en) 1999-06-14 1999-06-14 Device for producing double-layered glass including gas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11167383A JP2001002453A (en) 1999-06-14 1999-06-14 Device for producing double-layered glass including gas

Publications (1)

Publication Number Publication Date
JP2001002453A true JP2001002453A (en) 2001-01-09

Family

ID=15848699

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11167383A Pending JP2001002453A (en) 1999-06-14 1999-06-14 Device for producing double-layered glass including gas

Country Status (1)

Country Link
JP (1) JP2001002453A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003161673A (en) * 2001-07-17 2003-06-06 Bandag Licensing Corp Shearing graphic image machine
KR101027407B1 (en) * 2010-07-01 2011-04-11 (주)삼진창호글라스텍 An apparatus for charging gas into pair glass
WO2012078739A2 (en) * 2010-12-09 2012-06-14 Cabot Corporation Insulated units and methods for producing them
JP2013534901A (en) * 2010-06-28 2013-09-09 プラクスエア・テクノロジー・インコーポレイテッド Continuous gas filling method and apparatus for the manufacture of insulated glass units
CN104389484A (en) * 2014-11-13 2015-03-04 山东温声玻璃有限公司 Device for inflating hollow glass with inert gas

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003161673A (en) * 2001-07-17 2003-06-06 Bandag Licensing Corp Shearing graphic image machine
JP2009115810A (en) * 2001-07-17 2009-05-28 Bandag Inc Shear graphic image machine
JP4520090B2 (en) * 2001-07-17 2010-08-04 ブリジストン・バンダグ・エルエルシー Shear graphic image machine
JP4555374B2 (en) * 2001-07-17 2010-09-29 ブリジストン・バンダグ・エルエルシー Shear graphic image machine
JP2013534901A (en) * 2010-06-28 2013-09-09 プラクスエア・テクノロジー・インコーポレイテッド Continuous gas filling method and apparatus for the manufacture of insulated glass units
KR101027407B1 (en) * 2010-07-01 2011-04-11 (주)삼진창호글라스텍 An apparatus for charging gas into pair glass
WO2012078739A2 (en) * 2010-12-09 2012-06-14 Cabot Corporation Insulated units and methods for producing them
WO2012078739A3 (en) * 2010-12-09 2012-08-16 Cabot Corporation Insulated units and methods for producing them
CN104389484A (en) * 2014-11-13 2015-03-04 山东温声玻璃有限公司 Device for inflating hollow glass with inert gas
CN104389484B (en) * 2014-11-13 2016-04-13 山东温声玻璃有限公司 A kind of filling inert gas into hollow glass device

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