IT202200007589A1 - Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse - Google Patents

Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse Download PDF

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Publication number
IT202200007589A1
IT202200007589A1 IT102022000007589A IT202200007589A IT202200007589A1 IT 202200007589 A1 IT202200007589 A1 IT 202200007589A1 IT 102022000007589 A IT102022000007589 A IT 102022000007589A IT 202200007589 A IT202200007589 A IT 202200007589A IT 202200007589 A1 IT202200007589 A1 IT 202200007589A1
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Italy
Prior art keywords
biomass
production
levulinic acid
cellulose obtained
cellulose
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IT102022000007589A
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English (en)
Inventor
Daniele Casciello
Giovanni Pastena
Riccardo Bianchi
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Pabif Srl
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Priority to IT102022000007589A priority Critical patent/IT202200007589A1/it
Priority to PCT/IB2023/053844 priority patent/WO2023199284A1/en
Publication of IT202200007589A1 publication Critical patent/IT202200007589A1/it

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
IT102022000007589A 2022-04-15 2022-04-15 Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse IT202200007589A1 (it)

Priority Applications (2)

Application Number Priority Date Filing Date Title
IT102022000007589A IT202200007589A1 (it) 2022-04-15 2022-04-15 Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse
PCT/IB2023/053844 WO2023199284A1 (en) 2022-04-15 2023-04-14 Process and apparatus for producing levulinic acid from cellulose derived from biomass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT102022000007589A IT202200007589A1 (it) 2022-04-15 2022-04-15 Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse

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IT202200007589A1 true IT202200007589A1 (it) 2023-10-15

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IT102022000007589A IT202200007589A1 (it) 2022-04-15 2022-04-15 Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse

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IT (1) IT202200007589A1 (it)
WO (1) WO2023199284A1 (it)

Citations (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2840605A (en) 1957-04-26 1958-06-24 Heyden Newport Chemical Corp Method of making levulinic acid
EP0087294A1 (en) 1982-02-23 1983-08-31 Becton Dickinson and Company Radiation stabilization of polymeric material
EP0365665A1 (en) 1988-04-26 1990-05-02 Biofine Inc DEGRADATION OF LIGNOCELLULOSE.
US5892107A (en) 1996-11-08 1999-04-06 Arkenol, Inc. Method for the production of levulinic acid
ES2212866A1 (es) 2001-05-04 2004-08-01 Universidad Politecnica De Madrid Sistema de separacion fraccionada de la biomasa integral del cardo cynara carcunculus l.
EP1723099A1 (en) 2004-01-26 2006-11-22 Shell Internationale Researchmaatschappij B.V. Process for the reactive extraction of levulinic acid
EP1851186A1 (en) 2005-02-22 2007-11-07 Shell Internationale Research Maatschappij B.V. A process for permeation enhanced reactive extraction of levulinic acid
US20100312006A1 (en) 2009-06-09 2010-12-09 Meadwestvaco Corporation Production of levulinic acid and levulinate esters from biomass
ITFI20090210A1 (it) 2009-09-29 2011-03-30 Luciana Gabriella Angelini Procedimento per la totale ed efficiente conversione di arundo donax a dare furaldeide, acido levulinico e derivati ligninici
WO2011039635A2 (en) 2009-09-29 2011-04-07 Nova Pangaea Technologies Limited Method and system for fractionation of lignocellulosic biomass
US20110160479A1 (en) 2008-06-26 2011-06-30 POLIMERI EUROPA S.p.A., SAN DONATO MILANESE Process for the production of esters of levulinic acid from biomasses
US20120111322A1 (en) 2010-11-09 2012-05-10 Impulse Devices, Inc. Method and Apparatus for Treatment of Cellulosic Biomass Materials in a Cavitation Reactor
WO2012112529A1 (en) 2011-02-14 2012-08-23 Xyleco, Inc. Processing biomass
EP2537841A1 (en) 2011-06-22 2012-12-26 DSM IP Assets B.V. Continuous production of furfural and levulininc acid
CN102899950A (zh) 2012-10-25 2013-01-30 福建农林大学 一种超声波-微波同时辅助制备纳米纤维素的方法
US8383838B2 (en) 2008-03-01 2013-02-26 MERCK Patent Gesellschaft mit beschränkter Haftung 5-oxo-2,3,4,5-tetrahydro-benzo[b]oxepine-4-carboxylic acid amides and 2,3-dihydro-benzo[b]oxepine-4-carboxylic acid amides for treatment and prevention of diabetes typ 1 and 2
WO2013135965A1 (en) 2012-03-14 2013-09-19 Chempolis Oy Preparation of levulinic acid
EP2684875A1 (en) * 2012-07-13 2014-01-15 DSM IP Assets B.V. Process for the production of furfural and levulinic acid from lignocellulosic biomass
EP2712364A1 (en) 2012-07-13 2014-04-02 SAPPI Netherlands Services B.V. Low energy method for the preparation of non-derivatized nanocellulose
EP2780433A1 (en) 2011-11-14 2014-09-24 Shell Internationale Research Maatschappij B.V. Process for conversion of a cellulosic material
CN104074086A (zh) 2014-06-16 2014-10-01 南京泽朗医药科技有限公司 一种从苦菜中提取纤维素的方法
US20140315259A1 (en) 2013-03-15 2014-10-23 Edeniq, Inc. Cellulose co-feed for dry mill corn ethanol operations
EP2825519A1 (en) 2012-03-12 2015-01-21 Georgia-Pacific LLC Method for producing levulinic acid from lignocellulosis biomass
CN104292194A (zh) 2014-09-05 2015-01-21 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和快速变温法制备乙酰丙酸的方法
CN104292195A (zh) 2014-09-05 2015-01-21 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和调变流量制备乙酰丙酸的方法
CN104311411A (zh) 2014-09-15 2015-01-28 淮阴师范学院 多级酸水解制备乙酰丙酸的方法
US20150238923A1 (en) 2012-06-22 2015-08-27 Suganit Systems, Inc. Method and apparatus for treatment of biomass substrates
EP2928856A1 (en) 2012-12-07 2015-10-14 DSM IP Assets B.V. Process for the production of a biomass hydrolysate
US9174909B2 (en) 2012-02-02 2015-11-03 Wisconsin Alumni Research Foundation Two-stage, acid-catalyzed conversion of carbohydrates into levulinic acid
EP3047029A1 (en) 2013-09-18 2016-07-27 Georgia-Pacific LLC Method for producing organic acids and organic acid degradation compounds from biomass
EP3080304A1 (en) 2013-12-11 2016-10-19 Versalis S.p.A. Process for the production of sugars from biomass
EP3184518A1 (en) 2015-12-23 2017-06-28 Neste Oyj Combined levulinic acid and furfural production from biomass
WO2018013501A1 (en) 2016-07-14 2018-01-18 Api Intellectual Property Holdings, Llc Solvent-based processes for producing nanocellulose, and compositions and products produced therefrom
US20180194711A1 (en) 2017-01-11 2018-07-12 Battelle Memorial Institute Methods of making levulinic acid and alkyl levulinates from saccharides
EP3665147A1 (en) 2017-06-21 2020-06-17 Bio-On S.p.A. Process for producing levulinic acid
WO2020214835A1 (en) 2019-04-16 2020-10-22 University Of Louisville Research Foundation, Inc. One-pot acid-catalyzed levulinic acid production from lignocellulosic biomass
CN113214196A (zh) 2021-04-25 2021-08-06 武汉轻工大学 以木质纤维素类生物质为原料制备生物基化学品的方法

Patent Citations (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2840605A (en) 1957-04-26 1958-06-24 Heyden Newport Chemical Corp Method of making levulinic acid
EP0087294A1 (en) 1982-02-23 1983-08-31 Becton Dickinson and Company Radiation stabilization of polymeric material
EP0365665A1 (en) 1988-04-26 1990-05-02 Biofine Inc DEGRADATION OF LIGNOCELLULOSE.
US5892107A (en) 1996-11-08 1999-04-06 Arkenol, Inc. Method for the production of levulinic acid
ES2212866A1 (es) 2001-05-04 2004-08-01 Universidad Politecnica De Madrid Sistema de separacion fraccionada de la biomasa integral del cardo cynara carcunculus l.
EP1723099A1 (en) 2004-01-26 2006-11-22 Shell Internationale Researchmaatschappij B.V. Process for the reactive extraction of levulinic acid
EP1851186A1 (en) 2005-02-22 2007-11-07 Shell Internationale Research Maatschappij B.V. A process for permeation enhanced reactive extraction of levulinic acid
US8383838B2 (en) 2008-03-01 2013-02-26 MERCK Patent Gesellschaft mit beschränkter Haftung 5-oxo-2,3,4,5-tetrahydro-benzo[b]oxepine-4-carboxylic acid amides and 2,3-dihydro-benzo[b]oxepine-4-carboxylic acid amides for treatment and prevention of diabetes typ 1 and 2
US20110160479A1 (en) 2008-06-26 2011-06-30 POLIMERI EUROPA S.p.A., SAN DONATO MILANESE Process for the production of esters of levulinic acid from biomasses
US20100312006A1 (en) 2009-06-09 2010-12-09 Meadwestvaco Corporation Production of levulinic acid and levulinate esters from biomass
ITFI20090210A1 (it) 2009-09-29 2011-03-30 Luciana Gabriella Angelini Procedimento per la totale ed efficiente conversione di arundo donax a dare furaldeide, acido levulinico e derivati ligninici
WO2011039635A2 (en) 2009-09-29 2011-04-07 Nova Pangaea Technologies Limited Method and system for fractionation of lignocellulosic biomass
US20120111322A1 (en) 2010-11-09 2012-05-10 Impulse Devices, Inc. Method and Apparatus for Treatment of Cellulosic Biomass Materials in a Cavitation Reactor
WO2012112529A1 (en) 2011-02-14 2012-08-23 Xyleco, Inc. Processing biomass
EP2537841A1 (en) 2011-06-22 2012-12-26 DSM IP Assets B.V. Continuous production of furfural and levulininc acid
EP2780433A1 (en) 2011-11-14 2014-09-24 Shell Internationale Research Maatschappij B.V. Process for conversion of a cellulosic material
US9174909B2 (en) 2012-02-02 2015-11-03 Wisconsin Alumni Research Foundation Two-stage, acid-catalyzed conversion of carbohydrates into levulinic acid
EP2825519A1 (en) 2012-03-12 2015-01-21 Georgia-Pacific LLC Method for producing levulinic acid from lignocellulosis biomass
WO2013135965A1 (en) 2012-03-14 2013-09-19 Chempolis Oy Preparation of levulinic acid
US20150238923A1 (en) 2012-06-22 2015-08-27 Suganit Systems, Inc. Method and apparatus for treatment of biomass substrates
EP2712364A1 (en) 2012-07-13 2014-04-02 SAPPI Netherlands Services B.V. Low energy method for the preparation of non-derivatized nanocellulose
EP2872495A1 (en) 2012-07-13 2015-05-20 DSM IP Assets B.V. Process for the production of furfural and levulinic acid from lignocellulosic biomass
EP2684875A1 (en) * 2012-07-13 2014-01-15 DSM IP Assets B.V. Process for the production of furfural and levulinic acid from lignocellulosic biomass
CN102899950A (zh) 2012-10-25 2013-01-30 福建农林大学 一种超声波-微波同时辅助制备纳米纤维素的方法
EP2928856A1 (en) 2012-12-07 2015-10-14 DSM IP Assets B.V. Process for the production of a biomass hydrolysate
US20140315259A1 (en) 2013-03-15 2014-10-23 Edeniq, Inc. Cellulose co-feed for dry mill corn ethanol operations
EP3047029A1 (en) 2013-09-18 2016-07-27 Georgia-Pacific LLC Method for producing organic acids and organic acid degradation compounds from biomass
EP3080304A1 (en) 2013-12-11 2016-10-19 Versalis S.p.A. Process for the production of sugars from biomass
CN104074086A (zh) 2014-06-16 2014-10-01 南京泽朗医药科技有限公司 一种从苦菜中提取纤维素的方法
CN104292195A (zh) 2014-09-05 2015-01-21 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和调变流量制备乙酰丙酸的方法
CN104292194A (zh) 2014-09-05 2015-01-21 中国科学院广州能源研究所 一种生物质分级处理后制备糠醛和快速变温法制备乙酰丙酸的方法
CN104311411A (zh) 2014-09-15 2015-01-28 淮阴师范学院 多级酸水解制备乙酰丙酸的方法
EP3184518A1 (en) 2015-12-23 2017-06-28 Neste Oyj Combined levulinic acid and furfural production from biomass
WO2018013501A1 (en) 2016-07-14 2018-01-18 Api Intellectual Property Holdings, Llc Solvent-based processes for producing nanocellulose, and compositions and products produced therefrom
US20180194711A1 (en) 2017-01-11 2018-07-12 Battelle Memorial Institute Methods of making levulinic acid and alkyl levulinates from saccharides
EP3665147A1 (en) 2017-06-21 2020-06-17 Bio-On S.p.A. Process for producing levulinic acid
WO2020214835A1 (en) 2019-04-16 2020-10-22 University Of Louisville Research Foundation, Inc. One-pot acid-catalyzed levulinic acid production from lignocellulosic biomass
CN113214196A (zh) 2021-04-25 2021-08-06 武汉轻工大学 以木质纤维素类生物质为原料制备生物基化学品的方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
SARKER TUMPA R ET AL: "Hydrothermal pretreatment technologies for lignocellulosic biomass: A review of steam explosion and subcritical water hydrolysis", CHEMOSPHERE, PERGAMON PRESS, OXFORD, GB, vol. 284, 30 June 2021 (2021-06-30), XP086797665, ISSN: 0045-6535, [retrieved on 20210630], DOI: 10.1016/J.CHEMOSPHERE.2021.131372 *

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