IT1270972B - Procedimento ed apparecchiatura per l'analisi di composti volatili organici. - Google Patents

Procedimento ed apparecchiatura per l'analisi di composti volatili organici.

Info

Publication number
IT1270972B
IT1270972B ITMI930571A ITMI930571A IT1270972B IT 1270972 B IT1270972 B IT 1270972B IT MI930571 A ITMI930571 A IT MI930571A IT MI930571 A ITMI930571 A IT MI930571A IT 1270972 B IT1270972 B IT 1270972B
Authority
IT
Italy
Prior art keywords
analysis
procedure
equipment
volatile compounds
organic volatile
Prior art date
Application number
ITMI930571A
Other languages
English (en)
Inventor
Fausto Munari
Dimitris Kotzias
Matthew Duane
Original Assignee
Fisons Instr Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fisons Instr Spa filed Critical Fisons Instr Spa
Priority to ITMI930571A priority Critical patent/IT1270972B/it
Publication of ITMI930571A0 publication Critical patent/ITMI930571A0/it
Priority to PCT/EP1994/000889 priority patent/WO1994022009A2/en
Publication of ITMI930571A1 publication Critical patent/ITMI930571A1/it
Application granted granted Critical
Publication of IT1270972B publication Critical patent/IT1270972B/it

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N2030/022Column chromatography characterised by the kind of separation mechanism
    • G01N2030/025Gas chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • G01N2030/121Preparation by evaporation cooling; cold traps
    • G01N2030/122Preparation by evaporation cooling; cold traps cryogenic focusing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/32Control of physical parameters of the fluid carrier of pressure or speed
    • G01N2030/324Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

L'analisi di composti volatili organici in basse concentrazioni (ppb o ppt) viene effettuata facendo passare un flusso di campione attraverso una trappola fredda contenente pochi mg di impaccamento, con velocità di alimentazione del campione compresa nell'intervallo tra 50 e 1000 cm/sec; il campione così concentrato viene quindi desorbito per riscaldamento della trappola ed inviato all'analisi (figura 1).
ITMI930571A 1993-03-25 1993-03-25 Procedimento ed apparecchiatura per l'analisi di composti volatili organici. IT1270972B (it)

Priority Applications (2)

Application Number Priority Date Filing Date Title
ITMI930571A IT1270972B (it) 1993-03-25 1993-03-25 Procedimento ed apparecchiatura per l'analisi di composti volatili organici.
PCT/EP1994/000889 WO1994022009A2 (en) 1993-03-25 1994-03-22 A method and equipment for the analysis of volatile organic compounds

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ITMI930571A IT1270972B (it) 1993-03-25 1993-03-25 Procedimento ed apparecchiatura per l'analisi di composti volatili organici.

Publications (3)

Publication Number Publication Date
ITMI930571A0 ITMI930571A0 (it) 1993-03-25
ITMI930571A1 ITMI930571A1 (it) 1994-09-25
IT1270972B true IT1270972B (it) 1997-05-26

Family

ID=11365490

Family Applications (1)

Application Number Title Priority Date Filing Date
ITMI930571A IT1270972B (it) 1993-03-25 1993-03-25 Procedimento ed apparecchiatura per l'analisi di composti volatili organici.

Country Status (2)

Country Link
IT (1) IT1270972B (it)
WO (1) WO1994022009A2 (it)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8257951B2 (en) * 2002-10-28 2012-09-04 Little Sioux Corn Processors, LLC. Ethanol production process
ATE386265T1 (de) 2003-10-17 2008-03-15 Perkinelmer Las Inc Verfahren zur einführung von standardgas in ein probengefäss
CN102375041B (zh) 2011-09-16 2015-03-04 武汉市天虹仪表有限责任公司 一种在线挥发性有机物分析仪及其使用方法
CN103499662B (zh) * 2013-09-12 2015-01-28 苏州威阳环保科技有限公司 一种大气挥发性有机物取样分析装置及取样分析方法
KR101818841B1 (ko) * 2016-03-09 2018-01-16 포항공과대학교 산학협력단 휴대용 육불화황 분석 시스템
CN108627369B (zh) * 2017-03-20 2023-11-07 广州禾信仪器股份有限公司 大气挥发性有机物双级深冷在线富集浓缩采样系统及方法
CN109799302B (zh) * 2019-03-20 2021-08-31 上海市环境科学研究院 中等挥发性有机化合物近在线检测方法
CN112816644A (zh) * 2020-12-31 2021-05-18 杭州谱育科技发展有限公司 水中VOCs检测装置及方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3592064A (en) * 1969-02-18 1971-07-13 Bryggeriindustriens Forsknings Method for transferring a sample to be analyzed into the column of a gas chromatograph, and system for carrying out the method
US4998433A (en) * 1989-06-19 1991-03-12 Stumpf David K Method and means for condensing trace air contaminates from gases
US5141534A (en) * 1990-09-28 1992-08-25 The Regents Of The University Of Michigan Sample collection and inlet systems for gas chromatography apparatus
US5168746A (en) * 1991-06-03 1992-12-08 Hughes Aircraft Company Ambient ether vapor testing apparatus and method

Also Published As

Publication number Publication date
WO1994022009A3 (en) 1995-02-02
ITMI930571A1 (it) 1994-09-25
ITMI930571A0 (it) 1993-03-25
WO1994022009A2 (en) 1994-09-29

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Legal Events

Date Code Title Description
0001 Granted