IN2015DN01080A - - Google Patents

Info

Publication number
IN2015DN01080A
IN2015DN01080A IN1080DEN2015A IN2015DN01080A IN 2015DN01080 A IN2015DN01080 A IN 2015DN01080A IN 1080DEN2015 A IN1080DEN2015 A IN 1080DEN2015A IN 2015DN01080 A IN2015DN01080 A IN 2015DN01080A
Authority
IN
India
Prior art keywords
diketopiperazine
phosphonate esters
phosphonate
bisphosphonomethyl
salts
Prior art date
Application number
Inventor
Sebastian Burck
Frédéric Bruyneel
Patrick Notté
Original Assignee
Straitmark Holding Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Straitmark Holding Ag filed Critical Straitmark Holding Ag
Publication of IN2015DN01080A publication Critical patent/IN2015DN01080A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se)
    • C07F9/3804—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se) not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se)
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/04—Alpha- or beta- amino acids

Abstract

The present invention is related to a method for the synthesis of N- (phosphonomethyl)glycine or one of its derivatives selected from the group consisting of its salts, its phosphonate esters, or its phosphonate ester salts, which includes the steps of: • a) forming, in the presence an acid catalyst, a reaction mixture comprising 2,5- diketopiperazine, formaldehyde and a compound comprising one or more P-0-P anhydride moieties, said moieties having one P atom at the oxidation state (+ III) and the other P atom at the oxidation state (+III) or (+V), to form Ν,Ν'- bisphosphonomethyl-2,5- diketopiperazine, its mono- to tetra phosphonate esters, the dehydrated forms of Ν,Ν'- bisphosphonomethyl-2,5-diketopiperazine and the phosphonate esters of its dehydrated forms; • b) hydrolysing said N,N'-bisphosphonomethyl-2,5-diketopiperazine, its dehydrated forms or their phosphonate esters to obtain N- (phosphonomethyl)glycine or one of its derivatives selected from the group consisting of its salts, its phosphonate esters and its phosphonate ester salts.
IN1080DEN2015 2012-07-17 2013-07-17 IN2015DN01080A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12176756 2012-07-17
PCT/EP2013/065125 WO2014012991A1 (en) 2012-07-17 2013-07-17 Method for the synthesis of n-(phosphonomethyl)glycine

Publications (1)

Publication Number Publication Date
IN2015DN01080A true IN2015DN01080A (en) 2015-06-26

Family

ID=49034052

Family Applications (1)

Application Number Title Priority Date Filing Date
IN1080DEN2015 IN2015DN01080A (en) 2012-07-17 2013-07-17

Country Status (9)

Country Link
US (1) US9676799B2 (en)
EP (1) EP2875037B1 (en)
CN (1) CN104812764B (en)
BR (1) BR112015000995B1 (en)
ES (1) ES2609488T3 (en)
IN (1) IN2015DN01080A (en)
PL (1) PL2875037T3 (en)
RU (1) RU2674021C9 (en)
WO (1) WO2014012991A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113457654B (en) * 2021-06-02 2023-06-09 江西省科学院应用化学研究所 Carbon-based solid acid catalyst and preparation method and application method thereof

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Also Published As

Publication number Publication date
RU2674021C2 (en) 2018-12-04
PL2875037T4 (en) 2017-06-30
RU2015103310A (en) 2016-09-20
ES2609488T3 (en) 2017-04-20
BR112015000995B1 (en) 2020-04-28
BR112015000995A2 (en) 2017-06-27
CN104812764B (en) 2017-06-09
EP2875037A1 (en) 2015-05-27
RU2674021C9 (en) 2019-01-24
US9676799B2 (en) 2017-06-13
WO2014012991A1 (en) 2014-01-23
CN104812764A (en) 2015-07-29
PL2875037T3 (en) 2017-06-30
EP2875037B1 (en) 2016-09-07
US20150175636A1 (en) 2015-06-25

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