IL33275A - Preparation of hexaorgano-ditin compounds - Google Patents
Preparation of hexaorgano-ditin compoundsInfo
- Publication number
- IL33275A IL33275A IL6933275A IL3327569A IL33275A IL 33275 A IL33275 A IL 33275A IL 6933275 A IL6933275 A IL 6933275A IL 3327569 A IL3327569 A IL 3327569A IL 33275 A IL33275 A IL 33275A
- Authority
- IL
- Israel
- Prior art keywords
- formate
- preparation
- hexaorgano
- compounds
- grams
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title description 6
- BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 7
- 125000000217 alkyl group Chemical group 0.000 claims description 6
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 13
- -1 n-amyl Chemical group 0.000 description 12
- 239000000047 product Substances 0.000 description 9
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- POUGAXCXKDLEMK-UHFFFAOYSA-M tributylstannyl formate Chemical compound CCCC[Sn](CCCC)(CCCC)OC=O POUGAXCXKDLEMK-UHFFFAOYSA-M 0.000 description 6
- 238000004587 chromatography analysis Methods 0.000 description 4
- REDSKZBUUUQMSK-UHFFFAOYSA-N tributyltin Chemical compound CCCC[Sn](CCCC)CCCC.CCCC[Sn](CCCC)CCCC REDSKZBUUUQMSK-UHFFFAOYSA-N 0.000 description 4
- ZFXXTBRZIICKES-UHFFFAOYSA-M tripropylstannanylium formate Chemical compound C(=O)[O-].C(CC)[Sn+](CCC)CCC ZFXXTBRZIICKES-UHFFFAOYSA-M 0.000 description 4
- 239000012808 vapor phase Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000003085 diluting agent Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- DBGVGMSCBYYSLD-UHFFFAOYSA-N tributylstannane Chemical compound CCCC[SnH](CCCC)CCCC DBGVGMSCBYYSLD-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 239000003701 inert diluent Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 125000000582 cycloheptyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 125000004491 isohexyl group Chemical group C(CCC(C)C)* 0.000 description 1
- 125000001972 isopentyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000003760 magnetic stirring Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001280 n-hexyl group Chemical group C(CCCCC)* 0.000 description 1
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 150000002816 nickel compounds Chemical class 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- QKWDIJCUFKLSPQ-UHFFFAOYSA-N propylstannane Chemical compound CCC[SnH3] QKWDIJCUFKLSPQ-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000000547 substituted alkyl group Chemical group 0.000 description 1
- 125000005346 substituted cycloalkyl group Chemical group 0.000 description 1
- AFCAKJKUYFLYFK-UHFFFAOYSA-N tetrabutyltin Chemical compound CCCC[Sn](CCCC)(CCCC)CCCC AFCAKJKUYFLYFK-UHFFFAOYSA-N 0.000 description 1
- OIPBGNVROXPTQF-UHFFFAOYSA-M triethylstannyl formate Chemical compound CC[Sn](CC)(CC)OC=O OIPBGNVROXPTQF-UHFFFAOYSA-M 0.000 description 1
- WGVAEMZGVLMQFF-UHFFFAOYSA-M trioctylstannanylium formate Chemical compound C(=O)[O-].C(CCCCCCC)[Sn+](CCCCCCCC)CCCCCCCC WGVAEMZGVLMQFF-UHFFFAOYSA-M 0.000 description 1
- NSPWVJAKNXJHEP-UHFFFAOYSA-N tripropyltin Chemical compound CCC[Sn](CCC)CCC NSPWVJAKNXJHEP-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2288—Compounds with one or more Sn-metal linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Furniture Connections (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77332968A | 1968-11-04 | 1968-11-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL33275A0 IL33275A0 (en) | 1969-12-31 |
| IL33275A true IL33275A (en) | 1973-02-28 |
Family
ID=25097898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL6933275A IL33275A (en) | 1968-11-04 | 1969-10-29 | Preparation of hexaorgano-ditin compounds |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US3652618A (da) |
| JP (1) | JPS5016779B1 (da) |
| AT (1) | AT293436B (da) |
| BE (1) | BE741048A (da) |
| BR (1) | BR6913862D0 (da) |
| CH (1) | CH529169A (da) |
| DE (1) | DE1955241A1 (da) |
| DK (1) | DK131291B (da) |
| ES (1) | ES372808A1 (da) |
| GB (1) | GB1255829A (da) |
| IL (1) | IL33275A (da) |
| NL (1) | NL166690C (da) |
| NO (1) | NO131933C (da) |
| SE (1) | SE360362B (da) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4231083A1 (de) * | 1992-09-17 | 1994-03-24 | Witco Gmbh | Verfahren zur Herstellung von Distannanen |
| DE102004043231A1 (de) * | 2004-09-07 | 2006-03-09 | Biotronik Vi Patent Ag | Endoprothese aus einer Magnesiumlegierung |
-
1968
- 1968-11-04 US US773329A patent/US3652618A/en not_active Expired - Lifetime
-
1969
- 1969-09-29 JP JP44077721A patent/JPS5016779B1/ja active Pending
- 1969-10-23 ES ES372808A patent/ES372808A1/es not_active Expired
- 1969-10-27 DK DK567569AA patent/DK131291B/da unknown
- 1969-10-27 NL NL6916139.A patent/NL166690C/xx not_active IP Right Cessation
- 1969-10-29 IL IL6933275A patent/IL33275A/en unknown
- 1969-10-30 BE BE741048D patent/BE741048A/xx not_active IP Right Cessation
- 1969-11-03 NO NO4340/69A patent/NO131933C/no unknown
- 1969-11-03 CH CH1636569A patent/CH529169A/de not_active IP Right Cessation
- 1969-11-03 BR BR213862/69A patent/BR6913862D0/pt unknown
- 1969-11-03 DE DE19691955241 patent/DE1955241A1/de active Pending
- 1969-11-03 SE SE15017/69A patent/SE360362B/xx unknown
- 1969-11-04 GB GB54059/69A patent/GB1255829A/en not_active Expired
- 1969-11-04 AT AT1035869A patent/AT293436B/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CH529169A (de) | 1972-10-15 |
| ES372808A1 (es) | 1971-11-01 |
| AT293436B (de) | 1971-10-11 |
| NL6916139A (da) | 1970-05-08 |
| GB1255829A (en) | 1971-12-01 |
| NO131933B (da) | 1975-05-20 |
| DK131291C (da) | 1975-11-17 |
| IL33275A0 (en) | 1969-12-31 |
| BE741048A (da) | 1970-04-01 |
| SE360362B (da) | 1973-09-24 |
| US3652618A (en) | 1972-03-28 |
| NO131933C (da) | 1975-08-27 |
| DE1955241A1 (de) | 1970-06-11 |
| DK131291B (da) | 1975-06-23 |
| NL166690C (nl) | 1981-09-15 |
| JPS5016779B1 (da) | 1975-06-16 |
| BR6913862D0 (pt) | 1973-01-04 |
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