IE45288B1 - Improvements in or relating to pharmaceutical compostions for x-ray visualisation of the alimentary canal, and processes for preparing such compositions - Google Patents
Improvements in or relating to pharmaceutical compostions for x-ray visualisation of the alimentary canal, and processes for preparing such compositionsInfo
- Publication number
- IE45288B1 IE45288B1 IE1088/77A IE108877A IE45288B1 IE 45288 B1 IE45288 B1 IE 45288B1 IE 1088/77 A IE1088/77 A IE 1088/77A IE 108877 A IE108877 A IE 108877A IE 45288 B1 IE45288 B1 IE 45288B1
- Authority
- IE
- Ireland
- Prior art keywords
- compositions
- polyacrylamide
- barium sulphate
- agent
- grams
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 8
- 239000000203 mixture Substances 0.000 title claims description 46
- 238000012800 visualization Methods 0.000 title claims description 6
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims abstract description 56
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 27
- 239000008194 pharmaceutical composition Substances 0.000 claims abstract description 11
- 239000008135 aqueous vehicle Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000012153 distilled water Substances 0.000 claims description 9
- 239000004599 antimicrobial Substances 0.000 claims description 5
- 239000002562 thickening agent Substances 0.000 claims description 5
- 239000002518 antifoaming agent Substances 0.000 claims description 4
- 229910052788 barium Inorganic materials 0.000 abstract description 9
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 abstract description 9
- 210000001035 gastrointestinal tract Anatomy 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 24
- 239000000725 suspension Substances 0.000 description 17
- 238000002360 preparation method Methods 0.000 description 13
- 239000000796 flavoring agent Substances 0.000 description 11
- 235000013355 food flavoring agent Nutrition 0.000 description 10
- 230000003254 anti-foaming effect Effects 0.000 description 9
- 239000003651 drinking water Substances 0.000 description 9
- 235000020188 drinking water Nutrition 0.000 description 9
- 235000003599 food sweetener Nutrition 0.000 description 9
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 9
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 9
- 229960002216 methylparaben Drugs 0.000 description 9
- 229920001296 polysiloxane Polymers 0.000 description 9
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 description 9
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 description 9
- 239000003765 sweetening agent Substances 0.000 description 9
- 239000000499 gel Substances 0.000 description 8
- 238000009472 formulation Methods 0.000 description 7
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 6
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 6
- 239000000546 pharmaceutical excipient Substances 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 5
- 229920000159 gelatin Polymers 0.000 description 5
- 235000019322 gelatine Nutrition 0.000 description 5
- 210000000056 organ Anatomy 0.000 description 5
- 108010010803 Gelatin Proteins 0.000 description 4
- 239000008273 gelatin Substances 0.000 description 4
- 235000011852 gelatine desserts Nutrition 0.000 description 4
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 4
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 description 4
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 210000001072 colon Anatomy 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 238000000265 homogenisation Methods 0.000 description 3
- 229940071826 hydroxyethyl cellulose Drugs 0.000 description 3
- 210000004400 mucous membrane Anatomy 0.000 description 3
- 210000002784 stomach Anatomy 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- FJKROLUGYXJWQN-UHFFFAOYSA-M 4-hydroxybenzoate Chemical compound OC1=CC=C(C([O-])=O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-M 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 229960004106 citric acid Drugs 0.000 description 2
- 235000015165 citric acid Nutrition 0.000 description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 2
- 230000037406 food intake Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 210000004379 membrane Anatomy 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229960000281 trometamol Drugs 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 1
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- HWSISDHAHRVNMT-UHFFFAOYSA-N Bismuth subnitrate Chemical compound O[NH+]([O-])O[Bi](O[N+]([O-])=O)O[N+]([O-])=O HWSISDHAHRVNMT-UHFFFAOYSA-N 0.000 description 1
- 241000792859 Enema Species 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 229920000715 Mucilage Polymers 0.000 description 1
- 235000009421 Myristica fragrans Nutrition 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- 208000005374 Poisoning Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 241000222354 Trametes Species 0.000 description 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- -1 alkaline earth metal salt Chemical class 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 150000001621 bismuth Chemical class 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- 229940036348 bismuth carbonate Drugs 0.000 description 1
- 229960001482 bismuth subnitrate Drugs 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- GMZOPRQQINFLPQ-UHFFFAOYSA-H dibismuth;tricarbonate Chemical compound [Bi+3].[Bi+3].[O-]C([O-])=O.[O-]C([O-])=O.[O-]C([O-])=O GMZOPRQQINFLPQ-UHFFFAOYSA-H 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 210000001198 duodenum Anatomy 0.000 description 1
- 239000007920 enema Substances 0.000 description 1
- 229940079360 enema for constipation Drugs 0.000 description 1
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 1
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 150000004676 glycans Polymers 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 239000001115 mace Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 210000001331 nose Anatomy 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004804 polysaccharides Polymers 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000011158 quantitative evaluation Methods 0.000 description 1
- 230000009291 secondary effect Effects 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- WSWCOQWTEOXDQX-MQQKCMAXSA-N sorbic acid group Chemical group C(\C=C\C=C\C)(=O)O WSWCOQWTEOXDQX-MQQKCMAXSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- ZCUFMDLYAMJYST-UHFFFAOYSA-N thorium dioxide Chemical compound O=[Th]=O ZCUFMDLYAMJYST-UHFFFAOYSA-N 0.000 description 1
- 229910003452 thorium oxide Inorganic materials 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K49/00—Preparations for testing in vivo
- A61K49/04—X-ray contrast preparations
- A61K49/0404—X-ray contrast preparations containing barium sulfate
Landscapes
- Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7615975A FR2352544A1 (fr) | 1976-05-26 | 1976-05-26 | Nouveau medicament pour opacification barytee et procede de preparation de ce nouveau medicament |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE45288L IE45288L (en) | 1977-11-26 |
| IE45288B1 true IE45288B1 (en) | 1982-07-28 |
Family
ID=9173679
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE1088/77A IE45288B1 (en) | 1976-05-26 | 1977-05-26 | Improvements in or relating to pharmaceutical compostions for x-ray visualisation of the alimentary canal, and processes for preparing such compositions |
Country Status (13)
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL63876A0 (en) * | 1980-10-20 | 1981-12-31 | Population Res Inc | Radiopaque cyanoacrylates |
| US4477439A (en) * | 1981-04-13 | 1984-10-16 | Walter J. Monacelli | Treatment of irritated and excoriated areas around the stoma of ostomy patients |
| GR880100428A (el) * | 1988-06-29 | 1990-05-11 | Georgios Kallimanis | Μεθοδος παρασκευης γαλακτωδους θειικου βαριου,προς ληψιν ακτινογραφιων διπλης αντιθεσεως |
| JP2722218B2 (ja) * | 1988-09-22 | 1998-03-04 | 太田製薬株式会社 | 大腸ｘ線検査用硫酸バリウム造影剤 |
| US5013560A (en) * | 1989-03-17 | 1991-05-07 | The Procter & Gamble Company | Microbially-stable bismuth-containing liquid pharmaceutical suspensions |
| US5496535A (en) | 1991-04-12 | 1996-03-05 | Alliance Pharmaceutical Corp. | Fluorocarbon contrast media for use with MRI and radiographic imaging |
| US5342605A (en) * | 1992-05-01 | 1994-08-30 | Sterling Winthrop Inc. | Polymeric X-ray compositions containing iodinated polymeric beads |
| US5318768A (en) * | 1992-05-01 | 1994-06-07 | Sterling Winthrop Inc. | Polymeric x-ray contrast compositions containing an organic crystalline x-ray contrast agent |
| US5405600A (en) * | 1992-05-01 | 1995-04-11 | Sterling Winthrop Inc. | X-ray contrast compositions containing film-forming materials |
| US5443814A (en) * | 1992-05-01 | 1995-08-22 | Sterling Winthrop, Inc. | X-ray contrast compositions containing iodophenoxyalkanes and cellulose derivatives |
| US5352434A (en) * | 1992-05-01 | 1994-10-04 | Sterling Winthrop Inc. | X-ray contrast compositions containing a barium salt and film-forming materials |
| US5476646A (en) * | 1992-05-01 | 1995-12-19 | Sterling Winthrop Inc. | X-ray contrast compositions containing iodophenoxyalkanes and pharmaceutically acceptable clays |
| US5326553A (en) * | 1993-02-02 | 1994-07-05 | Sterling Winthrop Inc. | Compositions of iodophenoxy alkanes and iodophenyl ethers in film-forming materials for visualization of the gastrointestinal tract |
| US5424056A (en) * | 1993-03-01 | 1995-06-13 | Sterling Wintrhop Inc. | X-ray contrast compositions containing iodoaniline derivatives and pharmaceutically acceptable clays |
| US5330740A (en) * | 1993-03-01 | 1994-07-19 | Sterling Winthrop Inc. | Compositions of iodoaniline derivatives in film-forming materials for visualization of the gastrointestinal tract |
| US5310538A (en) * | 1993-03-11 | 1994-05-10 | Sterling Winthrop Inc. | Compositions of iodophenoxy alkylene ethers in film-forming materials for visualization of the gastrointestinal tract |
| US5312616A (en) * | 1993-03-11 | 1994-05-17 | Sterling Winthrop Inc. | Compositions of iodobenzoic acid derivatives in film-forming materials for visualization of the gastrointestinal tract |
| US5336484A (en) * | 1993-03-31 | 1994-08-09 | Sterling Winthrop Inc. | Compositions of iodophenyl esters and iodophenyl sulfonates in film-forming materials for visualization of the gastronintestinal tract |
| US5543132A (en) * | 1994-04-14 | 1996-08-06 | Sterling Winthrop Inc. | X-ray contrast compositions containing a barium salt and a cellulose derivative |
| US5368837A (en) * | 1994-04-14 | 1994-11-29 | Sterling Winthrop Inc. | X-ray contrast compositions containing an organic crystalline X-ray contrast agent and a cellulose derivative |
| US5525327A (en) * | 1994-04-14 | 1996-06-11 | Sterling Winthrop Inc. | Polymeric x-ray contrast compositions containing iodinated polymeric beads and microcrystaline cellulose |
| US5360604A (en) * | 1994-04-14 | 1994-11-01 | Sterling Winthrop Inc. | X-ray contrast compositions containing an organic crystalline X-ray contrast agent in combination with pharmaceutically acceptable clays |
| US5593657A (en) * | 1995-02-09 | 1997-01-14 | Nanosystems L.L.C. | Barium salt formulations stabilized by non-ionic and anionic stabilizers |
| ES2112765B1 (es) * | 1995-08-02 | 1999-03-01 | Cantabria Ind Farmaceutica Sa | Procedimiento para la obtencion de formulaciones de constraste radiologico, para exploraciones gastrointestinales de uso extemporaneo y directo. |
| AUPQ605500A0 (en) * | 2000-03-07 | 2000-03-30 | Medefield Pty Ltd | Stool marker |
| US7591998B2 (en) * | 2000-03-07 | 2009-09-22 | Kevin Tait | Stool marker |
| US20060009694A1 (en) * | 2004-05-17 | 2006-01-12 | Yousefzadeh David K | Methods of attenuating internal radiation exposure |
| US20080085892A1 (en) * | 2006-08-31 | 2008-04-10 | Sangeetha Kandeepan | Liquid dosage form of acetaminophen |
| JP5742087B2 (ja) * | 2008-08-29 | 2015-07-01 | オイレス工業株式会社 | 複層摺動部材及びそれを用いた自動車のラックピニオン式舵取装置におけるラックガイド |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1128922A (en) * | 1964-10-14 | 1968-10-02 | Chugai Pharmaceutical Co Ltd | Adjuvants for gastric and intestinal x-ray photographic examination |
| US3539682A (en) * | 1967-06-23 | 1970-11-10 | Astra Ab | X-ray contrast medium containing barium sulphate |
| FR2077687B1 (US06346242-20020212-C00066.png) * | 1970-02-05 | 1973-03-16 | Roussel Uclaf | |
| SE397473B (sv) * | 1974-03-14 | 1977-11-07 | Pharmacia Ab | Anvendningen av polymerpartiklar som tillsatsmedel i rontgenkontrastmedel baserade pa bariumsulfat eller liknande |
-
1976
- 1976-05-26 FR FR7615975A patent/FR2352544A1/fr active Granted
-
1977
- 1977-05-13 IL IL52081A patent/IL52081A/xx unknown
- 1977-05-18 ZA ZA00772966A patent/ZA772966B/xx unknown
- 1977-05-18 CA CA278,687A patent/CA1091579A/fr not_active Expired
- 1977-05-23 US US05/799,163 patent/US4120946A/en not_active Expired - Lifetime
- 1977-05-25 AU AU25488/77A patent/AU507889B2/en not_active Expired
- 1977-05-25 NL NL7705738A patent/NL7705738A/xx not_active Application Discontinuation
- 1977-05-25 BE BE177900A patent/BE855032A/xx unknown
- 1977-05-26 HU HU77RO00000931A patent/HU173006B/hu unknown
- 1977-05-26 DE DE19772723878 patent/DE2723878A1/de active Granted
- 1977-05-26 JP JP6053477A patent/JPS52145526A/ja active Granted
- 1977-05-26 IE IE1088/77A patent/IE45288B1/en unknown
- 1977-05-26 GB GB22229/77A patent/GB1553482A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| IE45288L (en) | 1977-11-26 |
| JPS52145526A (en) | 1977-12-03 |
| FR2352544A1 (fr) | 1977-12-23 |
| ZA772966B (en) | 1978-06-28 |
| GB1553482A (en) | 1979-09-26 |
| NL7705738A (nl) | 1977-11-29 |
| DE2723878C2 (US06346242-20020212-C00066.png) | 1987-10-22 |
| FR2352544B1 (US06346242-20020212-C00066.png) | 1978-10-20 |
| AU507889B2 (en) | 1980-02-28 |
| HU173006B (hu) | 1979-01-28 |
| IL52081A0 (en) | 1977-07-31 |
| JPS618044B2 (US06346242-20020212-C00066.png) | 1986-03-11 |
| US4120946A (en) | 1978-10-17 |
| BE855032A (fr) | 1977-11-25 |
| IL52081A (en) | 1980-05-30 |
| DE2723878A1 (de) | 1977-12-15 |
| CA1091579A (fr) | 1980-12-16 |
| AU2548877A (en) | 1978-11-30 |
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