IE43206L - Separating crystallizable materials from a multi-component¹system - Google Patents

Separating crystallizable materials from a multi-component¹system

Info

Publication number
IE43206L
IE43206L IE752653A IE265375A IE43206L IE 43206 L IE43206 L IE 43206L IE 752653 A IE752653 A IE 752653A IE 265375 A IE265375 A IE 265375A IE 43206 L IE43206 L IE 43206L
Authority
IE
Ireland
Prior art keywords
ice
heat exchanger
separating
columns
concentrate
Prior art date
Application number
IE752653A
Other versions
IE43206B1 (en
Original Assignee
D E J Internat Res Co B V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by D E J Internat Res Co B V filed Critical D E J Internat Res Co B V
Publication of IE43206L publication Critical patent/IE43206L/en
Publication of IE43206B1 publication Critical patent/IE43206B1/en

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25CPRODUCING, WORKING OR HANDLING ICE
    • F25C5/00Working or handling ice
    • F25C5/02Apparatus for disintegrating, removing or harvesting ice
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F5/00Coffee; Coffee substitutes; Preparations thereof
    • A23F5/24Extraction of coffee; Coffee extracts; Making instant coffee
    • A23F5/28Drying or concentrating coffee extract
    • A23F5/30Drying or concentrating coffee extract by freezing out the water
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08Concentrating or drying of juices
    • A23L2/12Concentrating or drying of juices by freezing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0013Crystallisation cooling by heat exchange by indirect heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/004Fractional crystallisation; Fractionating or rectifying columns
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0059General arrangements of crystallisation plant, e.g. flow sheets
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25CPRODUCING, WORKING OR HANDLING ICE
    • F25C1/00Producing ice
    • F25C1/04Producing ice by using stationary moulds
    • F25C1/06Producing ice by using stationary moulds open or openable at both ends

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • Tea And Coffee (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

1507034 Crystallisation process DEJ INTERNATIONAL RESEARCH CO BV 26 Nov 1975 [6 Dec 1974] 52900/74 Heading BIG A process for separating crystallisable material out of a multi - component liquid system comprises the following steps performed in sequence latchwise: (a) confining a batch of liquid in a heat exchanger, (b) applying cooling to the heat exchanger to crystallise at least part of the crystallisable material and create a substantially coherent matrix of crystals, (c) removing the material formed in step (b) from the heat exchanger, (d) breaking up the material from step (c) into a predetermined size and (e) separating crystallised material from the remainder of the multi - component system. Suitable aparatus, as shown in Fig. 1, for the freeze concentration of e.g. aqueous systems such as coffee extract and fruit juices, comprises a storage vessel (1), a number of shell and tube heat exchangers (3-12) mounted in parallel and connected to a central feed line, below the heat exchangers are an equal number of grinding means for breaking up the columns of ice and concentrate and simultaneously mixing the broken ice with recirculated concentrate and a washing column (13) for separating ice and concentrate. The process is carried out so that at the end of each freeze cycle the pump (2) pumps feed solution into the heat exchanger and so forces the columns of ice crystals and concentrate which have formed in the heat exchanger out of the exchanger, the columns of ice having first been released from the tube walls by briefly applying heat. A new freezing cycle starts when only a small frozen plug (28) remains in each tube (27). The frozen columns are broken up upon leaving the tubes by the knives (30) driven by a motor (33). The mixture of ice and concentrates enters the mixing vessel (32) at regular intervals and is transformed into a slurry for processing by the separating apparatus i.e. a washing column (13). [GB1507034A]
IE2653/75A 1974-12-06 1975-12-05 A process for separating crystallizable materials from a multi-component system IE43206B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB52900/74A GB1507034A (en) 1974-12-06 1974-12-06 Process and apparatus for separating crystallizable materials from a multi-component system

Publications (2)

Publication Number Publication Date
IE43206L true IE43206L (en) 1976-06-06
IE43206B1 IE43206B1 (en) 1981-01-14

Family

ID=10465753

Family Applications (1)

Application Number Title Priority Date Filing Date
IE2653/75A IE43206B1 (en) 1974-12-06 1975-12-05 A process for separating crystallizable materials from a multi-component system

Country Status (17)

Country Link
JP (1) JPS5178784A (en)
AT (1) AT362747B (en)
AU (1) AU504996B2 (en)
BE (1) BE836238A (en)
BR (1) BR7508075A (en)
CA (1) CA1033284A (en)
CH (1) CH604803A5 (en)
DE (1) DE2554878A1 (en)
DK (1) DK551775A (en)
FR (1) FR2293231A1 (en)
GB (1) GB1507034A (en)
IE (1) IE43206B1 (en)
IT (1) IT1051299B (en)
LU (1) LU73933A1 (en)
NL (1) NL7514031A (en)
SE (1) SE412993B (en)
ZA (1) ZA757433B (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DK138672B (en) * 1976-09-28 1978-10-16 Danske Sukkerfab Crystallization apparatus.
US5304384A (en) 1993-03-23 1994-04-19 Labatt Brewing Company Limited Improvements in production of fermented malt beverages
US5695795A (en) 1993-03-23 1997-12-09 Labatt Brewing Company Limited Methods for chill-treating non-distilled malted barley beverages
USRE36897E (en) 1993-03-23 2000-10-03 Labatt Brewing Company Limited Methods for chill treating non-distilled malted barley beverages
US5869114A (en) 1994-03-18 1999-02-09 Labatt Brewing Company Limited Production of fermented malt beverages
EP2130572A1 (en) * 2008-06-06 2009-12-09 Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO Rotating knife, washing column, and method for disintegrating a crystal bed in a washing column
DE102016202285B4 (en) * 2016-02-15 2022-03-03 Deutsches Zentrum für Luft- und Raumfahrt e.V. Heat transfer device, heat storage device and method for transferring heat
RU192489U1 (en) * 2019-04-26 2019-09-18 Федеральное государственное бюджетное образовательное учреждение высшего образования "Волгоградский государственный технический университет" (ВолгГТУ) Tubular mold
RU198654U1 (en) * 2020-04-23 2020-07-21 Федеральное государственное бюджетное образовательное учреждение высшего образования "Волгоградский государственный технический университет" (ВолгГТУ) TUBULAR CRYSTALLIZER

Also Published As

Publication number Publication date
FR2293231B1 (en) 1981-09-04
FR2293231A1 (en) 1976-07-02
ZA757433B (en) 1976-11-24
AU504996B2 (en) 1979-11-08
NL7514031A (en) 1976-06-09
AU8708875A (en) 1977-06-02
AT362747B (en) 1981-06-10
BE836238A (en) 1976-06-03
IT1051299B (en) 1981-04-21
IE43206B1 (en) 1981-01-14
CH604803A5 (en) 1978-09-15
ATA919375A (en) 1980-11-15
JPS5178784A (en) 1976-07-08
SE412993B (en) 1980-03-31
DE2554878A1 (en) 1976-06-16
DK551775A (en) 1976-06-07
LU73933A1 (en) 1976-07-01
SE7513699L (en) 1976-06-08
GB1507034A (en) 1978-04-12
BR7508075A (en) 1976-08-24
CA1033284A (en) 1978-06-20

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