IE32209L - Production of urea - Google Patents

Production of urea

Info

Publication number
IE32209L
IE32209L IE680894A IE89468A IE32209L IE 32209 L IE32209 L IE 32209L IE 680894 A IE680894 A IE 680894A IE 89468 A IE89468 A IE 89468A IE 32209 L IE32209 L IE 32209L
Authority
IE
Ireland
Prior art keywords
urea
excess
solution
synthesis zone
gaseous
Prior art date
Application number
IE680894A
Other versions
IE32209B1 (en
Inventor
M Guadalupi
U Zardi
Original Assignee
Snam Progetti
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Snam Progetti filed Critical Snam Progetti
Publication of IE32209L publication Critical patent/IE32209L/en
Publication of IE32209B1 publication Critical patent/IE32209B1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J17/00Gas-filled discharge tubes with solid cathode
    • H01J17/02Details
    • H01J17/04Electrodes; Screens
    • H01J17/06Cathodes
    • H01J17/066Cold cathodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2893/00Discharge tubes and lamps
    • H01J2893/0064Tubes with cold main electrodes (including cold cathodes)
    • H01J2893/0065Electrode systems
    • H01J2893/0066Construction, material, support, protection and temperature regulation of electrodes; Electrode cups
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/141Feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,184,004. Urea. SNAM PROGETTI S.p.A. 27 June, 1968 [29 Sept., 1967], No. 30814/68. Heading C2C. Urea production comprises feeding gaseous CO 2 and an excess of liquid or gaseous NH 3 to a synthesis zone in a reactor, reacting the CO 2 and NH 3 therein so as to produce, as the reaction product, a solution of urea contaminated with ammonium carbamate and containing the excess NH 3 , causing or allowing the said solution to flow as a thin film over a surface in a decomposition chamber in which the temperature and pressure are substantially the same, heated to an extent sufficient to cause at least part of the ammonium carbamate to decompose into gaseous CO 2 and NH 3 , recycling the decomposition products as well as the excess NH 3 to the synthesis zone, and recovering the urea solution having a reduced ammonium carbamate content. The thin liquid film may be obtained, e.g. by allowing the reaction product to drop along the inside wall of a heat exchanger or along the wall of part of the reactor other than the synthesis zone. Synthesis and decomposition may be effected at a temperature of 180- 350‹ C. and pressure of 100-300 atm. The presence of NH 3 excess and consequent dissolved NH 3 in the solution from the synthesis zone is essential and the usual NH 3 /CO 2 ratio is from 2À3:1 to 5À5:1. [GB1184004A]
IE894/68A 1967-09-29 1968-07-25 Process for the production of urea having a low carbamate content IE32209B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT2102767 1967-09-29

Publications (2)

Publication Number Publication Date
IE32209L true IE32209L (en) 1969-03-29
IE32209B1 IE32209B1 (en) 1973-05-16

Family

ID=11175595

Family Applications (1)

Application Number Title Priority Date Filing Date
IE894/68A IE32209B1 (en) 1967-09-29 1968-07-25 Process for the production of urea having a low carbamate content

Country Status (15)

Country Link
JP (1) JPS5432767B1 (en)
AT (1) AT290545B (en)
BE (1) BE719035A (en)
CH (1) CH487855A (en)
CS (1) CS155191B2 (en)
DE (1) DE1768776B2 (en)
DK (1) DK118396B (en)
ES (1) ES358855A1 (en)
FR (1) FR1576811A (en)
GB (1) GB1184004A (en)
IE (1) IE32209B1 (en)
LU (1) LU56630A1 (en)
NL (1) NL161137C (en)
NO (1) NO145949C (en)
SE (1) SE373574B (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BG35038A3 (en) * 1977-05-05 1984-01-16 Montedison Spa,It Method and installation for synthesis of urea
NL7713190A (en) * 1977-11-30 1979-06-01 Unie Van Kunstmestfab Bv METHOD AND DEVICE FOR THE REMOVAL OF AMMONIUM CARBAMATE FROM A UREEA SYNTHESIS SOLUTION.
IT1209532B (en) * 1984-04-20 1989-08-30 Snam Progetti PROCESS FOR THE SYNTHESIS OF UREA AND MATERIAL USED IN ITSELF.
IN169678B (en) * 1987-08-13 1991-11-30 Austral Pacific Fertilizers
IT1274362B (en) 1995-02-16 1997-07-17 Snam Progetti HIGH YIELD PROCEDURE FOR THE SYNTHESIS OF UREA
ITMI20120013A1 (en) 2012-01-09 2013-07-10 Saipem Spa PROCEDURE FOR THE SYNTHESIS OF UREA INCLUDING A STRIPPER FUND OF PASSIVATION
US20240092730A1 (en) 2021-12-20 2024-03-21 Stamicarbon B.V. Thermal stripping urea production

Also Published As

Publication number Publication date
NO145949C (en) 1982-06-30
SE373574B (en) 1975-02-10
CH487855A (en) 1970-03-31
DK118396B (en) 1970-08-17
NO145949B (en) 1982-03-22
CS155191B2 (en) 1974-05-30
BE719035A (en) 1969-01-16
IE32209B1 (en) 1973-05-16
NL161137C (en) 1980-01-15
ES358855A1 (en) 1970-05-16
AT290545B (en) 1971-06-11
NL6808895A (en) 1969-04-01
FR1576811A (en) 1969-08-01
GB1184004A (en) 1970-03-11
DE1768776A1 (en) 1971-09-16
DE1768776B2 (en) 1973-05-03
JPS5432767B1 (en) 1979-10-16
NL161137B (en) 1979-08-15
LU56630A1 (en) 1968-11-14

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