GB1423977A - Urea synthesis with heat recovery and ammonium carbamate recirculation - Google Patents

Urea synthesis with heat recovery and ammonium carbamate recirculation

Info

Publication number
GB1423977A
GB1423977A GB2138474A GB2138474A GB1423977A GB 1423977 A GB1423977 A GB 1423977A GB 2138474 A GB2138474 A GB 2138474A GB 2138474 A GB2138474 A GB 2138474A GB 1423977 A GB1423977 A GB 1423977A
Authority
GB
United Kingdom
Prior art keywords
urea
ammonia
carbon dioxide
carbamate
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2138474A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US369756A external-priority patent/US3886210A/en
Application filed by Individual filed Critical Individual
Publication of GB1423977A publication Critical patent/GB1423977A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1423977 Urea I MAVROVIC 14 May 1974 [13 June 1973] 21384/74 Heading C2C Urea is synthesized from ammonia and carbon dioxide in a process in which a first aqueous urea solution comprising urea, ammonium carbonate, ammonia and water is produced at elevated temperature and pressure, the process comprising (a) reducing the pressure and heating the first aqueous urea solution in a first carbamate decomposing zone to decompose from 10 to 60% by weight of the ammonium carbamate therein to ammonia and carbon dioxide, (b) heating the first aqueous urea solution in a second carbamate decomposing zone to decompose additional ammonium carbamate to ammonia and carbon dioxide and to produce a liquid phase comprising urea, water, residual ammonium carbamate and residual excess ammonia, and a gaseous phase comprising carbon dioxide, ammonia and water, (c) separating the gaseous phase and the liquid phase, and (d) contacting this gaseous phase, urea and fresh carbon dioxide to form ammonium carbonate in indirect heat exchange with the first aqueous urea solution, the quantity of urea so contacted being such that the reaction product has a urea to water weight ratio of 0À1 : 1 to 1À6 : 1.
GB2138474A 1973-06-13 1974-05-14 Urea synthesis with heat recovery and ammonium carbamate recirculation Expired GB1423977A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US369756A US3886210A (en) 1970-06-29 1973-06-13 Urea synthesis with improved heat recovery and ammonium carbamate recirculation

Publications (1)

Publication Number Publication Date
GB1423977A true GB1423977A (en) 1976-02-04

Family

ID=23456789

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2138474A Expired GB1423977A (en) 1973-06-13 1974-05-14 Urea synthesis with heat recovery and ammonium carbamate recirculation

Country Status (13)

Country Link
JP (1) JPS585189B2 (en)
AR (1) AR200786A1 (en)
BE (1) BE816142A (en)
BR (1) BR7404845D0 (en)
CA (1) CA1026374A (en)
DE (1) DE2425581A1 (en)
ES (1) ES426986A1 (en)
FR (2) FR2244755B1 (en)
GB (1) GB1423977A (en)
IN (1) IN140206B (en)
IT (1) IT1015048B (en)
NL (1) NL182219C (en)
TR (1) TR18243A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7062131B2 (en) 2019-03-18 2022-05-02 三菱電機株式会社 Plate heat exchanger and heat pump device equipped with it

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5189A (en) * 1974-06-20 1976-01-05 Sakuhei Fujita Magaripaipuniokeru anaakehoho

Also Published As

Publication number Publication date
FR2244755A1 (en) 1975-04-18
DE2425581A1 (en) 1975-01-09
CA1026374A (en) 1978-02-14
AR200786A1 (en) 1974-12-13
NL182219B (en) 1987-09-01
BR7404845D0 (en) 1975-09-30
TR18243A (en) 1976-11-10
FR2272984A1 (en) 1975-12-26
JPS5035115A (en) 1975-04-03
IN140206B (en) 1976-09-25
IT1015048B (en) 1977-05-10
JPS585189B2 (en) 1983-01-29
FR2272984B1 (en) 1979-07-13
FR2244755B1 (en) 1977-10-07
BE816142A (en) 1974-12-10
NL182219C (en) 1988-02-01
ES426986A1 (en) 1976-09-01
NL7407873A (en) 1974-12-17

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee