HUP9702406A1 - Folyamatos eljárás aromás szubsztrátumok dinitrálására - Google Patents
Folyamatos eljárás aromás szubsztrátumok dinitrálásáraInfo
- Publication number
- HUP9702406A1 HUP9702406A1 HU9702406A HUP9702406A HUP9702406A1 HU P9702406 A1 HUP9702406 A1 HU P9702406A1 HU 9702406 A HU9702406 A HU 9702406A HU P9702406 A HUP9702406 A HU P9702406A HU P9702406 A1 HUP9702406 A1 HU P9702406A1
- Authority
- HU
- Hungary
- Prior art keywords
- dinitration
- nitric acid
- continuous process
- aromatic substrates
- bifurcation
- Prior art date
Links
- 125000003118 aryl group Chemical group 0.000 title 1
- 238000010924 continuous production Methods 0.000 title 1
- 239000000758 substrate Substances 0.000 title 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 3
- 229910017604 nitric acid Inorganic materials 0.000 abstract 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical group OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000002490 anilino group Chemical group [H]N(*)C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/76—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by nitration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Polyesters Or Polycarbonates (AREA)
Abstract
A találmány tárgya főlyamatős eljárás alkilcsőpőrttal helyettesítettfenől- vagy anilinszármazékők dinitrálására, melynek sőrán lényegébenkénsavmentes salétrőmsavat használnak, és a dinitrálást egyetlenlépésben végzik egy csőreaktőrban, katalitikűsan hatásős mennyiségűkatalizátőr jelenlétében, amely a salétrőmsavat in sitűsalétrőmőssavvá alakítja át. ŕ
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT96TO001017A IT1289740B1 (it) | 1996-12-12 | 1996-12-12 | Procedimento continuo per la dinitrazione di substrati aromatici |
Publications (2)
Publication Number | Publication Date |
---|---|
HUP9702406A1 true HUP9702406A1 (hu) | 1999-06-28 |
HU223085B1 HU223085B1 (hu) | 2004-03-29 |
Family
ID=11415102
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU9702406A HU223085B1 (hu) | 1996-12-12 | 1997-12-11 | Folyamatos eljárás N-alkil-3,4-dimetil-benzol-amin dinitrálására |
Country Status (16)
Country | Link |
---|---|
US (1) | US5907062A (hu) |
EP (1) | EP0847984B1 (hu) |
JP (1) | JPH10298147A (hu) |
AR (1) | AR010697A1 (hu) |
AT (1) | ATE214360T1 (hu) |
AU (1) | AU721300B2 (hu) |
BR (1) | BR9705523A (hu) |
CA (1) | CA2221811A1 (hu) |
DE (1) | DE69711008T2 (hu) |
DK (1) | DK0847984T3 (hu) |
ES (1) | ES2170325T3 (hu) |
HU (1) | HU223085B1 (hu) |
IL (1) | IL122553A (hu) |
IT (1) | IT1289740B1 (hu) |
PT (1) | PT847984E (hu) |
ZA (1) | ZA9711099B (hu) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1293450B1 (it) * | 1997-07-14 | 1999-03-01 | Finchimica Srl | Procedimento per la purificazione di dinitroaniline. |
US5922913A (en) * | 1998-11-06 | 1999-07-13 | Srm Chemical, Ltd., Co. | Process for nitrating aromatic amines |
US7655840B2 (en) * | 2001-06-05 | 2010-02-02 | E. I. Du Pont De Nemours And Company | Alteration of embryo/endosperm size during seed development |
CN109320424B (zh) * | 2017-07-31 | 2021-12-21 | 江苏永安化工有限公司 | 一种二甲戊灵的纯化方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2951746A (en) * | 1957-02-25 | 1960-09-06 | Hercules Powder Co Ltd | Apparatus for stage-wise nitration of toluene |
US3726923A (en) * | 1970-03-16 | 1973-04-10 | Sherwin Williams Co | Process for the manufacture of n,n-dichloroalkyl-2,6-dinitro-4-alkyl aniline |
US3694513A (en) * | 1970-06-08 | 1972-09-26 | Dow Chemical Co | Direct nitration of alkylphenols with nitric acid |
US4621157A (en) * | 1984-05-07 | 1986-11-04 | Jerome A. Gross | Nitration processes |
IT1190440B (it) * | 1985-12-18 | 1988-02-16 | Finchimica Spa | Procedimento migliorato per la purificazione della trifluralina |
-
1996
- 1996-12-12 IT IT96TO001017A patent/IT1289740B1/it active IP Right Grant
-
1997
- 1997-11-18 AU AU45246/97A patent/AU721300B2/en not_active Ceased
- 1997-11-19 US US08/974,104 patent/US5907062A/en not_active Expired - Fee Related
- 1997-11-19 CA CA002221811A patent/CA2221811A1/en not_active Abandoned
- 1997-12-01 PT PT97121055T patent/PT847984E/pt unknown
- 1997-12-01 EP EP97121055A patent/EP0847984B1/en not_active Expired - Lifetime
- 1997-12-01 DK DK97121055T patent/DK0847984T3/da active
- 1997-12-01 DE DE69711008T patent/DE69711008T2/de not_active Expired - Fee Related
- 1997-12-01 AT AT97121055T patent/ATE214360T1/de not_active IP Right Cessation
- 1997-12-01 ES ES97121055T patent/ES2170325T3/es not_active Expired - Lifetime
- 1997-12-05 JP JP9352307A patent/JPH10298147A/ja active Pending
- 1997-12-10 ZA ZA9711099A patent/ZA9711099B/xx unknown
- 1997-12-11 BR BR9705523A patent/BR9705523A/pt not_active Application Discontinuation
- 1997-12-11 HU HU9702406A patent/HU223085B1/hu not_active IP Right Cessation
- 1997-12-11 IL IL12255397A patent/IL122553A/xx not_active IP Right Cessation
- 1997-12-11 AR ARP970105838A patent/AR010697A1/es active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
AR010697A1 (es) | 2000-06-28 |
IL122553A (en) | 2003-05-29 |
EP0847984B1 (en) | 2002-03-13 |
CA2221811A1 (en) | 1998-06-12 |
MX9709816A (es) | 1998-10-31 |
IL122553A0 (en) | 1998-06-15 |
IT1289740B1 (it) | 1998-10-16 |
DE69711008T2 (de) | 2002-10-10 |
DK0847984T3 (da) | 2002-05-21 |
US5907062A (en) | 1999-05-25 |
EP0847984A1 (en) | 1998-06-17 |
ATE214360T1 (de) | 2002-03-15 |
DE69711008D1 (de) | 2002-04-18 |
AU721300B2 (en) | 2000-06-29 |
BR9705523A (pt) | 1999-07-20 |
ES2170325T3 (es) | 2002-08-01 |
ITTO961017A1 (it) | 1998-06-12 |
ZA9711099B (en) | 1998-06-15 |
JPH10298147A (ja) | 1998-11-10 |
HU223085B1 (hu) | 2004-03-29 |
PT847984E (pt) | 2002-06-28 |
AU4524697A (en) | 1998-06-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
HFG4 | Patent granted, date of granting |
Effective date: 20040116 |
|
MM4A | Lapse of definitive patent protection due to non-payment of fees |