HUE053673T2 - Eljárás kaprolaktám tisztítására nyers kaprolaktám oldatból szerves oldószeres extrakció mellõzésével - Google Patents

Eljárás kaprolaktám tisztítására nyers kaprolaktám oldatból szerves oldószeres extrakció mellõzésével

Info

Publication number
HUE053673T2
HUE053673T2 HUE17838004A HUE17838004A HUE053673T2 HU E053673 T2 HUE053673 T2 HU E053673T2 HU E17838004 A HUE17838004 A HU E17838004A HU E17838004 A HUE17838004 A HU E17838004A HU E053673 T2 HUE053673 T2 HU E053673T2
Authority
HU
Hungary
Prior art keywords
caprolactam
purification
solution
organic solvent
solvent extraction
Prior art date
Application number
HUE17838004A
Other languages
English (en)
Inventor
Moro Anacleto Dal
Michele Cecchetto
Denis Jahic
Vid Margon
Original Assignee
Aquafilslo D O O
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aquafilslo D O O filed Critical Aquafilslo D O O
Publication of HUE053673T2 publication Critical patent/HUE053673T2/hu

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16Separation or purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • B01D11/0492Applications, solvents used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10Vacuum distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02Preparation of lactams
    • C07D201/04Preparation of lactams from or via oximes by Beckmann rearrangement
    • C07D201/06Preparation of lactams from or via oximes by Beckmann rearrangement from ketones by simultaneous oxime formation and rearrangement
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D223/00Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08Oxygen atoms
    • C07D223/10Oxygen atoms attached in position 2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)
HUE17838004A 2017-12-15 2017-12-15 Eljárás kaprolaktám tisztítására nyers kaprolaktám oldatból szerves oldószeres extrakció mellõzésével HUE053673T2 (hu)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17838004.4A EP3568389B1 (en) 2017-12-15 2017-12-15 Process for the purification of caprolactam from a solution of crude caprolactam without organic solvent extraction
PCT/SI2017/050010 WO2019117817A1 (en) 2017-12-15 2017-12-15 Process for the purification of caprolactam from a solution of crude caprolactam without organic solvent extraction

Publications (1)

Publication Number Publication Date
HUE053673T2 true HUE053673T2 (hu) 2021-07-28

Family

ID=61148459

Family Applications (1)

Application Number Title Priority Date Filing Date
HUE17838004A HUE053673T2 (hu) 2017-12-15 2017-12-15 Eljárás kaprolaktám tisztítására nyers kaprolaktám oldatból szerves oldószeres extrakció mellõzésével

Country Status (10)

Country Link
US (2) US10787417B2 (hu)
EP (1) EP3568389B1 (hu)
JP (1) JP6852181B2 (hu)
CN (1) CN110494420B (hu)
EA (1) EA038223B1 (hu)
ES (1) ES2860825T3 (hu)
HU (1) HUE053673T2 (hu)
PL (1) PL3568389T3 (hu)
SI (1) SI3568389T1 (hu)
WO (1) WO2019117817A1 (hu)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT201800021409A1 (it) * 2018-12-28 2020-06-28 Aquafil S P A Processo per la produzione di epsilon caprolattame dall’acido 6-aminocaproico.
IT202100028601A1 (it) 2021-11-10 2023-05-10 Aquafil S P A Procedimento per produrre epsilon-caprolattame mediante depolimerizzazione di policaprolattame (pa6).
CN115253380B (zh) * 2022-08-19 2023-09-01 清元智能科技研究院(湖北)有限公司 一种己内酰胺萃取系统和方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1258810A (hu) 1968-03-30 1971-12-30
DE1926932A1 (de) * 1968-07-19 1970-01-22 Leuna Werke Veb Verfahren zur Reinigung von Lactamen
DE2301587C3 (de) * 1973-01-13 1981-02-26 Bayer Ag, 5090 Leverkusen Verfahren zur Entfernung von Borsäure aus Lactamen
CH593934A5 (hu) 1974-09-03 1977-12-30 Inventa Ag
IT1113404B (it) * 1979-02-28 1986-01-20 Snia Viscosa Internazionale brevetti s.r.l.via brentano 2 milano
JPS57165364A (en) * 1981-04-06 1982-10-12 Unitika Ltd Purification of recovered lactam
US6162906A (en) * 1991-08-08 2000-12-19 Fmc Corporation Clarified konjac glucomannan
CN1262539C (zh) * 2001-03-01 2006-07-05 Dsmip财产有限公司 从有机溶剂中回收和纯化己内酰胺的方法
EP1764542A1 (de) * 2005-09-19 2007-03-21 Siemens Aktiengesellschaft Bausatz zur Erstellung einer Industrieanlage
JP2008056620A (ja) * 2006-08-31 2008-03-13 Toray Ind Inc 回収ε−カプロラクタムの精製法
DE102011055889B4 (de) * 2011-11-30 2013-08-01 Otc Gmbh Verfahren zur Herstellung eines Protein-Hydrolysates

Also Published As

Publication number Publication date
US10787417B2 (en) 2020-09-29
JP2020514350A (ja) 2020-05-21
EP3568389B1 (en) 2021-01-20
EA038223B1 (ru) 2021-07-27
CN110494420B (zh) 2023-05-12
US20210040036A1 (en) 2021-02-11
US11208380B2 (en) 2021-12-28
EA201991703A1 (ru) 2020-01-09
US20190382339A1 (en) 2019-12-19
EP3568389A1 (en) 2019-11-20
WO2019117817A1 (en) 2019-06-20
CN110494420A (zh) 2019-11-22
PL3568389T3 (pl) 2021-06-28
JP6852181B2 (ja) 2021-03-31
SI3568389T1 (sl) 2021-03-31
ES2860825T3 (es) 2021-10-05

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