HK1036971A1 - Production of organic compounds which are low in fluoride. - Google Patents
Production of organic compounds which are low in fluoride.Info
- Publication number
- HK1036971A1 HK1036971A1 HK01108038A HK01108038A HK1036971A1 HK 1036971 A1 HK1036971 A1 HK 1036971A1 HK 01108038 A HK01108038 A HK 01108038A HK 01108038 A HK01108038 A HK 01108038A HK 1036971 A1 HK1036971 A1 HK 1036971A1
- Authority
- HK
- Hong Kong
- Prior art keywords
- production
- organic compounds
- fluoride
- hlf
- low
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/64—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/15—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen containing halogen
- C07C53/16—Halogenated acetic acids
- C07C53/18—Halogenated acetic acids containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/185—Saturated compounds having only one carboxyl group and containing keto groups
- C07C59/21—Saturated compounds having only one carboxyl group and containing keto groups containing halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/14—Preparation of carboxylic acid esters from carboxylic acid halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Production of organic compounds (I) having a low content of hydrolyzable fluoride (HLF) involves contacting HLF-contaminated (I) with a removing agent for HLF selected from inorganic oxide sorbents (II) and onium salts (III) of carboxylic acids. An Independent claim is also included for 4-chloro-4,4-difluoroacetoacetic acid, 4,4-difluoroacetoacetic acid and their onium salts.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19829909A DE19829909C1 (en) | 1998-07-06 | 1998-07-06 | Reducing hydrolyzable fluorine content of organic compounds, especially halogenated carboxylic acids or derivatives for use e.g. as pharmaceutical or agrochemical intermediates |
DE19850010A DE19850010A1 (en) | 1998-10-30 | 1998-10-30 | Reducing hydrolyzable fluorine content of organic compounds, especially halogenated carboxylic acids or derivatives for use e.g. as pharmaceutical or agrochemical intermediates |
PCT/EP1999/004477 WO2000001647A2 (en) | 1998-07-06 | 1999-06-29 | Production of organic compounds which are low in fluoride |
Publications (1)
Publication Number | Publication Date |
---|---|
HK1036971A1 true HK1036971A1 (en) | 2002-01-25 |
Family
ID=26047200
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HK01108038A HK1036971A1 (en) | 1998-07-06 | 2001-11-15 | Production of organic compounds which are low in fluoride. |
Country Status (8)
Country | Link |
---|---|
EP (2) | EP1481958B1 (en) |
JP (1) | JP4621352B2 (en) |
CN (1) | CN1207256C (en) |
CA (1) | CA2336812A1 (en) |
DE (2) | DE59914714D1 (en) |
HK (1) | HK1036971A1 (en) |
HU (1) | HUP0102558A3 (en) |
WO (1) | WO2000001647A2 (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5340287B2 (en) * | 2007-08-16 | 2013-11-13 | ソルヴェイ(ソシエテ アノニム) | Process for the preparation of esters of 4-fluoro-substituted 3-oxo-alkanoic acids |
KR20100126562A (en) * | 2008-03-27 | 2010-12-01 | 솔베이 플루오르 게엠베하 | Preparation of fluorinated organic carbonates depleted in hf using a specific absorbent |
JP5521625B2 (en) * | 2010-02-22 | 2014-06-18 | セントラル硝子株式会社 | Method for producing difluoroacetic acid ester |
CN102304038B (en) * | 2011-06-11 | 2015-04-01 | 山东兴氟新材料有限公司 | Device and method for lowering concentration of fluorine ions carried in production of trifluoroacetic acid |
WO2015111726A1 (en) * | 2014-01-27 | 2015-07-30 | 旭硝子株式会社 | Method for suppressing corrosion of glass |
CN107778165A (en) * | 2016-08-30 | 2018-03-09 | 天津市科密欧化学试剂有限公司 | A kind of purification process of chromatographically pure trifluoroacetic acid |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1158490B (en) * | 1960-12-17 | 1963-12-05 | Hoechst Ag | Process for the production of fluorine-containing acetoacetic acid chlorides or their solutions |
GB1314607A (en) * | 1969-09-12 | 1973-04-26 | Kureha Chemical Ind Co Ltd | Method for recovering perfluorinated emulsifiers |
BE794525A (en) * | 1972-01-25 | 1973-07-25 | Hoechst Ag | PROCESS FOR PREPARING TRIFLUOROACETYL CHLORIDE |
JPS5993025A (en) * | 1982-11-16 | 1984-05-29 | Hodogaya Chem Co Ltd | Preparation of dichlorofluoroacetyl chloride |
DE3311751A1 (en) * | 1983-03-31 | 1984-10-04 | Hoechst Ag, 6230 Frankfurt | Purification of fluorohydrocarbons |
JPS60239437A (en) * | 1984-05-15 | 1985-11-28 | Asahi Glass Co Ltd | Production of trifluoroacetic acid and its chloride |
JPH0678270B2 (en) * | 1987-09-29 | 1994-10-05 | セントラル硝子株式会社 | Method for purifying fluorocarbon compound |
FR2644451B1 (en) * | 1989-03-20 | 1991-09-20 | Norsolor Sa | USE OF ZEOLITHS FOR THE PURIFICATION OF SATURATED CARBOXYLIC ACIDS WITH A RESIDUAL FLUORIDE CONTENT AND CORRESPONDING PURIFICATION METHOD |
DE4213154C1 (en) * | 1992-04-22 | 1993-06-17 | Hoechst Ag, 6230 Frankfurt, De | |
DE4313793A1 (en) * | 1993-04-27 | 1994-11-03 | Solvay Fluor & Derivate | Production of carboxylic acid halides and carboxylate salts |
ATE161819T1 (en) * | 1993-04-27 | 1998-01-15 | Solvay Fluor & Derivate | METHOD FOR PRODUCING CARBOXYLIC ACID ESTERS FROM CARBOXYLIC ACID HALIDES AND ALCOHOLS |
DE19732031C1 (en) * | 1997-07-25 | 1999-04-22 | Solvay Fluor & Derivate | 2-phase production of carboxylic acid esters |
-
1999
- 1999-06-29 CA CA002336812A patent/CA2336812A1/en not_active Abandoned
- 1999-06-29 DE DE59914714T patent/DE59914714D1/en not_active Expired - Fee Related
- 1999-06-29 HU HU0102558A patent/HUP0102558A3/en unknown
- 1999-06-29 CN CNB998071285A patent/CN1207256C/en not_active Expired - Fee Related
- 1999-06-29 EP EP04020820A patent/EP1481958B1/en not_active Expired - Lifetime
- 1999-06-29 DE DE59910530T patent/DE59910530D1/en not_active Expired - Fee Related
- 1999-06-29 JP JP2000558053A patent/JP4621352B2/en not_active Expired - Fee Related
- 1999-06-29 WO PCT/EP1999/004477 patent/WO2000001647A2/en active IP Right Grant
- 1999-06-29 EP EP99936463A patent/EP1094999B1/en not_active Expired - Lifetime
-
2001
- 2001-11-15 HK HK01108038A patent/HK1036971A1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO2000001647A3 (en) | 2000-04-06 |
CA2336812A1 (en) | 2000-01-13 |
EP1094999A2 (en) | 2001-05-02 |
DE59910530D1 (en) | 2004-10-21 |
JP2002526385A (en) | 2002-08-20 |
CN1207256C (en) | 2005-06-22 |
CN1305446A (en) | 2001-07-25 |
HUP0102558A2 (en) | 2001-11-28 |
JP4621352B2 (en) | 2011-01-26 |
HUP0102558A3 (en) | 2002-08-28 |
WO2000001647A2 (en) | 2000-01-13 |
DE59914714D1 (en) | 2008-05-08 |
EP1481958B1 (en) | 2008-03-26 |
EP1094999B1 (en) | 2004-09-15 |
EP1481958A1 (en) | 2004-12-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PC | Patent ceased (i.e. patent has lapsed due to the failure to pay the renewal fee) |
Effective date: 20090629 |