GB986037A - Process for making nitrocyclopropane - Google Patents

Process for making nitrocyclopropane

Info

Publication number
GB986037A
GB986037A GB20271/63A GB2027163A GB986037A GB 986037 A GB986037 A GB 986037A GB 20271/63 A GB20271/63 A GB 20271/63A GB 2027163 A GB2027163 A GB 2027163A GB 986037 A GB986037 A GB 986037A
Authority
GB
United Kingdom
Prior art keywords
nitropropane
halo
nitrocyclopropane
chloro
prepared
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB20271/63A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Abbott Laboratories
Original Assignee
Abbott Laboratories
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Abbott Laboratories filed Critical Abbott Laboratories
Publication of GB986037A publication Critical patent/GB986037A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/02—Systems containing only non-condensed rings with a three-membered ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Nitrocyclopropane is prepared by reacting a 1 halo-3-nitropropane comprising a major portion of 1-iodo-3-nitropropane with an inorganic compound selected from alkali metal hydroxide or carbonates such as sodium and potassium carbonate or bicarbonates preferably in an amount of between 1.0 and 2.5 moles per mole of 1-halo-3-nitropropane, in a reaction medium selected from water and a hydrocarbon solvent boiling above 80 DEG C., e.g. toluene. The 1-halo-3-nitropropane may be prepared by refluxing 1-chloro-3-nitropropane with excess alkali metal iodine in acetone. The 1-chloro-3-nitropropane may be produced by passing chlorine through a mixture of nitropropane and phosphorous pentoxide.
GB20271/63A 1962-06-04 1963-05-21 Process for making nitrocyclopropane Expired GB986037A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US19966262A 1962-06-04 1962-06-04

Publications (1)

Publication Number Publication Date
GB986037A true GB986037A (en) 1965-03-17

Family

ID=22738493

Family Applications (1)

Application Number Title Priority Date Filing Date
GB20271/63A Expired GB986037A (en) 1962-06-04 1963-05-21 Process for making nitrocyclopropane

Country Status (3)

Country Link
BE (1) BE632834A (en)
CH (1) CH407068A (en)
GB (1) GB986037A (en)

Also Published As

Publication number Publication date
CH407068A (en) 1966-02-15
BE632834A (en) 1963-11-27

Similar Documents

Publication Publication Date Title
ES413266A1 (en) Indenyl compounds
GB986037A (en) Process for making nitrocyclopropane
GB1321563A (en) Preparation of 3,5-dinitrobenzotrifluoride compounds
SE8102285L (en) SPRENGEMNESKOMPOSITION
GB1068038A (en) Process for the production of copper
ES412741A1 (en) Process for the preparation of alkaline hyperoxide
GB1082869A (en) Process for the manufacture of 2,2,3-trichlorobutane
GB992742A (en) Preparation of permonosulphates
JPS51151295A (en) Process for production of chlorine dioxide
ES373726A1 (en) Dehydrohalogenation of halogenated organic compounds in dimethyl sulfoxide solvent
GB1122034A (en) Process for the preparation of azines
GB959761A (en) Manufacture of azodicarbonamide
JPS5326898A (en) Anti-corrosive, flame-retardant polyurethane foam
ES351101A1 (en) Process for the manufacture of nitrosyl chloride
GB1062368A (en) New phthaloperinone dyes and their production
GB1011116A (en) Process of producing a 1-halo-1-nitroalkane, and 1-halo-1-nitroalkanes produced by the process
IL60022A (en) Process for the preparation of benzoxazolone from salicylamide
ES472908A2 (en) 15-Deoxy-16-substituted prostanoic acids
JPS5265538A (en) Flame retardant resin compositions
GB887666A (en) Process for the purification of 2-ethyl-cis-crotonoylurea
GB1087603A (en) Production of ªŠ-cyanocaproic acid
ZA762336B (en) Process for reducing chlorate content of aqueous alkali metal hydroxide solution which contains chlorate
GB591816A (en) Process for the production of nitro-olefines
DK139711B (en) Process for the production of storable sodium hydroxide.
GB1091365A (en) Process for producing 5-guanylic acid