GB982629A - A process for the purification of terephthalic acid - Google Patents
A process for the purification of terephthalic acidInfo
- Publication number
- GB982629A GB982629A GB1583363A GB1583363A GB982629A GB 982629 A GB982629 A GB 982629A GB 1583363 A GB1583363 A GB 1583363A GB 1583363 A GB1583363 A GB 1583363A GB 982629 A GB982629 A GB 982629A
- Authority
- GB
- United Kingdom
- Prior art keywords
- terephthalic acid
- solution
- purification
- molecular oxygen
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A process for the purification of terephthalic acid comprises dissolving the crude or impure terephthalic acid in an aliphatic carboxylic acid having 2 to 5 carbon atoms, e.g. acetic acid, at a temperature of 200 DEG to 300 DEG C. and under a pressure sufficient to maintain the solvent in a liquid phase, contacting the solution with a gaseous molecular oxygen or molecular oxygen containing gas, e.g. air, in the presence of at least one oxidation catalyst containing cobalt, manganese, chromium, cerium and lead or their compounds, then cooling the resulting solution to crystallize out pure terephthalic acid and thereafter separating it from the solution. Several examples are given.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1662562 | 1962-04-27 | ||
JP1662462 | 1962-04-27 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB982629A true GB982629A (en) | 1965-02-10 |
Family
ID=26353002
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1583363A Expired GB982629A (en) | 1962-04-27 | 1963-04-22 | A process for the purification of terephthalic acid |
Country Status (3)
Country | Link |
---|---|
DE (1) | DE1270030C2 (en) |
FR (1) | FR1355273A (en) |
GB (1) | GB982629A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3529021A (en) * | 1966-03-17 | 1970-09-15 | Mobil Oil Corp | Terephthalic acid purification process |
US5166420A (en) * | 1986-10-20 | 1992-11-24 | Mitsui Petrochemical Industries, Ltd. | Process for the production of high purity terephthalic acid |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2051804B (en) * | 1979-07-02 | 1983-10-12 | Ici Ltd | Preparation of aromatic carboxylic acids |
KR970000136B1 (en) * | 1993-09-28 | 1997-01-04 | 브이.피. 유리예프 | Process for producing highly purified benzenedicarboxylic acid isomers |
IT1319169B1 (en) * | 2000-07-14 | 2003-09-26 | Eurotecnica Dev & Licensing Sr | PROCEDURE FOR THE PURIFICATION OF AROMATIC CARBOXYLIC ACIDS. |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1081445B (en) * | 1954-05-03 | 1960-05-12 | Mid Century Corp | Process for the production of aromatic di- or polycarboxylic acids |
FR1137203A (en) * | 1954-12-15 | 1957-05-27 | Ici Ltd | Purification of terephthalic acid |
NL108519C (en) * | 1954-12-29 | |||
GB785051A (en) * | 1955-01-19 | 1957-10-23 | Ici Ltd | Purification of terephthalic acid |
DE1112975B (en) * | 1958-01-14 | 1961-08-24 | Belge Produits Chimiques Sa | Process and device for the pyrolysis of hydrocarbons |
DE1106751B (en) * | 1959-10-13 | 1961-05-18 | Huels Chemische Werke Ag | Process for the preparation of terephthalic acid |
-
0
- DE DENDAT1270030D patent/DE1270030C2/en not_active Expired
-
1963
- 1963-04-22 GB GB1583363A patent/GB982629A/en not_active Expired
- 1963-04-27 FR FR932973A patent/FR1355273A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3529021A (en) * | 1966-03-17 | 1970-09-15 | Mobil Oil Corp | Terephthalic acid purification process |
US5166420A (en) * | 1986-10-20 | 1992-11-24 | Mitsui Petrochemical Industries, Ltd. | Process for the production of high purity terephthalic acid |
Also Published As
Publication number | Publication date |
---|---|
DE1270030C2 (en) | 1973-07-19 |
FR1355273A (en) | 1964-03-13 |
DE1270030B (en) | 1968-06-12 |
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