GB971044A - Process for conditioning organic pigments - Google Patents
Process for conditioning organic pigmentsInfo
- Publication number
- GB971044A GB971044A GB3353960A GB3353960A GB971044A GB 971044 A GB971044 A GB 971044A GB 3353960 A GB3353960 A GB 3353960A GB 3353960 A GB3353960 A GB 3353960A GB 971044 A GB971044 A GB 971044A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- grinding
- hexachlorethane
- conditioned
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0002—Grinding; Milling with solid grinding or milling assistants
Landscapes
- Chemical & Material Sciences (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Photoreceptors In Electrophotography (AREA)
Abstract
Organic pigments are conditioned by grinding them in an aqueous grinding medium in the presence of an organic compound which is solid, which is soluble to the extent of not more than 5 parts by weight in 100 parts by weight of water at room temperature and which is capable of being removed by sublimation or by distillation with steam, or of a mixture of such organic compounds, and then separating the pigment from the grinding medium. Organic compounds mentioned are hexachlorethane, naphthalene, diphenyl, p-dichlorobenzene, hexachlorobenzene, phthalic anhydride, b -hexachlorocyclohexane, hexamethylethane, hexabromethane, chloranil and camphor. The aqueous medium may contain besides water, methanol, ethanol, isopropanol, phenol, cresol acetone, methyl ethyl ketone cyclohexanone, acetic acid, benzoic acid, phthalic acid or an ester thereof, methane sulphonic acid, benzene sulphonic acid, naphthalene sulphonic acid, pyridine, ethanolamine, stearic acid, resin acids, resin acid esters such as dihydroabietic acid esters of paraffin oil. The conditioned a -forms of copper phthalocyanine, copper phthalocyanine containing one or two atoms of chlorine or bromine and metal-free phthalocyanine are made by grinding a ratio of one part of the crude a - or b -forms at 5 DEG to 30 DEG C. with at most three parts of an aliphatic organic compound such as hexachlorethane and optionally in the presence of formaldehyde, acetaldehyde, propionaldehyde, butyraldehyde, glyoxal, paraformaldehyde, metaldehyde, paraldehyde, hexamethylene tetramine, urea, formamide, dimethylformamide, acetamide or urotropin. Alternatively the pigment may be treated with the aldehyde or amide after the grinding is completed. The conditioned b -form of the phthalocyanines are made by grinding the crude b -forms (a) using as organic compound an aromatic hydrocarbon or a halogenated aromatic hydrocarbon, or (b) using a ratio of at least three parts of hexachlorethane per part of pigment, or (c) using hexachlorethane at a temperature above 40 DEG C., or (d) using hexachlorethane together with naphthalene or a phenol. In examples pigments are conditioned of the phthalocyanine, disazo, dioxazine, nitro, quinacridone, indigo, thioindigo, naphthalic acid di-benzimidazole, perylene tetracarboxylic acid diimide, dianthraquinoryl, isoviolanthrone, flavanthrone, indanthrone and di-(pyrazoleanthronyl) series.ALSO:Organic pigments are conditioned by grinding them in an aqueous grinding medium in the presence of an organic compound which is solid, which is soluble to the extent of not more than 5 parts by weight in 100 parts by weight of water at room temperature and which is capable of being removed by sublimation or by distillation with steam, or of a mixture of such organic compounds, and then separating the pigment from the grinding medium. Organic compounds mentioned are hexachlorethane, naphthalene, diphenyl, p-dichlorobenzene, hexachlorobenzene, phthalic anhydride, b -hexachlorocyclohexane, hexamethylethane, hexabromethane, chloranil and camphor. The aqueous medium may contain besides water, methanol, ethanol, isopropanol, phenol, cresol, acetone, methyl ethyl ketone, cyclohexanone, acetic acid, benzoic acid, phthalic acid or an ester thereof, methane sulphonic acid, benzene sulphonic acid, naphthalene sulphonic acid, pyridine, ethanolamine, stearic acid, resin acids, resin acid esters such as dihydroabietic acid esters or paraffin oil. The conditioned a -forms of copper phthalocyanine, copper phthalocyanine containing one or two atoms of chlorine or bromine and metal free phthalocyanine are made by grinding a ratio of one part of the crude a - or b -forms at 5-30 DEG C. with at most three parts of an aliphatic organic compound such as hexachlorethane and optionally in the presence of formaldehyde, acetaldehyde, propionaldehyde, butyraldehyde, glyoxal, paraformaldehyde, metaldehyde, paraldehyde, hexamethylene tetramine, urea, formamide, dimethylformamide, acetamide or urotropin. Alternatively the pigment may be treated with the aldehyde or amide after the grinding is completed. The conditioned b -form of the phthalocyanines are made by grinding the crude b -forms (a) using as organic compound an aromatic hydrocarbon or a halogenated aromatic hydrocarbon or (b) using a ratio of at least three parts of hexachlorethane per part of pigment or (c) using hexachlorethane at a temperature above 40 DEG C. or (d) using hexachlorethane together with naphthalene or a phenol. In examples, pigments are conditioned of the phthalocyanine, disazo, dioxazine, nitro, quinacridone, indigo, thioindigo, naphthalic acid di-benzimidazole, perylene tetracarboxylic acid diimide, dianthraquinonyl, isoviolanthrone, flavanthrone, indanthrone and di-(pyrazoleanthronyl) series.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH7877959A CH382893A (en) | 1959-09-29 | 1959-09-29 | Process for conditioning pigments |
CH7877859A CH384114A (en) | 1959-09-29 | 1959-09-29 | Process for the production of flocculation-resistant phthalocyanine pigments |
CH987660 | 1960-09-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB971044A true GB971044A (en) | 1964-09-30 |
Family
ID=27176333
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3353960A Expired GB971044A (en) | 1959-09-29 | 1960-09-29 | Process for conditioning organic pigments |
Country Status (2)
Country | Link |
---|---|
ES (1) | ES261340A1 (en) |
GB (1) | GB971044A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4194921A (en) * | 1977-06-24 | 1980-03-25 | Ciba-Geigy Corporation | Pigment compositions and process for dust free pigment beads |
GB2177105A (en) * | 1985-07-05 | 1987-01-14 | Basf Ag | Conditioning of isoindoline pigments |
CN110229377A (en) * | 2019-06-28 | 2019-09-13 | 濮阳班德路化学有限公司 | A kind of dechlorination method of light dydrocarbon solvent |
EP4365158A1 (en) | 2022-11-04 | 2024-05-08 | PCC ROKITA Spolka Akcyjna | Method of selective paradichlorobenzene preparation with improved catalytic system recovery |
-
1960
- 1960-09-28 ES ES0261340A patent/ES261340A1/en not_active Expired
- 1960-09-29 GB GB3353960A patent/GB971044A/en not_active Expired
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4194921A (en) * | 1977-06-24 | 1980-03-25 | Ciba-Geigy Corporation | Pigment compositions and process for dust free pigment beads |
GB2177105A (en) * | 1985-07-05 | 1987-01-14 | Basf Ag | Conditioning of isoindoline pigments |
GB2177105B (en) * | 1985-07-05 | 1989-07-19 | Basf Ag | Conditioning isoindoline pigments |
CN110229377A (en) * | 2019-06-28 | 2019-09-13 | 濮阳班德路化学有限公司 | A kind of dechlorination method of light dydrocarbon solvent |
CN110229377B (en) * | 2019-06-28 | 2021-06-22 | 濮阳班德路化学有限公司 | Dechlorination method of carbon five solvent |
EP4365158A1 (en) | 2022-11-04 | 2024-05-08 | PCC ROKITA Spolka Akcyjna | Method of selective paradichlorobenzene preparation with improved catalytic system recovery |
Also Published As
Publication number | Publication date |
---|---|
ES261340A1 (en) | 1961-05-16 |
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