GB956780A - Improved production of adipic acid - Google Patents
Improved production of adipic acidInfo
- Publication number
- GB956780A GB956780A GB3008361A GB3008361A GB956780A GB 956780 A GB956780 A GB 956780A GB 3008361 A GB3008361 A GB 3008361A GB 3008361 A GB3008361 A GB 3008361A GB 956780 A GB956780 A GB 956780A
- Authority
- GB
- United Kingdom
- Prior art keywords
- adipic acid
- acid
- solvent
- treated
- oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 title abstract 20
- 239000001361 adipic acid Substances 0.000 title abstract 10
- 235000011037 adipic acid Nutrition 0.000 title abstract 10
- 239000003054 catalyst Substances 0.000 abstract 7
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 6
- 239000002904 solvent Substances 0.000 abstract 6
- 230000003647 oxidation Effects 0.000 abstract 5
- 238000007254 oxidation reaction Methods 0.000 abstract 5
- 150000001735 carboxylic acids Chemical class 0.000 abstract 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 3
- 239000000047 product Substances 0.000 abstract 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 2
- 238000002425 crystallisation Methods 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 229910001882 dioxygen Inorganic materials 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000012452 mother liquor Substances 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 150000002696 manganese Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
- C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US5086860A | 1960-08-22 | 1960-08-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB956780A true GB956780A (en) | 1964-04-29 |
Family
ID=21967989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3008361A Expired GB956780A (en) | 1960-08-22 | 1961-08-21 | Improved production of adipic acid |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE607309A (cs) |
| CH (1) | CH410897A (cs) |
| ES (1) | ES269997A1 (cs) |
| GB (1) | GB956780A (cs) |
| LU (1) | LU40519A1 (cs) |
| SE (1) | SE302958B (cs) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112521266A (zh) * | 2019-09-18 | 2021-03-19 | 中国石油化工股份有限公司 | 己二酸的生产方法 |
-
1961
- 1961-08-18 BE BE607309A patent/BE607309A/fr unknown
- 1961-08-18 LU LU40519D patent/LU40519A1/xx unknown
- 1961-08-18 SE SE833461A patent/SE302958B/xx unknown
- 1961-08-19 ES ES0269997A patent/ES269997A1/es not_active Expired
- 1961-08-21 GB GB3008361A patent/GB956780A/en not_active Expired
- 1961-08-22 CH CH978961A patent/CH410897A/fr unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112521266A (zh) * | 2019-09-18 | 2021-03-19 | 中国石油化工股份有限公司 | 己二酸的生产方法 |
| CN112521266B (zh) * | 2019-09-18 | 2023-04-07 | 中国石油化工股份有限公司 | 己二酸的生产方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| SE302958B (cs) | 1968-08-12 |
| ES269997A1 (es) | 1962-01-16 |
| CH410897A (fr) | 1966-04-15 |
| LU40519A1 (cs) | 1961-10-18 |
| BE607309A (fr) | 1961-12-18 |
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