GB912636A - Method and apparatus for producing submicron metals - Google Patents
Method and apparatus for producing submicron metalsInfo
- Publication number
- GB912636A GB912636A GB2186/59A GB218659A GB912636A GB 912636 A GB912636 A GB 912636A GB 2186/59 A GB2186/59 A GB 2186/59A GB 218659 A GB218659 A GB 218659A GB 912636 A GB912636 A GB 912636A
- Authority
- GB
- United Kingdom
- Prior art keywords
- metal
- heating
- cooling
- particles
- metal compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052751 metal Inorganic materials 0.000 title abstract 6
- 239000002184 metal Substances 0.000 title abstract 6
- 150000002739 metals Chemical class 0.000 title abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 5
- 238000001816 cooling Methods 0.000 abstract 4
- 150000002736 metal compounds Chemical class 0.000 abstract 4
- 238000000354 decomposition reaction Methods 0.000 abstract 3
- 239000007789 gas Substances 0.000 abstract 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 238000000576 coating method Methods 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000011261 inert gas Substances 0.000 abstract 2
- 239000013528 metallic particle Substances 0.000 abstract 2
- 239000000843 powder Substances 0.000 abstract 2
- 229910001369 Brass Inorganic materials 0.000 abstract 1
- 229910000831 Steel Inorganic materials 0.000 abstract 1
- 239000004809 Teflon Substances 0.000 abstract 1
- 229920006362 Teflon® Polymers 0.000 abstract 1
- 239000010951 brass Substances 0.000 abstract 1
- 229910052793 cadmium Inorganic materials 0.000 abstract 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000011521 glass Substances 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 150000004678 hydrides Chemical class 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000002923 metal particle Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 150000004767 nitrides Chemical class 0.000 abstract 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 abstract 1
- 150000002902 organometallic compounds Chemical class 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 230000005855 radiation Effects 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 229910052709 silver Inorganic materials 0.000 abstract 1
- 239000010959 steel Substances 0.000 abstract 1
- 229910052721 tungsten Inorganic materials 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/755—Nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0238—Impregnation, coating or precipitation via the gaseous phase-sublimation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/17—Metallic particles coated with metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/023—Hydrogen absorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/30—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/30—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
- B22F9/305—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis of metal carbonyls
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Combustion & Propulsion (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
912,636. Producing iron and other metallic particles; coating with metals. COMMONWEALTH ENGINEERING CORPORATION. Jan. 21, 1959, No. 2186/59. Classes 72, 82 (1) and 82 (2). Metallic particles (iÁ or smaller) are precipitated from a gaseous compound of the required metal by heating the compound to its decomposition temperature and thereafter rapidly cooling the gas to below the decomposition temperature so as to regulate the size of the particles. The metal compounds may be: carbonyls, hydrides, halides, nitrides and organometallic compounds. Fig. 1 shows a reaction vessel into which gaseous metal compounds are fed through one or more nozzles 12-14. Hot inert gas from centrally-mounted nozzles 11 provide the heating and decomposition zone and cool inert gas fed in at 28 provides for the cooling of the gases. Fig. 6 shows another reaction vessel in which heating zones A-D and cooling zone E are produced by feeding the appropriate hot or cold gases to chambers formed within the double walls of the vessel. The gaseous metal compounds are fed in through headers in the top of the vessel. Metal compounds which decompose in different heating zones may be used to produce a mixture of metal powders or a metal powder coated with one or more different metals. Reference is made to the production of the following combinations : W, Ag, Ni on steel ; Cu on ceramics ; Ni on Cu, Cd, Mg, brass, glass, " Teflon " (Registered Trade Mark); Al on Mg; Cr on Cu. Reference is also made to the passage of silica and colloidal clays through the reactor to produce metallic coatings thereon. The heating may also be effected by infra-red and highfrequency radiation and the metal particles may be coated with a stearate after cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2186/59A GB912636A (en) | 1959-01-21 | 1959-01-21 | Method and apparatus for producing submicron metals |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2186/59A GB912636A (en) | 1959-01-21 | 1959-01-21 | Method and apparatus for producing submicron metals |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB912636A true GB912636A (en) | 1962-12-12 |
Family
ID=9735093
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2186/59A Expired GB912636A (en) | 1959-01-21 | 1959-01-21 | Method and apparatus for producing submicron metals |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB912636A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0147839A2 (en) * | 1983-12-31 | 1985-07-10 | Veg-Gasinstituut N.V. | A process of the production of a catalyst |
| EP0166831A1 (en) * | 1983-03-14 | 1986-01-08 | E.I. Du Pont De Nemours And Company | Improved catalyst |
| EP0360203A1 (en) * | 1988-09-22 | 1990-03-28 | Energy Conversion Devices, Inc. | Method and apparatus for size reducing of metal hydride hydrogen storage material. |
| GB2229739A (en) * | 1989-02-23 | 1990-10-03 | Nobuo Mikoshiba | Sports ground surface |
| CN111454516A (en) * | 2020-03-02 | 2020-07-28 | 深圳市捷安纳米复合材料有限公司 | Virus killing polypropylene composite material and preparation method thereof |
-
1959
- 1959-01-21 GB GB2186/59A patent/GB912636A/en not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0166831A1 (en) * | 1983-03-14 | 1986-01-08 | E.I. Du Pont De Nemours And Company | Improved catalyst |
| EP0147839A2 (en) * | 1983-12-31 | 1985-07-10 | Veg-Gasinstituut N.V. | A process of the production of a catalyst |
| EP0147839A3 (en) * | 1983-12-31 | 1985-10-30 | Veg-Gasinstituut N.V. | A process of the production of a catalyst |
| EP0360203A1 (en) * | 1988-09-22 | 1990-03-28 | Energy Conversion Devices, Inc. | Method and apparatus for size reducing of metal hydride hydrogen storage material. |
| EP0440843A1 (en) * | 1988-09-22 | 1991-08-14 | Energy Conversion Devices, Inc. | Hydride reactor apparatus for hydrogen comminution of metal hydride hydrogen storage material |
| GB2229739A (en) * | 1989-02-23 | 1990-10-03 | Nobuo Mikoshiba | Sports ground surface |
| GB2229739B (en) * | 1989-02-23 | 1993-08-25 | Nobuo Mikoshiba | Thin film forming apparatus |
| CN111454516A (en) * | 2020-03-02 | 2020-07-28 | 深圳市捷安纳米复合材料有限公司 | Virus killing polypropylene composite material and preparation method thereof |
| CN111454516B (en) * | 2020-03-02 | 2023-06-02 | 深圳市捷安纳米复合材料有限公司 | Sterilizing polypropylene composite material and preparation method thereof |
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