GB880961A - Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof - Google Patents

Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof

Info

Publication number
GB880961A
GB880961A GB3036658A GB3036658A GB880961A GB 880961 A GB880961 A GB 880961A GB 3036658 A GB3036658 A GB 3036658A GB 3036658 A GB3036658 A GB 3036658A GB 880961 A GB880961 A GB 880961A
Authority
GB
United Kingdom
Prior art keywords
cyclohexylbutyl
adipate
acetate
reducing
ester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3036658A
Inventor
Edwin George Edward Hawkins
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Distillers Co Yeast Ltd
Distillers Co Ltd
Original Assignee
Distillers Co Yeast Ltd
Distillers Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Distillers Co Yeast Ltd, Distillers Co Ltd filed Critical Distillers Co Yeast Ltd
Priority to GB3036658A priority Critical patent/GB880961A/en
Publication of GB880961A publication Critical patent/GB880961A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/10—Esters; Ether-esters
    • C08K5/11—Esters; Ether-esters of acyclic polycarboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

A composition comprises a polymeric material formed from monomers containing a vinylidene or a vinyl group and di-(3-cyclohexylbutyl) adipate as plasticizer. Polymeric materials specified are vinyl chloride homopolymers or copolymers with vinylidene chloride, vinyl esters, acrylic acid esters or maleate esters. An example describes the incorporation of the ester into polyvinyl chloride stabilized with white lead and the results of tests on the product given and compared with results obtained on a similar composition containing di(2-ethylhexyl) phthalate.ALSO:The invention comprises di-(3-cyclohexylbutyl) adipate and a process for its preparation by reducing 4-methyl-4-phenyl-dioxan to form 3-cyclohexylbutanol and heating the alcohol with adipic acid or a lower alkyl ester thereof in the presence of an esterification catalyst or by reacting a methyl-styrene, paraformaldehyde, acetic acid and acetic anhydride, reducing the 3-phenylbutenyl acetates formed to 3-cyclohexylbutyl acetate and subjecting the acetate to ester interchange with a lower alkyl ester of adipic acid. 3-cyclohexylbutanol may also be prepared by reducing the 3-phenylbutenol obtained by hydrolysis of the acetate.
GB3036658A 1958-09-23 1958-09-23 Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof Expired GB880961A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3036658A GB880961A (en) 1958-09-23 1958-09-23 Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3036658A GB880961A (en) 1958-09-23 1958-09-23 Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof

Publications (1)

Publication Number Publication Date
GB880961A true GB880961A (en) 1961-10-25

Family

ID=10306528

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3036658A Expired GB880961A (en) 1958-09-23 1958-09-23 Di-(3-cyclohexylbutyl) adipate and plasticised compositions thereof

Country Status (1)

Country Link
GB (1) GB880961A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5013779A (en) * 1989-12-08 1991-05-07 Monsanto Company Plasticized polyvinyl butyral and interlayer thereof
EP1516865A1 (en) * 2003-09-20 2005-03-23 Celanese Chemicals Europe GmbH 3-(4'-methylcyclohexyl) butanol based carboxylic acid esters having low pour point

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5013779A (en) * 1989-12-08 1991-05-07 Monsanto Company Plasticized polyvinyl butyral and interlayer thereof
EP1516865A1 (en) * 2003-09-20 2005-03-23 Celanese Chemicals Europe GmbH 3-(4'-methylcyclohexyl) butanol based carboxylic acid esters having low pour point
US7196128B2 (en) 2003-09-20 2007-03-27 Celanese Chemicals Europe Gmbh Carboxylic esters based on limonene alcohol [3-(4′-methylcyclohexyl)butanol] and having a low melting point

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