GB875019A - Polyamide melt spinning process - Google Patents
Polyamide melt spinning processInfo
- Publication number
- GB875019A GB875019A GB5732/58A GB573258A GB875019A GB 875019 A GB875019 A GB 875019A GB 5732/58 A GB5732/58 A GB 5732/58A GB 573258 A GB573258 A GB 573258A GB 875019 A GB875019 A GB 875019A
- Authority
- GB
- United Kingdom
- Prior art keywords
- chamber
- water
- melt
- gas
- pool
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/04—Melting filament-forming substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/04—Preparatory processes
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/60—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyamides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Artificial Filaments (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Abstract
<PICT:0875019/IV (a)/1> In melt-spinning synthetic linear polyamides, the polyamide is melted in a closed heated chamber or fed in molten condition into a melt storage chamber and the pool of melt which, in either case, is formed in the lower portion of the chamber is exposed to a mixture of a gas and dry superheated steam, which occupies the free space in the chamber above the pool of melt, until it no longer evolves or absorbs water vapour and its water content remains constant, the volumetric rate of flow of melt through the chamber being sufficiently low to ensure that the period of residence of the melt in the chamber is sufficient to allow a condition of equilibrium to be reached with respect to the migration of water between the melt and the atmosphere in the chamber. The mixture of gas and steam in the melting or melt storage chamber is in free communication with the gas space in the upper portion of a second closed chamber which is at the same pressure as the first chamber but is maintained at a temperature below the boiling point of water at that pressure, the gas being saturated with water vapour in this second or humidifying chamber by introducing steam or water into the chamber in sufficient quantity to cause a pool of water to collect at the bottom of the chamber. The pressure of the atmosphere in both chambers is maintained at a constant predetermined value. As shown, the melt is introduced into a melt storage chamber 8 through a pipe 1 into an annular channel 2 from which it overflows, runs down the wall 3 of the chamber and collects in a sump 4, from which it is fed by a screw metering pump 5 through the outlet 6 to a spinning nozzle. The chamber 8 is closed by a cover plate 7 and is maintained at a constant predetermined temperature above the melting point of the polyamide by the circulation of a heating fluid through a jacket 7a. It communicates through a large diameter pipe 9 with a second closed chamber 10 into which water is sprayed by a pump 13 through the spray nozzle 11. Water collects in a sump at the bottom of the chamber 10 to form a pool of water 12 from which water is recycled by the pump 13, a small supply of fresh water being added to the circulation system through a valve 14. The level of the pool of water 12 is maintained constant by means of a float 16 and regulator 17 which controls an outlet valve 15. The chamber 10 is maintained at a constant temperature by means of a jacket 18 through which a fluid at a constant predetermined temperature is circulated. At the beginning of the spinning process the whole apparatus is evacuated and is then filled with an inert gas such as nitrogen through pipe 1. During spinning additional gas is introduced with the melt from a melting chamber through the pipe 1 and makes up for loss of gas during spinning. The pressure of the gas is preferably maintained slightly above atmospheric. In an alternative arrangement, the second or humidifying cylindrical chamber is provided with a central vertical tube concentric with the vertical walls of the chamber and the annular space between this tube and the walls of the chamber is filled with Raschig rings which are sprayed from above with water raised by means of a circulating pump from a pool of water formed in a sump at the bottom of the chamber. An inert gas such as nitrogen is circulated through the annular column of Raschig rings by means of an axial fan disposed in the central tube. Specification 730,617 is referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE875019X | 1957-03-08 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB875019A true GB875019A (en) | 1961-08-16 |
Family
ID=6817096
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB5732/58A Expired GB875019A (en) | 1957-03-08 | 1958-02-21 | Polyamide melt spinning process |
Country Status (5)
Country | Link |
---|---|
US (1) | US2943350A (en) |
BE (1) | BE565488A (en) |
FR (1) | FR1199568A (en) |
GB (1) | GB875019A (en) |
NL (2) | NL225522A (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL235546A (en) * | 1958-01-28 | |||
DE2702605C3 (en) * | 1977-01-22 | 1979-12-13 | Basf Ag, 6700 Ludwigshafen | Process for the production of higher molecular weight polyamides |
AU517825B2 (en) * | 1977-04-12 | 1981-08-27 | Union Carbide Corporation | Gear pump |
EP0092898B2 (en) * | 1982-04-28 | 2000-02-09 | E.I. Du Pont De Nemours And Company | Process for remelting polyamides |
DE3338294A1 (en) * | 1983-10-21 | 1985-05-02 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING DRY POLYCAPROLACTAM GRANULATE |
ATE67799T1 (en) | 1985-04-22 | 1991-10-15 | Basf Corp | PROCESS FOR HIGH-SPEED SPINNING POLYAMIDE FIBERS. |
US4952345A (en) * | 1989-02-10 | 1990-08-28 | E. I. Du Pont De Nemours And Company | Method for controlling polymer viscosity |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2571975A (en) * | 1947-05-10 | 1951-10-16 | Du Pont | Melt spinning process |
-
0
- BE BE565488D patent/BE565488A/xx unknown
- NL NL97740D patent/NL97740C/xx active
- NL NL225522D patent/NL225522A/xx unknown
-
1958
- 1958-02-21 GB GB5732/58A patent/GB875019A/en not_active Expired
- 1958-02-24 US US717161A patent/US2943350A/en not_active Expired - Lifetime
- 1958-03-06 FR FR1199568D patent/FR1199568A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
BE565488A (en) | |
US2943350A (en) | 1960-07-05 |
NL225522A (en) | |
NL97740C (en) | |
FR1199568A (en) | 1959-12-15 |
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