GB860674A - Improvements in or relating to the purification of sulphur - Google Patents

Improvements in or relating to the purification of sulphur

Info

Publication number
GB860674A
GB860674A GB12870/57A GB1287057A GB860674A GB 860674 A GB860674 A GB 860674A GB 12870/57 A GB12870/57 A GB 12870/57A GB 1287057 A GB1287057 A GB 1287057A GB 860674 A GB860674 A GB 860674A
Authority
GB
United Kingdom
Prior art keywords
sulphur
mesh
ore
fraction
chloride solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB12870/57A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB860674A publication Critical patent/GB860674A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/02—Preparation of sulfur; Purification
    • C01B17/0232—Purification, e.g. degassing
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/02—Preparation of sulfur; Purification
    • C01B17/027—Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/02—Preparation of sulfur; Purification
    • C01B17/027—Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur
    • C01B17/033—Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur using a liquid extractant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Removal Of Specific Substances (AREA)

Abstract

Sulphur is separated from a sulphur ore of a quality between 50 and 75 weight per cent of sulphur and of particle size all through 80-mesh B.S.S. by heating the ore in water or an aqueous calcium, magnesium, or zinc chloride solution to melt the sulphur, permitting cooling to solidify the sulphur, and classifying to separate the sulphur fraction of above 80 mesh particle size. The sulphur ore may be naturally occurring, filter cake containing sulphur, partially purified sulphur, oxide from gas plants, or any mixture of sulphur with inorganic waste, in which the sulphur content may be adjusted to 50-75% by adding pure sulphur or inorganic silicate. The ore may be comminuted to the desired size, preferably larger than 300 mesh and generally smaller than 100 mesh. The ore is placed in water or a concentrated chloride solution in a vol. ratio liquid to solid 3 : 1 to 10 : 1, and is heated with agitation at 125-135 DEG C., if necessary, under pressure. After cooling, the solid may be separated into two fractions, greater and smaller than 80 mesh, or into three fractions greater than 60 mesh, 60-80 mesh, and smaller than 80 mesh. The largest size fraction is pure sulphur, is washed, and may be further purified by fusion filtration, while the smallest size fraction is inorganic waste and may be leached with hot chloride solution. The middle fraction of a three-fraction separation may be recycled. The process may be batch or continuous.
GB12870/57A 1956-04-23 1957-04-23 Improvements in or relating to the purification of sulphur Expired GB860674A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IN860674X 1956-04-23

Publications (1)

Publication Number Publication Date
GB860674A true GB860674A (en) 1961-02-08

Family

ID=11076640

Family Applications (3)

Application Number Title Priority Date Filing Date
GB12870/57A Expired GB860674A (en) 1956-04-23 1957-04-23 Improvements in or relating to the purification of sulphur
GB9360/61A Expired GB912164A (en) 1956-04-23 1961-03-14 Improvements in or relating to the purification of sulphur
GB11119/61A Expired GB912165A (en) 1956-04-23 1961-03-27 Improvements in or relating to the purification of sulphur

Family Applications After (2)

Application Number Title Priority Date Filing Date
GB9360/61A Expired GB912164A (en) 1956-04-23 1961-03-14 Improvements in or relating to the purification of sulphur
GB11119/61A Expired GB912165A (en) 1956-04-23 1961-03-27 Improvements in or relating to the purification of sulphur

Country Status (1)

Country Link
GB (3) GB860674A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1229501B (en) * 1962-03-14 1966-12-01 Herbert James Elliott Process for the processing of sulfur or products containing sulfur
US4923482A (en) * 1986-04-15 1990-05-08 Sulexport-Intertrade A.G. Process for separating sulfur from ore

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3515709C1 (en) * 1985-05-02 1986-12-18 Union Rheinische Braunkohlen Kraftstoff AG, 5000 Köln Process for cleaning liquid sulfur

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1229501B (en) * 1962-03-14 1966-12-01 Herbert James Elliott Process for the processing of sulfur or products containing sulfur
US4923482A (en) * 1986-04-15 1990-05-08 Sulexport-Intertrade A.G. Process for separating sulfur from ore

Also Published As

Publication number Publication date
GB912165A (en) 1962-12-05
GB912164A (en) 1962-12-05

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